CN108949340A - A kind of preparation method of peony seed oil - Google Patents

A kind of preparation method of peony seed oil Download PDF

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Publication number
CN108949340A
CN108949340A CN201811074927.4A CN201811074927A CN108949340A CN 108949340 A CN108949340 A CN 108949340A CN 201811074927 A CN201811074927 A CN 201811074927A CN 108949340 A CN108949340 A CN 108949340A
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CN
China
Prior art keywords
peony
seed oil
peony seeds
seeds
frying
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201811074927.4A
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Chinese (zh)
Inventor
王立胜
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Anhui Great Foshan Yangxin Valley Tourism Development Co Ltd
Original Assignee
Anhui Great Foshan Yangxin Valley Tourism Development Co Ltd
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Application filed by Anhui Great Foshan Yangxin Valley Tourism Development Co Ltd filed Critical Anhui Great Foshan Yangxin Valley Tourism Development Co Ltd
Priority to CN201811074927.4A priority Critical patent/CN108949340A/en
Publication of CN108949340A publication Critical patent/CN108949340A/en
Withdrawn legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/02Pretreatment
    • C11B1/04Pretreatment of vegetable raw material
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/10Production of fats or fatty oils from raw materials by extracting
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/10Production of fats or fatty oils from raw materials by extracting
    • C11B1/108Production of fats or fatty oils from raw materials by extracting after-treatment, e.g. of miscellae

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Noodles (AREA)
  • General Preparation And Processing Of Foods (AREA)

Abstract

The invention discloses a kind of preparation methods of peony seed oil, a kind of production stage of the preparation method of peony seed oil includes: that (1) raw material is chosen: weighing the peony seeds of the full grains of certain mass number, the peony seeds completed will be chosen and be put into clear water and impregnated, the impurity and dust on surface are removed in soaking process, be dipped to tree peony seed surface seed peel fall off until, the peony seeds for then choosing underwater mature and plump are spare.The present invention can be reduced the moisture inside peony seeds as far as possible by drying, crushing and the setting of frying process; and the oil mass inside peony seeds can be made to be extracted to the greatest extent by the different extractions of two steps; and the setting of heating process can make impurity such as the water inside peony seed oil etc., this extraction mode can protect the nutritional ingredient inside peony seeds not to be lost as far as possible.

