CN109456619A - A kind of iron oxide pigment that high chroma is oxidation-stabilized - Google Patents
A kind of iron oxide pigment that high chroma is oxidation-stabilized Download PDFInfo
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- CN109456619A CN109456619A CN201811379297.1A CN201811379297A CN109456619A CN 109456619 A CN109456619 A CN 109456619A CN 201811379297 A CN201811379297 A CN 201811379297A CN 109456619 A CN109456619 A CN 109456619A
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- weight
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- iron oxide
- oxidation
- stabilized
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/22—Compounds of iron
- C09C1/24—Oxides of iron
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
- C09C3/006—Combinations of treatments provided for in groups C09C3/04 - C09C3/12
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
- C09C3/06—Treatment with inorganic compounds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
- C09C3/08—Treatment with low-molecular-weight non-polymer organic compounds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
- C09C3/10—Treatment with macromolecular organic compounds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
- C09C3/12—Treatment with organosilicon compounds
Abstract
The invention discloses a kind of iron oxide pigments that high chroma is oxidation-stabilized, and the constitutive material that it includes is according to parts by weight are as follows: iron oxide yellow particle 45-55 parts by weight, sodium acetate solution 30-36 parts by weight, nanometer silicon carbide 1-3 parts by weight, fourth sodium dioctyl sulfo 2-6 parts by weight, glycerine 12-18 parts by weight, aluminum sulfate 2-4 parts by weight, Sorbitan carboxylic ester 3-5 parts by weight, polyacrylate 3-5 parts by weight, mica powder 1-3 parts by weight, mould inhibitor 1-3 parts by weight, complexing agent 2-4 parts by weight and tackifier 3-5 parts by weight.Instant component prepares rationally science, and the iron oxide pigment coloration of preparation is high, and oxidation stability is good, convenient for storing for a long time, good weatherability, mobility are strong, form and aspect it is with low uncertainty, dispersibility is excellent, meets the market requirement of iron oxide pigment, is with a wide range of applications.
Description
Technical field
The present invention relates to pigment technology field more particularly to a kind of iron oxide pigments that high chroma is oxidation-stabilized.
Background technique
Iron oxide pigment is that have good dispersibility, a kind of excellent fast light and weatherability pigment.Iron oxide pigment
It refers mainly to using the oxide of iron as the iron oxide red of base substance, four class coloring pigment of iron oxide yellow, iron oxide black and cologne earth, wherein with oxidation
Based on iron oxide red (about account for iron oxide pigment 50%), micaceous iron oxide as rust resisting pigment and it is used as magnetic record material
The magnetic iron oxide of material also belongs to the scope of iron oxide pigment.Iron oxide is the second largest inorganic pigment for being only second to titanium white, and
First big colored organic pigments.In the iron oxide pigment all consumed, 70% or more is prepared with chemical synthesis process, is claimed
Be synthetic iron oxide.Synthetic iron oxide due to its synthesis purity is high, uniform particle sizes it is neat, and chromatography is wide, color is more, it is inexpensive,
It is nontoxic, have excellent coloring and application performance, have and absorb the performances such as ultraviolet light, thus be widely used in building materials, coating, plastics,
The fields such as electronics, tobacco, medicine, rubber, ceramics, ink, magnetic material, papermaking.
Iron oxide pigment is the biggish pigment variety of coating industry dosage and coating production line toning integral system
Host inorganic coloured material.
Currently, relative to organic pigment, with density, big, particle is not easy to grind domestic iron oxide pigment in the prior art
Mill, storage during granules of pigments be easy sedimentation the defects of, and dispersing agent iron oxide pigment adsorption active force it is small, desorption
Phenomenon is serious, after long-time storage, easily because the reasons such as dispersing agent desorption, granules of pigments are reunited cause under color power
Drop.
Therefore, before preparing the iron oxide pigment that oxidation-stabilized, coloration is high, good weatherability, mobility are strong there is very big market
Scape.
Summary of the invention
To overcome above-mentioned deficiency, the present invention provides a kind of iron oxide pigment that high chroma is oxidation-stabilized.
The present invention takes following technical scheme to realize: a kind of iron oxide pigment that high chroma is oxidation-stabilized, it is wrapped
The constitutive material included is according to parts by weight are as follows: iron oxide yellow particle 45-55 parts by weight, sodium acetate solution 30-36 parts by weight, nano-sized carbon
SiClx 1-3 parts by weight, glycerine 12-18 parts by weight, aluminum sulfate 2-4 parts by weight, take off fourth sodium dioctyl sulfo 2-6 parts by weight
Water D-sorbite acid esters 3-5 parts by weight, polyacrylate 3-5 parts by weight, mica powder 1-3 parts by weight, mould inhibitor 1-3 parts by weight,
Complexing agent 2-4 parts by weight and tackifier 3-5 parts by weight；
The iron oxide yellow particle be by the surface modification agent containing carbamate structures to ferric oxide yellow pigment into
The modification of row surface obtains.
