CN109370763A - A kind of preparation method of peony seed oil - Google Patents

A kind of preparation method of peony seed oil Download PDF

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Publication number
CN109370763A
CN109370763A CN201811610106.8A CN201811610106A CN109370763A CN 109370763 A CN109370763 A CN 109370763A CN 201811610106 A CN201811610106 A CN 201811610106A CN 109370763 A CN109370763 A CN 109370763A
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China
Prior art keywords
enzyme preparation
peony
seed
aqueous solution
oil
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CN201811610106.8A
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祖元刚
赵修华
葛云龙
祖述冲
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Northeast Forestry University
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Northeast Forestry University
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/02Pretreatment
    • C11B1/025Pretreatment by enzymes or microorganisms, living or dead
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/02Pretreatment
    • C11B1/04Pretreatment of vegetable raw material
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/06Production of fats or fatty oils from raw materials by pressing

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Biochemistry (AREA)
  • Microbiology (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Fats And Perfumes (AREA)

Abstract

The present invention provides a kind of preparation methods of peony seed oil, belong to edible oil processing technique field, the described method comprises the following steps: 1) being shelled, crushed to Paeonia suffruticosa seed, obtain tree peony kernel powder;2) step 1) the tree peony kernel powder and enzyme preparation aqueous solution are mixed, is digested, obtains enzymolysis liquid;3) enzymolysis liquid described in step 2) is dried, squeezes, obtains peony seed oil;Enzyme preparation described in step 2) includes one or more of cellulase, neutral proteinase, alkali protease, alpha-amylase, pectase and hemicellulase;The temperature of squeezing described in step 3) is 50~80 DEG C.Method of the invention has the advantages that Milling Efficiencty is high, oil yield is high, seed dregs of rice residual oil content is low.

