CN209636125U - A kind of process units for the urea that rises in value - Google Patents

A kind of process units for the urea that rises in value Download PDF

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Publication number
CN209636125U
CN209636125U CN201920199613.0U CN201920199613U CN209636125U CN 209636125 U CN209636125 U CN 209636125U CN 201920199613 U CN201920199613 U CN 201920199613U CN 209636125 U CN209636125 U CN 209636125U
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synergy liquid
synergy
liquid reaction
standing
slot
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张立岗
封建利
边利利
张进华
翟琛
王�锋
穆荣斌
孙伟民
王博
黄海明
王泉弟
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Shaanxi Shan Hua Coal Chemical Industry Group Co ltd
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Shaanxi Shan Hua Coal Chemical Industry Group Co ltd
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Abstract

The utility model provides a kind of process units of urea that rises in value, including two synergy liquid reaction kettles, two standing slots and chute feeder, two synergy liquid reaction kettles and two standing slots are connected to by the first pipe network system with chute feeder, the synergy liquid of the synergy liquid reaction kettle is delivered to chute feeder, or the synergy liquid after standing in the standing slot is delivered to chute feeder;Two synergy liquid reaction kettles are connected to by pipe-line system with two standing slots, in the same time, the synergy liquid prepared is sent to any one to stand in slot and be stood by an only synergy liquid reaction kettle, another synergy liquid reaction kettle prepares synergy liquid, another stands slot and stands synergy liquid.The utility model uses two sets of liquid dispensing containers (two synergy liquid reaction kettles and two standing slots), substantially meets full-time production dosage with liquid (4t) every time, reduces humic acid in synergy liquid and fluctuates and influence finished urea inherent quality.

Description

A kind of process units for the urea that rises in value
Technical field
The utility model relates to urea production equipment more particularly to a kind of process units for the urea that rises in value of rising in value.
Background technique
The urea that rises in value includes zinc corruption uraturia element, cereal element urea, humic acid urea etc..By taking zinc corruption uraturia element as an example, zinc is rotten Acid is a kind of small molecule humic acid fertilizer synergist containing microelement, extracts plant by special microbial fermentation technology Object natural active matter.Zinc corruption uraturia element is the increment urine that the rotten sour chelate fertilizer synergist production of zinc is added in common urea Element.
The process flow of increment urea is on the basis of conventional urea process flow, by the rotten sour synergy liquid of the zinc prepared (cereal element synergist, fulvic acid synergist) enters to stand slot by centrifugal pumping, then utilizes after being sent into chute feeder by centrifugal pump Metering pump is quantitatively adding in dual circulation inlet line solution, enters after being sufficiently mixed and output after granulation is sent to meet company standard The zinc corruption uraturia element of Q/SHHG 001-2016 and standard GB/T 2440-2001.
Existing increment urea plant, the preparation raw material synergy liquid time is longer, and fluctuation of concentration is big.Therefore, it is necessary to right Original process units is improved, to reduce the preparation time of raw material synergy liquid.
Summary of the invention
The utility model provides a kind of process units of urea that rises in value, and is cooperated using two sets of liquid dispensing containers, and two sets Liquid dispensing container substantially meets full-time production dosage, reduces humic acid in synergy liquid and fluctuates and influence finished urea inherent quality.
Realize that the technical solution of the utility model aim is as follows:
A kind of process units for the urea that rises in value, including two synergy liquid reaction kettles, two standing slots and chute feeder, two A synergy liquid reaction kettle and two standing slots are connected to by the first pipe network system with chute feeder, by the increasing of the synergy liquid reaction kettle Effect liquid is delivered to chute feeder, or the synergy liquid after standing in the standing slot is delivered to chute feeder;
Two synergy liquid reaction kettles are connected to by pipe-line system with two standing slots, in the same time, an only synergy The synergy liquid prepared is sent to any one to stand in slot and be stood by liquid reaction kettle, another synergy liquid reaction kettle prepares synergy liquid, Another stands slot and stands synergy liquid.
