CN109380602A - Perilla leaf oil preserved material adsorbs oil powder and preparation method thereof, application - Google Patents
Perilla leaf oil preserved material adsorbs oil powder and preparation method thereof, application Download PDFInfo
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- CN109380602A CN109380602A CN201710661596.3A CN201710661596A CN109380602A CN 109380602 A CN109380602 A CN 109380602A CN 201710661596 A CN201710661596 A CN 201710661596A CN 109380602 A CN109380602 A CN 109380602A
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- oil
- powder
- perilla leaf
- leaf
- preserved material
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/30—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K50/00—Feeding-stuffs specially adapted for particular animals
- A23K50/30—Feeding-stuffs specially adapted for particular animals for swines
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K50/00—Feeding-stuffs specially adapted for particular animals
- A23K50/70—Feeding-stuffs specially adapted for particular animals for birds
- A23K50/75—Feeding-stuffs specially adapted for particular animals for birds for poultry
Abstract
The invention belongs to field of animal feed, and in particular to a kind of perilla leaf oil preserved material absorption oil powder and its preparation method and application；It is prepared by the following method acquisition: the mixing of the fresh leaf of perilla leaf, cured leaf, half cured leaf and edible oil being infiltrated, wet-milling crushing, screening, adsorbing agent carrier is added to get perilla leaf oil preserved material absorption oil powder is arrived after obtaining the mixture of perilla leaf powder and edible oil；Case of wet attrition of the present invention overcomes loss of volatile oil, and using fresh leaf and half cured leaf, greatly improves utilization rate of active components and economic cost；Porkling energy short-term intervention is raised into the absorption oil powder addition of perilla leaf oil preserved material in pannage and alleviates body allergic reaction caused by Soybean antigen protein to the damaging action of gut barrier function, for reducing grice diarrhoea rate, reducing secondary infection, reduce the death rate, it is final to improve Animal husbandry production efficiency, with important application value, present invention addition can also reduce chick diarrhea rate and the death rate in chicken feed.
Description
Technical field
The invention belongs to field of animal feed, and in particular to a kind of perilla leaf oil preserved material absorption oil powder and preparation method thereof,
Using.
Background technique
With the fast development of living standard and aquaculture industry of China, people are to the pursuits of the livestock products amount of having Xiang Zhizhuan
Become, how to provide safety, the livestock products of green have been animal husbandry important directions.In pig breeding industry, Weaning Age generally shifts to an earlier date
To 3-4 week old, weanling pig face weaning stress simultaneously and be changed into suddenly the multiple influences such as the daily ration based on plant feed because
Element.Common feedstuffs raw material contains the feed antigen for the sucking pig intestinal health that has an impact mostly.For example Soybean antigen protein and big beans are former
Many anti-nutritional factors in material are to cause the one of the major reasons of diarrhea of weaned piglets and secondary enteric infection.Currently weaning
The incidence of intestines problem is generally reduced in pig starter feed by addition medicated feed additive, many times even 3-4
Middle antibiotic is added in combination feed.Currently, the external addition for having completely forbidden antibiotic in feed, therefore develop effective anti-
Raw element substitute becomes research hotspot.Also all there is a situation where in other animals of animal husbandry same or similar.Antibiotic replaces
It is the research emphasis of current animal husbandry for object.
The natural medicinal plants of dual-purpose of drug and food are nontoxic, noresidue, do not generate drug resistance, and general palatability is good,
Nutrition is higher, is the best substitute of antibiotic and chemical antibacterials in feed.It is suitable to medical and edible dual purpose plant selection to add
Work mode makes it suitable for feed industry application, while the native antigen for cooperating formula technique to reduce or weaken in feed is negatively made
With can effectively solve the problems, such as in feed that veterinary antibacterial is abused, animal food meat, egg, fowl and its product is effectively ensured
Safety, for maintenance human health and promote social economy's harmonious development be of great significance.
