CN109364856A - A kind of catalyst manufacturing equipment and method - Google Patents
A kind of catalyst manufacturing equipment and method Download PDFInfo
- Publication number
- CN109364856A CN109364856A CN201811396310.4A CN201811396310A CN109364856A CN 109364856 A CN109364856 A CN 109364856A CN 201811396310 A CN201811396310 A CN 201811396310A CN 109364856 A CN109364856 A CN 109364856A
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- Prior art keywords
- solid
- chamber
- liquid
- feeding chamber
- feed pipe
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
Abstract
The invention discloses a kind of catalyst manufacturing equipment and methods, including mixing chamber, the mixing chamber side is equipped with solid feeding chamber and the other side is equipped with liquid feeding chamber, the mixing chamber one side, which runs through to run through equipped with solid feed pipe and another side, is equipped with liquid feed pipe, the solid feed pipe and liquid feeding tube end are equipped with spray head, through equipped with air inlet pipe on the solid feeding chamber and liquid feeding chamber side wall, the air inlet pipe is equipped with blower, and the air inlet tube end is equipped with the first inert gas storage tank.The present invention can reduce the material residual in the intracavitary portion of solid feeding in the case where not influencing reaction result, avoid the waste of material, make liquid material and solid material that there is great contact area simultaneously, to accelerate its reaction rate, and it is more uniform to mix solid material and liquid material in reaction, design is reasonable, practicability with higher.
Description
Technical field
The present invention relates to organic synthesis novel catalyst technologies field, in particular to a kind of catalyst manufacturing equipment and side
Method.
Background technique
In the production preparation process of organic synthesis new catalyst, solid material and liquid material are generally comprised, no
With phase material in mixing with different fluid properties, therefore admixture is complicated, this results in producing in catalyst
It is easy to appear the situation that the mixing of solid material liquid material is uneven and reaction rate is slower in the process to occur, mixing is uneven
It will have a direct impact on the production efficiency and yields of organic synthesis new catalyst.
Therefore, it invents a kind of catalyst manufacturing equipment and method is necessary to solve the above problems.
Summary of the invention
The purpose of the present invention is to provide a kind of catalyst manufacturing equipment and methods, by utilizing the first inert gas storage
Inert gas in tank drives the pulverulent solids material in the intracavitary portion of solid feeding to enter mixing chamber and utilizes two opposite sprays
Head respectively sprays liquid material and powdered solid material, in order to reduce in the case where not influencing reaction result
The material in the intracavitary portion of solid feeding remains, and avoids the waste of material, while it is great that liquid material and solid material are had
Contact area, to accelerate its reaction rate, and it is more uniform to mix solid material and liquid material in reaction, design is closed
Reason, practicability with higher, to solve the problems mentioned in the above background technology.
To achieve the above object, the invention provides the following technical scheme: a kind of catalyst manufacturing equipment, including mixing chamber,
The mixing chamber side is equipped with solid feeding chamber and the other side is equipped with liquid feeding chamber, and the mixing chamber one side, which runs through, to be equipped with
Solid feed pipe and another side, which are run through, is equipped with liquid feed pipe, and the solid feed pipe is equipped with liquid feeding tube end
Through air inlet pipe is equipped on spray head, the solid feeding chamber and liquid feeding chamber side wall, the air inlet pipe is equipped with blower, institute
Air inlet tube end is stated equipped with the first inert gas storage tank, the solid feeding chamber intracavity bottom is equipped with the second bull stick and bottom
It is fixed with the second motor, second bull stick is equipped with crushing knife tool.
Preferably, the mixing chamber intracavity bottom is equipped with the first bull stick and bottom and is fixed with first motor, and described the
One bull stick side is equipped with cross bar, is fixed with agitating plate on the outside of the cross bar.
Preferably, first bull stick through mixing chamber intracavity bottom and extends to mixing chamber outside and first motor transmission
Connection.
Preferably, the mixing chamber, solid feeding chamber and liquid feeding top of chamber are equipped with top cover, the mixing chamber top
Through gas recovery pipe is equipped on top cover, the gas recovery pipe is equipped with valve.
Preferably, the gas recovery pipe end is equipped with gas separation equipment, and the gas separation equipment is equipped with gas transmission
Pipe, the connecting pin of the appendix is respectively equipped with waste gas treatment equipment and the second inert gas storage tank.