The utility model uses two sets of liquid dispensing containers (two synergy liquid reaction kettles and two standing slots), matches liquid (4t) every time Full-time production dosage is substantially met, reduces humic acid in synergy liquid and fluctuates and influence finished urea inherent quality.
First pipe network system is equipped with feeding engine, second pipe network as a further improvement of the utility model, System is equipped with dosing pump.The utility model is sent synergy liquid to chute feeder by feeding engine, in any synergy liquid reaction kettle Synergy liquid is pumped to any standing slot by ingredient, and feeding engine and dosing pump are centrifugal pump, adds two centrifugal pumps with fixation Pipeline transfers synergy liquid, reduces manpower, while solving environmental pollution.
The outlet end of the dosing pump is also piped by branch anti-with synergy liquid as a further improvement of the utility model, Kettle is answered to be connected to, the synergy solution prepared in synergy liquid reaction kettle is transported to branch through the second pipe network system by the dosing pump It is piped, the synergy solution in branch piping flow to this synergy liquid reaction kettle again.The utility model is prepared in synergy liquid reaction kettle to be increased During imitating liquid, the synergy liquid that autosynergism liquid reaction kettle flows out is led to synergy liquid reaction kettle, In by the piping of dosing pump export branch road Solution is played in synergy liquid preparation process and beats ringing, improves synergy liquid preparation efficiency.
Filter, the filter are additionally provided in second pipe network system as a further improvement of the utility model, Between dosing pump and two standing slots.The utility model installs filter between standing slot in dosing pump, reduces impurity Into system;Preferred filters are two, and dosing pump is arranged in parallel and stands between slot for two filters, and two filters are same When work, to synergy liquid carry out contaminant filter.
The peripheral wall for standing slot, which is equipped with, as a further improvement of the utility model, stands solution in slot for heating Steam pipe coil.The steam pipe coil of the utility model makes to stand synergy liquid temperature in slot and remains 40-50 DEG C, is always ensured that quiet It sets slot and is in flow regime.
Detailed description of the invention
Fig. 1 is the functional block diagram of process units.
In figure, 1, synergy liquid reaction kettle;11, steam;2, slot is stood;3, chute feeder;4, dosing pump;5, feeding engine;6, mistake Filter;7, flushing water;8, head is got rid of.
Specific embodiment
The utility model is described in detail in each embodiment shown in reference to the accompanying drawing, but it should be stated that, These embodiments are not limitation of the utility model, those of ordinary skill in the art according to these embodiments made by function Energy, method or equivalent transformation or substitution in structure, belong within the protection scope of the utility model.
In the description of the present embodiment, it is to be understood that term " center ", " longitudinal direction ", " transverse direction ", "upper", "lower", The orientation or positional relationship of the instructions such as "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outside" is It is based on the orientation or positional relationship shown in the drawings, is merely for convenience of description the invention and simplifies description, rather than indicate Or imply that signified device or element must have a particular orientation, be constructed and operated in a specific orientation, therefore cannot understand For the limitation to the invention.
In addition, term " first ", " second ", " third " etc. are used for description purposes only, it is not understood to indicate or imply Relative importance or the quantity for implicitly indicating indicated technical characteristic.The feature of " first ", " second " etc. is defined as a result, It can explicitly or implicitly include one or more of the features.In the description of the invention, unless otherwise indicated, The meaning of " plurality " is two or more.
Term " installation ", " connected ", " connection " shall be understood in a broad sense, for example, it may be being fixedly connected, be also possible to removable Connection is unloaded, or is integrally connected;It can be mechanical connection, be also possible to be electrically connected;It can be directly connected, it can also be in Between medium be indirectly connected, can be the connection inside two elements.For the ordinary skill in the art, can pass through Concrete condition understands concrete meaning of the above-mentioned term in the invention.
