CN109453537A - The crystallizer of crystallization and solution can be automatically separated - Google Patents
The crystallizer of crystallization and solution can be automatically separated Download PDFInfo
- Publication number
- CN109453537A CN109453537A CN201811397380.1A CN201811397380A CN109453537A CN 109453537 A CN109453537 A CN 109453537A CN 201811397380 A CN201811397380 A CN 201811397380A CN 109453537 A CN109453537 A CN 109453537A
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- crystallization
- box body
- solution
- stirred box
- plate
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0018—Evaporation of components of the mixture to be separated
- B01D9/0031—Evaporation of components of the mixture to be separated by heating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D2009/0086—Processes or apparatus therefor
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- Chemical & Material Sciences (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The invention discloses the crystallizers that can be automatically separated crystallization and solution, including stirred box body and crystallization cabinet, liquid pipe road was equipped between the stirred box body and the crystallization cabinet to be connected, agitating device is equipped at the top of the stirred box body, the agitating device includes motor, rotating bar and agitating paddle, the motor is placed at the top of the stirred box body, the rotating bar is connected to the power output end of the motor, and it protrudes into inside the stirred box body, the agitating paddle is mounted in the rotating bar, liquid inlet is equipped on the left of the stirred box body, right side is equipped with feeding inlet, the stirred box body bottom is equipped with taphole, the taphole is connected with the mistake liquid pipe road head end, after utilizing liquid pipe road that the intracorporal saturated solution of agitator tank is passed through crystallization cabinet, by the first crystallization plates , after the second crystallization plates and third crystallization plates, realize the effect of fractional crystallization and solution separation, improve crystalline rate and crystalline quality.
Description
Technical field
The present invention relates to crystalline compounds to store field, more particularly, to the crystallizer that can be automatically separated crystallization and solution.
Background technique
Gold potassium cyanide is important plating industrial chemicals, is the main gold-plated raw material of integrated circuit board or craftwork, main
It is used for plating and analytical reagent, the pharmaceuticals industry etc. of electronic product, can be acted on by potassium cyanide and aurous chloride and is made,
Since it is severe poisonous chemicals, toxicity substantially same potassium cyanide is about 0.1 gram of lethal dose, remaining molten after the crystallization of its solution is precipitated
Liquid still has also containing aurous cyanide potassium ion substance in its utility value, such as solution, so to its solution in crystallization process
Middle fractional crystallization and solution separation and recovery are necessary step.
Summary of the invention
The purpose of the present invention is to provide the crystallizers that can be automatically separated crystallization and solution, to solve in above-mentioned background technique
The problem of proposition.
To achieve the above object, the invention provides the following technical scheme:
The crystallizer of crystallization and solution can be automatically separated, including stirred box body and crystallization cabinet, the stirred box body with
Liquid pipe road was equipped between the crystallization cabinet to be connected, and agitating device was equipped at the top of the stirred box body, described stirs
Mixing device includes motor, rotating bar and agitating paddle, and the motor is placed at the top of the stirred box body, and the rotating bar connects
It is connected to the power output end of the motor, and is protruded into inside the stirred box body, the agitating paddle is mounted on described
Liquid inlet, right side are equipped in rotating bar, on the left of the stirred box body equipped with feeding inlet, the stirred box body bottom is equipped with molten
Liquid outlet, the taphole are connected with the mistake liquid pipe road head end, and described crosses liquid pipe end and the knot
Brilliant cabinet is connected, and the crystallization box house is respectively equipped with the first crystallization plates, the second crystallization plates and third knot from top to bottom
Brilliant plate, first crystallization plates include formed clamp plate, drainage plate, filter paper hole pattern and electric boiling plate, and the electric boiling plate is set
It is placed in the first crystallization plates bottom, the filter paper hole pattern is layed on the drainage plate, and the formed clamp plate is set
It is online to be placed in the filter paper hole, second crystallization plates and third crystallization plates also with the first crystallization plates internal structure
It is unanimously equipped with formed clamp plate, drainage plate, filter paper hole pattern and the electric boiling plate, the crystallization bottom of box is equipped with liquid
Mouthful.
As the further technical solution of the present invention, the formed clamp plate, drainage plate and filter paper hole pattern are odd test knot
Structure is assemblied in first crystallization plates, the second crystallization plates and third crystallization plates.
As the further technical solution of the present invention, the liquid inlet and the feeding inlet are equipped with meter.