Further, complexing agent of the present invention is phenylalanine.
Further, tackifier of the present invention are coumarone indene resin.
Further, the constitutive material of the invention that it includes is according to parts by weight are as follows: 45 parts by weight of iron oxide yellow particle, acetic acid
36 parts by weight of sodium solution, 1 parts by weight of nanometer silicon carbide, 6 parts by weight of fourth sodium dioctyl sulfo, 12 parts by weight of glycerine, sulfuric acid
4 parts by weight of aluminium, 3 parts by weight of Sorbitan carboxylic ester, 5 parts by weight of polyacrylate, 1 parts by weight of mica powder, antimildew disinfectant 3
5 parts by weight of parts by weight, 2 parts by weight of complexing agent and tackifier.
Further, the constitutive material of the invention that it includes is according to parts by weight are as follows: 50 parts by weight of iron oxide yellow particle, acetic acid
33 parts by weight of sodium solution, 2 parts by weight of nanometer silicon carbide, 4 parts by weight of fourth sodium dioctyl sulfo, 15 parts by weight of glycerine, sulfuric acid
3 parts by weight of aluminium, 4 parts by weight of Sorbitan carboxylic ester, 4 parts by weight of polyacrylate, 2 parts by weight of mica powder, antimildew disinfectant 2
4 parts by weight of parts by weight, 3 parts by weight of complexing agent and tackifier.
Further, the constitutive material of the invention that it includes is according to parts by weight are as follows: 55 parts by weight of iron oxide yellow particle, acetic acid
30 parts by weight of sodium solution, 3 parts by weight of nanometer silicon carbide, 2 parts by weight of fourth sodium dioctyl sulfo, 18 parts by weight of glycerine, sulfuric acid
2 parts by weight of aluminium, 5 parts by weight of Sorbitan carboxylic ester, 3 parts by weight of polyacrylate, 3 parts by weight of mica powder, antimildew disinfectant 1
3 parts by weight of parts by weight, 4 parts by weight of complexing agent and tackifier.
Further, the mixture of the present invention for 2- pyridine mercaptan -1- zinc oxide and calcium phosphate.
In summary the invention has the following advantages: instant component prepares rationally science, the iron oxide face of preparation
Expect that coloration is high, oxidation stability is good, and convenient for long-term storage, good weatherability, mobility are strong, form and aspect it is with low uncertainty, dispersibility is excellent,
The market requirement for meeting iron oxide pigment, is with a wide range of applications.
Specific embodiment
To be easy to understand the technical means, the creative features, the aims and the efficiencies achieved by the present invention, below with reference to
Specific embodiment, the present invention is further explained.
A kind of oxidation-stabilized iron oxide pigment of the high chroma of embodiment 1
A kind of iron oxide pigment that high chroma is oxidation-stabilized, the constitutive material that it includes is according to parts by weight are as follows: iron oxide yellow particle
45 parts by weight, 36 parts by weight of sodium acetate solution, 1 parts by weight of nanometer silicon carbide, 6 parts by weight of fourth sodium dioctyl sulfo, glycerine
12 parts by weight, 4 parts by weight of aluminum sulfate, 3 parts by weight of Sorbitan carboxylic ester, 5 parts by weight of polyacrylate, 1 weight of mica powder
Part, 5 parts by weight of 3 parts by weight of antimildew disinfectant, 2 parts by weight of complexing agent and tackifier；
The iron oxide yellow particle be by the surface modification agent containing carbamate structures to ferric oxide yellow pigment into
The modification of row surface obtains.
As priority scheme of the invention, complexing agent of the present invention is phenylalanine.
As priority scheme of the invention, tackifier of the present invention are coumarone indene resin.
As priority scheme of the invention, the mixture of the present invention for 2- pyridine mercaptan -1- zinc oxide and calcium phosphate.
A kind of oxidation-stabilized iron oxide pigment of the high chroma of embodiment 2
A kind of iron oxide pigment that high chroma is oxidation-stabilized, the constitutive material that it includes is according to parts by weight are as follows: iron oxide yellow particle
50 parts by weight, 33 parts by weight of sodium acetate solution, 2 parts by weight of nanometer silicon carbide, 4 parts by weight of fourth sodium dioctyl sulfo, glycerine
15 parts by weight, 3 parts by weight of aluminum sulfate, 4 parts by weight of Sorbitan carboxylic ester, 4 parts by weight of polyacrylate, 2 weight of mica powder
Part, 4 parts by weight of 2 parts by weight of antimildew disinfectant, 3 parts by weight of complexing agent and tackifier；
The iron oxide yellow particle be by the surface modification agent containing carbamate structures to ferric oxide yellow pigment into
The modification of row surface obtains.
