CN109371284A - A kind of high-performance cubic-textured metal base band and preparation method thereof - Google Patents

A kind of high-performance cubic-textured metal base band and preparation method thereof Download PDF

Info

Publication number
CN109371284A
CN109371284A CN201811540577.6A CN201811540577A CN109371284A CN 109371284 A CN109371284 A CN 109371284A CN 201811540577 A CN201811540577 A CN 201811540577A CN 109371284 A CN109371284 A CN 109371284A
Authority
CN
China
Prior art keywords
alloy
cold rolling
strip steel
rolled stock
steel rolled
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201811540577.6A
Other languages
Chinese (zh)
Other versions
CN109371284B (en
Inventor
刘志勇
刘朋飞
黎文峰
尚淑英
刘海瑞
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Henan Normal University
Original Assignee
Henan Normal University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Henan Normal University filed Critical Henan Normal University
Priority to CN201811540577.6A priority Critical patent/CN109371284B/en
Publication of CN109371284A publication Critical patent/CN109371284A/en
Application granted granted Critical
Publication of CN109371284B publication Critical patent/CN109371284B/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C14/00Alloys based on titanium
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D9/00Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
    • C21D9/52Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for wires; for strips ; for rods of unlimited length
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C1/00Making non-ferrous alloys
    • C22C1/02Making non-ferrous alloys by melting
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22FCHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
    • C22F1/00Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
    • C22F1/16Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of other metals or alloys based thereon
    • C22F1/18High-melting or refractory metals or alloys based thereon
    • C22F1/183High-melting or refractory metals or alloys based thereon of titanium or alloys based thereon
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/06Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the coating material
    • C23C14/14Metallic material, boron or silicon
    • C23C14/16Metallic material, boron or silicon on metallic substrates or on substrates of boron or silicon
    • C23C14/165Metallic material, boron or silicon on metallic substrates or on substrates of boron or silicon by cathodic sputtering
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/22Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
    • C23C14/34Sputtering
    • C23C14/35Sputtering by application of a magnetic field, e.g. magnetron sputtering
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/58After-treatment
    • C23C14/5806Thermal treatment

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Physical Vapour Deposition (AREA)

Abstract

The invention discloses a kind of high-performance cubic-textured metal base band and preparation method thereof.Ti-Al alloy cast ingot is obtained using smelting process, wherein the mass fraction of Al is 7%~10%, obtains the cold rolling Ti alloy strip steel rolled stock that final thickness is 30 μm~40 μm by cold rolling;After cold rolling Ti alloy strip steel rolled stock solution treatment, a layer thickness then is deposited as the Ni-9.3at.%W alloy of 100nm~500nm in the method that its surface uses magnetron sputtering, wherein vacuum degree is 0.2~0.8Pa, and sputtering power is 200W~270W;Finally the alloy strip steel rolled stock after magnetron sputtering is heat-treated, specifically comprises the processes of: 1260 DEG C~1300 DEG C heat preservation 15min.Present invention process is simple, and in liquid nitrogen temperature without ferromagnetism, yield strength is higher, is suitble to the industrialized production of textured metal base band.

