A kind of Mobile-phase reagent bottle
Technical field
The invention belongs to field of chemical equipment, more particularly, to a kind of Mobile-phase reagent bottle.
Background technique
The type of reagent bottle has wide-mouth, thin mouth;It is ground, a variety of without ground etc..Liquid chromatogram mobile phase reagent bottle is common
Have: U.S.'s Corning solvent bottle, Germany's Xiao Te solvent bottle.But existing Mobile-phase reagent bottle structure is simple, it has not been convenient to
Mobile-phase reagent is added during sample introduction, and opens mouth in adding procedure and is easy to fall into dust, volatilization mobile phase.For
This, we have proposed a kind of novel Mobile-phase reagent bottles to solve the above problems.
Summary of the invention
In view of this, the present invention is directed to propose a kind of Mobile-phase reagent bottle can be in sample to overcome the deficiencies of existing technologies
Mobile-phase reagent is added while sample introduction, can also reduce the falling into of dust, the volatilization of reagent in adding procedure to the greatest extent.
In order to achieve the above objectives, the technical scheme of the present invention is realized as follows:
A kind of Mobile-phase reagent bottle, it is characterised in that: including bottle body and bottle cap;
The bottle cap includes seal closure and filler cap;At least one inlet opening and at least one are equipped at the top of the seal closure
Air hole;Seal closure is detachably connected or is integrally formed in the upper end of filler cap;The lower end of the filler cap and bottle body are detachable
Connection;The filler cap includes the cone tank being provided at the top of it, and the taper trench bottom is integrally formed with one first diversion pipe;
First diversion pipe is connected to cone tank, and the first diversion pipe lower end extends in bottle body;The filler cap is equipped at least
One first through hole, all first through hole are respectively positioned in taper groove sidewall, and are mounted on outlet tube in all first through hole;Institute
There is outlet tube upper end to stretch out seal closure, lower end is removably connected with suction strainer head;Suction strainer head is located in bottle body, and can be from bottle body
Interior taking-up.
Further, the seal closure is equipped with several second through-holes, the quantity of the second through-hole and the quantity of first through hole
Quite, and position is corresponding;Outlet tube upper end passes through the top that the second corresponding through-hole extends to seal closure;First water conservancy diversion
Pipe, outlet tube are located at the intracorporal part of bottle and are vertically arranged with bottle body bottom;First diversion pipe lower end extends in bottle body
Close to the position of bottleneck;First diversion pipe lower end is equipped with one second diversion pipe, and the second water conservancy diversion bottom of the tube is away from bottle body bottom
Distance be 1-5mm.
Further, the second through-hole and the center line of first through hole are overlapped, and upper and lower position is corresponding;Inlet opening is located at funnel
The position far from the second through-hole is covered, upright projection is fallen on cone tank inner wall.
Further, a stopple, and stopple and the inlet opening or ventilative where it are mounted in inlet opening and air hole
Interporal lacuna connection;The material of stopple is polytetrafluoroethylene (PTFE).
Further, a stopple is installed, and stopple is connect with feed liquor interporal lacuna in inlet opening;The material of stopple is poly- four
Vinyl fluoride.
Further, being equipped at the top of air hole only allows the check valve that gas passes through in bottle body.
Further, the filler cap lower end is threadedly coupled with bottle body, and filler cap upper end detachably connects with seal closure upper end
The mode connect is to be threadedly coupled;The filler cap lower surface and the position of inlet opening face are equipped with filter screen.
Further, the filler cap includes a cylindrical body, is provided with the cone tank, bottom downwards at the top of the cylindrical body
It is provided with cylinder shape groove upwards;Cylinder shape groove inner surface is equipped with the internal screw thread for connecting with bottle body;Cylinder shape groove and
The top of one diversion pipe is concordant.
Further, the first diversion pipe, outlet tube are located at the intracorporal part of bottle and are vertically arranged with bottle body bottom;First leads
Distance of the flow tube away from bottle body bottom is 1-5mm;Suction strainer head is threadedly coupled or is connected together with outlet tube.
Further, the material of the bottle body is high-boron-silicon glass, and the material of bottle cap is polypropylene.
Compared with the existing technology, a kind of Mobile-phase reagent bottle of the present invention has the advantage that
(1) bottle cap of the Mobile-phase reagent bottle is made of filler cap and seal closure two parts, during sample introduction, even if stream
Dynamic phase reagent amount is inadequate, still can continue to add Mobile-phase reagent the case where not stopping liquid phase work, both be avoided that and added
Add Mobile-phase reagent to generate bubble in the process, and can guarantee that experiment smoothly carries out glibly.
(2) design of the Mobile-phase reagent bottle, before avoiding the drawbacks of open addition Mobile-phase reagent, funnelform bottle
It covers during adding mobile phase, reduces the falling into of dust, the volatilization of reagent.