Purple perilla also known as weak, red Soviet Union, common perilla, fragrant Soviet Union etc., are annual upright draft, belong to Dicotyledoneae, Asteridae,
Labiatae.It purple perilla and belongs to radix scutellariae, Prunella vulgaris, rosemary of Lamiaceae plant etc. and is considered to have anti-inflammatory, antiallergy, antioxygen
The activity of change.The anti-allergic effects of perilla leaf are particularly subject to pay close attention to.Perilla leaf oil is extremely wide in pharmaceuticals industry purposes, it is smooth
Sell one of main component of Chinese patent drug ageratum oral liquid and apricot Soviet Union granules for treating common cold, relieve heat relieving coughing syrup and Jieji ' ningsou
One of main component of piece.Meanwhile perilla leaf is also the traditional food spice in China and the collocation diatery supplement of some fresh food,
Such as China and East Asia are from ancient times just common edible with perilla leaf collocation raw fish, seafood etc., can effectively reduce the generation of seafood allergy.
Purple perilla adaptability is preferable simultaneously, can plant throughout the country.
Perilla leaf has anti-corrosion, antibacterial, anti-inflammatory, inhibition allergic reaction and anti-tumor necrosis factor effect.It is ground from existing
From the point of view of studying carefully result, the anti-allergic effects of perilla leaf are definite.The effective component of perilla leaf is primarily present in volatile oil.Perilla leaf oil
Extraction by steam distillation is mostly used at present.Steam distillation extraction yield is typically only 0.5%, has been reported that SCF-CO 2
5.13% can be reached, generally recovery rate is very low.And the non-refractories such as some volatile oil components such as anthocyanin, cause purple perilla
Leaf effective component causes damages.Perilla leaf crude protein is up to 24.89%, contains amino acid in 16, and calcium phosphorus content is higher.Perilla leaf sheet
Body is suitable for directly applying in feed, ranks " feedstuff catalogue-can feeding natural plants " (Ministry of Agriculture, No. 1773).
Perilla leaf powder is that crushed after being dried is made.But perilla leaf powder specific gravity very little, it has not been convenient to transport and be not easy in feed addition and
It mixes.Yi Fare when perilla leaf crushes meticulous, dry and crushing process will cause a degree of loss of effective components.
Summary of the invention
The present invention be solve perilla leaf powder made from existing drying and crushing it is not convenient for transportation and be not easy in feed addition and
It mixes, and dry the technical issues of will cause a degree of loss of effective components with crushing process, a kind of perilla leaf oil is provided
Preserved material adsorbs oil powder and preparation method thereof.
In order to solve the above-mentioned technical problem, the technical solution adopted by the present invention are as follows: a kind of perilla leaf oil preserved material absorption oil powder,
Be prepared by the following method acquisition: by perilla leaf and edible oil be by weight infiltration is mixed in 1-99:99-1, wet-milling crushes,
Adsorbing agent carrier is added after obtaining the mixture of perilla leaf powder and edible oil to get oily to the absorption of perilla leaf oil preserved material in screening
Powder, the additional amount of the adsorbing agent carrier are the 1-99% that perilla leaf oil preserved material adsorbs oil powder gross weight；The adsorbing agent carrier is
Rice bran meal, popcorn, zeolite powder, maize cob meal, litter shell powder, mountain flour, medical stone powder, bean cake powder, wheat-middlings and flour one kind
Or it any several mixes in any proportion.
The perilla leaf is at least one of fresh leaf of purple perilla, cured leaf and half cured leaf.
The mixture of perilla leaf powder and edible oil is additionally added antioxidant, the antioxidant after adsorbing agent carrier is added
Additional amount be perilla leaf oil preserved material adsorb oil powder gross weight 0.1-5%.
The mixture of perilla leaf powder and edible oil is additionally added mould inhibitor after adsorbing agent carrier is added, and the mould inhibitor adds
Entering amount is the 0.1-50% that perilla leaf oil preserved material adsorbs oil powder gross weight.
