CN109370301A - A kind of oily solid soluble ink and processing technology again - Google Patents

A kind of oily solid soluble ink and processing technology again Download PDF

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Publication number
CN109370301A
CN109370301A CN201811312756.4A CN201811312756A CN109370301A CN 109370301 A CN109370301 A CN 109370301A CN 201811312756 A CN201811312756 A CN 201811312756A CN 109370301 A CN109370301 A CN 109370301A
Authority
CN
China
Prior art keywords
soluble ink
oily solid
organic pigment
inorganic pigment
pigment
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201811312756.4A
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Chinese (zh)
Inventor
苏志福
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Xiamen Yitong Ink And Wash Co Ltd
Original Assignee
Xiamen Yitong Ink And Wash Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Xiamen Yitong Ink And Wash Co Ltd filed Critical Xiamen Yitong Ink And Wash Co Ltd
Priority to CN201811312756.4A priority Critical patent/CN109370301A/en
Publication of CN109370301A publication Critical patent/CN109370301A/en
Pending legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/02—Printing inks
    • C09D11/10—Printing inks based on artificial resins
    • C09D11/102—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions other than those only involving unsaturated carbon-to-carbon bonds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/02—Printing inks
    • C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
    • C09D11/037—Printing inks characterised by features other than the chemical nature of the binder characterised by the pigment
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/02—Printing inks
    • C09D11/10—Printing inks based on artificial resins
    • C09D11/102—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions other than those only involving unsaturated carbon-to-carbon bonds
    • C09D11/104—Polyesters
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/02—Printing inks
    • C09D11/10—Printing inks based on artificial resins
    • C09D11/106—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C09D11/107—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds from unsaturated acids or derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/02—Printing inks
    • C09D11/10—Printing inks based on artificial resins
    • C09D11/106—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C09D11/108—Hydrocarbon resins

Abstract

The invention discloses a kind of oily solid soluble ink and processing technology again, raw material proportioning is formed by following degree: solid propenoic acid 15-25%, solid polyamide 20-30%, polyester resin 10-20%, chlorinated polypropylene 10-25%, organic pigment or inorganic pigment 30%, oleoresin is put into blender to carry out being uniformly mixed stirring, temperature is in resin softening point polymerization reaction, pressure is in 8hPa or less, 500 ~ 800r/min of mixing speed, organic pigment or inorganic pigment are added after being stirred to react 3-4 hours, temperature is controlled at 50 DEG C ~ 70 DEG C, after being kept stirring speed continuation 10 ~ 20min of uniform stirring, after the above mixture is put into 10 ~ 20min of kneader kneading, again by going out after the dispersion of high-speed flow milling apparatus The features such as material, obtained oily solid soluble ink again after being overpressurized, stirred, mixed, mediated, being crushed, production security height, convenient transportation, high production efficiency, good, environmentally friendly, easy to use stability.