As the further technical solution of the present invention, the taphole is pumped equipped with first pressure, the mistake liquid pipe
Road is pumped by described crystallization top of the box one end equipped with second pressure.
As the further technical solution of the present invention, the agitating paddle is spiral paddle.
As the further technical solution of the present invention, the formed clamp plate, drainage plate, filter paper hole pattern outside are equipped with pumping
Button.
The beneficial effects of the present invention are: after utilizing liquid pipe road that the intracorporal saturated solution of agitator tank is passed through crystallization cabinet,
After the first crystallization plates, the second crystallization plates and third crystallization plates, realizes the effect of fractional crystallization and solution separation, pass through starting
After electric boiling plate, the electric boiling plate saturated solution online to the filter paper hole on the first crystallization plates carries out heating crystalline, and crystallization is precipitated
Pressing molding pressing plate afterwards squeezes out remaining solution, opens drainage plate, remaining solution is put on the crystallization plates of the second level, such as
This is repeated once, and surplus solution is put on third crystallization plates, finally from liquid outlet pass-out, realizes fractional crystallization and solution separation
Effect, improve crystalline rate and crystalline quality.
Detailed description of the invention
Fig. 1 is schematic diagram of internal structure of the present invention.
Fig. 2 is the first crystallization plates of the invention, the second crystallization plates and third crystallization plates structural schematic diagram.
Wherein: stirred box body 1, crosses liquid pipe road 3, motor 4, rotating bar 5, agitating paddle 6, liquid inlet 7, pan feeding at crystallization cabinet 2
Mouth 8, taphole 9, the first crystallization plates 10, the second crystallization plates 11, third crystallization plates 12, formed clamp plate 13, drainage plate 14, filter paper
Hole pattern 15, liquid outlet 17, meter 18, first pressure pump 19, second pressure pump 20, takes out button 21 at electric boiling plate 16.
Specific embodiment
Embodiments of the present invention will be described with preferred embodiment with reference to the accompanying drawing.
It please refers to shown in Fig. 1 and Fig. 2 combination, the crystallizer of crystallization and solution, including stirred box body 1 and knot can be automatically separated
Brilliant cabinet 2 was equipped with liquid pipe road 3 between the stirred box body 1 and the crystallization cabinet 2 and was connected, the agitator tank
Agitating device is equipped at the top of body 1, the agitating device includes motor 4, rotating bar 5 and agitating paddle 6, and the motor 4 is placed in
1 top of stirred box body, the rotating bar 5 is connected to the power output end of the motor 4, and protrudes into described stir
It mixes inside cabinet 1, the agitating paddle 6 is mounted in the rotating bar 5, and liquid inlet is equipped on the left of the stirred box body 1
7, right side is equipped with feeding inlet 8, and 1 bottom of stirred box body is equipped with taphole 9, the taphole 9 and the mistake
3 head end of liquid pipe road is connected, and 3 end of mistake liquid pipe road is connected with the crystallization cabinet 2, the crystallization cabinet 2
Inside is respectively equipped with the first crystallization plates 10, the second crystallization plates 11 and third crystallization plates 12, first crystallization plates from top to bottom
10 include formed clamp plate 13, drainage plate 14, filter paper hole pattern 15 and electric boiling plate 16, and the electric boiling plate 16 is set to described
First crystallization plates, 10 bottom, the filter paper hole pattern 15 are layed on the drainage plate 14, and the formed clamp plate 13 is arranged
In on the filter paper hole pattern 15, second crystallization plates 11 and third crystallization plates 12 are also and in first crystallization plates 10
Portion's structure is unanimously equipped with formed clamp plate 13, drainage plate 14, filter paper hole pattern 15 and the electric boiling plate 16, the crystallization case
2 bottom of body is equipped with liquid outlet 17, and the formed clamp plate 13, drainage plate 14 and filter paper hole pattern 15 are odd test Standard in institute
In the first crystallization plates 10, the second crystallization plates 11 and the third crystallization plates 12 stated, put into from the liquid inlet 7 and feeding inlet 8 molten
Liquid and material start the motor 4, and the motor 4 drives the rotating bar 5 to rotate, and the agitating paddle 6 is to described
Stirred box body 1 in solution and after material is sufficiently stirred, from 9 pass-out of taphole, by the mistake liquid pipe road 3
Into in the crystallization cabinet 2, start the electric boiling plate 16, electric boiling plate 16 is to the filter paper hole on the first crystallization plates 10
Saturated solution on net 15 carries out heating crystalline, after crystallization is precipitated after pressing molding pressing plate 13, extracts the formed clamp plate 13 out,
Remaining solution is squeezed out, the drainage plate 14 is opened, remaining solution is put on second level crystallization plates 11, is so repeated
Above-mentioned steps are primary, surplus solution are put on the third crystallization plates 12, finally from 17 pass-out of liquid outlet, realize classification knot
The effect that crystalline substance is separated with solution improves crystalline rate and crystalline quality.
