CN109364693A - One kind is for recyclable device associated with organic solvent condensate and adsorption desorption - Google Patents
One kind is for recyclable device associated with organic solvent condensate and adsorption desorption Download PDFInfo
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- CN109364693A CN109364693A CN201811358454.0A CN201811358454A CN109364693A CN 109364693 A CN109364693 A CN 109364693A CN 201811358454 A CN201811358454 A CN 201811358454A CN 109364693 A CN109364693 A CN 109364693A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
- B01D53/06—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with moving adsorbents, e.g. rotating beds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
- B01D5/0057—Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/002—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by condensation
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Analytical Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Separation Of Gases By Adsorption (AREA)
- Treating Waste Gases (AREA)
Abstract
The invention discloses one kind for recyclable device associated with organic solvent condensate and adsorption desorption, is related to Technologies for Recovery of Organic Solvents field.The present invention includes adsorption desorption case and cooling cylinder；Adsorption desorption case includes adsorption chamber and desorption chamber；Adsorption chamber and the inner wall of desorption chamber are mounted with support rod；Two support rod one end are rotatably connected to drive roll；Two support rod other ends are rotatably connected to driven voller；Two support rod medial surface uniform arrays have connection rod；Several connection rods are between drive roll and driven voller；Pass through absorption V belt translation connection between drive roll and driven voller；One surface of support rod is fixed with fixed frame；One surface of fixed frame is fixed with motor；Absorption chamber lower surface offers the first air inlet；First air inlet entrance is fixed with filter screen；First air inlet is fixedly connected with rapid steamer by pipeline.The present invention recycles carry out adsorption desorption back and forth by adsorption desorption integral structure and absorption band, keeps the organic solvent purity extracted higher, effect is more preferable.
Description
Technical field
The invention belongs to Technologies for Recovery of Organic Solvents fields, are used for organic solvent condensate and adsorption desorption more particularly to one kind
Associated with recyclable device.
Background technique
In chemical production process, organic solvent is frequently used for the processes such as the dissolution, purification, purification of chemical products,
And be directly discharged in air in vacuum drying, vacuum distillation, plasticizing forming and suction filtration process, cause serious bad border dirty
Dye and the wasting of resources, while also increasing security risk.With the rapid development of China's chemical industry, the usage amount of organic solvent
The trend increased year by year is just presented, therefore, the research to organic solvent recovery device improves recovery efficiency, can be in chemical industry row
It is applied in industry production, there is wide practical value.
The method of recycling organic solvent mainly has condensation method, absorption process and membrane separation process at present；Wherein condensation method and absorption
For method due to easy to operate, equipment and technology is of less demanding, so that the two methods application is wider.The present invention passes through condensation and adsorption desorption
Associated with technology, expand organic solvent recycling the technical field scope of application；And be utilized adsorption desorption follows bad structure repeatedly,
It improves the rate of recovery of organic solvent and reduces the energy consumption of recovery system.
Summary of the invention
The purpose of the present invention is to provide one kind for recyclable device associated with organic solvent condensate and adsorption desorption, passes through suction
Desorption case and absorption band follow bad structure repeatedly, solve that existing organic solvent recovery device is single and recovery efficiency is not high asks
Topic.
In order to solve the above technical problems, the present invention is achieved by the following technical solutions:
The present invention is a kind of for recyclable device associated with organic solvent condensate and adsorption desorption, including adsorption desorption case and condensation
Case:
The adsorption desorption case includes adsorption chamber and desorption chamber；The adsorption chamber and the inner wall of desorption chamber are mounted with support
Bar；Two described support rod one end are rotatably connected to drive roll；Two support rod other ends are rotatably connected to driven voller；Two
A support rod medial surface uniform array has connection rod；Several connection rods are between drive roll and driven voller；It is described
Pass through absorption V belt translation connection between drive roll and driven voller；One surface of support rod is fixed with fixed frame；The fixed frame
One surface is fixed with motor；The adsorption desorption case keeps the structure of adsorption desorption case more compact by the structure that adsorption desorption is integrated；
The bad adsorption structure that follows of the absorption band makes the purification of organic solvent higher.