(3) using the aperture feed liquor on bottle cap, rather than bottle cap is opened directly from the mode of bottle body entrance feed liquor, Ke Yigeng
Good ground avoids falling into for dust.
Detailed description of the invention
The attached drawing for constituting a part of the invention is used to provide further understanding of the present invention, schematic reality of the invention
It applies example and its explanation is used to explain the present invention, do not constitute improper limitations of the present invention.In the accompanying drawings:
Fig. 1 is the perspective view (not including stopple) of Mobile-phase reagent bottle described in the embodiment of the present invention 1;
Fig. 2 is the top view of Mobile-phase reagent bottle described in the embodiment of the present invention 1;
Fig. 3 is the cross-sectional view in the face A-A in Fig. 2;
Fig. 4 is the enlarged drawing in Fig. 3 at A;
Fig. 5 is the enlarged drawing in Fig. 3 at B;
Fig. 6 is the vertical profile structure chart of Mobile-phase reagent bottle described in the embodiment of the present invention 2.
Description of symbols:
1- bottle body;2- bottle cap;201- seal closure;202- filler cap;2021- cone tank;2022- cylindrical body;2023- cylinder
Connected in star;3- inlet opening;4- air hole;The first diversion pipe of 5-;6- first through hole;7- outlet tube;8- suction strainer head;9- second is logical
Hole;The second diversion pipe of 11-.
Specific embodiment
It should be noted that in the absence of conflict, the feature in embodiment and embodiment in the present invention can phase
Mutually combination.
In the description of the present invention, it is to be understood that, term " center ", " longitudinal direction ", " transverse direction ", "upper", "lower",
The orientation or positional relationship of the instructions such as "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outside" is
It is based on the orientation or positional relationship shown in the drawings, is merely for convenience of description of the present invention and simplification of the description, rather than instruction or dark
Show that signified device or element must have a particular orientation, be constructed and operated in a specific orientation, therefore should not be understood as pair
Limitation of the invention.In addition, term " first ", " second " etc. are used for description purposes only, it is not understood to indicate or imply phase
To importance or implicitly indicate the quantity of indicated technical characteristic.The feature for defining " first ", " second " etc. as a result, can
To explicitly or implicitly include one or more of the features.In the description of the present invention, unless otherwise indicated, " multiple "
It is meant that two or more.
In the description of the present invention, it should be noted that unless otherwise clearly defined and limited, term " installation ", " phase
Even ", " connection " shall be understood in a broad sense, for example, it may be being fixedly connected, may be a detachable connection, or be integrally connected;It can
To be mechanical connection, it is also possible to be electrically connected;It can be directly connected, can also can be indirectly connected through an intermediary
Connection inside two elements.For the ordinary skill in the art, above-mentioned term can be understood by concrete condition
Concrete meaning in the present invention.
The present invention will be described in detail below with reference to the accompanying drawings and embodiments.
Embodiment 1
As shown in Figs. 1-5, a kind of Mobile-phase reagent bottle, including bottle body 1 and bottle cap 2;The bottle cap 2 includes seal closure 201
With filler cap 202;At least one inlet opening 3 and at least one air hole 4 are equipped at the top of the seal closure 201;Seal closure 201 1
The body formed upper end in filler cap 202;The lower end of the filler cap 202 is detachably connected with bottle body 1;The filler cap 202 wraps
The cone tank 2021 being provided at the top of it is included, 2021 bottom of cone tank is integrally formed with one first diversion pipe 5;Described first
Diversion pipe 5 is connected to cone tank 2021, and 5 lower end of the first diversion pipe extends in bottle body 1;The filler cap 202 is equipped with one
First through hole 6, first through hole 6 is located on 2021 side wall of cone tank, and outlet tube 7 is equipped in first through hole 6;The outlet tube
Seal closure 201 is stretched out in 7 upper ends, and lower end is detachably connected suction strainer head 8;The suction strainer head 8 is located in bottle body 1, and can be out of bottle body 1
It takes out.It should be noted that the shape of cone tank 2021 is cone, cone tank 2021 and the first diversion pipe 5 constitute a leakage
Bucket-shaped guiding device.Suction strainer head is commercial product.The aperture of inlet opening 3 is 1/8 inch bore.The number of inlet opening 3 and air hole 4
Amount can need to be arranged according to sample introduction with ventilative, and the quantity of inlet opening 3 and air hole 4 is 1 in the present embodiment.
Wherein, the seal closure 201 is equipped with the second through-hole 9, and 7 upper end of outlet tube passes through the second through-hole 9 and extends to sealing
The top of lid 201.Second through-hole 9 and the center line of first through hole 6 are overlapped, and upper and lower position is corresponding.