Description

A kind of preparation method of peony seed oil
Technical field
The present invention relates to edible oil processing technique field more particularly to a kind of preparation methods of peony seed oil.
Background technique
Peony seed oil is a kind of new resource food grease.Alpha-linolenic acid is rich in peony seed oil.Alpha-linolenic acid is to constitute carefully The basic substance of after birth and biological enzyme, plays a decisive role to human health, be human health it is required but general lack of one Kind essential nutrients.Peony seed oil has very high health care and medical value.Although peony seeds are a kind of high oil content oil plants, Fat content is up to 32%~34%, but peony seeds kind grain is hard, and existing press apparatus is for squeezing peony seed oil not It can reach ideal oil yield and squeezing effect, such as traditional extrusion Technology in Pressing seed dregs of rice residual oil content 10% or so, spiral shell Spinning squeezes seed technology dregs of rice residual oil content 8% or so.
Summary of the invention
The purpose of the present invention is to provide a kind of method for preparing peony seed oil, this method has Milling Efficiencty high, fuel-displaced The advantage that rate is high, seed dregs of rice residual oil content is low.
In order to achieve the above-mentioned object of the invention, the present invention the following technical schemes are provided:
The present invention provides a kind of preparation methods of peony seed oil, comprising the following steps:
1) it shelled, crushed to Paeonia suffruticosa seed, obtain tree peony kernel powder;
2) step 1) the tree peony kernel powder and enzyme preparation aqueous solution are mixed, is digested, obtains enzymolysis liquid;
3) enzymolysis liquid described in step 2) is dried, squeezes, obtains peony seed oil;
Enzyme preparation described in step 2) includes cellulase, neutral proteinase, alkali protease, alpha-amylase, pectase One or more of with hemicellulase;
The temperature of squeezing described in step 3) is 50~80 DEG C.
Preferably, the mass ratio of tree peony kernel powder and enzyme preparation aqueous solution is 8~15:1~3 in step 2);The enzyme system The mass ratio of enzyme preparation and water is 0.01~3:10~100 in agent aqueous solution.
It preferably, further include preparation enzyme preparation aqueous solution before tree peony kernel powder and the mixing of enzyme preparation aqueous solution;The enzyme Preparation aqueous solution the preparation method comprises the following steps: enzyme preparation is dissolved in the water, activated, obtain enzyme preparation aqueous solution;The activation Temperature be 30~50 DEG C.
Preferably, the time of the activation is 5~30min.
Preferably, the temperature of enzymatic hydrolysis described in step 2) is 30~50 DEG C;The time of the enzymatic hydrolysis is 4~12h.
Preferably, temperature dry described in step 3) is 50~80 DEG C;The time of the drying is 4~10h.
Preferably, the partial size of the Paeonia suffruticosa seed powder is 1~2mm.
Preferably, the Paeonia suffruticosa seed is phoenix pellet Paeonia suffruticosa seed.
Preferably, the number of the step 3) squeezing is 2 times.
Preferably, the equipment of the step 3) squeezing is pressafiner.
Beneficial effects of the present invention: the present invention provides a kind of preparation method of peony seed oil, this method passes through to tree peony Seed benevolence is crushed, and is capable of increasing the contact area of peony seeds benevolence Yu enzyme preparation aqueous solution, and then sufficiently digest;Also, pass through Enzymolysis processing destroys the special microstructure that pectin, albumen, starch and grease are formed in peony seeds, discharges grease;And with Pressing temperature is arranged in traditional technology to compare for 120 DEG C or more, the present invention can squeeze under conditions of 50~80 DEG C, low Temperature and pressure squeeze the nutritional ingredient that can be sufficiently reserved peony seed oil, and high temperature can be such that peony seed oil quickly aoxidizes, rancid rotten.By testing Card, the method for the present invention improve 32.1%~43.2% compared with conventional press method Milling Efficiencty, and pressing temperature is low, and residual oil content reduces 1.5%~3.2%, oil yield improves 1.68%~6.12%.
Specific embodiment
The present invention provides a kind of preparation methods of peony seed oil, comprising the following steps:
1) it shelled, crushed to Paeonia suffruticosa seed, obtain tree peony kernel powder;
2) step 1) the tree peony kernel powder and enzyme preparation aqueous solution are mixed, is digested, obtains enzymolysis liquid;
3) enzymolysis liquid described in step 2) is dried, squeezes, obtains peony seed oil.
The present invention shells to Paeonia suffruticosa seed, crushes, and obtains tree peony kernel powder.In the present invention, the Paeonia suffruticosa seed is excellent It is selected as mature Paeonia suffruticosa seed (endosperm development is complete, and seed is full, without rancid);The kind of the Paeonia suffruticosa seed is preferably that phoenix pellet is male Red seed;The phoenix pellet Paeonia suffruticosa seed is easy to get with raw material, advantage at low cost.
In the present invention, the equipment of the shelling is preferably hulling machine, more preferably the dedicated hulling machine of peony seeds,;It is described male The red dedicated hulling machine of seed is purchased from Jiangsu Hongbo Machinery Manufacture Co., Ltd.;The effect of the hulling machine is sieved to peony seeds Divide, shelling, then carries out selection by winnowing and obtain peony seeds benevolence;It is first because peony seeds granule size is different in specific implementation process of the invention Sieve varigrained peony seeds first with 4 kinds of different pore size (90mm, 80mm, 70mm, 60mm) cylinder round sifter Point, 4 kinds of varigrained peony seeds after screening are shelled, then carry out pneumatic separation device respectively, finally obtains peony seeds benevolence.