The absorption chamber lower surface offers the first air inlet；The first air inlet entrance is fixed with filtering
Net；First air inlet is fixedly connected with rapid steamer by pipeline；Spiral evaporation tube is fixed with inside the rapid steamer；Institute
The upper surface for stating adsorption chamber offers the first gas outlet；The filter screen can effectively filter dust, drop in organic exhaust gas
Impurity；The spiral evaporation tube can reinforce the heating effect of rapid steamer.The nitrogen making machine, which generates nitrogen and will be desorbed, indoor to be had
Machine gas is taken out of.
The inner wall of the desorption chamber is fixed with nitrogen making machine；The medial surface of the desorption chamber offers mounting hole；The installation
Microwave emitter is fixedly installed with inside hole；The nitrogen making machine generate nitrogen will be desorbed indoor organic gas take out of and nitrogen not
Condensation organic gas can be interfered.
The cooling cylinder one side offers the second air inlet；The another side of the cooling cylinder offers the second outlet
Mouthful；Fixed several U-typed condenser pipes inside the cooling cylinder；An air-cooler is fixed outside the cooling cylinder；The cooling cylinder
A plate is fixed in the inclination of bottom week side；The cooling cylinder inner surface offers discharge port；The discharge port is fixed by sebific duct
Connect a narrow-mouthed bottle；The U-typed condenser pipe and cold wind function effectively accelerate cooling efficiency fast-refrigerating；The oblique plate
Setting be in order to which organic gas condensing is at can smoothly flow to narrow-mouthed bottle after organic solvent.
Further, the motor is fixedly connected by fixed frame with support rod；The motor lower surface is fixedly mounted one
A pedestal；Output shaft one end of the motor is fixed with driving wheel by shaft coupling；Described support rod one end is mounted with axis
It holds；The bearing is fixed with driven wheel；The driving wheel and driven wheel are sequentially connected by belt；The driven wheel and drive roll
It is fixedly connected.The transmission connection of the driving wheel and driven wheel is applied to motor on drive roll；The drive roll and driven voller
Transmission connection drive the movement of absorption band so that absorption band follows bad absorption.
Further, the absorption band is that protective layer and absorptive media layers are combined；The absorption band protective layer uses
Glass fiber filter cloth or polytetrafluoroethylene (PTFE)；The absorption band absorptive media layers are by active carbon fiber felt, active carbon cotton, seed activity
One or both of charcoal, sieve particle or two or more compositions；The active carbon fiber felt, active carbon cotton, seed activity
Charcoal, sieve particle can preferably play the role of absorbing organic solvent.
The invention has the following advantages:
The present invention follows bad adsorption desorption structure by absorption band, so that the organic solvent purity extracted is higher, efficiency is more preferable；
Adsorption desorption case keeps its structure more compact by the structure that adsorption desorption is integrated, easy to use；The generation nitrogen of nitrogen making machine will take off
Attached indoor organic gas is taken out of, and nitrogen not will do it condensation interference, voluntarily flow out from the second gas outlet.
Certainly, it implements any of the products of the present invention and does not necessarily require achieving all the advantages described above at the same time.
Detailed description of the invention
In order to illustrate the technical solution of the embodiments of the present invention more clearly, will be described below to embodiment required
Attached drawing is briefly described, it should be apparent that, drawings in the following description are only some embodiments of the invention, for ability
For the those of ordinary skill of domain, without creative efforts, it can also be obtained according to these attached drawings other attached
Figure.