As priority scheme of the invention, complexing agent of the present invention is phenylalanine.
As priority scheme of the invention, tackifier of the present invention are coumarone indene resin.
As priority scheme of the invention, the mixture of the present invention for 2- pyridine mercaptan -1- zinc oxide and calcium phosphate.
A kind of oxidation-stabilized iron oxide pigment of the high chroma of embodiment 3
A kind of iron oxide pigment that high chroma is oxidation-stabilized, the constitutive material that it includes is according to parts by weight are as follows: iron oxide yellow particle
55 parts by weight, 30 parts by weight of sodium acetate solution, 3 parts by weight of nanometer silicon carbide, 2 parts by weight of fourth sodium dioctyl sulfo, glycerine
18 parts by weight, 2 parts by weight of aluminum sulfate, 5 parts by weight of Sorbitan carboxylic ester, 3 parts by weight of polyacrylate, 3 weight of mica powder
Part, 3 parts by weight of 1 parts by weight of antimildew disinfectant, 4 parts by weight of complexing agent and tackifier；
The iron oxide yellow particle be by the surface modification agent containing carbamate structures to ferric oxide yellow pigment into
The modification of row surface obtains.
As priority scheme of the invention, complexing agent of the present invention is phenylalanine.
As priority scheme of the invention, tackifier of the present invention are coumarone indene resin.
As priority scheme of the invention, the mixture of the present invention for 2- pyridine mercaptan -1- zinc oxide and calcium phosphate.
The above is the embodiment of the present invention, therefore all according to the institute of structure, feature and principle described in the present patent application range
The equivalent change or modification done, is included in the scope of the patent application of the present invention.
Claims (7)
1. a kind of iron oxide pigment that high chroma is oxidation-stabilized, it is characterised in that: the constitutive material that it includes is according to parts by weight are as follows:
Iron oxide yellow particle 45-55 parts by weight, sodium acetate solution 30-36 parts by weight, nanometer silicon carbide 1-3 parts by weight, butyric acid dioctyl ester
Sodium sulfonate 2-6 parts by weight, glycerine 12-18 parts by weight, aluminum sulfate 2-4 parts by weight, Sorbitan carboxylic ester 3-5 parts by weight,
Polyacrylate 3-5 parts by weight, mica powder 1-3 parts by weight, mould inhibitor 1-3 parts by weight, complexing agent 2-4 parts by weight and tackifier
3-5 parts by weight；
The iron oxide yellow particle be by the surface modification agent containing carbamate structures to ferric oxide yellow pigment into
The modification of row surface obtains.
2. a kind of oxidation-stabilized iron oxide pigment of high chroma according to claim 1, it is characterised in that: the complexing agent
For phenylalanine.
3. a kind of oxidation-stabilized iron oxide pigment of high chroma according to claim 1, it is characterised in that: the tackifier
For coumarone indene resin.
4. a kind of oxidation-stabilized iron oxide pigment of high chroma according to claim 1, it is characterised in that: the group that it includes
At raw material according to parts by weight are as follows: 45 parts by weight of iron oxide yellow particle, 36 parts by weight of sodium acetate solution, 1 parts by weight of nanometer silicon carbide,
6 parts by weight of fourth sodium dioctyl sulfo, 12 parts by weight of glycerine, 4 parts by weight of aluminum sulfate, 3 parts by weight of Sorbitan carboxylic ester,
5 parts by weight of polyacrylate, 1 parts by weight of mica powder, 5 weight of 3 parts by weight of antimildew disinfectant, 2 parts by weight of complexing agent and tackifier
Measure part.
5. a kind of oxidation-stabilized iron oxide pigment of high chroma according to claim 1, it is characterised in that: the group that it includes
At raw material according to parts by weight are as follows: 50 parts by weight of iron oxide yellow particle, 33 parts by weight of sodium acetate solution, 2 parts by weight of nanometer silicon carbide,
4 parts by weight of fourth sodium dioctyl sulfo, 15 parts by weight of glycerine, 3 parts by weight of aluminum sulfate, 4 parts by weight of Sorbitan carboxylic ester,
4 parts by weight of polyacrylate, 2 parts by weight of mica powder, 4 weight of 2 parts by weight of antimildew disinfectant, 3 parts by weight of complexing agent and tackifier
Measure part.