In order to allow the inner wall of cone tank to play the drainage of a similar glass bar, inlet opening 3 is located at funnel
Far from the side of the second through-hole 9 on lid 202, and guarantee that its upright projection is fallen on 2021 inner wall of cone tank.
In order to avoid impurity enters bottle body, in not sample introduction, a stopple is mounted in inlet opening 3 and air hole 4 and (is not existed
It is drawn in attached drawing);Again in order to guarantee that inlet opening 3 at this time can serve as an air hole, so by stopple and its where into
Fluid apertures 3 or air hole 4 are arranged to the form of gap connection, and the gas in such bottle body 1 can be from the feed liquor where stopple and its
Bottle body is flowed out in gap between hole 3 or air hole 4;The material of stopple is polytetrafluoroethylene (PTFE).
In order to guarantee that filler cap 202 and bottle body 1 are detachable, 202 lower end of filler cap is threadedly coupled with bottle body 1.It is described
First diversion pipe, 5 lower end extends to the position in bottle body 1 close to bottleneck;In order to facilitate water conservancy diversion, the first diversion pipe 5, outlet tube 7
It is vertically arranged with 1 bottom of bottle body in the part in bottle body 1;First diversion pipe, 5 lower end is equipped with one second diversion pipe 11,
Distance of second diversion pipe, 11 bottom away from 1 bottom of bottle body is 3mm, this distance can guarantee the second diversion pipe 11 in use process
In as far as possible be located at liquid level below.In addition, diversion pipe is arranged to the shape that the first diversion pipe 5 and the second diversion pipe 11 are split
Formula, on the one hand, since 5 length of the first diversion pipe is shorter, it can be facilitated to take out from bottle body with filler cap 202;On the other hand,
It can according to need, adjust the diameter of diversion pipe, such as by the different of the diameter of the first diversion pipe 5 and the second diversion pipe 11 setting
Sample makes the diameter of the second diversion pipe 11 less than the first diversion pipe 5.
Wherein, the filler cap 202 includes a cylindrical body 2022, and 2022 top of cylindrical body is provided with downwards the taper
Slot 2021, bottom are provided with cylinder shape groove 2023 upwards;2023 inner surface of cylinder shape groove is equipped in for connecting with bottle body 1
Screw thread;Cylinder shape groove 2023 is concordant with the top of the first diversion pipe 5.
In order to facilitate replacing and installing outlet tube 7, suction strainer head 8 is threadedly coupled with outlet tube 7.
Wherein, the material of the bottle body 1 is high-boron-silicon glass, and bottle body 1 is brown.The material of bottle cap 2 is polypropylene.
It, can also be in 202 lower surface of filler cap and 3 face of inlet opening in order to the solvent or additive entered from inlet opening
Position on a filter screen (filter screen is not drawn into figure) is set.
In use, 7 upper end of outlet tube is connect with subsequent liquid phase pipeline, in the insufficient situation of Mobile-phase reagent, beat
The stopple being mounted at inlet opening 3 is opened, solvent addition is carried out by inlet opening 3, due to cone tank 2021,5 and of the first diversion pipe
Second diversion pipe 11 has been integrally formed a funnelform guiding device, and the second diversion pipe 11 is located at below liquid level, therefore is adding
During sample, liquid addition operation is carried out using the drainage of funnelform guiding device, it can be to avoid the generation of bubble;?
Under the premise of not generating bubble, suction strainer head 8 can continue lyosoption, and solvent is drawn entire reagent bottle by outlet tube 7, is made
It enters liquid phase pipeline.
Embodiment 2
As shown in fig. 6, a kind of Mobile-phase reagent bottle, including bottle body 1 and bottle cap 2;
The bottle cap 2 includes seal closure 201 and filler cap 202;At least one inlet opening is equipped at the top of the seal closure 201
3 and at least one air hole 4;Seal closure 201 is detachably connected on the upper end of filler cap 202;The lower end of the filler cap 202 with
Bottle body 1 is detachably connected;The filler cap 202 includes the cone tank 2021 being provided at the top of it, 2021 bottom of cone tank
Integrally formed with one first diversion pipe 5;First diversion pipe 5 is connected to cone tank 2021, and 5 lower end of the first diversion pipe extends
To bottle body 1;The filler cap 202 is equipped with a first through hole 6, and first through hole 6 is located on 2021 side wall of cone tank, and first
Outlet tube 7 is installed in through-hole 6;Seal closure 201 is stretched out in 7 upper end of outlet tube, and lower end is detachably connected suction strainer head 8;It is described
Suction strainer head 8 is located in bottle body 1, and can be taken out out of bottle body 1.It should be noted that the shape of cone tank 2021 is cone, cone
Shape slot 2021 and the first diversion pipe 5 constitute a funnelform guiding device.Suction strainer head is commercial product.The aperture of inlet opening 3
For 1/16 inch bore.The quantity of inlet opening 3 and air hole 4 can need to be arranged according to sample introduction with ventilative, inlet opening 3 in the present embodiment
Quantity with air hole 4 is 1.