Further, the liquid inlet 7 and the feeding inlet 8 are equipped with meter 18, pass through the meter
18 metering blanking can control the component that feeds intake, and guarantee solution and solute proportion saturation just.
Further, the taphole 9 is equipped with first pressure pump 19, and the mistake liquid pipe road 3 leans on the crystallization
2 top one end of cabinet is equipped with second pressure pump 20, will be mixed in the stirred box body 1 by the pressurization of first pressure pump 19
Saturated solution extraction is closed, by the setting of the second pressure pump 20, water level is promoted to the mistake liquid pipe road 3, it is convenient full
It is passed through with solution in the crystallization cabinet 1
Further, the agitating paddle 6 is spiral paddle, is set as spirally capable of further promoting its stirring
Rate accelerates incorporation time, save the cost.
Further, the formed clamp plate 13, drainage plate 14, be equipped with pumping on the outside of filter paper hole pattern 15 and buckle 21, pass through pumping
Mouth 21 can be convenient for users to the extraction manually of the formed clamp plate 13, drainage plate 14, filter paper hole pattern 15.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims
Variation is included within the present invention.Any reference signs in the claims should not be construed as limiting the involved claims.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiments being understood that.
Claims (6)
1. the crystallizer of crystallization and solution can be automatically separated, including stirred box body (1) and crystallization cabinet (2), which is characterized in that institute
It was equipped with liquid pipe road (3) between the stirred box body (1) stated and the crystallization cabinet (2) to be connected, the stirred box body (1)
Top is equipped with agitating device, and the agitating device includes motor (4), rotating bar (5) and agitating paddle (6), the motor (4)
It is placed at the top of the stirred box body (1), the rotating bar (5) is connected to the power output end of the motor (4), and stretches
Enter stirred box body (1) inside, the agitating paddle (6) is mounted in the rotating bar (5), the stirred box body
(1) left side is equipped with liquid inlet (7), right side is equipped with feeding inlet (8), and the stirred box body (1) bottom is equipped with taphole (9),
The taphole (9) is connected with described mistake liquid pipe road (3) head end, mistake liquid pipe road (3) end and described
Crystallization cabinet (2) is connected, and is respectively equipped with the first crystallization plates (10), the second knot from top to bottom inside the crystallization cabinet (2)
Brilliant plate (11) and third crystallization plates (12), first crystallization plates (10) include formed clamp plate (13), drainage plate (14), filter paper
Hole pattern (15) and electric boiling plate (16), the electric boiling plate (16) is set to described the first crystallization plates (10) bottom, described
Filter paper hole pattern (15) be layed on the drainage plate (14), the formed clamp plate (13) is set to the filter paper hole pattern
(15) on, second crystallization plates (11) and third crystallization plates (12) also with described the first crystallization plates (10) internal structure one
It causes to be equipped with formed clamp plate (13), drainage plate (14), filter paper hole pattern (15) and the electric boiling plate (16), the crystallization case
Body (2) bottom is equipped with liquid outlet (17).
2. the crystallizer according to claim 1 for being automatically separated crystallization and solution, which is characterized in that the molding pressure
Plate (13), drainage plate (14) and filter paper hole pattern (15) are odd test Standard in first crystallization plates (10), the second knot
In brilliant plate (11) and third crystallization plates (12).
3. the crystallizer according to claim 1 for being automatically separated crystallization and solution, which is characterized in that the liquid inlet
(7) meter (18) are equipped with the feeding inlet (8).
4. the crystallizer according to claim 1 for being automatically separated crystallization and solution, which is characterized in that the solution goes out
Mouth (9) is equipped with first pressure pump (19), and the mistake liquid pipe road (3) is by described crystallization cabinet (2) the top one end equipped with second
Pressure pump (20).
5. the crystallizer according to claim 1 for being automatically separated crystallization and solution, which is characterized in that the agitating paddle
It (6) is spiral paddle.
