CN109480049A - Chewing gum and preparation method thereof - Google Patents
Chewing gum and preparation method thereof Download PDFInfo
- Publication number
- CN109480049A CN109480049A CN201811607485.5A CN201811607485A CN109480049A CN 109480049 A CN109480049 A CN 109480049A CN 201811607485 A CN201811607485 A CN 201811607485A CN 109480049 A CN109480049 A CN 109480049A
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- chewing gum
- matrix
- formula
- sugar
- compound represented
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- 229940112822 chewing gum Drugs 0.000 title claims abstract description 84
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
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- 150000001875 compounds Chemical class 0.000 claims abstract description 41
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- 235000011176 polyphosphates Nutrition 0.000 description 1
- 235000020610 powder formula Nutrition 0.000 description 1
- HELXLJCILKEWJH-NCGAPWICSA-N rebaudioside A Chemical compound O([C@H]1[C@H](O)[C@@H](CO)O[C@H]([C@@H]1O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)O[C@]12C(=C)C[C@@]3(C1)CC[C@@H]1[C@@](C)(CCC[C@]1([C@@H]3CC2)C)C(=O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O HELXLJCILKEWJH-NCGAPWICSA-N 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000004208 shellac Substances 0.000 description 1
- 229940113147 shellac Drugs 0.000 description 1
- ZLGIYFNHBLSMPS-ATJNOEHPSA-N shellac Chemical compound OCCCCCC(O)C(O)CCCCCCCC(O)=O.C1C23[C@H](C(O)=O)CCC2[C@](C)(CO)[C@@H]1C(C(O)=O)=C[C@@H]3O ZLGIYFNHBLSMPS-ATJNOEHPSA-N 0.000 description 1
- 235000013874 shellac Nutrition 0.000 description 1
- 235000011888 snacks Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G4/00—Chewing gum
- A23G4/06—Chewing gum characterised by the composition containing organic or inorganic compounds
- A23G4/12—Chewing gum characterised by the composition containing organic or inorganic compounds containing microorganisms or enzymes; containing paramedical or dietetical agents, e.g. vitamins
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Microbiology (AREA)
- Nutrition Science (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Confectionery (AREA)
Abstract
The invention discloses a kind of chewing gums and preparation method thereof.Every chewing gum includes 0.5~0.7wt% of formula (I) compound represented, 9~13wt% of sugar alcohol, 40~60wt% of matrix, 0.09~0.14wt% of citric acid, 10~14wt% of 0.1~0.5wt% of lubricant, 0.15~0.45wt% of softening agent and water.Contain formula (I) compound represented and citric acid in chewing gum of the invention, thus bacterial growth in long-acting inhibition oral cavity.
Description
Technical field
The present invention relates to a kind of chewing gums and preparation method thereof.
Background technique
As a kind of snack food, chewing gum is favored by people.Chewing gum has fresh breath, cleaning oral cavity, takes exercise
Facial muscle and the effect relieved stress.The time of majority's chew gum is longer, is easy being sticked on chewing gum
Bacterium chew chamber of answering back, the growth of bacterium is caused even into abdominal cavity.Therefore, it is necessary to a kind of, and the mouth with bactericidal bacteriostasis is fragrant
Sugar.
A kind of oral preparations of gum formats are disclosed in CN1599594A, can be existed in the form of chewing gum, are wrapped
Containing polyphosphate, hydrated SiO 2, fluoride sources, the extract of plant origin or active constituent and antibacterial/disinfectant agents.
A kind of oral cavity composition of insoluble non-cationic fungicide is disclosed in CN1204506A, inside it is porous due to joined
Calcium carbonate improves the activity of non-cationic fungicide.
Summary of the invention
In view of this, it is an object of that present invention to provide a kind of chewing gum, it being capable of long-acting bacteriostatic.Another object of the present invention
It is to provide the preparation method of the chewing gum.
On the one hand, the present invention provides the chewing gum for containing formula (I) compound represented, and every chewing gum is by including such as the following group
Point raw material be prepared: 0.5~0.7wt% of formula (I) compound represented, 9~13wt% of sugar alcohol, 40~60wt% of matrix,
0.09~0.15wt% of citric acid, 8~15wt% of 0.1~0.5wt% of lubricant, 0.15~0.45wt% of softening agent and water；
In formula (I), R1、R2And R3Separately it is selected from fluorine, chlorine or bromine.