Description

A kind of preparation method of peony seed oil
Technical field
The present invention relates to food technology field, specially a kind of preparation method of peony seed oil.
Background technique
Peony seed oil, also known as peony oil are the woody nut plant oils extracted by peony seeds, are that China is distinctive, because of it It is full of nutrition and unique, and have medical care effect, it is the treasure in vegetable oil by relevant expert is known as " best oil in the world, " Product, and the health care edible oil and fat that China is exclusive.
Now traditional peony seed oil mostly uses greatly the mode of squeezing to extract during the manufacturing, but squeezes male Red seed oil extract rate is lower, and peony seeds itself are more precious, will cause pole to peony seeds in the lower situation of recovery rate Big waste, and wherein nutritional ingredient can also be extracted not enough to a certain extent, for this purpose, it is proposed that a kind of system of peony seed oil Preparation Method.
Summary of the invention
The purpose of the present invention is to provide a kind of preparation methods of peony seed oil, are asked with solve to propose in background technique Topic.
To achieve the above object, the invention provides the following technical scheme: a kind of preparation method of peony seed oil, described one kind The production stage of the preparation method of peony seed oil includes:
(1) raw material is chosen: weighing the peony seeds of the full grains of certain mass number, will choose the peony seeds completed and be put into clear water In impregnated, in soaking process remove surface impurity and dust, be dipped to tree peony seed surface seed peel fall off until, then The peony seeds for choosing underwater mature and plump are spare;
(2) dry: the peony seeds for the mature and plump that step (1) is chosen carry out drying and processing, and drying temperature is 45-50 DEG C, dry It does to peony seeds internal moisture lower than 10%;
(3) it crushes: the peony seeds that step (2) drying is completed is subjected to pulverization process, the sieve sieve of 40-60 mesh is crossed after the completion of crushing It selects spare;
(4) frying: step (3) are crushed to the peony seeds completed and carry out frying, frying temperature is 80-90 DEG C, and the frying time is 15- 20min;
(5) it extracts:
S1: dehydrated alcohol is added in the peony seeds after completing to step (4) frying until impregnating peony seeds, then impregnates 3-3.5h, being subsequently placed into vacuum degree is to carry out vacuum hydro-extraction in environment that vacuum degree is 0.08-0.1MPa to obtain a mao peony seed oil;
S2: carrying out subcritical abstraction with butane then to a certain amount of solvent is added in the hair peony seed oil extracted in S1 step, The peony seed oil of certain purity can be obtained;
(6) it heating: the peony seed oil that step (5) obtains being put into heat pump and is heated, heating temperature is 110-130 DEG C, And constantly it is stirred, mixing speed 30-40r/min, heating 30-40min until pasta bubble-free can be obtained it is male Red seed oil.
The present invention can be subtracted the moisture inside peony seeds as far as possible by drying, crushing and the setting of frying process It is few, and the oil mass inside peony seeds can be made to be extracted to the greatest extent by the different extractions of two steps, and heating process Impurity such as water inside peony seed oil etc. can be made by being arranged, and this extraction mode can protect the battalion inside peony seeds as far as possible Forming point will not be lost.
Specific embodiment
Technical scheme in the embodiment of the invention is clearly and completely described, it is clear that described embodiment is only It is a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, ordinary skill people Member's every other embodiment obtained without making creative work, shall fall within the protection scope of the present invention.
Embodiment one:
A kind of preparation method of peony seed oil, a kind of production stage of the preparation method of peony seed oil include:
(1) raw material is chosen: weighing the peony seeds of the full grains of certain mass number, will choose the peony seeds completed and be put into clear water In impregnated, in soaking process remove surface impurity and dust, be dipped to tree peony seed surface seed peel fall off until, then The peony seeds for choosing underwater mature and plump are spare;
(2) dry: the peony seeds for the mature and plump that step (1) is chosen carry out drying and processing, and drying temperature is 45 DEG C, are dried to Peony seeds internal moisture is lower than 10%;
(3) it crushes: the peony seeds that step (2) drying is completed is subjected to pulverization process, the sieve screening of 40 mesh is crossed after the completion of crushing It is spare;
(4) frying: step (3) are crushed to the peony seeds completed and carry out frying, frying temperature is 80 DEG C, and the frying time is 15min;
(5) it extracts:
S1: dehydrated alcohol is added in the peony seeds after completing to step (4) frying until impregnating peony seeds, then impregnates 3h, being subsequently placed into vacuum degree is to carry out vacuum hydro-extraction in environment that vacuum degree is 0.08MPa to obtain a mao peony seed oil;
S2: carrying out subcritical abstraction with butane then to a certain amount of solvent is added in the hair peony seed oil extracted in S1 step, The peony seed oil of certain purity can be obtained;
(6) it heats: the peony seed oil that step (5) obtains being put into heat pump and is heated, heating temperature is 110 DEG C, not Disconnected to be stirred to it, mixing speed 30r/min, heating 30min are until peony seed oil can be obtained in pasta bubble-free.
Embodiment two:
A kind of preparation method of peony seed oil, a kind of production stage of the preparation method of peony seed oil include:
(1) raw material is chosen: weighing the peony seeds of the full grains of certain mass number, will choose the peony seeds completed and be put into clear water In impregnated, in soaking process remove surface impurity and dust, be dipped to tree peony seed surface seed peel fall off until, then The peony seeds for choosing underwater mature and plump are spare;
(2) dry: the peony seeds for the mature and plump that step (1) is chosen carry out drying and processing, and drying temperature is 50 DEG C, are dried to Peony seeds internal moisture is lower than 10%;
(3) it crushes: the peony seeds that step (2) drying is completed is subjected to pulverization process, the sieve screening of 60 mesh is crossed after the completion of crushing It is spare;
(4) frying: step (3) are crushed to the peony seeds completed and carry out frying, frying temperature is 90 DEG C, and the frying time is 20min;
(5) it extracts:
S1: dehydrated alcohol is added in the peony seeds after completing to step (4) frying until impregnating peony seeds, then impregnates 3.5h, being subsequently placed into vacuum degree is to carry out vacuum hydro-extraction in environment that vacuum degree is 0.1MPa to obtain a mao peony seed oil;
S2: carrying out subcritical abstraction with butane then to a certain amount of solvent is added in the hair peony seed oil extracted in S1 step, The peony seed oil of certain purity can be obtained;
(6) it heats: the peony seed oil that step (5) obtains being put into heat pump and is heated, heating temperature is 130 DEG C, not Disconnected to be stirred to it, mixing speed 40r/min, heating 40min are until peony seed oil can be obtained in pasta bubble-free.
Embodiment three:
A kind of preparation method of peony seed oil, a kind of production stage of the preparation method of peony seed oil include:
(1) raw material is chosen: weighing the peony seeds of the full grains of certain mass number, will choose the peony seeds completed and be put into clear water In impregnated, in soaking process remove surface impurity and dust, be dipped to tree peony seed surface seed peel fall off until, then The peony seeds for choosing underwater mature and plump are spare;
(2) dry: the peony seeds for the mature and plump that step (1) is chosen carry out drying and processing, and drying temperature is 48 DEG C, are dried to Peony seeds internal moisture is lower than 10%;
(3) it crushes: the peony seeds that step (2) drying is completed is subjected to pulverization process, the sieve screening of 50 mesh is crossed after the completion of crushing It is spare;
(4) frying: step (3) are crushed to the peony seeds completed and carry out frying, frying temperature is 85 DEG C, and the frying time is 18min;
(5) it extracts:
S1: dehydrated alcohol is added in the peony seeds after completing to step (4) frying until impregnating peony seeds, then impregnates 3.2h, being subsequently placed into vacuum degree is to carry out vacuum hydro-extraction in environment that vacuum degree is 0.09MPa to obtain a mao peony seed oil;
S2: carrying out subcritical abstraction with butane then to a certain amount of solvent is added in the hair peony seed oil extracted in S1 step, The peony seed oil of certain purity can be obtained;
(6) it heats: the peony seed oil that step (5) obtains being put into heat pump and is heated, heating temperature is 120 DEG C, not Disconnected to be stirred to it, mixing speed 35r/min, heating 35min are until peony seed oil can be obtained in pasta bubble-free.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding And modification, the scope of the present invention is defined by the appended.