A kind of catalyst manufacturing method, further comprising the steps of including the catalyst manufacturing equipment:
S1: opening the top cover of solid feeding top of chamber, and solid material is added in solid feeding chamber；
S2: and then drive the crushing knife tool on the second bull stick to rotate using the second motor, by solid material grind into powder
Shape；
S3: and then liquid material is added in liquid feeding chamber；
S4: the rare gas in the first inert gas storage tank is sent into solid by air inlet pipe and sent by starting blower, blower
Expect in chamber and liquid feeding chamber, rare gas enters in solid feed pipe jointly after mixing with solid material powder and sent by solid
The spray head of expects pipe end is in that divergent shape sprays upwards, the intracavitary portion's liquid material of the liquid feeding then pressure as caused by rare gas
Power enters liquid feed pipe, and then the spray head of liquid feeding tube end sprays downwards；
S5: and then contact with each other between liquid material and powdered two spray heads of solid material and send reaction, it reacts
Mixture afterwards falls into mixing chamber bottom, while driving the agitating plate on the first bull stick to rotate using first motor, to mixture
It is stirred.
Technical effect and advantage of the invention:
1, the present invention passes through the powder using the inert gas drive intracavitary portion of solid feeding in the first inert gas storage tank
Last shape solid material is entered mixing chamber and is respectively sprayed liquid material and powdered solid material using two opposite spray heads
Out, in order to which the material that can reduce the intracavitary portion of solid feeding in the case where not influencing reaction result remains, material is avoided
Waste, while making liquid material and solid material that there is great contact area, to accelerate its reaction rate, and make solid-state
Material and liquid material mixed in reaction it is more uniform, design rationally, practicability with higher；
2, by being equipped with gas separation equipment, in order to the tail gas for being generated reaction using gas separation equipment and enter mixed
Expect that the rare gas in intracavitary portion is collected and is separated, to carry out repeated collection utilization to rare gas, reduces
Reaction end gas can also be handled using waste gas treatment equipment while reaction cost, avoid direct emission pollution atmosphere
It happens.
Detailed description of the invention
Fig. 1 is overall structure diagram of the invention.
Fig. 2 is mixing chamber schematic diagram of internal structure of the invention.
Fig. 3 is gas separation equipment structural schematic diagram of the invention.
In figure: 1 mixing chamber, 2 solid feeding chambers, 3 liquid feeding chambers, 4 solid feed pipes, 5 liquid feed pipes, 6 spray heads, 7
First bull stick, 8 first motors, 9 cross bars, 10 agitating plates, 11 top covers, 12 gas recovery pipes, 13 valves, 14 gas separation equipments,
15 appendixs, 16 waste gas treatment equipments, 17 second inert gas storage tanks, 18 second bull sticks, 19 crushing knife tools, 20 second electricity
Machine, 21 air inlet pipe, 22 blowers, 23 first inert gas storage tanks.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other
Embodiment shall fall within the protection scope of the present invention.
Embodiment 1
The present invention provides a kind of catalyst manufacturing equipment as shown in Figs. 1-3, including mixing chamber 1, the mixing chambers 1 one
Side is equipped with solid feeding chamber 2 and the other side is equipped with liquid feeding chamber 3, and 1 one side of mixing chamber, which runs through, is equipped with solid feeding
Pipe 4 and another side, which are run through, is equipped with liquid feed pipe 5, and the solid feed pipe 4 is equipped with spray head with 5 end of liquid feed pipe
6, through air inlet pipe 21 is equipped on 3 side wall of the solid feeding chamber 2 and liquid feeding chamber, the air inlet pipe 21 is equipped with blower
22,21 end of air inlet pipe is equipped with the first inert gas storage tank 23.
Further, in the above-mentioned technical solutions, 1 intracavity bottom of mixing chamber is equipped with the first bull stick 7 and bottom is solid
Surely it is equipped with first motor 8,7 side of the first bull stick is equipped with cross bar 9, is fixed with agitating plate 10 on the outside of the cross bar 9.
Further, in the above-mentioned technical solutions, first bull stick 7 through 1 intracavity bottom of mixing chamber and extends to mixed
Expect that 1 outside of chamber is sequentially connected with first motor 8, in order to which first motor 8 drives the agitating plate 10 on the first bull stick 7 to rotate, from
And mixture is stirred, accelerate reaction rate again.
Further, in the above-mentioned technical solutions, the mixing chamber 1, solid feeding chamber 2 and 3 top of liquid feeding chamber are equal
Equipped with top cover 11, through gas recovery pipe 12 is equipped on 1 top header 11 of mixing chamber, the gas recovery pipe 12 is equipped with
Valve 13.
Further, in the above-mentioned technical solutions, 12 end of gas recovery pipe is equipped with gas separation equipment 14, described
Gas separation equipment 14 is equipped with appendix 15, and the connecting pin of the appendix 15 is respectively equipped with waste gas treatment equipment 16 and second
Inert gas storage tank 17.
Further, in the above-mentioned technical solutions, 2 intracavity bottom of solid feeding chamber is equipped with the second bull stick 18 and bottom
Portion is fixed with the second motor 20, and second bull stick 18 is equipped with crushing knife tool 19, in order to which the second motor 20 drives second
Crushing knife tool 19 on bull stick 18 rotates, so that solid material is ground into powder.