Chewing gum according to the present invention, it is preferable that the R1、R2And R3It is chlorine.
Chewing gum according to the present invention, it is preferable that formula (I) compound represented and the weight ratio of citric acid be 4~
6:1。
Chewing gum according to the present invention, it is preferable that the weight ratio of the matrix and water is 3~5:1；The matrix and softening
The weight ratio of agent is 150~170:1；The weight ratio of the matrix and lubricant is 150~170:1.
Chewing gum according to the present invention, it is preferable that the raw material also includes 0.35~0.6wt% of auxiliary material, the auxiliary material choosing
From one of pigment, sugar, non-sugar sweetener and essence or a variety of.
Chewing gum according to the present invention, it is preferable that the sugar alcohol is selected from maltitol, D-sorbite, xylitol, lactose
One of alcohol, antierythrite or mannitol are a variety of；
The matrix is selected from tunny gum, gutta-percha, butyl natural gum, hydrogenated rosin glyceride, polymerized rosin glycerol ester
And one of disproportionated rosin glyceride or a variety of；
The lubricant is selected from triglycerides, glycerol, isopropanol, polyethylene glycol 200, polyethylene glycol 400 or polyethylene glycol
One of 600 or a variety of；With
The softening agent be selected from propylene glycol, Arabic gum, fatty glyceride, pectin, alginic acid, alginate, phosphatide,
One of gelatin, hydrogenated vegetable oil or sucrose fatty ester are a variety of.
Chewing gum according to the present invention, it is preferable that every chewing gum is prepared by the raw material comprising following component: formula
(I) 0.55~0.65wt% of compound represented, 10~12wt% of sugar alcohol, 45~55wt% of matrix, citric acid 0.11~
0.13wt%, 10~14wt% of 0.2~0.4wt% of lubricant, 0.25~0.35wt% of softening agent and water.
Chewing gum according to the present invention, it is preferable that every chewing gum is prepared by the raw material comprising following component: formula
(I) 0.55~0.65wt% of compound represented, 10~12wt% of mannitol, 45~55wt% of matrix, citric acid 0.11~
0.13wt%, 10~14wt% of 0.2~0.4wt% of glycerol, 0.25~0.35wt% of Arabic gum and water.
Chewing gum according to the present invention, it is preferable that every chewing gum is prepared by the raw material of following component: formula (I) institute
0.55~0.65wt% of compound for showing, 10~12wt% of mannitol, 45~55wt% of matrix, citric acid 0.11~
0.13wt%, 0.2~0.4wt% of glycerol, 0.25~0.35wt% of Arabic gum, 10~14wt% of water, white granulated sugar 20~
26wt%, 0.2~0.3wt% of 0.08~0.12wt% of essence, 0.10~0.14wt% of pigment and non-sugar sweetener；Its
In, the non-sugar sweetener be selected from steviol glycoside, glycyrrhizin, mogroside, acesulfame potassium, Aspartame, Sucralose and
One of isomaltoketose is a variety of.
On the other hand, the present invention provides a kind of preparation method of chewing gum containing formula (I) compound represented, including such as
Lower step:
(1) it will crush and be uniformly mixed comprising first raw material of formula (I) compound represented, sugar alcohol and softening agent, obtain
Partial size is 150 μm of first mixtures below；
(2) it will be mixed comprising the second raw material of citric acid and water, boil and stir 20~60min, be cooled to 60~80 DEG C,
The second mixture is made；
(3) matrix, lubricant, the first mixture and the second mixture after 70~90 DEG C of softenings are uniformly mixed, it is cooling
Post-processing molding, obtains the chewing gum.
Contain formula (I) compound represented and citric acid in chewing gum of the invention, thus bacterium in long-acting inhibition oral cavity
Growth.Preferred embodiment according to the present invention can give full play to the bacteriostasis of chewing gum.
Specific embodiment
The present invention is further illustrated combined with specific embodiments below, but protection scope of the present invention is not limited to
This.
< chewing gum >
Chewing gum of the invention is prepared by the raw material comprising following component: formula (I) compound represented 0.5~
0.7wt%, 9~13wt% of sugar alcohol, 40~60wt% of matrix, 0.09~0.15wt% of citric acid, 0.1~0.5wt% of lubricant,
8~15wt% of 0.15~0.45wt% of softening agent and water.The weight of every chewing gum can be 0.5~3g, preferably 1~
2.5g, more preferably 1~2.5g.