Description

A kind of high-performance cubic-textured metal base band and preparation method thereof
Technical field
The present invention relates to high temperature coating superconducting tape industrialization textured metal base band technology of preparing more particularly to high-performance are vertical Square textured metal base band and preparation method thereof.
Background technique
For the textured metal substrate of coating superconducting band, Ni based alloy is due to being research with good comprehensive performance The material of personnel's first choice.Texture Ni-5at.%W alloy base band is to study most mature base band, has had more units can at present To commercially produce, but its mechanical property needs to improve, and Ni-5at.%W alloy liquid nitrogen temperature have it is ferromagnetic Property, it will cause magnetic hystersis loss in the application of alternating current, the performance of coating superconducting band needs to be further increased.
Occurs the report about composite baseband in recent years, composite baseband can effectively solve Ni-5at.%W alloy mechanics Performance and ferromagnetic problem, but the preparation process of composite baseband is complex, cost is also higher, thus in industrialized production In have defect.Studies have shown that when the atomic percentage content of tungsten be greater than 9.3at.% when, nickel-tungsten alloy base-band liquid nitrogen temperature without Ferromagnetism, and its mechanical property also increases, but the cubic texture intensity formed by cold rolling and recrystallization annealing compared with Low, how to form strong cubic texture in high-tungsten alloy is the key that prepare high-performance nickel-tungsten alloy base-band.
Summary of the invention
One of the object of the invention is to provide a kind of high-performance cubic-textured metal base band, in the nickel tungsten of high W content Middle formation strong cubic texture.
Another object of the present invention is to provide a kind of method for preparing high-performance cubic-textured metal base band, in high W content Nickel tungsten in form strong cubic texture.
For this purpose, the present invention provides a kind of high-performance cubic-textured metal base band, including the cold rolling with a thickness of 30 μm~40 μm Ti alloy strip steel rolled stock and the Ni-9.3at.%W alloy firm formed on the Ti alloy strip steel rolled stock surface by magnetron sputtering, the Ti The mass fraction of Al is 7%~10% in alloy strip steel rolled stock, the Ni-9.3at.%W alloy firm with a thickness of 100nm~500nm, Also, before forming the Ni-9.3at.%W alloy firm by magnetron sputtering, the cold rolling Ti alloy strip steel rolled stock is heated to 1390 DEG C~1420 DEG C heat preservation 10min~15min are forming the Ni-9.3at.%W alloy firm then by air-cooled immediately Afterwards, temperature 15min of the cold rolling Ti alloy strip steel rolled stock at 1260 DEG C~1300 DEG C.
On the other hand, the present invention provides a kind of preparation method of high-performance cubic-textured metal base band, comprising the following steps: The preparation of step 1:Ti alloy strip steel rolled stock: using smelting process obtain Ti-Al alloy cast ingot, wherein the mass fraction of Al be 7%~ 10%, the cold rolling Ti alloy strip steel rolled stock that final thickness is 30 μm~40 μm is obtained by cold rolling;Step 2: cold rolling Ti alloy is carried out Solution treatment: being heated to 1390 DEG C~1420 DEG C heat preservation 10min~15min for above-mentioned cold rolling Ti alloy strip steel rolled stock, empty immediately after It is cold;Step 3:Ti alloy surface uses magnetron sputtering Ni-9.3at.%W alloy firm: by the Ti alloy after above-mentioned solution treatment The method that strip surface uses magnetron sputtering deposits a layer thickness for the Ni-9.3at.%W alloy of 100nm~500nm, wherein very Reciprocal of duty cycle is 0.2~0.8Pa, and sputtering power is 200W~270W;Step 4: heat is carried out to aforementioned Ni-9.3at.%W alloy firm Processing: the alloy strip steel rolled stock after magnetron sputtering is heat-treated, specifically comprises the processes of: 1260 DEG C~1300 DEG C heat preservation 15min.
It is preferred that in step 1, the mass fraction of Al is 8%, the cold rolling Ti alloy strip steel rolled stock obtained by cold rolling Final thickness is 40 μm.
It is preferred that in step 1, the mass fraction of Al is 7%, the cold rolling Ti alloy strip steel rolled stock obtained by cold rolling Final thickness is 30 μm.
It is preferred that in step 2, by the cold rolling Ti alloy strip steel rolled stock be heated to 1390 DEG C of heat preservation 10min~ 15min, it is air-cooled immediately after.
It is preferred that in step 2, by the cold rolling Ti alloy strip steel rolled stock be heated to 1420 DEG C of heat preservation 10min~ 15min, it is air-cooled immediately after.
It is preferred that in step 3, Ni-9.3at.%W alloy with a thickness of 100nm, vacuum degree 0.2Pa, sputtering Power is 200W~270W.