Fig. 1 is the operation schematic diagram that organic solvent condensate and adsorption desorption are combined recyclable device；
Fig. 2 is the structural schematic diagram for adsorbing band；
Fig. 3 is the schematic diagram of internal structure for adsorbing band；
Fig. 4 is the structural schematic diagram of motor；
In attached drawing, parts list represented by the reference numerals are as follows:
1- adsorption desorption case, 2- cooling cylinder, 3- motor, 4- evaporator, 5- microwave emitter, 101- adsorption chamber, 102- desorption
Room, 103- support rod, 104- drive roll, 105- driven voller, 106- connection rod, 107- adsorb band, 108- fixed frame, 109- first
Air inlet, 110- filter screen, the first gas outlet 111-, 112- nitrogen making machine, the second air inlet of 201-, the second gas outlet 202-,
203- U-typed condenser pipe, 204- air-cooler, 205- plate, 206- discharge port, 301- pedestal, 302- shaft coupling, 303- is actively
Wheel, 304- bearing, 305- driven wheel, 306- belt, the spiral evaporation tube of 401-, 501- waveguide, 502- magnetron.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts all other
Embodiment shall fall within the protection scope of the present invention.
It please refers to shown in Fig. 1-4, the present invention is a kind of for recyclable device associated with organic solvent condensate and adsorption desorption, packet
Include adsorption desorption case 1 and cooling cylinder 2；Adsorption desorption case 1 includes adsorption chamber 101 and desorption chamber 102；Adsorption chamber 101 and desorption chamber it is interior
Wall is mounted with support rod 103；Two 103 one end of support rod are rotatably connected to drive roll 104；Two support rods 103 are another
End is rotatably connected to driven voller 105；Two 103 medial surface uniform arrays of support rod have connection rod 106；18 connection 106, rod
Between drive roll 104 and driven voller 105；It is sequentially connected between drive roll 104 and driven voller 105 by absorption band 107；Support
103 1 surface of bar is fixed with fixed frame 108；108 1 surface of fixed frame is fixed with motor 3；101 lower surface of adsorption chamber offers
One air inlet 109；First air inlet, 109 entrance is fixed with filter screen 110；First air inlet 109 is fixedly connected by pipeline
There is rapid steamer 4；Spiral evaporation tube 401 is fixed with inside rapid steamer 4；The upper surface of adsorption chamber 101 offers the first gas outlet
111；The inner wall of desorption chamber 102 is fixed with nitrogen making machine 112；The medial surface of desorption chamber 102 offers mounting hole 113；Mounting hole 113
Inside is fixedly installed with microwave emitter 5；2 one side of cooling cylinder offers the second air inlet 201；The another side of cooling cylinder 2
Offer the second gas outlet 202；U-typed condenser pipe 203 is fixed inside cooling cylinder 2；An air-cooler is fixed outside condenser pipe 2
204；A plate 205 is fixed in the inclination of 2 bottom week side of cooling cylinder；2 inner surface of cooling cylinder offers discharge port 206；Discharge port 206
A narrow-mouthed bottle 207 is fixedly connected with by sebific duct.
Wherein as shown in figure 4, motor 3 is fixedly connected by fixed frame 108 with support rod 103；The fixed peace in 3 lower surface of motor
Fill a pedestal 301；Output shaft one end of motor 3 is fixed with driving wheel 303 by shaft coupling 302；The installation of 103 one end of support rod
It is fixed with bearing 304；Bearing 304 is fixed with driven wheel 305；Driving wheel 303 is sequentially connected with driven wheel 305 by belt 306；
Driven wheel 305 is fixedly connected with drive roll 104.
Wherein as shown in fig. 2, absorption band 107 is that protective layer and absorptive media layers are combined；Absorption 101 protective layer of band is adopted
With glass fiber filter cloth or polytetrafluoroethylene (PTFE)；101 absorptive media layers of band are adsorbed by active carbon fiber felt, active carbon cotton, seed activity
Composition described above in one or both of charcoal, sieve particle or two.