In formula (I), R1、R2And R3Separately it is selected from fluorine, chlorine or bromine.According to embodiment of the present invention, R1、R2
And R3It is chlorine.
Chewing gum of the invention contains formula (I) compound represented and citric acid.It can be with it is a discovery of the invention that the two is combined
Bacterial growth in long-acting inhibition oral cavity.Formula (I) compound represented can be penetrated in bacteria cell wall, by the albumen in cytoplasm
Qualitative change is played to inhibit bacterial growth in oral cavity and cleans antibacterial effect.In the present invention, formula (I) in every chewing gum
The content of compound represented is 0.5~0.7wt%, preferably 0.55~0.65wt%.
In chewing gum of the invention, in every chewing gum the content of citric acid be 0.09~0.15wt%, preferably 0.1
~0.13wt%, more preferably 0.11~0.12wt%.The present invention is found surprisingly that, by formula (I) compound represented and lemon
Acid combination, has effects that bacterial growth in long-acting inhibition oral cavity.In the present invention, it is preferable that formula (I) compound represented
Weight ratio with citric acid is 4~6:1, preferably 4.5~5.5:1, more preferably 4.8~5.2:1.
Sugar alcohol in the present invention can be selected from maltitol, D-sorbite, xylitol, lactitol, antierythrite or sweet dew
One of sugar alcohol is a variety of, preferably one of D-sorbite, xylitol or mannitol or a variety of, more preferably sweet dew
Sugar alcohol.The content of sugar alcohol described in every chewing gum can be 9~13wt%, preferably 10~12wt%, more preferably 10.5
~11.5wt%.
Matrix of the invention can be selected from tunny gum, gutta-percha, butyl natural gum, hydrogenated rosin glyceride, polymerization pine
One of fragrant glyceride and disproportionated rosin glyceride are a variety of；Preferably butyl natural gum, hydrogenated rosin glyceride, polymerization pine
One of fragrant glyceride and disproportionated rosin glyceride are a variety of, more preferably hydrogenated rosin glyceride.In every chewing gum
The content of matrix can be 40~60wt%, preferably 45~55wt%, more preferably 48~52wt%.Matrix is as chewing gum
Matrix, in mastication processes, formula (I) compound represented in chewing gum is in contact with tooth and mucous membrane of mouth, has
Comprehensively the effect of cleaning oral cavity.
Softening agent in the present invention is selected from propylene glycol, Arabic gum, fatty glyceride, pectin, alginic acid, alginic acid
One of salt, phosphatide, gelatin, hydrogenated vegetable oil and sucrose fatty ester are a variety of, preferably Arabic gum, gelatin and sugarcane
One of sugar fatty acid ester is a variety of, more preferably Arabic gum.In every chewing gum the content of softening agent be 0.15~
0.45wt%, preferably 0.2~0.4wt%, more preferably 0.25~0.32wt%.
Lubricant of the invention is selected from triglycerides, glycerol, isopropanol, polyethylene glycol 200, polyethylene glycol 400 or poly- second
One of glycol 600 is a variety of, preferably one of triglycerides, glycerol, isopropanol and polyethylene glycol 400 or more
Kind, more preferably triglycerides or glycerol.The content of lubricant can be 0.1~0.5wt% in every chewing gum, preferably
0.2~0.4wt%, more preferably 0.25~0.33wt%.
In the present invention, the weight ratio of the matrix and water is 3~5:1, preferably 3.5~4.5:1, more preferably 3.9
~4.2:1；The weight ratio of the matrix and softening agent be 150~170:1, preferably 160~170:1, more preferably 165~
170:1；The weight ratio of the matrix and lubricant is 150~170:1, preferably 160~170:1, more preferably 165~170:
1.Softening agent can soften matrix in chewing gum of the present invention, and lubricant can keep the moisture content inside chewing gum, adjust glue
The weight ratio of base and water, softening agent and lubricant can make chewing gum with more mouthfeel.
According to embodiment of the present invention, every chewing gum is prepared by the raw material comprising following component: formula (I)
0.55~0.65wt% of compound represented, 10~12wt% of sugar alcohol, 45~55wt% of matrix, citric acid 0.11~
0.13wt%, 10~14wt% of 0.2~0.4wt% of lubricant, 0.25~0.35wt% of softening agent and water.