It is preferred that in step 3, Ni-9.3at.%W alloy with a thickness of 500nm, vacuum degree 0.8Pa, sputtering Power is 270W.
It is preferred that with 1260 DEG C of heat preservation 15min in step 4.
It is preferred that with 1300 DEG C of heat preservation 15min in step 4.
The present invention plates one layer thin of Ni-9.3at.%W alloy in Ti alloy surface, can close in surface layer Ni-9.3at.%W Strong cubic texture is formed in gold.For the base band of acquisition without ferromagnetism, yield strength is higher, also, present invention process is simple, is easy control System is suitble to industrialized production.
The present invention provides a kind of method of new preparation high-performance cubic-textured metal base band as a result, to obtain high-performance Coating superconducting band has found new approach.
Detailed description of the invention
It will be briefly described attached drawing used in this application below, it should be apparent that, these attached drawings are for explaining only the invention Design.
Fig. 1 is gained alloy base band surface (111) face pole figure in embodiment 1.
Fig. 2 is gained alloy base band surface (111) face pole figure in embodiment 2.
Specific embodiment
The embodiment of high-intensitive nickel-tungsten alloy base-band of strong cubic texture of the invention and preparation method thereof is described below.
The embodiment recorded herein is specific specific embodiment of the invention, for illustrating design of the invention, Be it is explanatory and illustrative, should not be construed as the limitation to embodiment of the present invention and the scope of the invention.Except what is recorded herein Outside embodiment, those skilled in the art can also based on the claim of this application book and specification disclosure of that using aobvious and The other technical solutions being clear to, these technical solutions include the embodiment recorded herein is made it is any it is obvious replacement and The technical solution of modification.
Embodiment 1
The step of preparation method of the embodiment of the present invention 1, is as follows:
Ti-Al alloy cast ingot is obtained using melting, wherein the mass fraction of Al is 8%, obtains final thickness by cold rolling For 40 μm of cold rolling Ti alloy strip steel rolled stock;
Above-mentioned cold rolling Ti alloy strip steel rolled stock is heated to 1420 DEG C of heat preservation 10min, it is air-cooled immediately after;
The method that Ti alloy strip steel rolled stock surface after above-mentioned solution treatment uses magnetron sputtering is deposited into a layer thickness as 100nm Ni-9.3at.%W alloy, wherein vacuum degree be 0.2Pa, sputtering power be 200W~270W;
Alloy strip steel rolled stock after magnetron sputtering is heat-treated, specifically comprises the processes of: 1260 DEG C of heat preservation 15min.
The yield strength of the alloy base band at room temperature is 510MPa, and (111) the face pole figure on surface was as shown in Figure 1, explanation should Base band surface obtains strong cubic texture.
The high-performance cubic-textured metal base band of the present embodiment include with a thickness of 40 μm cold rolling Ti alloy strip steel rolled stock and The Ni-9.3at.%W alloy firm that the Ti alloy strip steel rolled stock surface is formed by magnetron sputtering.The base band of acquisition is bent without ferromagnetism It is higher to take intensity.
Embodiment 2
The step of preparation method of the embodiment of the present invention 2, is as follows:
Ti-Al alloy cast ingot is obtained using melting, wherein the mass fraction of Al is 7%, obtains final thickness by cold rolling For 30 μm of cold rolling Ti alloy strip steel rolled stock;
Above-mentioned cold rolling Ti alloy strip steel rolled stock is heated to 1390 DEG C of heat preservation 10min, it is air-cooled immediately after;
The method that Ti alloy strip steel rolled stock surface after above-mentioned solution treatment uses magnetron sputtering is deposited into a layer thickness as 500nm Ni-9.3at.%W alloy, wherein vacuum degree be 0.8Pa, sputtering power 270W;
Alloy strip steel rolled stock after magnetron sputtering is heat-treated, specifically comprises the processes of: 1300 DEG C of heat preservation 15min.
The yield strength of the alloy base band at room temperature is 500MPa, and (111) the face pole figure on surface was as shown in Fig. 2, explanation should Base band surface obtains strong cubic texture.
The high-performance cubic-textured metal base band of the present embodiment include with a thickness of 30 μm cold rolling Ti alloy strip steel rolled stock and The Ni-9.3at.%W alloy firm that the Ti alloy strip steel rolled stock surface is formed by magnetron sputtering.The base band of acquisition is bent without ferromagnetism It is higher to take intensity.
