CN109399618A - A kind of reaction unit preparing automobile-used graphene - Google Patents
A kind of reaction unit preparing automobile-used graphene Download PDFInfo
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- CN109399618A CN109399618A CN201811644863.7A CN201811644863A CN109399618A CN 109399618 A CN109399618 A CN 109399618A CN 201811644863 A CN201811644863 A CN 201811644863A CN 109399618 A CN109399618 A CN 109399618A
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- reaction chamber
- pipe
- reactive tank
- sparge pipe
- partition
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/15—Nano-sized carbon materials
- C01B32/182—Graphene
- C01B32/184—Preparation
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- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Nanotechnology (AREA)
- Inorganic Chemistry (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The invention discloses a kind of reaction units for preparing automobile-used graphene, including reaction chamber, sparge pipe and reactive tank, the inside of the reaction chamber is fixedly installed with partition, the reaction chamber is provided with upper cavity and lower cavity by the partition, the upper cavity is internally provided with the reactive tank, the reactive tank is fixedly mounted on the top of the partition, the reactive tank is internally provided with sparge pipe, the sparge pipe is fixedly mounted on the inside of the reactive tank by sparge pipe fixed link, one end of the sparge pipe is connected with recycling outlet by pipe connecting sleeve, the side of the reaction chamber is fixedly installed with water pump, the recycling outlet is fixedly mounted on the top of the water pump, the bottom of the water pump is fixedly installed with function of circular water absorption pipe, having heaters is fixedly mounted in the inside of the lower cavity.The present invention makes the present apparatus have the characteristics that temperature raising speed fastly and be heated evenly by the way that a series of structure is arranged.
Description
Technical field
The present invention relates to technical field of graphene preparation, specially a kind of reaction unit for preparing automobile-used graphene.
Background technique
Graphene is a kind of Two-dimensional Carbon nanometer material for forming hexangle type in honeycomb lattice with sp2 hybridized orbit by carbon atom
Material, since being found, graphene causes the strong research interest of scientific circles, since graphene has monatomic thickness
Degree, therefore be widely used as the basic unit of various labyrinths, in recent years, low cost, the large scale preparation of graphene
Obtain tremendous development.
But it is existing be used as the reaction unit for preparing graphene, during graphite alkene reaction, temperature control effect is bad,
The speed of heating is slow, and is also easy to the phenomenon that temperature distribution is non-uniform occur, so that graphene is during reaction
Reaction effect is poor, therefore the progress for being unfavorable for accelerating reaction prepares vehicle to solve this series of problems we have proposed a kind of
It is solved the problems, such as with the reaction unit of graphene.
Summary of the invention
The purpose of the present invention is to provide a kind of reaction units for preparing automobile-used graphene, to solve in above-mentioned background technique
The problem of proposition.
To achieve the above object, the invention provides the following technical scheme: a kind of reaction unit for preparing automobile-used graphene, packet
Include reaction chamber, sparge pipe and reactive tank, the inside of the reaction chamber is fixedly installed with partition, both ends of the partition and described anti-
Answer the inner wall of case two sides by being welded and fixed, and the reaction chamber is provided with upper cavity and lower cavity by the partition,
The upper cavity is internally provided with the reactive tank, and the reactive tank is fixedly mounted on the top of the partition, described anti-
The sparge pipe that is internally provided with of slot is answered, the sparge pipe is fixedly mounted on the inside of the reactive tank by sparge pipe fixed link,
One end of the sparge pipe is connected with recycling outlet by pipe connecting sleeve, and the side of the reaction chamber is fixedly installed with water
Pump, the recycling outlet are fixedly mounted on the top of the water pump, and the bottom of the water pump is fixedly installed with function of circular water absorption pipe,
One end of the function of circular water absorption pipe extends to the inside of the reactive tank by the pipe connecting sleeve, the lower cavity it is interior
Having heaters is fixedly mounted in portion, is provided with two heat conducting pipes at the top of the heater, the heat conducting pipe pass through the partition and
The reactive tank, the bottom end inside the reactive tank are fixedly installed with heating tube, and the both ends of the heating tube are respectively at two institutes
Heat conducting pipe connection is stated, one end at the top of the reaction chamber is hinged with articulated shaft, and the reaction chamber is hingedly pacified by the articulated shaft
Equipped with case lid, the bottom of the case lid is provided with rubber seal chock plug, and the rubber seal chock plug passes through seccotine fixed bonding
Handle is welded at the top of the bottom of the case lid, the case lid, the side of the handle is provided with escape pipe, the outlet
Pipe is fixedly mounted on the inside of the case lid, and pipe lid is provided at the top of the escape pipe.