Embodiment 1:
By taking existing zinc corruption uraturia element as an example, the scheme of the present embodiment is discussed in detail.Existing zinc corruption uraturia element is mating to match The raw material synergy liquid time processed is longer, and fluctuation of concentration is big;Self priming pump pumps liquid of appreciating and enlarging and easily causes damage, and joint connection in site leather hose It is more, cause environment to influence;When production increment urea, capacitance liquid level meter instruction is wrong, and live visor is difficult to observe;Molten hopper without Liquid level facility, with liquid with reference to difficult;Urea particle intensity is low;
Analysis: preparation synergy liquid measure is 2 tons to trial production period synergy liquid reaction kettle 1 every time, and synergy liquid fills two tons every time Bucket causes in two tons of buckets solution humic acid content difference, urinates finished product because pump intake accesses 1 bottom of synergy liquid reaction kettle Humic acid content impacts in element, need frequently to adjust metering pump knob under same produce load stablize in finished urea Quality.
Contain 30% or so bursting type hollow granule in finished urea particle, analyzed through technology, is contained in humic acid material Caused by insoluble impurity, urine from granulation spray head circumgyration incision be small liquid pearl, due to effect interior impure and in surface tension Under, hollow granule is formd, finished urea intensity is caused to decline.
During preparing synergy liquid, add microelement after, solution stirred and high temperature after generate foam, synergist adds It after adding to evaporation section, causes urine to blister at secondary vacuum seperator collector, influences capacitance liquid level meter instruction and deviate, and formed Urine foam (include and do not allow impurity) easily cause aperture clogs at the top of prilling spry, cause spray head overflow, generated in belt big The blister particle for measuring peanut grain size, influences urea external quality.
With small-sized self priming pump with standing slot 2 before acidproof hose conveying synergy liquid to metering pump, operating process when trial production It is complex, and easily production environment is polluted.
During the present embodiment device produces zinc corruption uraturia element, workload control adds synergist about in 18t/h 12Kg/t, former 1 preparation ability of synergy liquid reaction kettle once only meets about 8 hours dosages, therefore carries out more to the synergy liquid reaction kettle 1 1 equipment of synergy liquid reaction kettle is changed and added, substantially meets full-time production dosage with liquid every time, reduces humic acid in synergy liquid It fluctuates and influences finished urea inherent quality.The core improvement of the present embodiment is:
1, it is installed filter 6 two (operation one is standby) in synergy liquid reaction kettle 1 to 2 outlet of centrifugal pump of slot is stood, it is built-in 80 mesh filter screen of detachable, periodically carries out cleaning cleaning to filter screen;It prevents from a large amount of insoluble impurity from entering to stand in slot 2.
2, synergy liquid ton bucket storage be not easy to keep the temperature, therefore add two volumes be 4t stand slot 2, peripheral hardware steam pipe coil, It stands synergy liquid temperature in slot 2 and remains 40-50 DEG C, be always ensured that liquid fluidity state;The standing slot 2 has molten simultaneously Liquid stands effect, and matched solution does not allow impurity to be sink to slot bottom after 10 hours or more standings;Impurity is avoided to enter system, it is right The external quality of urea impacts.The position of steam pipe coil is to stand to wind from up to down outside slot 2.Tank liquid needs to protect Good fluidity is held, temperature is controlled at 40-50 DEG C, and the excessively high moisture that will cause of temperature largely evaporates, and synergy liquid concentration changes, The too low liquid physical state that will cause of temperature changes, poor fluidity
3, to avoid a large amount of foams of solution generation after addition microelement from impacting production system and finished urea, In A small amount of auxiliary agent is manually added in chute feeder 3 eliminates foam.
4, it adds two centrifugal pumps (dosing pump 4+ feeding engine 5) and transfers synergy liquid with fixed pipelines, reduce manpower, solve simultaneously It has determined environmental pollution.
It should be noted that the synergy liquid reaction kettle of the present embodiment includes external kettle body, interior autoclave body, in insertion inside autoclave body Rabbling mechanism, interior autoclave body are located at the inner cavity of external kettle body, insulating layer are additionally provided with before external kettle body and interior autoclave body, and interior autoclave body is clamped In the upper end of external kettle body, the top of interior autoclave body is equipped with kettle cover, and kettle cover blocks the opening of interior autoclave body, and rabbling mechanism is inserted into from kettle cover Inside interior autoclave body.The liquid outlet of synergy liquid reaction kettle is located at the bottom end of interior autoclave body, and the inlet of synergy liquid reaction kettle is located at interior kettle The top of body.