Description

A kind of oily solid soluble ink and processing technology again
Technical field
The invention belongs to technical field of ink, in particular to a kind of oily solid soluble ink and processing technology again.
Background technique
Raw material used by traditional Printing ink producing be liquid resin, organic pigment, inorganic pigment, raw material with it is organic molten After agent mixing, the fineness packed products for causing 20UM are ground through sand mill, solvent largely volatilizees in production process, produces risk pole Degree is high, and organic pigment, inorganic pigment waste, cost of material is high, and liquid ink transport is inconvenient, and transportation logistics are at high cost.
Our company has developed a kind of oily solid soluble ink formula and processing technology again, does not need to grind, directly plus Enter solvent, 20% organic pigment and solvent can be saved, do not have solvent volatilization in production, production security is high, solid ink transport Convenient, transportation logistics are at low cost, and organic pigment or inorganic pigment dosage are few, and cost of material is low, and it is raw to solve traditional liquid ink The deficiencies of production. art is complicated, transport is inconvenient, it is high, at high cost to produce risk, the wasting of resources.
Summary of the invention
To solve, above-mentioned prior art liquid ink production technology is complicated, transport is inconvenient, production risk is high, cost The problems such as height, the wasting of resources；
The present invention provides a kind of oily solid soluble ink, including oleoresin and organic pigment or inorganic pigment again, raw material It is formulated as follows:
A, the composition of raw materials degree of oleoresin is 70%, is specifically formed by following degree:
Solid propenoic acid 15-25%；
Solid polyamide 20-30%；
Polyester resin 10-20%；
Chlorinated polypropylene 10-25%；
B, the composition of raw materials degree of organic pigment or inorganic pigment is 30%.
As improvement of the present invention, the organic pigment color be red, yellow, it is blue in any, nothing Machine pigment color is black.
As a further refinement of the present invention, the organic pigment is quinacridone, dioxazines, anthraquinone, indigoids, phthalocyanine In any or several mixing；The inorganic pigment be titanium dioxide, silicate, phosphate, hydroxide, sulfide, Any or several mixing in iron oxide.
The present invention provides a kind of oily solid soluble ink processing technology again, by oleoresin put into blender into Row is uniformly mixed stirring, and temperature is in 80-100 DEG C of polymerization reaction, and pressure is in 8hPa hereinafter, 500 ~ 800r/min of mixing speed；It stirs Organic pigment or inorganic pigment is added after mixing reaction 3-4 hours, temperature is controlled at 50 DEG C ~ 70 DEG C, is kept stirring speed continuation After 10 ~ 20min of uniform stirring；After the above mixture is put into 10 ~ 20min of kneader kneading, then is ground and set by high-speed flow Back-up discharges after dissipating；Oily solid soluble ink again is made after being overpressurized, stirred, mixed, mediated, being ground.
The beneficial effects of the present invention are:
One is formulated oily solid obtained soluble ink, resin formula has used polymerisation process again using new, from basic On solve that Printing ink producing risk is high, and solvent is volatile, and being produced into for ink is effectively reduced in the deficiency of liquid transporting inconvenience The features such as this, greatly improves production efficiency, and production safety, the utilization of resources is high-quality, and stability is good.
Secondly, it is pollution-free in production process, ink plays important work to environmental protection almost without organic solvent volatilization With to no damage to human body；Simultaneously in use, the health of people will not be impacted, it will not be to the environment of surrounding Cause atmosphere pollution.
Thirdly, organic solvent-free volatilization in production process of the present invention, at least save 20% organic pigment and solvent.
Four, soluble ink is easy to use again for oily solid of the invention, saves the time, and when use is not required to be sanded again, directly Connecing addition solvent can use.
Specific embodiment
It is described in detail the following detailed description of the preferred embodiment of the present invention, so that advantages and features of the invention can be more It is easy to be readily appreciated by one skilled in the art, so as to make a clearer definition of the protection scope of the present invention.
For the difference of the oily solid purposes that soluble ink uses again, the specific share of each component also has one in formula A little differences apply in life and work for different purposes using different proportions is significantly more efficient, solid with regard to oiliness below The difference formula of body soluble ink purposes again illustrates:
Embodiment one
Oleoresin matches as follows:
Solid propenoic acid 18.5%；
Solid polyamide 22.5%；
Polyester resin 18.8%；
Chlorinated polypropylene 10.2%；
Organic pigment or inorganic pigment 30%.
Organic pigment color be red, yellow, blue in it is any, inorganic pigment color be black.
Organic pigment is quinacridone, dioxazines, anthraquinone, indigoids, any or several mixing in phthalocyanine；Inorganic face Expect for any or several mixing in titanium dioxide, silicate, phosphate, hydroxide, sulfide, iron oxide.
It puts oleoresin into blender to carry out being uniformly mixed stirring, temperature polymerize in 125-130 DEG C of resin softening point Reaction, pressure is in 8hPa hereinafter, 500 ~ 800r/min of mixing speed；Organic pigment or nothing are added after being stirred to react 3-4 hours Machine pigment, temperature control is in resin softening point, after being kept stirring speed continuation 10 ~ 20min of uniform stirring；The above mixture is thrown Enter after mediating 10 ~ 20min to kneader, then by discharging after the dispersion of high-speed flow milling apparatus；It is overpressurized, stirred, mixed, pinched It closes, oily solid soluble ink again is made after crushing.
Embodiment two
Oleoresin matches as follows:
Solid propenoic acid 12.8%；
Solid polyamide 17.3%；
Polyester resin 9.8%；
Chlorinated polypropylene 10.1%；
Titanium dioxide 50%.
Inorganic pigment is titanium dioxide.
It puts oleoresin into blender to carry out being uniformly mixed stirring, temperature polymerize in 125-130 DEG C of resin softening point Reaction, pressure is in 8hPa hereinafter, 500 ~ 800r/min of mixing speed；Organic pigment or nothing are added after being stirred to react 3-4 hours Machine pigment, temperature control is in resin softening point, after being kept stirring speed continuation 10 ~ 20min of uniform stirring；The above mixture is thrown Enter after mediating 10 ~ 20min to kneader, then by discharging after the dispersion of high-speed flow milling apparatus；It is overpressurized, stirred, mixed, pinched It closes, oily solid soluble ink again is made after crushing.
Above-described embodiment and non-limiting product form and style of the invention, the ordinary skill people of any technical field The appropriate changes or modifications that member does it, all should be regarded as not departing from patent category of the invention.