Preferably, the gap location on the inside of the reaction chamber is provided with heat preserving and insulating material on the outside of the reactive tank.
Preferably, the bottom of the reaction chamber is welded with movable pulley mounting blocks, and the reaction chamber is pacified by the movable pulley
Dress block is movably installed with movable pulley.
Preferably, the sparge pipe is formed by transverse tube and vertical tube are prefabricated, and the number of the transverse tube is six, the vertical tube
Number is five, and the surface of the transverse tube and the vertical tube offers spray orifice.
Preferably, the bottom of described case lid one end is provided with latch segment, and one end at the top of the reaction chamber offers locking
Slot, the latch segment match with the locking slot, and the side of the locking slot is movably installed with clamping screw.
Preferably, the both ends of the water pump are welded with fixed block, and the internal activity of the fixed block is equipped with fixed spiral shell
Nail, the water pump are fixedly mounted on the side of the reaction chamber by the fixed block and the fixing screws.
Compared with prior art, the beneficial effects of the present invention are:
(1), the present invention is equipped with sparge pipe by the inside in reactive tank, is heated by heater, then control water pump, so that this
Device can carry out effective cycle alternation to the water inside reactive tank, so that the water inside entire reactive tank is carrying out heat exchange
When speed it is fast, stationary temperature can be rapidly achieved.
(2), for sparge pipe of the present invention by transverse tube and the prefabricated serpentine-like structure of vertical tube, the surface of sparge pipe offers several
Spray orifice, so that the water engaging surface product inside sparge pipe and reactive tank is big, when carrying out hot and cold water alternating, on the basis of rapid temperature-raising
On, so that the inside of entire reactive tank is heated evenly.
(3), the present invention by the bottom in reaction chamber is equipped with movable pulley, so that the present apparatus is easy to remove, when use more
Add conveniently.
(4), case lid is equipped with by the top movable in reaction chamber, and the bottom of case lid is provided with rubber seal plug
Head, so that the good airproof performance of present apparatus entirety.
Detailed description of the invention
Fig. 1 is whole structural schematic diagram of the invention；
Fig. 2 is the structural schematic diagram of sparge pipe of the invention；
Fig. 3 is the enlarged drawing in Fig. 1 of the invention at A.
In figure: 1, movable pulley；2, movable pulley mounting blocks；3, reaction chamber；4, heater；5, function of circular water absorption pipe；6, fixed block；
7, water pump；8, fixing screws；9, recycling outlet；10, pipe connecting sleeve；11, escape pipe；12, Guan Gai；13, handle；14, case
Lid；15, articulated shaft；16, rubber seal chock plug；17, upper cavity；18, sparge pipe；19, sparge pipe fixed link；20, thermal insulation separation
Hot material；21, reactive tank；22, heating tube；23；Heat conducting pipe；24, partition；25, lower cavity；26, clamping screw；31, it locks
Slot；141, latch segment；181, transverse tube；182, vertical tube；183, spray orifice.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other
Embodiment shall fall within the protection scope of the present invention.
Fig. 1-3 is please referred to, the present invention provides a kind of technical solution: a kind of reaction unit technical side preparing automobile-used graphene
Case, including reaction chamber 3, sparge pipe 18 and reactive tank 21, the inside of reaction chamber 3 are fixedly installed with partition 24, the both ends of partition 24
Inner wall with 3 two sides of reaction chamber is by being welded and fixed, and reaction chamber 3 is provided with upper cavity 17 and lower cavity by partition 24
25, upper cavity 17 is internally provided with reactive tank 21, and reactive tank 21 is fixedly mounted on the top of partition 24, reactive tank 21 it is interior
Portion is provided with sparge pipe 18, and sparge pipe 18 is fixedly mounted on the inside of reactive tank 21, sparge pipe 18 by sparge pipe fixed link 19
One end recycling outlet 9 is connected with by pipe connecting sleeve 10, the side of reaction chamber 3 is fixedly installed with water pump 7, cyclic water outlet
Pipe 9 is fixedly mounted on the top of water pump 7, and the bottom of water pump 7 is fixedly installed with function of circular water absorption pipe 5, and one end of function of circular water absorption pipe 5 is logical
Piping connector sleeve 10 extends to the inside of reactive tank 21, and having heaters 4, heater 4 is fixedly mounted in the inside of lower cavity 25
Top be provided with two heat conducting pipes 23, heat conducting pipe 23 passes through partition 24 and reactive tank 21, and the bottom end inside reactive tank 21 is fixed
Heating tube 22 is installed, the both ends of heating tube 22 are connected respectively at two heat conducting pipes 23, and the one end at 3 top of reaction chamber is hingedly hinged
Spindle 15, reaction chamber 3 are hingedly equipped with case lid 14 by articulated shaft 15, and the bottom of case lid 14 is provided with rubber seal chock plug 16,
Rubber seal chock plug 16 is fixedly bonded to the bottom of case lid 14 by seccotine, and the top of case lid 14 is welded with handle 13, handle
13 side is provided with escape pipe 11, and escape pipe 11 is fixedly mounted on the inside of case lid 14, and the top of escape pipe 11 is provided with
Pipe lid 12.