It please join shown in Fig. 1, Fig. 1 is the functional block diagram of process units.The process units of the increment urea of the present embodiment, including Two synergy liquid reaction kettles, 1, two standing slot 2 and chute feeder 3, two synergy liquid reaction kettles 1 and two standing slots 2 pass through First pipe network system is connected to chute feeder 3, the synergy liquid of synergy liquid reaction kettle 1 is delivered to chute feeder 3, or will stand slot 2 Synergy liquid after interior standing is delivered to chute feeder 3;Two synergy liquid reaction kettles 1 are connected to by pipe-line system with two standing slots 2, In the same time, the synergy liquid prepared is sent to any one to stand in slot 2 and be stood by an only synergy liquid reaction kettle 1, another A synergy liquid reaction kettle 1 prepares synergy liquid, another stands slot 2 and stands synergy liquid.The present embodiment is using two sets of synergy liquid reactions Two synergy liquid reaction kettles 1 of kettle 1(and two standing slots 2), full-time production dosage is substantially met with liquid (4t) every time, reduces increasing Humic acid fluctuates and influences finished urea inherent quality in effect liquid.
In the present embodiment, preferably the first pipe network system is equipped with feeding engine 5, and the second pipe network system is equipped with dosing pump 4.The present embodiment is sent synergy liquid to chute feeder 3 by feeding engine 5, and the synergy liquid in any synergy liquid reaction kettle 1 passes through ingredient Pump 4 is sent to any standing slot 2, and feeding engine 5 and dosing pump 4 are centrifugal pump, is added two centrifugal pumps with fixed pipelines and is transferred increasing Liquid is imitated, reduces manpower, while solving environmental pollution.
In the present embodiment, the outlet end of preferred formulations pump 4 is also piped by branch is connected to synergy liquid reaction kettle 1, The synergy solution prepared in synergy liquid reaction kettle 1 is transported to branch piping through the second pipe network system by dosing pump 4, and branch is matched Synergy solution in pipe flow to this synergy liquid reaction kettle 1 again.The present embodiment during synergy liquid reaction kettle 1 prepares synergy liquid, The synergy liquid that autosynergism liquid reaction kettle 1 flows out is led to synergy liquid reaction kettle 1 by the piping of 4 export branch road of dosing pump, in synergy liquid system Solution is played during standby and beats ringing, improves synergy liquid preparation efficiency.
In the present embodiment, filter 6 is preferably additionally provided in the second pipe network system, filter 6 is located at dosing pump 4 and two Between a standing slot 2.The present embodiment, to installation filter 6 between slot 2 is stood, reduces impurity and enters system in dosing pump 4;It is preferred that Filter 6 is two, and setting in dosing pump 4 and is stood between slot 2 two filters 6 parallel, and two filters 6 work at the same time, Contaminant filter is carried out to synergy liquid.
In the present embodiment, the peripheral wall for preferably standing slot 2 is equipped with for heating the steam disc for standing solution in slot 2 Pipe.The steam pipe coil of the present embodiment makes to stand synergy liquid temperature in slot 2 and remains 40-50 DEG C, is always ensured that standing slot 2 is in Flow regime.
Embodiment 2:
On the basis of embodiment 1, the present embodiment to synergy liquid with the improvement of liquid facility after, external quality is more in urea Stablize, process and operation are more easy, are both able to satisfy production requirement without in addition increasing staff.
1, increase synergy liquid reaction kettle 1 two, substantially meet full-time production dosage with liquid (4t) every time, reduce in synergy liquid Humic acid fluctuates and influences finished urea inherent quality;
2, filter 6 two are installed to 2 outlet of centrifugal pump of slot is stood in synergy liquid reaction kettle 1, reduces impurity and enters system;
3, two centrifugal pumps are added and transfer synergy liquid with fixed pipelines, reduce manpower, while solving environmental pollution and asking Topic.