Claims (4)

1. a kind of oily solid soluble ink again, it is characterised in that: the oily solid again soluble ink include oleoresin and Organic pigment or inorganic pigment, composition of raw materials are as follows:
A, the composition of raw materials degree of oleoresin is 70%, is specifically formed by following degree:
Solid propenoic acid 15-25%；
Solid polyamide 20-30%；
Polyester resin 10-20%；
Chlorinated polypropylene 10-25%；
B, the composition of raw materials degree of organic pigment or inorganic pigment is 30%.
2. a kind of oily solid according to claim 1 soluble ink again, it is characterised in that: the organic pigment color is Red, yellow, blue in it is any, the inorganic pigment color be black.
3. a kind of oily solid according to claim 1 soluble ink again, it is characterised in that: the organic pigment is quinoline a word used for translation Pyridine ketone, dioxazines, anthraquinone, indigoids, any or several mixing in phthalocyanine；The inorganic pigment is titanium dioxide, silicic acid Salt, phosphate, hydroxide, sulfide, any or several mixing in iron oxide.
4. a kind of oily solid soluble ink processing technology again, it is characterised in that: by oleoresin put into blender into Row is uniformly mixed stirring, and temperature is in resin softening point polymerization reaction, and pressure is in 8hPa hereinafter, 500 ~ 800r/min of mixing speed； Be added organic pigment or inorganic pigment after being stirred to react 3-4 hours, temperature control in resin softening point, be kept stirring speed after After continuous 10 ~ 20min of uniform stirring；The above mixture is put into after kneader mediates 10 ~ 20min, then is ground by high-speed flow It discharges after equipment dispersion；Oily solid soluble ink again is made after being overpressurized, stirred, mixed, mediated, being crushed.
CN201811312756.4A 2018-11-06 2018-11-06 A kind of oily solid soluble ink and processing technology again Pending CN109370301A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201811312756.4A CN109370301A (en) 2018-11-06 2018-11-06 A kind of oily solid soluble ink and processing technology again

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201811312756.4A CN109370301A (en) 2018-11-06 2018-11-06 A kind of oily solid soluble ink and processing technology again

Publications (1)

Publication Number Publication Date
CN109370301A true CN109370301A (en) 2019-02-22

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CN201811312756.4A Pending CN109370301A (en) 2018-11-06 2018-11-06 A kind of oily solid soluble ink and processing technology again

Country Status (1)

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CN (1) CN109370301A (en)

Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN85101158A (en) * 1985-04-01 1987-01-10 佳能公司 The adhesive resin that the preparation toner is used contains the toner of this adhesive resin and their production method
CN1849563A (en) * 2003-09-18 2006-10-18 澳大利亚研究实验室持股有限公司 Marking liquid method of preparation and product produced thereby
CN102153911A (en) * 2010-02-11 2011-08-17 施乐公司 Process for preparing stable pigmented curable solid inks
CN102203679A (en) * 2008-10-30 2011-09-28 大日精化工业株式会社 Process for production of pigment/resin composition, coloring agent and coloring method
JP2012219145A (en) * 2011-04-06 2012-11-12 Dic Corp Method for producing aqueous pigment dispersion for inkjet recording, and aqueous ink for inkjet recording
CN103703081A (en) * 2011-07-22 2014-04-02 大日精化工业株式会社 Greenish blue pigment, colorant composition containing the pigment, and image recording material
CN103814089A (en) * 2011-08-30 2014-05-21 富士胶片株式会社 Novel compound having triazine side chain, colored composition, inkjet ink, inkjet recording method, color filter, and color toner
CN106170519A (en) * 2014-09-26 2016-11-30 Ga化学私人有限公司 Black ink composition
JP2017114926A (en) * 2015-12-21 2017-06-29 Dic株式会社 Manufacturing method of aqueous pigment dispersion
CN107783390A (en) * 2016-08-25 2018-03-09 佳能株式会社 Toner

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN85101158A (en) * 1985-04-01 1987-01-10 佳能公司 The adhesive resin that the preparation toner is used contains the toner of this adhesive resin and their production method
CN1849563A (en) * 2003-09-18 2006-10-18 澳大利亚研究实验室持股有限公司 Marking liquid method of preparation and product produced thereby
CN102203679A (en) * 2008-10-30 2011-09-28 大日精化工业株式会社 Process for production of pigment/resin composition, coloring agent and coloring method
CN102153911A (en) * 2010-02-11 2011-08-17 施乐公司 Process for preparing stable pigmented curable solid inks
JP2012219145A (en) * 2011-04-06 2012-11-12 Dic Corp Method for producing aqueous pigment dispersion for inkjet recording, and aqueous ink for inkjet recording
CN103703081A (en) * 2011-07-22 2014-04-02 大日精化工业株式会社 Greenish blue pigment, colorant composition containing the pigment, and image recording material
CN103814089A (en) * 2011-08-30 2014-05-21 富士胶片株式会社 Novel compound having triazine side chain, colored composition, inkjet ink, inkjet recording method, color filter, and color toner
CN106170519A (en) * 2014-09-26 2016-11-30 Ga化学私人有限公司 Black ink composition
JP2017114926A (en) * 2015-12-21 2017-06-29 Dic株式会社 Manufacturing method of aqueous pigment dispersion
CN107783390A (en) * 2016-08-25 2018-03-09 佳能株式会社 Toner

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
董炎明等: "《高分子结构与性能》", 31 January 2010, 华东理工大学出版社 *

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Application publication date: 20190222

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