Working method of the present invention:
Referring to Figure of description 1 and attached drawing 2, the top cover 11 at 2 top of solid feeding chamber is opened, solid is added in solid material
In feeding chamber 2, then the crushing knife tool 19 on the second bull stick 18 is driven to rotate using the second motor 20, so that solid material be ground
It clays into power shape, then liquid material is added in liquid feeding chamber 3, start blower 22, blower 22 is by air inlet pipe 21 by the
Rare gas in one inert gas storage tank 23 is sent into solid feeding chamber 2 and liquid feeding chamber 3, rare gas and solid
Enter jointly in solid feed pipe 4 after the mixing of feed powder end and sprayed upwards in divergent shape by the spray head 6 of 4 end of solid feed pipe,
Then the pressure as caused by rare gas enters liquid feed pipe 5 to 3 interior liquid material of liquid feeding chamber, then liquid feeding
The spray head 6 of 5 end of pipe sprays downwards, then contacts with each other simultaneously between liquid material and powdered two spray heads 6 of solid material
Reaction is sent, the mixture after reaction falls into 1 bottom of mixing chamber, while driving the stirring on the first bull stick 7 using first motor 8
Plate 10 rotates, to be stirred to mixture, accelerates reaction rate again, the present invention is by utilizing the first inert gas storage
The pulverulent solids material inside inert gas drive solid feeding chamber 2 in tank 23 enters mixing chamber 1 and utilization two opposite
Spray head 6 liquid material and powdered solid material are sprayed respectively, in order to can be the case where not influencing reaction result
The lower material residual reduced inside solid feeding chamber 2, avoids the waste of material, while liquid material and solid material are had
Great contact area to accelerate its reaction rate, while keeping the mixing in reaction of solid material and liquid material more equal
Even, design is reasonable, practicability with higher；
Referring to Figure of description 3, by being equipped with gas separation equipment 14, in order to be reacted using gas separation equipment 14
The tail gas of generation and the rare gas entered inside mixing chamber 1 are collected and are separated, thus to rare gas into
Row repeated collection utilizes, and can also be handled using waste gas treatment equipment 16 reaction end gas while reducing reaction cost,
The case where avoiding direct emission from polluting atmosphere generation.
Embodiment 2
A kind of catalyst manufacturing method, further comprising the steps of including the catalyst manufacturing equipment:
S1: the top cover 11 at 2 top of solid feeding chamber is opened, solid material is added in solid feeding chamber 2；
S2: and then drive the crushing knife tool 19 on the second bull stick 18 to rotate using the second motor 20, solid material is ground
At powdered；
S3: and then liquid material is added in liquid feeding chamber 3；
S4: starting blower 22, blower 22 are sent the rare gas in the first inert gas storage tank 23 by air inlet pipe 21
Enter in solid feeding chamber 2 and liquid feeding chamber 3, rare gas enters solid feed pipe 4 after mixing with solid material powder jointly
In and by the spray head 6 of 4 end of solid feed pipe upwards in divergent shape spray, 3 interior liquid material of liquid feeding chamber is then due to dilute
There is pressure caused by gas to enter liquid feed pipe 5, then the spray head 6 of 5 end of liquid feed pipe sprays downwards；
S5: and then contact with each other between liquid material and powdered two spray heads 6 of solid material and send reaction, it reacts
Mixture afterwards falls into 1 bottom of mixing chamber, while driving the agitating plate 10 on the first bull stick 7 to rotate using first motor 8, to mixed
Object is closed to be stirred.
Finally, it should be noted that the foregoing is only a preferred embodiment of the present invention, it is not intended to restrict the invention,
Although the present invention is described in detail referring to the foregoing embodiments, for those skilled in the art, still may be used
To modify the technical solutions described in the foregoing embodiments or equivalent replacement of some of the technical features,
All within the spirits and principles of the present invention, any modification, equivalent replacement, improvement and so on should be included in of the invention
Within protection scope.
Claims (6)
1. a kind of catalyst manufacturing equipment, including mixing chamber (1), it is characterised in that: sent equipped with solid mixing chamber (1) side
Expect that chamber (2) and the other side are equipped with liquid feeding chamber (3), mixing chamber (1) one side run through be equipped with solid feed pipe (4) with
And another side is run through equipped with liquid feed pipe (5), the solid feed pipe (4) and liquid feed pipe (5) end are equipped with spray
Head (6), through equipped with air inlet pipe (21), the air inlet pipe on the solid feeding chamber (2) and liquid feeding chamber (3) side wall
(21) blower (22) are equipped with, air inlet pipe (21) end is equipped with the first inert gas storage tank (23), the solid feeding
Chamber (2) intracavity bottom is equipped with the second bull stick (18) and bottom is fixed with the second motor (20), on second bull stick (18)
Equipped with crushing knife tool (19).
