CN109464710A - A kind of silicone catheter development RTV liquid end socket glue - Google Patents
A kind of silicone catheter development RTV liquid end socket glue Download PDFInfo
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- CN109464710A CN109464710A CN201811543649.2A CN201811543649A CN109464710A CN 109464710 A CN109464710 A CN 109464710A CN 201811543649 A CN201811543649 A CN 201811543649A CN 109464710 A CN109464710 A CN 109464710A
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- end socket
- kneader
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L31/00—Materials for other surgical articles, e.g. stents, stent-grafts, shunts, surgical drapes, guide wires, materials for adhesion prevention, occluding devices, surgical gloves, tissue fixation devices
- A61L31/04—Macromolecular materials
- A61L31/06—Macromolecular materials obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L31/00—Materials for other surgical articles, e.g. stents, stent-grafts, shunts, surgical drapes, guide wires, materials for adhesion prevention, occluding devices, surgical gloves, tissue fixation devices
- A61L31/02—Inorganic materials
- A61L31/028—Other inorganic materials not covered by A61L31/022 - A61L31/026
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L31/00—Materials for other surgical articles, e.g. stents, stent-grafts, shunts, surgical drapes, guide wires, materials for adhesion prevention, occluding devices, surgical gloves, tissue fixation devices
- A61L31/14—Materials characterised by their function or physical properties, e.g. injectable or lubricating compositions, shape-memory materials, surface modified materials
- A61L31/18—Materials at least partially X-ray or laser opaque
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- Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Heart & Thoracic Surgery (AREA)
- Surgery (AREA)
- General Health & Medical Sciences (AREA)
- Epidemiology (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- Vascular Medicine (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physics & Mathematics (AREA)
- Optics & Photonics (AREA)
- Inorganic Chemistry (AREA)
- Materials For Medical Uses (AREA)
- Media Introduction/Drainage Providing Device (AREA)
Abstract
The invention discloses a kind of silicone catheter development RTV liquid end socket glue, including body material and liquid charging stock, the body material includes hydroxyl endblocked polydimethylsiloxane, methyl triacetoxysilane and white carbon black, raw material includes two type dry suspensoid agent of barium sulfate and pigment, the specific gravity of the body material and liquid charging stock is 7-9, the body material is grouped as by each group of following mass fraction: 60-90 parts of hydroxyl endblocked polydimethylsiloxane, 1-5 parts of methyl triacetoxysilane, 10-30 parts of white carbon black, the liquid charging stock is grouped as by each group of following mass fraction: 7-11 parts of two type dry suspensoid agent of barium sulfate, 1-5 parts of pigment, the pigment is set as the copper-bath of blue, it may be arranged as other colors, such as green and red etc..The preparation method of silicone catheter development RTV liquid end socket glue, durability degree and corrosion resistance that can be high-strength increase service life to a certain extent.
Description
Technical field
The invention belongs to clinical treatment urethral catheterization technical fields, and in particular to a kind of silicone catheter development RTV liquid end socket
Glue, the invention further relates to a kind of preparation methods of silicone catheter development RTV liquid end socket glue.
Background technique
Medically, catheter is per urethram inserted into bladder, drains urine.Urethral catheterization be divided into catheter retaining urethral catheterization and
Two kinds of the urethral catheterization of having a rest property.The former catheter is retained in always in patient body, just pulls out or regularly replace new pipe in state of an illness license.
The latter is then primary every urethral catheterization in 4-6 hours, extracts catheter after bladder emptying.Indwelling catheter operating procedure is by urethral catheterization
Pipe is inserted into appropriate depth (women 2-4cm, male 20-22cm), after seeing urine outflow, is inserted into 1-2cm.Then urethral catheterization is fixed
Pipe, connects drainage bag.It removes barriers situation for urine such as the retention of urine, the retention of urines.It is worth noting that, catheter should not repeat to make
With otherwise user is possible to by bacterium infection.But conventionally fabricated catheter durability degree is not high, along with use when
Between it is general longer, and need to import patient's body, it is therefore desirable to the catheter more renewed in time not only increases medical treatment cost,
And it is time-consuming and laborious.
Therefore it is directed to this status, there is an urgent need to design and produce a kind of silicone catheter development RTV liquid end socket glue, with
Meet the needs of actual use.
Summary of the invention
The purpose of the present invention is to provide a kind of silicone catheter development RTV liquid end socket glue, to solve above-mentioned background skill
The problem of being proposed in art.