Above embodiments are merely to the specific specific embodiment for illustrating design of the invention and selecting, in these realities It applies in example, specific technological parameter might not be configured to limitation of the scope of the invention.Illustrate step by step below of the invention The preferred scope of some technological parameters of the preparation method of high-performance cubic-textured metal base band.
The preparation of step 1:Ti alloy strip steel rolled stock:
Ti-Al alloy cast ingot is obtained using smelting process, wherein the mass fraction of Al is 7%~10%, is obtained by cold rolling The cold rolling Ti alloy strip steel rolled stock that final thickness is 30 μm~40 μm.
Step 2: solution treatment is carried out to cold rolling Ti alloy:
Above-mentioned cold rolling Ti alloy strip steel rolled stock is heated to 1390 DEG C~1420 DEG C heat preservation 10min~15min, it is empty immediately after It is cold.
Step 3:Ti alloy surface uses magnetron sputtering Ni-9.3at.%W alloy firm:
The method that Ti alloy strip steel rolled stock surface after above-mentioned solution treatment uses magnetron sputtering is deposited into a layer thickness as 100nm The Ni-9.3at.%W alloy of~500nm, wherein vacuum degree is 0.2~0.8Pa, and sputtering power is 200W~270W.
Step 4: aforementioned Ni-9.3at.%W alloy firm is heat-treated:
Alloy strip steel rolled stock after magnetron sputtering is heat-treated, specifically comprises the processes of: 1260 DEG C~1300 DEG C heat preservation 15min.
High-performance cubic-textured metal base band of the invention includes the cold rolling Ti alloy strip that thickness range is 30 μm~40 μm Material and the Ni-9.3at.%W alloy firm formed on the Ti alloy strip steel rolled stock surface by magnetron sputtering, the Ti alloy strip steel rolled stock The mass fraction range of middle Al is 7%~10%, and the Ni-9.3at.%W alloy firm thickness range is 100nm~500nm, Also, before forming the Ni-9.3at.%W alloy firm by magnetron sputtering, the cold rolling Ti alloy strip steel rolled stock is heated to 1390 DEG C~1420 DEG C heat preservation 10min~15min are forming the Ni-9.3at.%W alloy firm then by air-cooled immediately Afterwards, temperature 15min of the cold rolling Ti alloy strip steel rolled stock at 1260 DEG C~1300 DEG C.
The present invention plates one layer thin of Ni-9.3at.%W alloy in Ti alloy surface, can close in surface layer Ni-9.3at.%W Strong cubic texture is formed in gold.For the base band of acquisition without ferromagnetism, yield strength is higher, also, present invention process is simple, is easy control System is suitble to industrialized production.
In the prior art, the mechanical property of Ni-5at.%W alloy needs to improve, and Ni-5at.%W alloy There is ferromagnetism in liquid nitrogen temperature, will cause magnetic hystersis loss in the application of alternating current, the performance of coating superconducting band need In further increasing.Although composite baseband can effectively solve the problems, such as Ni-5at.%W alloy mechanical property and ferromagnetic, Be composite baseband preparation process it is complex, cost is also higher, thus needs further to carry out it in industrialized production It improves.When the atomic percentage content of tungsten is greater than 9.3at.%, nickel-tungsten alloy base-band in liquid nitrogen temperature without ferromagnetism, and its power Performance is learned also to increase, but it is lower by the cubic texture intensity that cold rolling and recrystallization annealing are formed, how to be closed in high tungsten It is the key that prepare high-performance nickel-tungsten alloy base-band that strong cubic texture is formed in gold.
Present invention employs the techniques of specific preparation high-performance cubic-textured metal base band, solve and exist in the prior art The technology barrier of strong cubic texture is formed in high-tungsten alloy, so as to prepare the higher high-performance of no ferromagnetism, yield strength Cubic-textured metal base band, and simple process, are easy to control, and are suitble to industrialized production.
As a result, skilled artisans appreciate that: the present invention provides a kind of new preparation high-performance cubic-textured metal Base band and preparation method thereof solves technology barrier present in the prior art, to obtain high-performance cubic-textured metal base band Have found new approach.
The embodiment of high-performance cubic-textured metal base band of the invention and preparation method thereof is illustrated above. It can be with for for example specific technological parameter of specific features of high-performance cubic-textured metal base band of the invention and preparation method thereof It is specifically designed according to the effect of the feature of above-mentioned disclosure, these designs are that those skilled in the art can be realized.And And each technical characteristic of above-mentioned disclosure is not limited to disclosed and other feature combination, those skilled in the art can also root Carry out other combinations between each technical characteristic according to the purpose of invention, be subject to realize the present invention purpose.