Claims (1)

1. a kind of preparation method of peony seed oil, it is characterised in that: a kind of production stage of the preparation method of peony seed oil Include:
(1) raw material is chosen: weighing the peony seeds of the full grains of certain mass number, will choose the peony seeds completed and be put into clear water In impregnated, in soaking process remove surface impurity and dust, be dipped to tree peony seed surface seed peel fall off until, then The peony seeds for choosing underwater mature and plump are spare;
(2) dry: the peony seeds for the mature and plump that step (1) is chosen carry out drying and processing, and drying temperature is 45-50 DEG C, dry It does to peony seeds internal moisture lower than 10%;
(3) it crushes: the peony seeds that step (2) drying is completed is subjected to pulverization process, the sieve sieve of 40-60 mesh is crossed after the completion of crushing It selects spare;
(4) frying: step (3) are crushed to the peony seeds completed and carry out frying, frying temperature is 80-90 DEG C, and the frying time is 15- 20min;
(5) it extracts:
S1: dehydrated alcohol is added in the peony seeds after completing to step (4) frying until impregnating peony seeds, then impregnates 3-3.5h, being subsequently placed into vacuum degree is to carry out vacuum hydro-extraction in environment that vacuum degree is 0.08-0.1MPa to obtain a mao peony seed oil;
S2: carrying out subcritical abstraction with butane then to a certain amount of solvent is added in the hair peony seed oil extracted in S1 step, The peony seed oil of certain purity can be obtained;
(6) it heating: the peony seed oil that step (5) obtains being put into heat pump and is heated, heating temperature is 110-130 DEG C, And constantly it is stirred, mixing speed 30-40r/min, heating 30-40min until pasta bubble-free can be obtained it is male Red seed oil.
CN201811074927.4A 2018-09-14 2018-09-14 A kind of preparation method of peony seed oil Withdrawn CN108949340A (en)

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Application Number Priority Date Filing Date Title
CN201811074927.4A CN108949340A (en) 2018-09-14 2018-09-14 A kind of preparation method of peony seed oil

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Application Number Priority Date Filing Date Title
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Publication Number Publication Date
CN108949340A true CN108949340A (en) 2018-12-07

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113150872A (en) * 2021-05-07 2021-07-23 四川省运好农业开发有限公司 Comprehensive-nutrition peony essential oil refining method
CN116919856A (en) * 2023-05-26 2023-10-24 广州舒雪健康科技有限公司 Preparation process and application of oil-based skin care and moisturizing oil prepared from peony seed oil, olive oil and camellia oil

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113150872A (en) * 2021-05-07 2021-07-23 四川省运好农业开发有限公司 Comprehensive-nutrition peony essential oil refining method
CN116919856A (en) * 2023-05-26 2023-10-24 广州舒雪健康科技有限公司 Preparation process and application of oil-based skin care and moisturizing oil prepared from peony seed oil, olive oil and camellia oil

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Application publication date: 20181207