To achieve the above object, the RTV liquid end socket the invention provides the following technical scheme: a kind of silicone catheter develops
Glue, including body material and liquid charging stock, the body material include hydroxyl endblocked polydimethylsiloxane, methyl triacetyl oxygen
Base silane and white carbon black, the liquid charging stock include two type dry suspensoid agent of barium sulfate and pigment, and the body material and liquid are former
The specific gravity of material is 7-9, and surplus is water;
The body material is grouped as by each group of following mass fraction: hydroxyl endblocked polydimethylsiloxane 60-90
Part, 1-5 parts of methyl triacetoxysilane, 10-30 parts of white carbon black;
The liquid charging stock is grouped as by each group of following mass fraction: 7-11 parts of two type dry suspensoid agent of barium sulfate,
1-5 parts of pigment.
Preferably, the pigment is set as the copper-bath of blue.
Preferably, the body material is grouped as by each group of following mass fraction: hydroxy-end capped polydimethylsiloxanes
70-80 parts of alkane, 2-4 parts of methyl triacetoxysilane, 15-25 parts of white carbon black.
Preferably, the liquid charging stock is grouped as by each group of following mass fraction: barium sulfate two type dry suspensoid agent
8-10 parts, 1-3 parts of pigment.
A kind of preparation method of silicone catheter development RTV liquid end socket glue, comprising the following steps:
S1, feedstock processing: body material is mixed according to specified component, is ground after being sufficiently mixed, then by liquid
Raw material is mixed according to specified component, and after being sufficiently mixed, body material is poured into liquid charging stock, is added according to degree of mixing suitable
Aqueous obtains mixed composition;
S2, kneader processing: importing in kneader in mixed composition, is stirred kneading uniformly, in kneading process first
Air in machine is exhausted, keeps it under vacuum state completely, kneader is heated to 40 degrees Celsius, revolving speed is maintained at 300-
1000r/min at the uniform velocity stirs 1-2h;
S3, cooling and shaping: being cooled to 30 degrees Celsius of 10min for kneader, then imports the mixed material in kneader
Ready mold.
Preferably, the model of the kneader is set as yil-3000L, and the body material is ground to 200 mesh.
Technical effect and advantage of the invention: the preparation method of silicone catheter development RTV liquid end socket glue, by setting
The hydroxyl endblocked polydimethylsiloxane set, so that the catheter being successfully prepared enhances durability, methyl triacetoxyl group silicon
Alkane as good crosslinking agent so that be stained with close it is more stable, also increase its durability degree to a certain extent, white carbon black is with super strength
Toughness and corrosion resistance also greatly improves the function of product, increased two type dry suspensoid agent of barium sulfate, so that product also possesses
X-ray is absorbed, has the function of radiography, when convenient for the operation such as radiography, finds the position of product, silicone catheter development
The preparation method of RTV liquid end socket glue, durability degree and corrosion resistance that can be high-strength increase service life to a certain extent.
Specific embodiment
Below in conjunction with the content of the embodiment of the present invention, technical solution in the embodiment of the present invention carries out clear, complete
Ground description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based on this
Embodiment in invention, every other reality obtained by those of ordinary skill in the art without making creative efforts
Example is applied, shall fall within the protection scope of the present invention.
Embodiment 1
A kind of silicone catheter development RTV liquid end socket glue, including body material and liquid charging stock, the body material packet
Hydroxyl endblocked polydimethylsiloxane, methyl triacetoxysilane and white carbon black are included, the liquid charging stock includes barium sulfate two
The specific gravity of type dry suspensoid agent and pigment, the body material and liquid charging stock is 7-9, and surplus is water;
The body material is grouped as by each group of following mass fraction: 60 parts of hydroxyl endblocked polydimethylsiloxane,
1 part of methyl triacetoxysilane, 10 parts of white carbon black;
The liquid charging stock is grouped as by each group of following mass fraction: 7 parts of two type dry suspensoid agent of barium sulfate, pigment
1 part.
Specifically, the pigment is set as the copper-bath of blue, may be arranged as other colors, for example, green and
Red etc..
A kind of preparation method of silicone catheter development RTV liquid end socket glue, comprising the following steps:
S1, feedstock processing: body material is mixed according to specified component, is ground after being sufficiently mixed, then by liquid
Raw material is mixed according to specified component, and after being sufficiently mixed, body material is poured into liquid charging stock, is added according to degree of mixing suitable
Aqueous obtains mixed composition;
S2, kneader processing: importing in kneader in mixed composition, is stirred kneading uniformly, in kneading process first
Air in machine is exhausted, keeps it under vacuum state completely, kneader is heated to 40 degrees Celsius, revolving speed is maintained at 300-
1000r/min at the uniform velocity stirs 1-2h;
S3, cooling and shaping: being cooled to 30 degrees Celsius of 10min for kneader, then imports the mixed material in kneader
Ready mold.