A method of preparing perilla leaf oil preserved material absorption oil powder, comprising the following steps:
A, the edible oil that perilla leaf and temperature are -18 DEG C~300 DEG C is mixed and is infiltrated, the perilla leaf and edible oil
Weight ratio be 1-99:99-1；Then it impregnates 0-2 hours；The perilla leaf be fresh leaf of purple perilla, cured leaf and half cured leaf at least
It is a kind of；
B, the mixture of the resulting perilla leaf of step a and edible oil pulverizer wet-milling is crossed to crush；
C, by the smashed mixture sieving of step b or filters pressing, the big dregs of screening removal perilla leaf obtain perilla leaf powder
The mixture at end and edible oil, selected grit number are 10-100 mesh；
D, adsorbing agent carrier is added in the mixture of perilla leaf powder and edible oil to mix, the addition of the adsorbing agent carrier
Amount be perilla leaf oil preserved material adsorb oil powder gross weight 1-99%, the adsorbing agent carrier be rice bran meal, popcorn, zeolite powder,
Maize cob meal, litter shell powder, mountain flour, medical stone powder, bean cake powder, wheat-middlings and flour one kind, or any several mix in any proportion
It closes.
The edible oil be soya-bean oil, coconut oil, corn oil, cottonseed oil, rapeseed oil, sunflower oil, siritch, peanut oil,
Coconut oil, palm oil, chicken fat, duck oil, butter, lard and phosphatide oil one or any of several mix in any proportion.
Mixture is additionally added antioxidant and mould inhibitor after adsorbing agent carrier is added in step d, and the antioxidant adds
Entering amount is the 0.1-5% that perilla leaf oil preserved material adsorbs oil powder gross weight, and the mould inhibitor additional amount is perilla leaf oil preserved material absorption oil
The 0.1%-50% of powder gross weight.
Perilla leaf oil preserved material absorption oil powder is as feeding made from the perilla leaf oil preserved material absorption oil powder or preparation method
Expect the purposes of raw material.
Compared with the prior art, the invention has the following beneficial effects:
Using case of wet attrition after oil immersion in the present invention, loss of volatile oil is overcome, and can use fresh leaf and half cured leaf,
Greatly improve utilization rate of active components and economic cost.
Perilla leaf oil preserved material absorption oil powder addition of the present invention raises porkling energy short-term intervention in pannage and alleviates soybean
Body allergic reaction caused by antigen protein to the damaging action of gut barrier function, for reduce grice diarrhoea rate, reduce it is secondary
Infection reduces the death rate, final to improve Animal husbandry production efficiency, has important application value.Present invention addition is raised in chick
Also chick diarrhea rate and the death rate can be reduced in material.
Specific embodiment
Embodiment 1
A method of preparing perilla leaf oil preserved material absorption oil powder, comprising the following steps:
A, perilla leaf and edible oil are mixed infiltration at normal temperature, the weight ratio of the perilla leaf and edible oil is 1:
1；Then it impregnates 2 hours；The edible oil is soya-bean oil；The perilla leaf is fresh leaf of purple perilla, cured leaf and half cured leaf；
B, the mixture of the resulting perilla leaf of step a and edible oil pulverizer wet-milling is crossed to crush；
C, the smashed mixture of step b is sieved, the big dregs of screening removal perilla leaf obtain perilla leaf powder and food
With the mixture of oil, selected grit number is 30 mesh；
D, adsorbing agent carrier is added in the mixture of perilla leaf powder and edible oil to mix, the addition of the adsorbing agent carrier
Amount is that perilla leaf oil preserved material adsorbs the 50% of oil powder gross weight, and the adsorbing agent carrier is rice bran meal.Add perilla leaf oil preserved material
Adsorb 3% antioxidant of oil powder gross weight.