2. a kind of catalyst manufacturing equipment according to claim 1, it is characterised in that: mixing chamber (1) intracavity bottom
It is fixed with first motor (8) equipped with the first bull stick (7) and bottom, the first bull stick (7) side is equipped with cross bar (9), institute
It states and is fixed with agitating plate (10) on the outside of cross bar (9).
3. a kind of catalyst manufacturing equipment according to claim 2, it is characterised in that: first bull stick (7) is through mixed
Material chamber (1) intracavity bottom simultaneously extends to mixing chamber (1) outside and first motor (8) transmission connection.
4. a kind of catalyst manufacturing equipment according to claim 1, it is characterised in that: the mixing chamber (1), solid feeding
It is equipped with top cover (11) at the top of chamber (2) and liquid feeding chamber (3), through equipped with gas on mixing chamber (1) top header (11)
Body recovery tube (12), the gas recovery pipe (12) are equipped with valve (13).
5. a kind of catalyst manufacturing equipment according to claim 4, it is characterised in that: gas recovery pipe (12) end
Equipped with gas separation equipment (14), the gas separation equipment (14) is equipped with appendix (15), the company of the appendix (15)
It connects end and is respectively equipped with waste gas treatment equipment (16) and the second inert gas storage tank (17).
6. a kind of catalyst manufacturing method, which is characterized in that including catalyst manufacturing equipment as described in claim 1, also wrap
Include following steps:
S1: opening the top cover (11) at the top of solid feeding chamber (2), and solid material is added in solid feeding chamber (2)；
S2: and then drive the crushing knife tool (19) on the second bull stick (18) to rotate using the second motor (20), solid material is ground
It clays into power shape；
S3: and then liquid material is added in liquid feeding chamber (3)；
S4: starting blower (22), blower (22) pass through air inlet pipe (21) for the rare gas in the first inert gas storage tank (23)
Body is sent into solid feeding chamber (2) and liquid feeding chamber (3), and rare gas enters solid after mixing with solid material powder jointly
It is sprayed upwards in divergent shape in feed pipe (4) and by the spray head (6) of solid feed pipe (4) end, the internal liquid of liquid feeding chamber (3)
Then the pressure as caused by rare gas enters liquid feed pipe (5) to state material, then the spray head of liquid feed pipe (5) end
(6) it sprays downwards；
S5: and then contact with each other between liquid material and powdered two spray heads (6) of solid material and send reaction, after reaction
Mixture fall into mixing chamber (1) bottom, while driving the agitating plate (10) on the first bull stick (7) to revolve using first motor (8)
Turn, mixture is stirred.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811396310.4A CN109364856A (en) | 2018-11-22 | 2018-11-22 | A kind of catalyst manufacturing equipment and method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811396310.4A CN109364856A (en) | 2018-11-22 | 2018-11-22 | A kind of catalyst manufacturing equipment and method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109364856A true CN109364856A (en) | 2019-02-22 |
Family
ID=65377358
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811396310.4A Withdrawn CN109364856A (en) | 2018-11-22 | 2018-11-22 | A kind of catalyst manufacturing equipment and method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109364856A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20160074854A1 (en) * | 2013-04-19 | 2016-03-17 | Thyssenkrupp Industrial Solutions Ag | Method and device for producing shell catalysts |
| CN206008568U (en) * | 2016-08-23 | 2017-03-15 | 北京科林索尔环境修复有限责任公司 | A kind of chemical material dissolution equipment with solid material breaker |
| CN106693596A (en) * | 2016-12-29 | 2017-05-24 | 成都国珈星际固态锂电科技有限公司 | Inert gas recovery system and method |
| CN207906862U (en) * | 2018-02-09 | 2018-09-25 | 长乐力恒锦纶科技有限公司 | A kind of material pressing device of titania slurry |
-
2018
- 2018-11-22 CN CN201811396310.4A patent/CN109364856A/en not_active Withdrawn
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20160074854A1 (en) * | 2013-04-19 | 2016-03-17 | Thyssenkrupp Industrial Solutions Ag | Method and device for producing shell catalysts |
| CN206008568U (en) * | 2016-08-23 | 2017-03-15 | 北京科林索尔环境修复有限责任公司 | A kind of chemical material dissolution equipment with solid material breaker |
| CN106693596A (en) * | 2016-12-29 | 2017-05-24 | 成都国珈星际固态锂电科技有限公司 | Inert gas recovery system and method |
| CN207906862U (en) * | 2018-02-09 | 2018-09-25 | 长乐力恒锦纶科技有限公司 | A kind of material pressing device of titania slurry |
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| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20190222 |
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| WW01 | Invention patent application withdrawn after publication |