Specifically, the model of the kneader is set as yil-3000L, the body material is ground to 200 mesh.
Embodiment 2
A kind of silicone catheter development RTV liquid end socket glue, including body material and liquid charging stock, the body material packet
Hydroxyl endblocked polydimethylsiloxane, methyl triacetoxysilane and white carbon black are included, the liquid charging stock includes barium sulfate two
The specific gravity of type dry suspensoid agent and pigment, the body material and liquid charging stock is 7-9, and surplus is water;
The body material is grouped as by each group of following mass fraction: 90 parts of hydroxyl endblocked polydimethylsiloxane,
5 parts of methyl triacetoxysilane, 30 parts of white carbon black;
The liquid charging stock is grouped as by each group of following mass fraction: 11 parts of two type dry suspensoid agent of barium sulfate, face
5 parts of material.
Specifically, the pigment is set as the copper-bath of blue, may be arranged as other colors, for example, green and
Red etc..
A kind of preparation method of silicone catheter development RTV liquid end socket glue, comprising the following steps:
S1, feedstock processing: body material is mixed according to specified component, is ground after being sufficiently mixed, then by liquid
Raw material is mixed according to specified component, and after being sufficiently mixed, body material is poured into liquid charging stock, is added according to degree of mixing suitable
Aqueous obtains mixed composition;
S2, kneader processing: importing in kneader in mixed composition, is stirred kneading uniformly, in kneading process first
Air in machine is exhausted, keeps it under vacuum state completely, kneader is heated to 40 degrees Celsius, revolving speed is maintained at 300-
1000r/min at the uniform velocity stirs 1-2h;
S3, cooling and shaping: being cooled to 30 degrees Celsius of 10min for kneader, then imports the mixed material in kneader
Ready mold.
Specifically, the model of the kneader is set as yil-3000L, the body material is ground to 200 mesh.
Embodiment 3
A kind of silicone catheter development RTV liquid end socket glue, including body material and liquid charging stock, the body material packet
Hydroxyl endblocked polydimethylsiloxane, methyl triacetoxysilane and white carbon black are included, the liquid charging stock includes barium sulfate two
The specific gravity of type dry suspensoid agent and pigment, the body material and liquid charging stock is 7-9, and surplus is water;
The body material is grouped as by each group of following mass fraction: 70 parts of hydroxyl endblocked polydimethylsiloxane,
2 parts of methyl triacetoxysilane, 15 parts of white carbon black;
The liquid charging stock is grouped as by each group of following mass fraction: 8 parts of two type dry suspensoid agent of barium sulfate, pigment
2 parts.
Specifically, the pigment is set as the copper-bath of blue, may be arranged as other colors, for example, green and
Red etc..
A kind of preparation method of silicone catheter development RTV liquid end socket glue, comprising the following steps:
S1, feedstock processing: body material is mixed according to specified component, is ground after being sufficiently mixed, then by liquid
Raw material is mixed according to specified component, and after being sufficiently mixed, body material is poured into liquid charging stock, is added according to degree of mixing suitable
Aqueous obtains mixed composition;
S2, kneader processing: importing in kneader in mixed composition, is stirred kneading uniformly, in kneading process first
Air in machine is exhausted, keeps it under vacuum state completely, kneader is heated to 40 degrees Celsius, revolving speed is maintained at 300-
1000r/min at the uniform velocity stirs 1-2h;
S3, cooling and shaping: being cooled to 30 degrees Celsius of 10min for kneader, then imports the mixed material in kneader
Ready mold.
Specifically, the model of the kneader is set as yil-3000L, the body material is ground to 200 mesh.
Embodiment 4
A kind of silicone catheter development RTV liquid end socket glue, including body material and liquid charging stock, the body material packet
Hydroxyl endblocked polydimethylsiloxane, methyl triacetoxysilane and white carbon black are included, the liquid charging stock includes barium sulfate two
The specific gravity of type dry suspensoid agent and pigment, the body material and liquid charging stock is 7-9, and surplus is water;
The body material is grouped as by each group of following mass fraction: 80 parts of hydroxyl endblocked polydimethylsiloxane,
4 parts of methyl triacetoxysilane, 25 parts of white carbon black;
The liquid charging stock is grouped as by each group of following mass fraction: 10 parts of two type dry suspensoid agent of barium sulfate, face
4 parts of material.