Embodiment 2
A method of preparing perilla leaf oil preserved material absorption oil powder, comprising the following steps:
A, perilla leaf and edible oil are mixed infiltration at normal temperature, the weight ratio of the perilla leaf and edible oil is 1:
10；The edible oil is the mixture of siritch, peanut oil, coconut oil, palm oil, butter, lard, phosphatide oil；The purple perilla
Leaf is fresh leaf of purple perilla, cured leaf and half cured leaf；
B, the mixture of the resulting perilla leaf of step a and edible oil pulverizer wet-milling is crossed to crush；
C, the smashed mixture of step b is sieved, the big dregs of screening removal perilla leaf obtain perilla leaf powder and food
With the mixture of oil, selected grit number is 10 mesh；
D, adsorbing agent carrier is added in the mixture of perilla leaf powder and edible oil to mix, the addition of the adsorbing agent carrier
Amount is that perilla leaf oil preserved material adsorbs the 99% of oil powder gross weight, and the adsorbing agent carrier is rice bran meal, popcorn, zeolite powder, secondary
The mixture of powder；Add 0.5% mould inhibitor of perilla leaf oil preserved material absorption oil powder gross weight.
Embodiment 3
A method of preparing perilla leaf oil preserved material absorption oil powder, comprising the following steps:
A, perilla leaf and edible oil are mixed infiltration at normal temperature, the weight ratio of the perilla leaf and edible oil is
10:1；Then it impregnates 1 hour；The edible oil be soya-bean oil, coconut oil, sunflower oil, corn oil, cottonseed oil, rapeseed oil it is mixed
Close object；The perilla leaf is fresh leaf of purple perilla, cured leaf and half cured leaf；
B, the mixture of the resulting perilla leaf of step a and edible oil pulverizer wet-milling is crossed to crush；
C, by the smashed mixture sieving of step b or filters pressing, the big dregs of screening removal perilla leaf obtain perilla leaf powder
The mixture at end and edible oil, selected grit number are 100 mesh；
D, adsorbing agent carrier is added in the mixture of perilla leaf powder and edible oil to mix, the addition of the adsorbing agent carrier
Amount is that perilla leaf oil preserved material adsorbs the 60% of oil powder gross weight, and the adsorbing agent carrier is popcorn；Add perilla leaf oil immersion
5% antioxidant of agent absorption oil powder gross weight.
Embodiment 4
A method of preparing perilla leaf oil preserved material absorption oil powder, comprising the following steps:
A, perilla leaf and edible oil are mixed infiltration at normal temperature, the weight ratio of the perilla leaf and edible oil is
Then 99:1 impregnates 0.5 hour；The edible oil is the mixture of cottonseed oil, rapeseed oil；The perilla leaf be fresh leaf of purple perilla,
Cured leaf and half cured leaf；
B, the mixture of the resulting perilla leaf of step a and edible oil pulverizer wet-milling is crossed to crush；
C, by the smashed mixture sieving of step b or filters pressing, the big dregs of screening removal perilla leaf obtain perilla leaf powder
The mixture at end and edible oil, selected grit number are 60 mesh；
D, adsorbing agent carrier is added in the mixture of perilla leaf powder and edible oil to mix, the addition of the adsorbing agent carrier
Amount is that perilla leaf oil preserved material adsorbs the 1% of oil powder gross weight, and the adsorbing agent carrier is maize cob meal, litter shell powder, mountain flour, medical stone
The mixture of powder, bean cake powder.0.1% ethoxyquinoline of perilla leaf oil preserved material absorption oil powder gross weight is added as anti-oxidant
Agent, 50% calcium formate of gross weight is as mould inhibitor.