Liquid equipment is set up using old material, installs synergy liquid Agitation Tank one, raw materials hole, inside peace is arranged in top Dress one, blender, this system decomposition of effluent ammonia-nitrogen content are lower than 10mg/L, can be used as and use with liquid, had both reduced outer displacement, Fresh desalted water has been saved again;Firstly, humic acid material and system decomposition of effluent are proportionally added into Agitation Tank, stir evenly, Certain temperature is kept, the reaction was continued for rear addition microelement, and configured synergy liquid is sent after analysis is qualified using dosing pump 4 It is stood to slot 2 is stood, in addition, the piping of outlet of centrifugal pump branch leads to Agitation Tank, solution can be played in synergy liquid preparation process Ringing is beaten, synergy liquid preparation efficiency is improved;After storage synergy liquid transfers to chute feeder 3 using feeding engine 5 in standing slot 2, Dual circulation system is pumped to by metering to mix with urine, after heated separation, is pumped by urea melting to prilling spry.
It has produced qualified nearly 20,000 tons of zinc corruption uraturia element at present to put goods on the market, supply falls short of demand for product;Increment urea is in city at present There is biggish development space in field, and the set technological transformation device can also produce the increment urea such as cereal element, fulvic acid from now on, has biggish Utility value
The urea technique original process of the present embodiment does not make any changes, and the rotten sour synergy liquid of the zinc prepared passes through centrifugal pumping Enter to stand slot 2, then is sent into after chute feeder 3 by centrifugal pump and is quantitatively adding dual circulation inlet line solution using metering pump In, enter after being sufficiently mixed and output after granulation is sent to meet company standard Q/SHHG 001-2016 and standard GB/T 2440- 2001 zinc corruption uraturia element.
Tool of the series of detailed descriptions listed above only for the feasible embodiment of the utility model Body explanation, they are all without departing from made by the utility model skill spirit not to limit the protection scope of the utility model Equivalent implementations or change should be included within the scope of protection of this utility model.
It is obvious to a person skilled in the art that the present invention is not limited to the details of the above exemplary embodiments, and And without departing substantially from the spirit or essential attributes of the utility model, it can realize that this is practical new in other specific forms Type.Therefore, in all respects, the present embodiments are to be considered as illustrative and not restrictive, this is practical new The range of type is indicated by the appended claims rather than the foregoing description, it is intended that containing for the equivalent requirements of the claims will be fallen in All changes in justice and range are embraced therein.It should not treat any reference in the claims as limiting Related claim.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art The other embodiments being understood that.

Claims (5)

1. a kind of process units for the urea that rises in value, which is characterized in that including two synergy liquid reaction kettles (1), two standing slots (2) and chute feeder (3), two synergy liquid reaction kettles (1) and two standing slots (2) pass through the first pipe network system and chute feeder (3) it is connected to, the synergy liquid of the synergy liquid reaction kettle (1) is delivered to chute feeder (3), or will be quiet in the standing slot (2) The synergy liquid postponed is delivered to chute feeder (3);
Two synergy liquid reaction kettles (1) are connected to by the second pipe network system with two standing slots (2), in the same time, only one The synergy liquid prepared is sent to any one to stand in slot (2) and be stood by a synergy liquid reaction kettle (1), another synergy liquid reaction kettle (1) synergy liquid is prepared, another stands slot (2) and stands synergy liquid.
2. process units according to claim 1, which is characterized in that first pipe network system is equipped with feeding engine (5), Second pipe network system is equipped with dosing pump (4).
3. process units according to claim 2, which is characterized in that the outlet end of the dosing pump (4) also passes through branch Piping is connected to synergy liquid reaction kettle (1), the synergy solution that the dosing pump (4) will prepare in synergy liquid reaction kettle (1) It is transported to branch piping through the second pipe network system, the synergy solution in branch piping flow to synergy liquid reaction kettle (1) again.
4. process units according to claim 2, which is characterized in that be additionally provided with filter in second pipe network system (6), the filter (6) is located between dosing pump (4) and two standing slots (2).
5. process units according to claim 1-4, which is characterized in that set on the peripheral wall for standing slot (2) Have for heating the steam pipe coil for standing slot (2) interior solution.
CN201920199613.0U 2019-02-15 2019-02-15 A kind of process units for the urea that rises in value Active CN209636125U (en)

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