Specifically, the pigment is set as the copper-bath of blue, may be arranged as other colors, for example, green and
Red etc..
A kind of preparation method of silicone catheter development RTV liquid end socket glue, comprising the following steps:
S1, feedstock processing: body material is mixed according to specified component, is ground after being sufficiently mixed, then by liquid
Raw material is mixed according to specified component, and after being sufficiently mixed, body material is poured into liquid charging stock, is added according to degree of mixing suitable
Aqueous obtains mixed composition;
S2, kneader processing: importing in kneader in mixed composition, is stirred kneading uniformly, in kneading process first
Air in machine is exhausted, keeps it under vacuum state completely, kneader is heated to 40 degrees Celsius, revolving speed is maintained at 300-
1000r/min at the uniform velocity stirs 1-2h;
S3, cooling and shaping: being cooled to 30 degrees Celsius of 10min for kneader, then imports the mixed material in kneader
Ready mold.
Specifically, the model of the kneader is set as yil-3000L, the body material is ground to 200 mesh.
Embodiment 5
A kind of silicone catheter development RTV liquid end socket glue, including body material and liquid charging stock, the body material packet
Hydroxyl endblocked polydimethylsiloxane, methyl triacetoxysilane and white carbon black are included, the liquid charging stock includes barium sulfate two
The specific gravity of type dry suspensoid agent and pigment, the body material and liquid charging stock is 7-9, and surplus is water;
The body material is grouped as by each group of following mass fraction: 75 parts of hydroxyl endblocked polydimethylsiloxane,
3 parts of methyl triacetoxysilane, 20 parts of white carbon black;
The liquid charging stock is grouped as by each group of following mass fraction: 9 parts of two type dry suspensoid agent of barium sulfate, pigment
3 parts.
Specifically, the pigment is set as the copper-bath of blue, may be arranged as other colors, for example, green and
Red etc..
A kind of preparation method of silicone catheter development RTV liquid end socket glue, comprising the following steps:
S1, feedstock processing: body material is mixed according to specified component, is ground after being sufficiently mixed, then by liquid
Raw material is mixed according to specified component, and after being sufficiently mixed, body material is poured into liquid charging stock, is added according to degree of mixing suitable
Aqueous obtains mixed composition;
S2, kneader processing: importing in kneader in mixed composition, is stirred kneading uniformly, in kneading process first
Air in machine is exhausted, keeps it under vacuum state completely, kneader is heated to 40 degrees Celsius, revolving speed is maintained at 300-
1000r/min at the uniform velocity stirs 1-2h;
S3, cooling and shaping: being cooled to 30 degrees Celsius of 10min for kneader, then imports the mixed material in kneader
Ready mold.
Specifically, the model of the kneader is set as yil-3000L, the body material is ground to 200 mesh.
Finally, it should be noted that the foregoing is only a preferred embodiment of the present invention, it is not intended to restrict the invention,
Although the present invention is described in detail referring to the foregoing embodiments, for those skilled in the art, still may be used
To modify the technical solutions described in the foregoing embodiments or equivalent replacement of some of the technical features,
All within the spirits and principles of the present invention, any modification, equivalent replacement, improvement and so on should be included in of the invention
Within protection scope.
Claims (6)
- The RTV liquid end socket glue 1. a kind of silicone catheter develops, it is characterised in that: described including body material and liquid charging stock Body material includes hydroxyl endblocked polydimethylsiloxane, methyl triacetoxysilane and white carbon black, the liquid charging stock packet Include two type dry suspensoid agent of barium sulfate and pigment, the specific gravity of the body material and liquid charging stock is 7-9, and surplus is water;The body material is grouped as by each group of following mass fraction: 60-90 parts of hydroxyl endblocked polydimethylsiloxane, first 1-5 parts of base triacetoxysilane, 10-30 parts of white carbon black;The liquid charging stock is grouped as by each group of following mass fraction: 7-11 parts of two type dry suspensoid agent of barium sulfate, pigment 1-5 parts.
- The RTV liquid end socket glue 2. a kind of silicone catheter according to claim 1 develops, it is characterised in that: the pigment It is set as the copper-bath of blue.
- The RTV liquid end socket glue 3. a kind of silicone catheter according to claim 1 develops, it is characterised in that: the main body Raw material is grouped as by each group of following mass fraction: 70-80 parts of hydroxyl endblocked polydimethylsiloxane, methyl triacetoxyl group 2-4 parts of silane, 15-25 parts of white carbon black.
- The RTV liquid end socket glue 4. a kind of silicone catheter according to claim 1 develops, it is characterised in that: the liquid Raw material is grouped as by each group of following mass fraction: 8-10 parts, 1-3 parts of pigment of two type dry suspensoid agent of barium sulfate.