In the present invention, the time of the crushing is preferably 3~5min, more preferably 4min;The present invention is to the crushing Temperature is not particularly limited;The equipment of the pulverization process is preferably pulverizer, is more preferably had purchased from million Shen science and technology of Shanghai The multifunctional crusher of limit company;The partial size of the smashed tree peony kernel powder is preferably 1~2mm;The effect of the crushing It is to come into full contact with peony seeds benevolence with enzyme preparation, digests more complete.
Enzyme preparation is dissolved in the water by the present invention, is activated, and enzyme preparation aqueous solution is obtained;In the present invention, the enzyme system Agent preferably includes one in cellulase, neutral proteinase, alkali protease, alpha-amylase, pectase and hemicellulase Kind is several, more preferably cellulase and alpha-amylase, most preferably alpha-amylase;The alpha-amylase can destroy tree peony The special microstructure that pectin, albumen, starch and grease are formed in seed, sufficiently release peony seed oil.
In the present invention, the mass ratio of the enzyme preparation and water is preferably 0.01~3:10~100, and more preferably 1~2.5: 15~50, more preferably 2:20;The temperature of the activation is preferably 30~60 DEG C, more preferably 35~55 DEG C, more preferably 50 ℃;The time of the activation is preferably 5~30min, more preferably 10~25min, most preferably 15~20min;The activation The effect of processing is to improve enzyme activity, and then improve enzymolysis efficiency.
The present invention mixes tree peony kernel powder and enzyme preparation aqueous solution after obtaining tree peony kernel powder and enzyme preparation aqueous solution It closes, is digested, obtain enzymolysis liquid;The quality of the tree peony kernel powder and enzyme preparation aqueous solution is preferably 8~15:1~3, more Preferably 10~12:2.
In the present invention, the mixed temperature is preferably 40~60 DEG C, and more preferably 50 DEG C;The present invention is to the mixed time There is no particular/special requirement, is subject to and is uniformly mixed;The mixed mode is preferably stirred;The frequency being stirred is excellent It is selected as 30min/ times, the time stirred every time is preferably 15~20min;The revolving speed of the stirring is preferably 80rpm;Of the invention In specific implementation process, the time tentatively stirred is 20min, then stirs 1 time (mixing time 5min) to enzymatic hydrolysis every 30min Terminate, speed of agitator 80r/min;The temperature of the enzymatic hydrolysis is preferably 30~60 DEG C, and more preferably 35~55 DEG C, more preferably 50℃;The time of the enzymatic hydrolysis is preferably 4~12h, more preferably 6~10h, most preferably 8h;The effect of the enzymatic hydrolysis is broken The special microstructure that pectin, albumen, starch and grease are formed in bad peony seeds, and then oil yield is improved, reduce seed dregs of rice Residual oil Rate.
The present invention is dried enzymolysis liquid after obtaining enzymolysis liquid, and squeezing obtains peony seed oil;The temperature of the drying Preferably 40~90 DEG C of degree, more preferably 45~80 DEG C, most preferably 50~70 DEG C;The time of the drying is preferably 4~ 10h, more preferably 6~8h, most preferably 7h;The water content of solid content is preferably 4%~10% after the drying, more preferably 6%~7%;The water content of solid content is 4%~10% after setting drying in the present invention, advantageously reduces seed dregs of rice Residual oil after squeezing Rate;The mode of the drying is preferably dried;The equipment of the drying is preferably that electric drying oven with forced convection is (safe purchased from Tianjin Si Te Instrument Ltd., model: WGLL-625BE type);The temperature of the squeezing is preferably 50~80 DEG C, more preferably 30~ 60 DEG C, most preferably 40~50 DEG C;The squeezing number is preferably 2 times;The equipment of the squeezing is preferably pressafiner, more Preferably Changbai Mountain board oil press of the Changchun rich people up to the development of oil press Co., Ltd, model: CBS-95, treating capacity: 50kg/ h。
A kind of preparation method of peony seed oil provided by the invention is described in detail below with reference to embodiment, still They cannot be interpreted as limiting the scope of the present invention.
A kind of preparation method of the peony seed oil of embodiment 1
After mature phoenix pellet Paeonia suffruticosa seed shelling is crushed, weighs 10g alpha-amylase and be dissolved in 1kg water, at 50 DEG C 15min is activated in water bath with thermostatic control, the enzyme preparation aqueous solution of activation is uniformly mixed with 5kg tree peony kernel powder, in 50 DEG C of item 6h is digested under part, the temperature of air dry oven is set as 55 DEG C, is squeezed after drying 6h with pressafiner, detection is (uncommon Ma board hand-held infrared temperature measurement gun, model: AS852B) pressing temperature be 61 DEG C, squeezing number be 2 times, used time 4.5min, pressure Squeezing efficiency is 1.11kg/min, and gained 1.41kg oil product is peony seed oil, oil yield 28.24%.Utilize Soxhlet extraction side Method detects seed dregs of rice residual oil content, the results show that detection seed dregs of rice residual oil content is 4.8%.
A kind of preparation method of the peony seed oil of embodiment 2