6. the crystallizer according to claim 1 for being automatically separated crystallization and solution, which is characterized in that the molding pressure
Plate (13), drainage plate (14), filter paper hole pattern (15) outside are equipped with pumping and buckle (21).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811397380.1A CN109453537A (en) | 2018-11-22 | 2018-11-22 | The crystallizer of crystallization and solution can be automatically separated |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811397380.1A CN109453537A (en) | 2018-11-22 | 2018-11-22 | The crystallizer of crystallization and solution can be automatically separated |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109453537A true CN109453537A (en) | 2019-03-12 |
Family
ID=65611248
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811397380.1A Pending CN109453537A (en) | 2018-11-22 | 2018-11-22 | The crystallizer of crystallization and solution can be automatically separated |
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| Country | Link |
|---|---|
| CN (1) | CN109453537A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111097192A (en) * | 2019-12-27 | 2020-05-05 | 宁波乐维实业有限公司 | Separation device and separation method for triethylene diamine and ethanolamine |
| CN114668094A (en) * | 2022-03-10 | 2022-06-28 | 林磊 | Selenium-rich fruit and vegetable solid beverage and production process thereof |
Citations (8)
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|---|---|---|---|---|
| CN1251362A (en) * | 1999-09-28 | 2000-04-26 | 常州市常宇化工厂 | Industrialzed preparing method for high-purity alpha-nitro-naphthalene |
| JP2004194647A (en) * | 2003-04-28 | 2004-07-15 | Matsushita Electric Ind Co Ltd | Protein crystallization condition-screening device |
| CN2855495Y (en) * | 2005-11-16 | 2007-01-10 | 南京师范大学 | Multi-stage segamental continuous crystallizer |
| CN105664522A (en) * | 2016-03-25 | 2016-06-15 | 刘云海 | Chemical experiment efficient crystallization device |
| CN205472715U (en) * | 2016-03-31 | 2016-08-17 | 青岛阿库卡稀有金属有限公司 | Rehenic acid ammonium crystallization purification device |
| CN207237341U (en) * | 2017-07-25 | 2018-04-17 | 四川赛卓药业股份有限公司 | A kind of rapid crystallization system in intermediate of cefixime production technology |
| CN207641033U (en) * | 2017-11-07 | 2018-07-24 | 南京师范大学 | A kind of continuous multi-stage axial direction stirred crystallization and filtering integral device |
| CN108675333A (en) * | 2018-08-29 | 2018-10-19 | 河北云瑞化工设备有限公司 | The Continuous Cooling Crystallization technique of potassium alum is detached from lithium-containing solution |
-
2018
- 2018-11-22 CN CN201811397380.1A patent/CN109453537A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1251362A (en) * | 1999-09-28 | 2000-04-26 | 常州市常宇化工厂 | Industrialzed preparing method for high-purity alpha-nitro-naphthalene |
| JP2004194647A (en) * | 2003-04-28 | 2004-07-15 | Matsushita Electric Ind Co Ltd | Protein crystallization condition-screening device |
| CN2855495Y (en) * | 2005-11-16 | 2007-01-10 | 南京师范大学 | Multi-stage segamental continuous crystallizer |
| CN105664522A (en) * | 2016-03-25 | 2016-06-15 | 刘云海 | Chemical experiment efficient crystallization device |
| CN205472715U (en) * | 2016-03-31 | 2016-08-17 | 青岛阿库卡稀有金属有限公司 | Rehenic acid ammonium crystallization purification device |
| CN207237341U (en) * | 2017-07-25 | 2018-04-17 | 四川赛卓药业股份有限公司 | A kind of rapid crystallization system in intermediate of cefixime production technology |
| CN207641033U (en) * | 2017-11-07 | 2018-07-24 | 南京师范大学 | A kind of continuous multi-stage axial direction stirred crystallization and filtering integral device |
| CN108675333A (en) * | 2018-08-29 | 2018-10-19 | 河北云瑞化工设备有限公司 | The Continuous Cooling Crystallization technique of potassium alum is detached from lithium-containing solution |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111097192A (en) * | 2019-12-27 | 2020-05-05 | 宁波乐维实业有限公司 | Separation device and separation method for triethylene diamine and ethanolamine |
| CN114668094A (en) * | 2022-03-10 | 2022-06-28 | 林磊 | Selenium-rich fruit and vegetable solid beverage and production process thereof |
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| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
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| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20190312 |