6. a kind of oxidation-stabilized iron oxide pigment of high chroma according to claim 1, it is characterised in that: the group that it includes
At raw material according to parts by weight are as follows: 55 parts by weight of iron oxide yellow particle, 30 parts by weight of sodium acetate solution, 3 parts by weight of nanometer silicon carbide,
2 parts by weight of fourth sodium dioctyl sulfo, 18 parts by weight of glycerine, 2 parts by weight of aluminum sulfate, 5 parts by weight of Sorbitan carboxylic ester,
3 parts by weight of polyacrylate, 3 parts by weight of mica powder, 3 weight of 1 parts by weight of antimildew disinfectant, 4 parts by weight of complexing agent and tackifier
Measure part.
7. a kind of oxidation-stabilized iron oxide pigment of high chroma according to claim 1, it is characterised in that: described is 2- pyrrole
The mixture of pyridine mercaptan -1- zinc oxide and calcium phosphate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811379297.1A CN109456619A (en) | 2018-11-19 | 2018-11-19 | A kind of iron oxide pigment that high chroma is oxidation-stabilized |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811379297.1A CN109456619A (en) | 2018-11-19 | 2018-11-19 | A kind of iron oxide pigment that high chroma is oxidation-stabilized |
Publications (1)
| Publication Number | Publication Date |
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| CN109456619A true CN109456619A (en) | 2019-03-12 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201811379297.1A Pending CN109456619A (en) | 2018-11-19 | 2018-11-19 | A kind of iron oxide pigment that high chroma is oxidation-stabilized |
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Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101760043A (en) * | 2009-03-23 | 2010-06-30 | 昆山市世名科技开发有限公司 | Low-foamed organic yellow pigment suspension for coloring plain-color base paper |
| CN103031023A (en) * | 2012-12-20 | 2013-04-10 | 广州市番禺科迪色彩有限公司 | Method for preparing iron oxide black water-based color paste with high performance-price ratio |
| CN104059435A (en) * | 2014-07-02 | 2014-09-24 | 苏州世名科技股份有限公司 | Iron oxide pigment water-based color paste for production line color matching and preparation method thereof |
| CN105567034A (en) * | 2016-02-02 | 2016-05-11 | 芜湖县双宝建材有限公司 | Rustproof anti-corrosion modified paint with high abrasion resistance |
| CN105851057A (en) * | 2011-11-17 | 2016-08-17 | 堺化学工业株式会社 | Surface treated zinc oxide powder, antibacterial agent, and antibacterial composition |
| CN107200359A (en) * | 2016-03-17 | 2017-09-26 | 北京中金瑞丰环保科技有限公司 | A kind of iron oxide pigment and its production method |
| CN108034305A (en) * | 2017-12-28 | 2018-05-15 | 常熟世名化工科技有限公司 | A kind of iron oxide pigment mill base and preparation method thereof |
| CN108719338A (en) * | 2018-06-01 | 2018-11-02 | 安徽中弘科技发展有限公司 | A kind of ordor removing mould inhibitor and preparation method thereof |
-
2018
- 2018-11-19 CN CN201811379297.1A patent/CN109456619A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101760043A (en) * | 2009-03-23 | 2010-06-30 | 昆山市世名科技开发有限公司 | Low-foamed organic yellow pigment suspension for coloring plain-color base paper |
| CN105851057A (en) * | 2011-11-17 | 2016-08-17 | 堺化学工业株式会社 | Surface treated zinc oxide powder, antibacterial agent, and antibacterial composition |
| CN103031023A (en) * | 2012-12-20 | 2013-04-10 | 广州市番禺科迪色彩有限公司 | Method for preparing iron oxide black water-based color paste with high performance-price ratio |
| CN104059435A (en) * | 2014-07-02 | 2014-09-24 | 苏州世名科技股份有限公司 | Iron oxide pigment water-based color paste for production line color matching and preparation method thereof |
| CN105567034A (en) * | 2016-02-02 | 2016-05-11 | 芜湖县双宝建材有限公司 | Rustproof anti-corrosion modified paint with high abrasion resistance |
| CN107200359A (en) * | 2016-03-17 | 2017-09-26 | 北京中金瑞丰环保科技有限公司 | A kind of iron oxide pigment and its production method |
| CN108034305A (en) * | 2017-12-28 | 2018-05-15 | 常熟世名化工科技有限公司 | A kind of iron oxide pigment mill base and preparation method thereof |
| CN108719338A (en) * | 2018-06-01 | 2018-11-02 | 安徽中弘科技发展有限公司 | A kind of ordor removing mould inhibitor and preparation method thereof |
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Application publication date: 20190312 |
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