After mature phoenix pellet Paeonia suffruticosa seed shelling is crushed, weighs 0.1kg alpha-amylase and be dissolved in 10kg water, at 50 DEG C Water bath with thermostatic control in activate 20min, the enzyme preparation aqueous solution of activation is uniformly mixed with 50kg tree peony kernel powder, at 50 DEG C Under the conditions of digest 6h, the temperature of air dry oven is set as 55 DEG C, is squeezed after drying 6h with pressafiner, detection pressure Squeezing temperature is 60 DEG C, and squeezing number is 2 times, used time 44.2min, Milling Efficiencty 1.13kg/min, and gained 13.35kg oil product is For peony seed oil, oil yield 27%.Seed dregs of rice residual oil content is detected using Soxhlet extraction method, testing result shows seed dregs of rice residual oil content It is 4.6%.
A kind of preparation method of the peony seed oil of embodiment 3
After mature phoenix pellet Paeonia suffruticosa seed shelling is crushed, weighs 0.4kg alpha-amylase and be dissolved in 40kg water, at 50 DEG C Water bath with thermostatic control in activate 20min, the enzyme preparation aqueous solution of activation is uniformly mixed with 200kg tree peony kernel powder, at 50 DEG C Under conditions of digest 6h, the temperature of air dry oven is set as 55 DEG C, is squeezed after drying 6h with pressafiner, is detected Pressing temperature is 65 DEG C, and squeezing number is 2 times, used time 172.3min, Milling Efficiencty 1.16kg/min, gained 53.62kg Oil product is peony seed oil, oil yield 26.81%.Seed dregs of rice residual oil content is detected using Soxhlet extraction method, the results show that detection Seed dregs of rice residual oil content is 4.7%.
A kind of preparation method of the peony seed oil of embodiment 4
After mature phoenix pellet Paeonia suffruticosa seed shelling is crushed, weighs 0.05kg alkali protease and be dissolved in 5kg water, 50 DEG C water bath with thermostatic control in activate 20min, the enzyme preparation aqueous solution of activation is uniformly mixed with 25kg tree peony kernel powder, at 50 DEG C Under conditions of digest 6h, the temperature of air dry oven is set as 55 DEG C, is squeezed after drying 6h with pressafiner, is detected Pressing temperature is 67 DEG C, and squeezing number is 2 times, used time 22.6min, Milling Efficiencty 1.11kg/min, gained 6.11kg oil product As peony seed oil, oil yield 24.7%.Seed dregs of rice residual oil content is detected using Soxhlet extraction method, the results show that seed dregs of rice Residual oil Rate is 5.9%.
A kind of preparation method of the peony seed oil of embodiment 5
After mature phoenix pellet Paeonia suffruticosa seed shelling is crushed, weighs 0.05kg acid protease and be dissolved in 5kg water, 50 DEG C water bath with thermostatic control in activate 20min, the enzyme preparation aqueous solution of activation is uniformly mixed with 25kg tree peony kernel powder, at 50 DEG C Under conditions of digest 6h, the temperature of air dry oven is set as 55 DEG C, is squeezed after drying 6h with pressafiner, is detected Pressing temperature is 68 DEG C, and squeezing number is 2 times, used time 22.8min, Milling Efficiencty 1.10kg/min, gained 6.21kg oil product As peony seed oil, oil yield 24.9%.Seed dregs of rice residual oil content is detected using Soxhlet extraction method, the results show that seed dregs of rice Residual oil Rate is 5.8%.
A kind of preparation method of the peony seed oil of embodiment 6
After mature phoenix pellet Paeonia suffruticosa seed shelling is crushed, weighs 0.05kg pectase and be dissolved in 5kg water, at 50 DEG C 20min is activated in water bath with thermostatic control, the enzyme preparation aqueous solution of activation is uniformly mixed with 25kg tree peony kernel powder, in 50 DEG C of item 6h is digested under part, the temperature of air dry oven is set as 55 DEG C, is squeezed after drying 6h with pressafiner, detection squeezing Temperature is 62 DEG C, and squeezing number is 2 times, used time 23.4min, Milling Efficiencty 1.07kg/min, and gained 6.0kg oil product is as male Red seed oil, oil yield 24.1%.Seed dregs of rice residual oil content is detected using Soxhlet extraction method, the results show that seed dregs of rice residual oil content is 6.1%.
A kind of preparation method of the peony seed oil of embodiment 7
After mature phoenix pellet Paeonia suffruticosa seed shelling is crushed, weighs 0.05kg cellulase and be dissolved in 5kg water, at 50 DEG C Water bath with thermostatic control in activate 20min, the enzyme preparation aqueous solution of activation is uniformly mixed with 25kg tree peony kernel powder, at 50 DEG C Under the conditions of digest 6h, the temperature of air dry oven is set as 55 DEG C, is squeezed after drying 6h with pressafiner, detection pressure Squeezing temperature is 70 DEG C, and squeezing number is 2 times, used time 23.1min, Milling Efficiencty 1.08kg/min, and gained 5.95kg oil product is For peony seed oil, oil yield 23.8%.Seed dregs of rice residual oil content is detected using Soxhlet extraction method, the results show that seed dregs of rice residual oil content It is 6.3%.
Comparative example 1
Directly peony seeds are squeezed using pressafiner, 50kg shelling peony seeds (not digesting) is squeezed, and is pressed Squeezing number is used time 61.5min, Milling Efficiencty 0.81kg/min twice, and detection pressing temperature is 105 DEG C, obtains 11.06kg Peony seed oil, oil yield 22.12%.Detecting seed dregs of rice residual oil content is 7.8%.
As seen from the above embodiment, the present invention provides a kind of preparation method of peony seed oil, the residual oil content of this method is 4.6%~6.3%, oil yield is 23.8%~28.24%;Compared with comparative example 1, Milling Efficiencty improves 32.1%~ 43.2%, residual oil content reduces 1.5%~3.2%, and oil yield improves 1.68%~6.12%.
The above is only a preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art For member, various improvements and modifications may be made without departing from the principle of the present invention, these improvements and modifications are also answered It is considered as protection scope of the present invention.