Claims (10)

1. a kind of high-performance cubic-textured metal base band, including the cold rolling Ti alloy strip steel rolled stock with a thickness of 30 μm~40 μm and at this The Ni-9.3at.%W alloy firm that Ti alloy strip steel rolled stock surface is formed by magnetron sputtering, the quality of Al in the Ti alloy strip steel rolled stock Score is 7%~10%, and the Ni-9.3at.%W alloy firm splashes with a thickness of 100nm~500nm by magnetic control It penetrates before forming the Ni-9.3at.%W alloy firm, the cold rolling Ti alloy strip steel rolled stock is heated to 1390 DEG C~1420 DEG C heat preservations 10min~15min, then by air-cooled immediately, after forming the Ni-9.3at.%W alloy firm, the cold rolling Ti alloy strip Temperature 15min of the material at 1260 DEG C~1300 DEG C.
2. a kind of preparation method of high-performance cubic-textured metal base band as described in claim 1, comprising the following steps:
The preparation of step 1:Ti alloy strip steel rolled stock:
Ti-Al alloy cast ingot is obtained using smelting process, wherein the mass fraction of Al is 7%~10%, is obtained finally by cold rolling With a thickness of 30 μm~40 μm of cold rolling Ti alloy strip steel rolled stock;
Step 2: solution treatment is carried out to cold rolling Ti alloy:
Above-mentioned cold rolling Ti alloy strip steel rolled stock is heated to 1390 DEG C~1420 DEG C heat preservation 10min~15min, it is air-cooled immediately after;
Step 3:Ti alloy surface uses magnetron sputtering Ni-9.3at.%W alloy firm:
By the method that the Ti alloy strip steel rolled stock surface after above-mentioned solution treatment uses magnetron sputtering deposit a layer thickness for 100nm~ The Ni-9.3at.%W alloy of 500nm, wherein vacuum degree is 0.2~0.8Pa, and sputtering power is 200W~270W;
Step 4: aforementioned Ni-9.3at.%W alloy firm is heat-treated:
Alloy strip steel rolled stock after magnetron sputtering is heat-treated, specifically comprises the processes of: 1260 DEG C~1300 DEG C heat preservation 15min.
3. preparation method as claimed in claim 2, wherein in step 1, the mass fraction of Al is 8%, is obtained by cold rolling The final thickness of cold rolling Ti alloy strip steel rolled stock is 40 μm.
4. preparation method as claimed in claim 2, wherein in step 1, the mass fraction of Al is 7%, is obtained by cold rolling The final thickness of cold rolling Ti alloy strip steel rolled stock is 30 μm.
5. preparation method as claimed in claim 2, wherein in step 2, the cold rolling Ti alloy strip steel rolled stock is heated to 1390 DEG C 10min~15min is kept the temperature, it is air-cooled immediately after.
6. preparation method as claimed in claim 2, wherein in step 2, the cold rolling Ti alloy strip steel rolled stock is heated to 1420 DEG C 10min~15min is kept the temperature, it is air-cooled immediately after.
7. preparation method as claimed in claim 2, wherein in step 3, Ni-9.3at.%W alloy with a thickness of 100nm, very Reciprocal of duty cycle is 0.2Pa, and sputtering power is 200W~270W.
8. preparation method as claimed in claim 2, wherein in step 3, Ni-9.3at.%W alloy with a thickness of 500nm, very Reciprocal of duty cycle is 0.8Pa, sputtering power 270W.
9. preparation method as claimed in claim 2, wherein with 1260 DEG C of heat preservation 15min in step 4.
10. preparation method as claimed in claim 2, wherein with 1300 DEG C of heat preservation 15min in step 4.
CN201811540577.6A 2018-12-17 2018-12-17 High-performance cubic texture metal base band and preparation method thereof Expired - Fee Related CN109371284B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201811540577.6A CN109371284B (en) 2018-12-17 2018-12-17 High-performance cubic texture metal base band and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201811540577.6A CN109371284B (en) 2018-12-17 2018-12-17 High-performance cubic texture metal base band and preparation method thereof

Publications (2)

Publication Number Publication Date
CN109371284A true CN109371284A (en) 2019-02-22
CN109371284B CN109371284B (en) 2020-11-03

Family

ID=65374154

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201811540577.6A Expired - Fee Related CN109371284B (en) 2018-12-17 2018-12-17 High-performance cubic texture metal base band and preparation method thereof

Country Status (1)

Country Link
CN (1) CN109371284B (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2023120631A1 (en) * 2021-12-24 2023-06-29 日本製鉄株式会社 Titanium alloy foil, display panel, and method for manufacturing display panel