Chewing gum of the invention can also include auxiliary material, and the auxiliary material is in pigment, sugar, non-sugar sweetener and essence
It is one or more.The content for the auxiliary material that every chewing gum contains be 8~29wt%, preferably 12~28wt%, more preferably
15~25wt%.Pigment is preferably natural food colour, the natural food colour be preferably shellac color, carthamin yellow,
One of beet red, capsorubin, turmeric, bata-carotene, copper chlorophyllin sodium salt, dark reddish brown element are a variety of, more preferably safflower
Uranidin, beet red, turmeric, bata-carotene are further preferably turmeric, bata-carotene.Sugar can be selected from glucose, fructose, wheat
One of bud sugar, lactose or sucrose are a variety of, preferably one of sucrose, fructose or maltose or a variety of, more preferably
Sucrose or maltose.The form of sucrose is white granulated sugar or continuous granulated sugar in the present invention.The non-sugar sweetener can be selected from
One of steviol glycoside, glycyrrhizin, mogroside, acesulfame potassium, Aspartame, Sucralose and isomaltoketose are more
Kind.Also preferably one of steviol glycoside, glycyrrhizin, mogroside and Aspartame or a variety of, more preferably stevia rebaudianum
Glucosides or mogroside.Essence can be selected from any one of fruit essence, Mint Essence, flavoring rose essence and osmanthus flower fragrance.
A preferred embodiment according to the present invention, the auxiliary material include essence, pigment, non-sugar sweetener and white granulated sugar, and every
Grain chewing gum contains 0.08~0.12wt% of essence, 0.1~0.14wt% of pigment, 0.2~0.3wt% of non-sugar sweetener and
20~26wt% of white granulated sugar.
According to embodiment of the present invention, every chewing gum is prepared by the raw material comprising following component: formula (I)
0.55~0.65wt% of compound represented, 10~12wt% of mannitol, 45~55wt% of matrix, citric acid 0.11~
0.13wt%, 10~14wt% of 0.2~0.4wt% of glycerol, 0.25~0.35wt% of Arabic gum and water.It is according to the present invention
One preferred embodiment, every chewing gum are prepared by the raw material comprising following component: formula (I) compound represented 0.55
~0.65wt%, 10~12wt% of mannitol, 45~55wt% of matrix, 0.11~0.13wt% of citric acid, glycerol 0.2~
0.4wt%, 0.25~0.35wt% of Arabic gum, 10~14wt% of water, 0.08~0.12wt% of essence, pigment 0.1~
20~26wt% of 0.14wt%, 0.2~0.3wt% of non-sugar sweetener and white granulated sugar.
According to another implementation of the invention, every chewing gum is prepared by the raw material of following component in the present invention
It arrives: 0.55~0.65wt% of formula (I) compound represented, 10~12wt% of mannitol, 45~55wt% of matrix, citric acid
0.11~0.13wt%, 0.2~0.4wt% of glycerol, 0.25~0.35wt% of Arabic gum, 10~14wt% of water, essence 0.08
20~26wt% of~0.12wt%, 0.1~0.14wt% of pigment, 0.2~0.3wt% of non-sugar sweetener and white granulated sugar.
< preparation method >
The preparation method of chewing gum of the invention includes the following steps:
(1) it will crush and be uniformly mixed comprising first raw material of the formula (I) compound represented, sugar alcohol and softening agent,
Obtaining partial size is 150 μm of first mixtures below；
(2) it will be mixed comprising the second raw material of citric acid and water, boil and stir 20~60min, be cooled to 60~80 DEG C,
The second mixture is made；
(3) matrix, lubricant, the first mixture and the second mixture after 70~90 DEG C of softenings are uniformly mixed, it is cooling
Post-processing molding, obtains the chewing gum.