Claims (10)

1. a kind of preparation method of peony seed oil, comprising the following steps:
1) it shelled, crushed to Paeonia suffruticosa seed, obtain tree peony kernel powder;
2) step 1) the tree peony kernel powder and enzyme preparation aqueous solution are mixed, is digested, obtains enzymolysis liquid;
3) enzymolysis liquid described in step 2) is dried, squeezes, obtains peony seed oil;
Enzyme preparation described in step 2) includes cellulase, neutral proteinase, alkali protease, alpha-amylase, pectase and half One or more of cellulase;
The temperature of squeezing described in step 3) is 50~80 DEG C.
2. the method according to claim 1, wherein in step 2) tree peony kernel powder and enzyme preparation aqueous solution matter Amount is than being 8~15:1~3;The mass ratio of enzyme preparation and water is 0.01~3:10~100 in the enzyme preparation aqueous solution.
3. method according to claim 1 or 2, which is characterized in that before tree peony kernel powder and the mixing of enzyme preparation aqueous solution, It further include preparation enzyme preparation aqueous solution;The enzyme preparation aqueous solution the preparation method comprises the following steps: enzyme preparation is dissolved in the water, live Change, obtains enzyme preparation aqueous solution;The temperature of the activation is 30~50 DEG C.
4. according to the method described in claim 3, it is characterized in that, the time of the activation is 5~30min.
5. the method according to claim 1, wherein the temperature of enzymatic hydrolysis described in step 2) is 30~50 DEG C;Institute The time for stating enzymatic hydrolysis is 4~12h.
6. the method according to claim 1, wherein temperature dry described in step 3) is 50~80 DEG C;Institute Stating the dry time is 4~10h.
7. the method according to claim 1, wherein the partial size of the Paeonia suffruticosa seed powder is 1~2mm.
8. the method according to claim 1, wherein the Paeonia suffruticosa seed is phoenix pellet Paeonia suffruticosa seed.
9. the method according to claim 1, wherein the number of the step 3) squeezing is 2 times.
10. according to claim 1 or method described in 9, which is characterized in that the equipment of the step 3) squeezing is screw press Machine.
CN201811610106.8A 2018-12-27 2018-12-27 A kind of preparation method of peony seed oil Pending CN109370763A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112920886A (en) * 2021-01-07 2021-06-08 龙池牡丹实业有限公司 Enzymolysis preparation method of peony seed micromolecule oil

Citations (4)

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Publication number Priority date Publication date Assignee Title
CN102746938A (en) * 2012-07-14 2012-10-24 中国农业科学院油料作物研究所 Method for preparing grease and protein from oil seed kernels by aqueous enzymatic method
CN103820205A (en) * 2014-03-21 2014-05-28 南京飞马食品有限公司 Method for preparing highly unsaturated camellia seed clean oil by using biological enzyme method
CN105602700A (en) * 2015-12-22 2016-05-25 江苏国色天香油用牡丹科技发展有限公司 Preparation method of cold-pressed peony seed oil with high oil yield
CN108753432A (en) * 2018-05-30 2018-11-06 山东省科学院生物研究所 A kind of method that aqueous enzymatic method prepares granada seed oil

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102746938A (en) * 2012-07-14 2012-10-24 中国农业科学院油料作物研究所 Method for preparing grease and protein from oil seed kernels by aqueous enzymatic method
CN103820205A (en) * 2014-03-21 2014-05-28 南京飞马食品有限公司 Method for preparing highly unsaturated camellia seed clean oil by using biological enzyme method
CN105602700A (en) * 2015-12-22 2016-05-25 江苏国色天香油用牡丹科技发展有限公司 Preparation method of cold-pressed peony seed oil with high oil yield
CN108753432A (en) * 2018-05-30 2018-11-06 山东省科学院生物研究所 A kind of method that aqueous enzymatic method prepares granada seed oil

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112920886A (en) * 2021-01-07 2021-06-08 龙池牡丹实业有限公司 Enzymolysis preparation method of peony seed micromolecule oil

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