- 5. a kind of a kind of preparation method of silicone catheter development RTV liquid end socket glue described in claim 1, feature exist In: the following steps are included:S1, feedstock processing: body material is mixed according to specified component, is ground after being sufficiently mixed, then by liquid charging stock It mixes according to specified component, after being sufficiently mixed, body material is poured into liquid charging stock, suitable water is added according to degree of mixing Liquid obtains mixed composition;S2, kneader processing: importing in kneader in mixed composition, is stirred kneading uniformly, first exhausts in kneading process Air in machine keeps it under vacuum state completely, kneader is heated to 40 degrees Celsius, revolving speed is maintained at 300-1000r/ Min at the uniform velocity stirs 1-2h;S3, cooling and shaping: being cooled to 30 degrees Celsius of 10min for kneader, then imports the mixed material in kneader and prepares Good mold.
- 6. a kind of preparation method of silicone catheter development RTV liquid end socket glue according to claim 5, feature exist In: the model of the kneader is set as yil-3000L, and the body material is ground to 200 mesh.
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CN201811543649.2A CN109464710A (en) | 2018-12-17 | 2018-12-17 | A kind of silicone catheter development RTV liquid end socket glue |
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CN201811543649.2A CN109464710A (en) | 2018-12-17 | 2018-12-17 | A kind of silicone catheter development RTV liquid end socket glue |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112169138A (en) * | 2020-10-30 | 2021-01-05 | 苏州伟康医疗器械有限公司 | End cap bonding process of catheter and catheter |
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CN1733841A (en) * | 2005-08-23 | 2006-02-15 | 广州吉必时科技实业有限公司 | Low cost room temperature silicon sulfide rubber composition |
GB2433497A (en) * | 2005-12-20 | 2007-06-27 | Dow Corning | Hydrophobic gypsum |
CN102558869A (en) * | 2011-12-21 | 2012-07-11 | 吴江朗科化纤有限公司 | Vulcanizing silicone rubber composite |
CN202682103U (en) * | 2012-03-31 | 2013-01-23 | 深圳市库珀科技发展有限公司 | Urinary catheterization support frame with developing soft head |
CN104710962A (en) * | 2015-03-26 | 2015-06-17 | 深圳诚立胜新材料科技有限公司 | Room-temperature vulcanized silicone rubber adhesive and preparation method thereof |
CN105038252A (en) * | 2015-08-13 | 2015-11-11 | 岳胜武 | Condensed type one-component room temperature vulcanized development adhesive and preparation method thereof |
CN205885943U (en) * | 2016-05-23 | 2017-01-18 | 南通伊诺精密塑胶导管有限公司 | J type catheter with strengthening rib |
CN107286339A (en) * | 2017-06-15 | 2017-10-24 | 苏州度博迈医疗科技有限公司 | A kind of preparation method and applications of antibacterial silicon rubber |
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US5932650A (en) * | 1996-01-26 | 1999-08-03 | General Electric Company | One component room temperature vulcanizable (RTV) silicone sealant with improved high temperature adhesion |
CN1733841A (en) * | 2005-08-23 | 2006-02-15 | 广州吉必时科技实业有限公司 | Low cost room temperature silicon sulfide rubber composition |
GB2433497A (en) * | 2005-12-20 | 2007-06-27 | Dow Corning | Hydrophobic gypsum |
CN102558869A (en) * | 2011-12-21 | 2012-07-11 | 吴江朗科化纤有限公司 | Vulcanizing silicone rubber composite |
CN202682103U (en) * | 2012-03-31 | 2013-01-23 | 深圳市库珀科技发展有限公司 | Urinary catheterization support frame with developing soft head |
CN104710962A (en) * | 2015-03-26 | 2015-06-17 | 深圳诚立胜新材料科技有限公司 | Room-temperature vulcanized silicone rubber adhesive and preparation method thereof |
CN105038252A (en) * | 2015-08-13 | 2015-11-11 | 岳胜武 | Condensed type one-component room temperature vulcanized development adhesive and preparation method thereof |
CN205885943U (en) * | 2016-05-23 | 2017-01-18 | 南通伊诺精密塑胶导管有限公司 | J type catheter with strengthening rib |
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Publication number | Priority date | Publication date | Assignee | Title |
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CN112169138A (en) * | 2020-10-30 | 2021-01-05 | 苏州伟康医疗器械有限公司 | End cap bonding process of catheter and catheter |
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Application publication date: 20190315 |