In step (1), first by each ingredient in the first raw material be crushed to partial size be 150 μm hereinafter, preferably 120 μm with
Under, more preferably 100 μm or less.Using above-mentioned partial size, is conducive to each ingredient and is uniformly mixed.Preferred implementation side according to the present invention
Formula, first raw material also includes auxiliary material, the auxiliary material be it is described above, details are not described herein again.It can be by smashed formula (I)
Compound represented, optional auxiliary material, softening agent and sugar alcohol are uniformly mixed using conventional method；It can also be by smashed formula
(I) compound represented, softening agent and optional auxiliary material are uniformly mixed, and gradient mixing method is then used with part sugar alcohol, such as
Equivalent gradient mixing method is uniformly mixed.According to embodiment of the present invention, first by formula (I) compound represented, softening
Agent and auxiliary material are uniformly mixed, and obtain primary mix；Then by the primary mix with etc. the sugar alcohols of quality be uniformly mixed,
It repeats 2~5 times, obtains the first mixture.Above-mentioned equivalent gradient mixing method be conducive to formula (I) compound represented, auxiliary material (if having),
Softening agent is uniformly mixed with sugar alcohol.
In step (2), the second raw material may include sugar.Sugar, citric acid and water can be mixed using conventional method equal
It is even, then boil.Boiling required temperature is 100~150 DEG C, preferably 100~120 DEG C, more preferably 100~110 DEG C.It boils
Time is 20~60min, preferably 30~50min, more preferably 30~40min.Preferred embodiment according to the present invention, sugar,
The weight ratio of citric acid and water is 180~210:1:90~105, preferably 190~205:1:95~100, more preferably 195
~203:1:97~100.
In step (3), the softening temperature of matrix can be 70~90 DEG C, preferably 75~85 DEG C, more preferably 80 DEG C.Glue
Base, lubricant, the first mixture and the second mixture hybrid mode profit is preferably sequentially added into the matrix after softening
Lubrication prescription, the first mixture and the second mixture are uniformly mixed, then cool down.Cooling temperature can be 30~70 DEG C, preferably
35~50 DEG C, more preferably 35~45 DEG C.
A preferred embodiment according to the present invention:
(1) formula (I) compound represented, sugar alcohol, softening agent and auxiliary material are crushed to partial size is 120 μm or less；By powder
Formula (I) compound represented, softening agent, auxiliary material and sugar alcohol after broken are uniformly mixed using equivalent gradient mixing method, obtain first
Mixture；
(2) after mixing by water and sugar, be repeatedly added and citric acid and be uniformly mixed in batches, the sugar, citric acid and
The weight ratio of water is 190~205:1:95~100, by the mixture of uniformly mixed sugar, citric acid and water 100~120
DEG C 30~50min is boiled and stirred, is cooled to 60~80 DEG C, obtains the second mixture；
(3) matrix, lubricant, the first mixture and the second mixture after 75~85 DEG C of softenings are uniformly mixed,
35~50 DEG C of post-processing moldings are cooled to, chewing gum is obtained.
A specific embodiment according to the present invention:
(1) by formula (I) compound represented, mannitol, Arabic gum and essence, pigment, non-sugar sweetener etc.
It is 120 μm or less that auxiliary material, which is crushed to partial size,；By smashed formula (I) compound represented, Arabic gum, auxiliary material and sweet dew
Sugar alcohol is uniformly mixed using equivalent gradient mixing method, obtains the first mixture；
(2) after mixing by water and white granulated sugar, citric acid is repeatedly added in batches and is uniformly mixed, the white granulated sugar, lemon
The weight ratio of lemon acid and water is 190~205:1:95~100, by the mixing of uniformly mixed white granulated sugar, citric acid and water
Object boils and stirs 30~50min at 100~120 DEG C, is cooled to 60~80 DEG C, obtains the second mixture；
(3) matrix, glycerol, the first mixture and the second mixture after 75~85 DEG C of softenings are uniformly mixed, it is cold
But it is formed to 35~50 DEG C of post-processings, obtains chewing gum.
Embodiment 1
The formula of chewing gum is as follows:
Compound 12.5g shown in following formula, mannitol 230g, matrix 1000g, citric acid 2.47g, white granulated sugar
494.67g, Arabic gum 6g, essence 2g, pigment 2.5g, steviol glycoside 5g, glycerol 6g and water 244.86g.