Preferably, 21 outside of reactive tank and the gap location of 3 inside of reaction chamber are provided with heat preserving and insulating material 20, so that entirely
The heat insulation and preservation effect of reaction chamber 3 is good, and heat is not allowed easy to lose.
Preferably, the bottom of reaction chamber 3 is welded with movable pulley mounting blocks 2, and reaction chamber 3 passes through 2 activity of movable pulley mounting blocks
Movable pulley 1 is installed, so that the present apparatus is easy to remove.
Preferably, sparge pipe 18 is by transverse tube 181 and vertical tube 182 is prefabricated forms, and the number of transverse tube 181 is six, vertical tube 182
Number be five, and the surface of transverse tube 181 and vertical tube 182 offers spray orifice 183, so that in sparge pipe 18 and reactive tank 21
The water engaging surface product in portion is big, when carrying out hot and cold water alternating, on the basis of rapid temperature-raising so that the inside of entire reactive tank 21 by
It is hot uniform.
Preferably, the bottom of 14 one end of case lid is provided with latch segment 141, and the one end at 3 top of reaction chamber offers locking slot
31, latch segment 141 matches with locking slot 31, and the side of locking slot 31 is movably installed with clamping screw 26, is locked by control
Bolt 26 can be opened and closed case lid 14, and be fixed.
Preferably, the both ends of water pump 7 are welded with fixed block 6, and the internal activity of fixed block 6 is equipped with fixing screws 8, water
Pump 7 is fixedly mounted on the side of reaction chamber 3 by fixed block 6 and fixing screws 8, so that water pump 7 firmly installs.
Working principle: the invention passes through movable pulley 1 first and the present apparatus is moved to the specified position used, by reacting
The inside of slot 21 is equipped with sparge pipe 18, and one end of sparge pipe 18 connects recycling outlet 9, one end connection of recycling outlet 9
Water pump 7 so that the water inside reactive tank 21 carries out effective cycle alternation, then passes through control heater 4 by controlling water pump 7
It is heated, heater 4 transfers heat to the heating tube 22 of 21 inner bottom of reactive tank by heat conducting pipe 23, thus for reaction
Water inside slot 21 is heated, so that speed of the water inside entire reactive tank 21 when carrying out heat exchange is fast, it can be quick
Reach stationary temperature, by transverse tube 181 and the prefabricated serpentine-like structure of vertical tube 182, the surface of sparge pipe 18 opens up sparge pipe 18
There are several spray orifices 183, so that the water engaging surface product inside sparge pipe 18 and reactive tank 21 is big, when carrying out hot and cold water alternating,
On the basis of rapid temperature-raising, so that the inside of entire reactive tank 21 is heated evenly, by controlling clamping screw 26, openable and pass
Closed box lid 14, and be fixed, the bottom of case lid 14 is provided with rubber seal chock plug 16, so that close inside entire reaction chamber 3
Envelope property is good, and 21 outside of reactive tank and the gap location of 3 inside of reaction chamber are provided with heat preserving and insulating material 20, so that entire reaction
The heat insulation and preservation effect of case 3 is good, and heat is not allowed easy to lose, and the top of case lid 14 is welded with handle 13, convenient for opening case lid 14, mentions
The side of hand 13 is provided with escape pipe 11, and escape pipe 11 is fixedly mounted on the inside of case lid 14, and the top setting of escape pipe 11
There is pipe lid 12, the gas that generates is discharged when can be by opening pipe lid 12 for graphite alkene reaction, or escape pipe 11 is connected other
Gas pipeline generates when convenient for graphite alkene reaction so that gas when graphite alkene reaction at generation is delivered to other equipment
Gas is utilized.