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105525146A (en) * 2016-01-17 2016-04-27 北京工业大学 Method for improving content of cubic texture of Ni9.3W base band for YBCO superconductor
CN106825104A (en) * 2017-01-25 2017-06-13 郑州师范学院 A kind of high intensity nickel-tungsten alloy base-band of strong cubic texture and preparation method thereof
CN108359946A (en) * 2018-04-08 2018-08-03 苏州诺弘添恒材料科技有限公司 A kind of preparation method of titanium magnalium lightweight memorial alloy film

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105525146A (en) * 2016-01-17 2016-04-27 北京工业大学 Method for improving content of cubic texture of Ni9.3W base band for YBCO superconductor
CN106825104A (en) * 2017-01-25 2017-06-13 郑州师范学院 A kind of high intensity nickel-tungsten alloy base-band of strong cubic texture and preparation method thereof
CN108359946A (en) * 2018-04-08 2018-08-03 苏州诺弘添恒材料科技有限公司 A kind of preparation method of titanium magnalium lightweight memorial alloy film

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2023120631A1 (en) * 2021-12-24 2023-06-29 日本製鉄株式会社 Titanium alloy foil, display panel, and method for manufacturing display panel
JP7447362B2 (en) 2021-12-24 2024-03-11 日本製鉄株式会社 Titanium alloy foil, display panel, and display panel manufacturing method

Also Published As

Publication number Publication date
CN109371284B (en) 2020-11-03

Similar Documents

Publication Publication Date Title
CN102756512B (en) Low-magnetism or magnetism-free and high-strength Ni-W alloy composite base band and preparation method thereof
US20170037504A1 (en) Method for preparing rare-earth permanent magnetic material with grain boundary diffusion using composite target by vapor deposition
CN108039259A (en) A kind of infiltration has the neodymium iron boron magnetic body of heavy rare earth and the method in neodymium iron boron magnetic body surface penetration heavy rare earth
CN103952592B (en) The preparation method of nonmagnetic conductor of high-temperature superconductor coat cubic texture nickel-base alloy base band
CN102500638B (en) Method for producing high-cube-texture high-tungsten-content NI (nickel)-W (tungsten) alloy substrate bands
CN101635185B (en) Method for preparing Ni-W alloy base band with non/low magnetic cubic texture
CN103060701B (en) Preparation method for non-oriented high-silicon electrical steel ribbon
WO2020155113A1 (en) Preparation method for rare earth diffused magnet and rare earth diffused magnet
CN106825104B (en) A kind of high intensity nickel-tungsten alloy base-band of strong cubic texture and preparation method thereof
CN106399756B (en) A kind of preparation method of high-performance cubic texture nickel-base alloy base band
CN107267901B (en) A kind of preparation method of the high intensity without ferromagnetism texture Ni-W alloy base bands
CN109371284A (en) A kind of high-performance cubic-textured metal base band and preparation method thereof
CN109371286A (en) A kind of iron-free magnetic cubic texture Ni base alloy baseband and preparation method thereof
CN109536907B (en) High-strength strong-cube-texture layered composite baseband and preparation method thereof
CN109576644A (en) A kind of method of prepares coating conductor high-tungsten alloy base band
CN109811310B (en) Non-ferromagnetic, high-strength and strong-cube-texture nickel-tungsten composite baseband and preparation method thereof
CN106702216B (en) A kind of preparation method of iron-free magnetic cubic texture nickel-tungsten alloy base-band
CN109338161A (en) A kind of cubic texture nickel alloy base band and preparation method thereof
CN109930099B (en) Preparation method of high-strength strong-cube-texture Cu-Fe-Zr-P alloy baseband
CN109604546A (en) A kind of high-intensitive, strong cubic texture nickel tungsten base band preparation method
CN109355519A (en) A kind of preparation method improving iron-free magnetic cubic texture acid bronze alloy base band intensity
CN109531067A (en) A kind of no ferromagnetism texture cupro-nickel/nickel tungsten composite baseband and preparation method thereof
CN109735778A (en) A kind of preparation method of high intensity cubic-textured metal base band
CN106868344B (en) A kind of preparation method of high-performance cubic texture Ni-12at.%W alloy base bands
CN105537562A (en) Method for preparing ferromagnetism-free and high-strength texture copper-nickel alloy composite substrate

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20201103

Termination date: 20211217

CF01 Termination of patent right due to non-payment of annual fee