It is prepared as follows chewing gum:
(1) by 12.5g above compound, 230g mannitol, 6g Arabic gum, 2g essence, 2.5g pigment and 5g sweet tea
It is 120 μm or less that synanthrin glycosides, which is crushed to partial size,.By smashed compound, mannitol, Arabic gum, essence, pigment and
Steviol glycoside is uniformly mixed using equivalent gradient mixing method, obtains the first mixture；
(2) after mixing by 244.86g water and 494.67g white granulated sugar, the lemon that total amount is 2.47g is repeatedly added in batches
Acid is simultaneously uniformly mixed (weight ratio of white granulated sugar, citric acid and water is 200.3:1:99.1), is boiled 40min at 120 DEG C, is cooled down
To 70 DEG C, the second mixture is made；
(3) matrix, 6g glycerol, the first mixture and the second mixture after 80 DEG C of softenings are uniformly mixed, are cooled to 45
DEG C post-processing molding, obtains chewing gum.The specification of every chewing gum is 0.5g/, 1g/, 1.5g/, 2g/, 2.5g/
Or 3g/.The antibacterial test result of every kind of specification chewing gum is referring to table 2.
Comparative example 1
The citric acid 2.47g in embodiment 1 is omitted, remaining condition is same as Example 1, the antibacterial test of gained chewing gum
As a result referring to table 2.
Comparative example 2
The compound 12.5g in embodiment 1 is omitted, remaining condition is same as Example 1, the antibacterial test of gained chewing gum
As a result referring to table 2.
Comparative example 3
The weight of citric acid in embodiment 1 is replaced with into 1.2g, remaining condition is same as Example 1, gained chewing gum
Antibacterial test result is referring to table 2.
Experimental example 1
1, experimental method
Before being tested, not chew gum in 2 hours, the influence to avoid other factors to sample.With 20ml's
10wt% ethanol solution is gargled, and different size chewing gum is chewed after 1 hour, is then gargled simultaneously with the 10wt% ethanol solution of 20ml
It spits into container, precision measures 0.5ml mouthwash solution, is evenly coated in the culture medium that specification is 9cm, 37 DEG C are put into after sealing
Bacterium cultivation is carried out in incubator, and the antibacterial situation of each sample is characterized by the size of statistics clump count and bacterium colony.It will not
The sample A of chew gum is as a control group.
Table 1, sample collection method
| Number | Chewing gum specification | Chew time | Gained sample ID |
| Control group | — | — | Sample A |
| Embodiment 1 | 0.5g/ | 10min | Sample B |
| Embodiment 1 | 1g/ | 10min | Sample C |
| Embodiment 1 | 1.5g/ grain | 10min | Sample D |
| Embodiment 1 | 2g/ | 10min | Sample E |
| Embodiment 1 | 2.5g/ grain | 10min | Sample F |
| Embodiment 1 | 3g/ | 10min | Sample G |
| Embodiment 1 | 3g/ | 10min | Sample H |
| Comparative example 1 | 1g/ | 10min | Sample I |
| Comparative example 2 | 1g/ | 10min | Sample J |
| Comparative example 3 | 1g/ | 10min | Sample K |
Remarks: 2h is obtained after the sample H chewing gum that specification is 3g/ in chewing embodiment 1.
2, test result
Chewing gum is antibacterial to the results are shown in Table 2.
The antibacterial test result of table 2, chewing gum
As known from Table 2, each specification chewing gum all has the effect of inhibiting bacterial growth in oral cavity and antibacterial effect in embodiment 1
Fruit is better than comparative example 1 to 3；It is 0.5g/ that antibacterial and long-acting bacteriostatic effect when wherein chewing gum specification is 1g/, which is better than specification,
Chewing gum, and as chewing gum specification becomes larger, fungistatic effect is without significant change.
Present invention is not limited to the embodiments described above, without departing from the essence of the present invention, this field skill
Any deformation, improvement, the replacement that art personnel are contemplated that each fall within the scope of the present invention.
Claims (10)
1. a kind of chewing gum, which is characterized in that every chewing gum is prepared by the raw material comprising following component: shown in formula (I)
0.5~0.7wt% of compound, 9~13wt% of sugar alcohol, 40~60wt% of matrix, 0.09~0.15wt% of citric acid, lubricant
8~15wt% of 0.1~0.5wt%, 0.15~0.45wt% of softening agent and water；
In formula (I), R1、R2And R3Separately it is selected from fluorine, chlorine or bromine.
2. chewing gum according to claim 1, which is characterized in that the R1、R2And R3It is chlorine.
3. chewing gum according to claim 1, which is characterized in that the weight ratio of formula (I) compound represented and citric acid
For 4~6:1.