One concrete application of the present embodiment are as follows: organic solvent becomes organic gas by the high temperature evaporation of evaporator, has
Machine gas enters adsorption chamber by filter screen filtration from the first air inlet, and motor, which is opened, drives absorption band rotation, organic gas quilt
It is adsorbed on absorption to take into desorption chamber, remaining foreign gas is flowed out from the first gas outlet；Indoor microwave emitter is desorbed
Microwave being generated organic gas is desorbed, nitrogen making machine generates nitrogen and organic gas is driven to enter cooling cylinder from the second air inlet,
Organic gas after adsorption desorption, which is dropped on plate by the condensation liquefaction of condenser pipe at organic solvent, to be flowed into narrow-mouthed bottle, cold
Remaining nitrogen is discharged from the second gas outlet in solidifying case.
In the description of this specification, the description of reference term " one embodiment ", " example ", " specific example " etc. means
Particular features, structures, materials, or characteristics described in conjunction with this embodiment or example are contained at least one implementation of the invention
In example or example.In the present specification, schematic expression of the above terms may not refer to the same embodiment or example.
Moreover, particular features, structures, materials, or characteristics described can be in any one or more of the embodiments or examples to close
Suitable mode combines.
Present invention disclosed above preferred embodiment is only intended to help to illustrate the present invention.There is no detailed for preferred embodiment
All details are described, are not limited the invention to the specific embodiments described.Obviously, according to the content of this specification,
It can make many modifications and variations.These embodiments are chosen and specifically described to this specification, is in order to better explain the present invention
Principle and practical application, so that skilled artisan be enable to better understand and utilize the present invention.The present invention is only
It is limited by claims and its full scope and equivalent.
Claims (3)
1. one kind is for recyclable device associated with organic solvent condensate and adsorption desorption, it is characterised in that: including adsorption desorption case (1) and
Cooling cylinder (2)；
The adsorption desorption case (1) includes adsorption chamber (101) and desorption chamber (102)；The inner wall of adsorption chamber (101) and desorption chamber
It is mounted with support rod (103)；Two described support rod (103) one end are rotatably connected to drive roll (104)；Two branch
Strut (103) other end is rotatably connected to driven voller (105)；Two support rod (103) medial surface uniform arrays have connection
Rod (106)；Several connection rods (106) are located between drive roll (104) and driven voller (105)；The drive roll (104) with
It is sequentially connected between driven voller (105) by absorption band (107)；(103) one surface of support rod is fixed with fixed frame
(108)；(108) one surface of fixed frame is fixed with motor (3)；
Adsorption chamber (101) lower surface offers the first air inlet (109)；First air inlet (109) entrance is fixed
There are filter screen (110)；First air inlet (109) is fixedly connected with rapid steamer (4) by pipeline；In the rapid steamer (4)
Portion is fixed with spiral evaporation tube (401)；The upper surface of the adsorption chamber (101) offers the first gas outlet (111)；
The inner wall of the desorption chamber (102) is fixed with nitrogen making machine (112)；The medial surface of the desorption chamber (102) offers installation
Hole (113)；Microwave emitter (5) are fixedly installed with inside the mounting hole (113)；
Cooling cylinder (2) one side offers the second air inlet (201)；The another side of the cooling cylinder (2) offers
Two gas outlets (202)；Fixed several U-typed condenser pipes (203) inside the cooling cylinder (2)；It is fixed outside the cooling cylinder (2)
One air-cooler (204)；A plate (205) are fixed in cooling cylinder (2) the bottom week side inclination；The interior table of the cooling cylinder (2)
Face offers discharge port (206)；The discharge port (206) is fixedly connected with a narrow-mouthed bottle (207) by sebific duct.
2. one kind according to claim 1 exists for recyclable device, feature associated with organic solvent condensate and adsorption desorption
In the motor (3) is fixedly connected by fixed frame (108) with support rod (103)；Motor (3) lower surface is fixedly mounted
One pedestal (301)；Output shaft one end of the motor (3) is fixed with driving wheel (303) by shaft coupling (302)；The branch
Strut (103) one end is mounted with bearing (304)；The bearing (304) is fixed with driven wheel (305)；The driving wheel
(303) it is sequentially connected with driven wheel (305) by belt (306)；The driven wheel (305) is fixedly connected with drive roll (104).