Embodiment 5
A method of preparing perilla leaf oil preserved material absorption oil powder, comprising the following steps:
A, perilla leaf and edible oil are mixed infiltration at normal temperature, the weight ratio of the perilla leaf and edible oil is
99:1；The edible oil is the mixture of chicken fat, duck oil, butter, lard and phosphatide oil；The perilla leaf is fresh leaf of purple perilla, does
Leaf and half cured leaf；
B, the mixture of the resulting perilla leaf of step a and edible oil pulverizer wet-milling is crossed to crush；
C, by the smashed mixture sieving of step b or filters pressing, the big dregs of screening removal perilla leaf obtain perilla leaf powder
The mixture at end and edible oil, selected grit number are 20 mesh；
D, adsorbing agent carrier is added in the mixture of perilla leaf powder and edible oil to mix, the addition of the adsorbing agent carrier
Amount is that perilla leaf oil preserved material adsorbs the 20% of oil powder gross weight, and the adsorbing agent carrier is the mixture of zeolite powder, wheat-middlings and flour；
Add 1% antioxidant of perilla leaf oil preserved material absorption oil powder gross weight, 1% mould inhibitor of gross weight.
Zoopery
The absorption oil powder of perilla leaf oil preserved material prepared by embodiment 1 is added in the porkling feed containing 20% dregs of beans, institute
The additive amount for stating perilla leaf oil preserved material absorption oil powder in porkling feed is the 5% of feed gross weight, with added with perilla leaf oil preserved material
The porkling feed for adsorbing oil powder is fed porkling 30 days, is counted by experimental data, diarrhea of weaned piglets rate averagely reduces by 10%, adopts
Appetite averagely improves 5%, and daily gain averagely improves 10% or so.
Finally, it should be noted that the above embodiments are only used to illustrate the technical solution of the present invention., rather than its limitations；To the greatest extent
Pipe present invention has been described in detail with reference to the aforementioned embodiments, those skilled in the art should understand that: its according to
So be possible to modify the technical solutions described in the foregoing embodiments, or to some or all of the technical features into
Row equivalent replacement；And these are modified or replaceed, various embodiments of the present invention technology that it does not separate the essence of the corresponding technical solution
The range of scheme.
Claims (8)
1. a kind of perilla leaf oil preserved material adsorbs oil powder, which is characterized in that perilla leaf oil preserved material absorption oil powder is prepared by the following method
It obtains: being by weight that infiltration is mixed in 1-99:99-1, wet-milling crushes, screening by perilla leaf and edible oil, obtain perilla leaf
Adsorbing agent carrier is added after the mixture of powder and edible oil and adsorbs oil powder to get to perilla leaf oil preserved material, the adsorbent carries
The additional amount of body is the 1-99% that perilla leaf oil preserved material adsorbs oil powder gross weight；The adsorbing agent carrier be rice bran meal, popcorn,
Zeolite powder, maize cob meal, litter shell powder, mountain flour, medical stone powder, bean cake powder, wheat-middlings and flour one or any of several by any
Ratio mixing.
2. perilla leaf oil preserved material according to claim 1 adsorbs oil powder, which is characterized in that the perilla leaf is that purple perilla is fresh
At least one of leaf, cured leaf and half cured leaf.
3. perilla leaf oil preserved material according to claim 1 adsorbs oil powder, which is characterized in that perilla leaf powder and edible oil
Mixture is additionally added antioxidant after adsorbing agent carrier is added, and the additional amount of the antioxidant is perilla leaf oil preserved material absorption oil
The 0.1-5% of powder gross weight.
4. perilla leaf oil preserved material according to claim 1 adsorbs oil powder, which is characterized in that perilla leaf powder and edible oil
Mixture is additionally added mould inhibitor after adsorbing agent carrier is added, and the additional amount of the mould inhibitor is that perilla leaf oil preserved material absorption oil powder is total
The 0.1-50% of weight.