4. chewing gum according to claim 1, which is characterized in that the weight ratio of the matrix and water is 3~5:1；It is described
The weight ratio of matrix and softening agent is 150~170:1；The weight ratio of the matrix and lubricant is 150~170:1.
5. chewing gum according to claim 1, which is characterized in that the raw material also includes 8~29wt% of auxiliary material, described auxiliary
Material is selected from one of pigment, sugar, non-sugar sweetener and essence or a variety of.
6. described in any item chewing gums according to claim 1~5, which is characterized in that the sugar alcohol is selected from maltitol, sorb
One of sugar alcohol, xylitol, lactitol, antierythrite or mannitol are a variety of；
The matrix be selected from tunny gum, gutta-percha, butyl natural gum, hydrogenated rosin glyceride, polymerized rosin glycerol ester and
One of disproportionated rosin glyceride is a variety of；
The lubricant is in triglycerides, glycerol, isopropanol, polyethylene glycol 200, polyethylene glycol 400 or Macrogol 600
It is one or more；With
The softening agent is selected from propylene glycol, Arabic gum, fatty glyceride, pectin, alginic acid, alginate, phosphatide, bright
One of glue, hydrogenated vegetable oil or sucrose fatty ester are a variety of.
7. chewing gum according to claim 1 or 2, which is characterized in that every chewing gum is by the raw material comprising following component
It is prepared: 0.55~0.65wt% of formula (I) compound represented, 10~12wt% of sugar alcohol, 45~55wt% of matrix, citric acid
0.11~0.13wt%, 10~14wt% of 0.2~0.4wt% of lubricant, 0.25~0.35wt% of softening agent and water.
8. chewing gum according to claim 1 or 2, which is characterized in that every chewing gum is by the raw material comprising following component
It is prepared: 0.55~0.65wt% of formula (I) compound represented, 10~12wt% of mannitol, 45~55wt% of matrix, lemon
0.11~0.13wt% of lemon acid, 10~14wt% of 0.2~0.4wt% of glycerol, 0.25~0.35wt% of Arabic gum and water.
9. chewing gum according to claim 1 or 2, which is characterized in that every chewing gum is prepared by the raw material of following component
It obtains: 0.55~0.65wt% of formula (I) compound represented, 10~12wt% of mannitol, 45~55wt% of matrix, citric acid
0.11~0.13wt%, 0.2~0.4wt% of glycerol, 0.25~0.35wt% of Arabic gum, 10~14wt% of water, white granulated sugar 20
~26wt%, 0.2~0.3wt% of 0.08~0.12wt% of essence, 0.10~0.14wt% of pigment and non-sugar sweetener；Its
In, the non-sugar sweetener be selected from steviol glycoside, glycyrrhizin, mogroside, acesulfame potassium, Aspartame, Sucralose and
One of isomaltoketose is a variety of.
10. the preparation method of described in any item chewing gums according to claim 1~9, which is characterized in that the preparation method packet
Include following steps:
(1) it will crush and be uniformly mixed comprising first raw material of formula (I) compound represented, sugar alcohol and softening agent, and obtain partial size
For 150 μm of first mixtures below；
(2) it will be mixed comprising the second raw material of citric acid and water, boil and stir 20~60min, be cooled to 60~80 DEG C, be made
Second mixture；
(3) matrix, lubricant, the first mixture and the second mixture after 70~90 DEG C of softenings are uniformly mixed, are added after cooling
Work molding, obtains the chewing gum.
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| CN201811607485.5A CN109480049A (en) | 2018-12-27 | 2018-12-27 | Chewing gum and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201811607485.5A CN109480049A (en) | 2018-12-27 | 2018-12-27 | Chewing gum and preparation method thereof |
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| CN109480049A true CN109480049A (en) | 2019-03-19 |
Family
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111869782A (en) * | 2020-05-11 | 2020-11-03 | 华南师范大学 | Antibacterial chewing gum for children and preparation method thereof |
| CN112262909A (en) * | 2020-10-28 | 2021-01-26 | 中山市华南现代中医药城发展有限公司 | Starch-based chewing-resistant chewing gum and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111869782A (en) * | 2020-05-11 | 2020-11-03 | 华南师范大学 | Antibacterial chewing gum for children and preparation method thereof |
| CN112262909A (en) * | 2020-10-28 | 2021-01-26 | 中山市华南现代中医药城发展有限公司 | Starch-based chewing-resistant chewing gum and preparation method thereof |
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