3. one kind according to claim 1 exists for recyclable device, feature associated with organic solvent condensate and adsorption desorption
In the absorption band (103) is that protective layer and absorptive media layers are combined；Absorption band (101) protective layer uses glass
Filter cloth or polytetrafluoroethylene (PTFE)；Absorption band (101) absorptive media layers are by active carbon fiber felt, active carbon cotton, seed activity
One or both of charcoal, sieve particle or two or more compositions.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811358454.0A CN109364693A (en) | 2018-11-15 | 2018-11-15 | One kind is for recyclable device associated with organic solvent condensate and adsorption desorption |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811358454.0A CN109364693A (en) | 2018-11-15 | 2018-11-15 | One kind is for recyclable device associated with organic solvent condensate and adsorption desorption |
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| Publication Number | Publication Date |
|---|---|
| CN109364693A true CN109364693A (en) | 2019-02-22 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811358454.0A Pending CN109364693A (en) | 2018-11-15 | 2018-11-15 | One kind is for recyclable device associated with organic solvent condensate and adsorption desorption |
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| Country | Link |
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| CN (1) | CN109364693A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110339713A (en) * | 2019-08-23 | 2019-10-18 | 崔小勤 | A kind of processing system and its treatment process of volatile organic matter |
| CN110931658A (en) * | 2019-11-14 | 2020-03-27 | Tcl华星光电技术有限公司 | Vacuum drying device |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5882381A (en) * | 1996-03-28 | 1999-03-16 | Modern Equipment Company, Inc. | Thermal desorption system |
| US20110056220A1 (en) * | 2009-06-08 | 2011-03-10 | Mario Caggiano | PH2OCP - portable water and climatic production system |
| CN104906919A (en) * | 2015-07-01 | 2015-09-16 | 北京华创朗润环境科技有限公司 | Belt type adsorption and microwave desorption organic waste gas purification method and device |
| CN204841355U (en) * | 2015-07-01 | 2015-12-09 | 北京华创朗润环境科技有限公司 | Microwave desorption organic waste gas purifier is adsorbed to belt |
| CN106422647A (en) * | 2016-11-15 | 2017-02-22 | 杭州捷瑞空气处理设备有限公司 | Low-liquidus-temperature organic waste gas recycling apparatus |
-
2018
- 2018-11-15 CN CN201811358454.0A patent/CN109364693A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5882381A (en) * | 1996-03-28 | 1999-03-16 | Modern Equipment Company, Inc. | Thermal desorption system |
| US20110056220A1 (en) * | 2009-06-08 | 2011-03-10 | Mario Caggiano | PH2OCP - portable water and climatic production system |
| CN104906919A (en) * | 2015-07-01 | 2015-09-16 | 北京华创朗润环境科技有限公司 | Belt type adsorption and microwave desorption organic waste gas purification method and device |
| CN204841355U (en) * | 2015-07-01 | 2015-12-09 | 北京华创朗润环境科技有限公司 | Microwave desorption organic waste gas purifier is adsorbed to belt |
| CN106422647A (en) * | 2016-11-15 | 2017-02-22 | 杭州捷瑞空气处理设备有限公司 | Low-liquidus-temperature organic waste gas recycling apparatus |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110339713A (en) * | 2019-08-23 | 2019-10-18 | 崔小勤 | A kind of processing system and its treatment process of volatile organic matter |
| CN110931658A (en) * | 2019-11-14 | 2020-03-27 | Tcl华星光电技术有限公司 | Vacuum drying device |
| CN110931658B (en) * | 2019-11-14 | 2022-02-22 | Tcl华星光电技术有限公司 | Vacuum drying device |
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Application publication date: 20190222 |
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