5. a kind of method for preparing perilla leaf oil preserved material absorption oil powder as described in claim 1, which is characterized in that including following
Step:
A, the edible oil that perilla leaf and temperature are -18 DEG C~300 DEG C is mixed and is infiltrated, the weight of the perilla leaf and edible oil
Amount is than being 1-99:99-1；Then it impregnates 0-2 hours；The perilla leaf is at least one in fresh leaf of purple perilla, cured leaf and half cured leaf
Kind；
B, the mixture of the resulting perilla leaf of step a and edible oil pulverizer wet-milling is crossed to crush；
C, by the sieving of step b smashed mixture or filters pressing, the big dregs of screening removal perilla leaf, obtain perilla leaf powder and
The mixture of edible oil, selected grit number are 10-100 mesh；
D, adsorbing agent carrier is added in the mixture of perilla leaf powder and edible oil to mix, the additional amount of the adsorbing agent carrier is
Perilla leaf oil preserved material adsorbs the 1-99% of oil powder gross weight, and the adsorbing agent carrier is rice bran meal, popcorn, zeolite powder, corn
Core powder, litter shell powder, mountain flour, medical stone powder, bean cake powder, wheat-middlings and flour one kind, or any several mix in any proportion.
6. the method according to claim 5 for preparing perilla leaf oil preserved material absorption oil powder, which is characterized in that the edible oil
For soya-bean oil, coconut oil, corn oil, cottonseed oil, rapeseed oil, sunflower oil, siritch, peanut oil, coconut oil, palm oil, chicken fat,
Duck oil, butter, lard and phosphatide oil one or any of several mix in any proportion.
7. the method according to claim 5 for preparing perilla leaf oil preserved material absorption oil powder, which is characterized in that mixed in step d
It closes after adsorbing agent carrier is added in object and is additionally added antioxidant and mould inhibitor, the additional amount of the antioxidant is perilla leaf oil preserved material
The 0.1-5% of oil powder gross weight is adsorbed, the mould inhibitor additional amount is the 0.1-50% that perilla leaf oil preserved material adsorbs oil powder gross weight.
8. the described in any item perilla leaf oil preserved material absorption oil powders of Claims 1 to 4 or claim 5~7 are described in any item
Perilla leaf oil preserved material made from preparation method adsorbs purposes of the oil powder as feedstuff.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710661596.3A CN109380602B (en) | 2017-08-04 | 2017-08-04 | Perilla leaf oil immersion agent adsorption oil powder and preparation method and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710661596.3A CN109380602B (en) | 2017-08-04 | 2017-08-04 | Perilla leaf oil immersion agent adsorption oil powder and preparation method and application thereof |
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| CN109380602A true CN109380602A (en) | 2019-02-26 |
| CN109380602B CN109380602B (en) | 2021-10-26 |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101602982A (en) * | 2008-06-11 | 2009-12-16 | 湖北中烟工业有限责任公司 | The step-by-step extracting method of purple perilla and extract obtained application in cigarette |
| CN102342329A (en) * | 2011-10-10 | 2012-02-08 | 雅安太时生物科技有限公司 | Processing technique for producing condiment oil with fresh peppers and tea oil |
| CN103120283A (en) * | 2011-11-19 | 2013-05-29 | 计英 | Fermented soya beans with perilla leaves |
| CN105106738A (en) * | 2015-10-09 | 2015-12-02 | 皖南医学院 | Emulsion for preventing and treating mosquito bites and preparation method of emulsion |
-
2017
- 2017-08-04 CN CN201710661596.3A patent/CN109380602B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101602982A (en) * | 2008-06-11 | 2009-12-16 | 湖北中烟工业有限责任公司 | The step-by-step extracting method of purple perilla and extract obtained application in cigarette |
| CN102342329A (en) * | 2011-10-10 | 2012-02-08 | 雅安太时生物科技有限公司 | Processing technique for producing condiment oil with fresh peppers and tea oil |
| CN103120283A (en) * | 2011-11-19 | 2013-05-29 | 计英 | Fermented soya beans with perilla leaves |
| CN105106738A (en) * | 2015-10-09 | 2015-12-02 | 皖南医学院 | Emulsion for preventing and treating mosquito bites and preparation method of emulsion |
Non-Patent Citations (1)
| Title |
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| （美）斯特凡妮•托尔斯著: "《纯天然美体DIY手册 93种手工保养品配方》", 28 February 2015, 上海科学技术文献出版社 * |
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