It should be noted that, in this document, relational terms such as first and second and the like are used merely to a reality
Body or operation are distinguished with another entity or operation, are deposited without necessarily requiring or implying between these entities or operation
In any actual relationship or order or sequence.Moreover, the terms "include", "comprise" or its any other variant are intended to
Non-exclusive inclusion, so that the process, method, article or equipment including a series of elements is not only wanted including those
Element, but also including other elements that are not explicitly listed, or further include for this process, method, article or equipment
Intrinsic element.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (6)
1. a kind of reaction unit for preparing automobile-used graphene, including reaction chamber (3), sparge pipe (18) and reactive tank (21), special
Sign is: the inside of the reaction chamber (3) is fixedly installed with partition (24), the both ends of the partition (24) and the reaction chamber
(3) inner wall of two sides is by being welded and fixed, and the reaction chamber (3) by the partition (24) be provided with upper cavity (17) and
Lower cavity (25), the upper cavity (17) are internally provided with the reactive tank (21), the fixed peace of the reactive tank (21)
Mounted in the top of the partition (24), the reactive tank (21) is internally provided with sparge pipe (18), and the sparge pipe (18) is logical
The inside that sparge pipe fixed link (19) is fixedly mounted on the reactive tank (21) is crossed, one end of the sparge pipe (18) passes through pipeline
Connector sleeve (10) is connected with recycling outlet (9), and the side of the reaction chamber (3) is fixedly installed with water pump (7), described to recycle
Water pipe (9) is fixedly mounted on the top of the water pump (7), and the bottom of the water pump (7) is fixedly installed with function of circular water absorption pipe (5),
One end of the function of circular water absorption pipe (5) extends to the inside of the reactive tank (21) by the pipe connecting sleeve (10), described
Having heaters (4) are fixedly mounted in the inside of lower cavity (25), are provided with two heat conducting pipes at the top of the heater (4)
(23), the heat conducting pipe (23) passes through the partition (24) and the reactive tank (21), the internal bottom end of the reactive tank (21)
It is fixedly installed with heating tube (22), the both ends of the heating tube (22) are described anti-respectively at two heat conducting pipe (23) connections
One end at the top of case (3) is answered to be hinged with articulated shaft (15), the reaction chamber (3) is hingedly equipped with case by the articulated shaft (15)
It covers (14), the bottom of the case lid (14) is provided with rubber seal chock plug (16), and the rubber seal chock plug (16) passes through strength
Glue is fixedly bonded to the bottom of the case lid (14), is welded with handle (13) at the top of the case lid (14), the handle (13)
Side be provided with escape pipe (11), the escape pipe (11) is fixedly mounted on the inside of the case lid (14), and the outlet
Pipe lid (12) are provided at the top of pipe (11).
2. a kind of reaction unit for preparing automobile-used graphene according to claim 1, it is characterised in that: the reactive tank
(21) outside is provided with heat preserving and insulating material (20) with the gap location on the inside of the reaction chamber (3).
3. a kind of reaction unit for preparing automobile-used graphene according to claim 1, it is characterised in that: the reaction chamber
(3) bottom is welded with movable pulley mounting blocks (2), and the reaction chamber (3) is movably installed with by the movable pulley mounting blocks (2)
Movable pulley (1).
4. a kind of reaction unit for preparing automobile-used graphene according to claim 1, it is characterised in that: the sparge pipe
(18) by transverse tube (181) and vertical tube (182) is prefabricated forms, the number of the transverse tube (181) is six, the vertical tube (182)
Number is five, and the surface of the transverse tube (181) and the vertical tube (182) offers spray orifice (183).
5. a kind of reaction unit for preparing automobile-used graphene according to claim 1, it is characterised in that: the case lid (14)
The bottom of one end is provided with latch segment (141), and one end at the top of the reaction chamber (3) offers locking slot (31), the locking
Block (141) matches with the locking slot (31), and the side of the locking slot (31) is movably installed with clamping screw (26).
6. a kind of reaction unit for preparing automobile-used graphene according to claim 1, it is characterised in that: the water pump (7)
Both ends be welded with fixed block (6), the internal activity of the fixed block (6) is equipped with fixing screws (8), the water pump (7)
The side of the reaction chamber (3) is fixedly mounted on by the fixed block (6) and the fixing screws (8).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811644863.7A CN109399618A (en) | 2018-12-30 | 2018-12-30 | A kind of reaction unit preparing automobile-used graphene |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811644863.7A CN109399618A (en) | 2018-12-30 | 2018-12-30 | A kind of reaction unit preparing automobile-used graphene |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109399618A true CN109399618A (en) | 2019-03-01 |
Family
ID=65461598
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811644863.7A Withdrawn CN109399618A (en) | 2018-12-30 | 2018-12-30 | A kind of reaction unit preparing automobile-used graphene |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109399618A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113875933A (en) * | 2021-10-19 | 2022-01-04 | 安徽信息工程学院 | Instant noodle cooking all-in-one machine |
-
2018
- 2018-12-30 CN CN201811644863.7A patent/CN109399618A/en not_active Withdrawn
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113875933A (en) * | 2021-10-19 | 2022-01-04 | 安徽信息工程学院 | Instant noodle cooking all-in-one machine |
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Application publication date: 20190301 |