Wherein, the seal closure 201 is equipped with the second through-hole 9, and 7 upper end of outlet tube passes through the second through-hole 9 and extends to sealing
The top of lid 201.Wherein, the second through-hole 9 and the center line of first through hole 6 are overlapped, and upper and lower position is corresponding.
In order to allow the inner wall of cone tank to play the drainage of a similar glass bar, inlet opening 3 is located at funnel
Far from the side of the second through-hole 9 on lid 202, upright projection is fallen on 2021 inner wall of cone tank.
In order to avoid impurity enters bottle body, in not sample introduction, a stopple is installed in inlet opening 3;And in order to guarantee at this time
Inlet opening 3 can serve as an air hole, so stopple need to be arranged to the form that gap is connect with the inlet opening 3 where it,
Gas in this way in bottle body 1 can flow out bottle body 1 from the gap between the inlet opening 3 where stopple and its;The material of stopple
For polytetrafluoroethylene (PTFE).
Wherein, being equipped at the top of air hole 4 only allows the check valve that gas passes through in bottle body 1.
In order to guarantee that filler cap 202 and bottle body 1, seal closure 201 are detachable, 202 lower end of filler cap and 1 spiral shell of bottle body
Line connection, 202 upper end of filler cap is connect with 201 threaded upper ends of seal closure.
Wherein, the filler cap 202 includes a cylindrical body 2022, and 2022 top of cylindrical body is provided with downwards the taper
Slot 2021, bottom are provided with cylinder shape groove 2023 upwards;2023 inner surface of cylinder shape groove is equipped in for connecting with bottle body 1
Screw thread;Cylinder shape groove 2023 is concordant with the top of the first diversion pipe 5.
In order to facilitate water conservancy diversion, while diversion effect can be made preferable, the first diversion pipe 5, outlet tube 7 are located in bottle body 1
Part is vertically arranged with 1 bottom of bottle body;Distance of first diversion pipe 5 away from 1 bottom of bottle body is 5mm, this distance can guarantee
First diversion pipe 5 is located at liquid level or less as far as possible in use.In addition, it should be noted that, the present embodiment is by first
The length of diversion pipe 5 is arranged long, extends to it near 1 bottom of bottle body, in this way while not influencing diversion effect,
It can be convenient the first diversion pipe and filler cap integral disassembly, assembly, do not have to especially find the second diversion pipe as in Example 1 again,
And it can avoid due to connecting the problem of unsmooth or connection is broken down between diversion pipe.
In order to facilitate replacing and install outlet tube 7, suction strainer head 8 and 7 grafting of outlet tube.
Wherein, the material of the bottle body 1 is high-boron-silicon glass, and the material of bottle cap 2 is polypropylene.
It, can also be in 202 lower surface of filler cap and 3 face of inlet opening in order to the solvent or additive entered from inlet opening
Position on a filter screen (filter screen is not drawn into figure) is set.
In use, 7 upper end of outlet tube is connect with subsequent liquid phase pipeline, in the insufficient situation of Mobile-phase reagent, beat
The stopple being mounted at inlet opening 3 is opened, solvent addition is carried out by inlet opening 3, since cone tank 2021, the first diversion pipe 5 are whole
Body constitutes a funnelform guiding device, and the first diversion pipe 5 is located at below liquid level, therefore during sample-adding, utilizes leakage
The drainage of bucket-shaped guiding device carries out liquid addition operation, can be to avoid the generation of bubble;Before not generating bubble
It puts, suction strainer head 8 can continue lyosoption, and solvent is drawn entire reagent bottle by outlet tube 7, makes it into liquid-phase tube
Road.
Embodiment 3
Mobile-phase reagent bottle described in the present embodiment with it is almost the same in embodiment 2, the difference is that:
The filler cap 202 is equipped with 2 first through hole 6, and all first through hole 6 are respectively positioned on 2021 side wall of cone tank,
And outlet tube 7 is mounted in all first through hole 6;Seal closure 201 is stretched out in all 7 upper ends of outlet tube, and lower end is detachable
It is connected with suction strainer head 8;All suction strainer heads 8 are each provided in bottle body 1, and can be taken out out of bottle body 1.The setting of outlet tube quantity,
It can be determined according to liquid demand out, for example the intracorporal reagent of bottle is needed to enter in multiple mobile phases, multiple outlet tubes are just arranged in that;
Otherwise, then such to embodiment 2, an outlet tube is set.
The seal closure 201 is equipped with 2 the second through-holes 9, and the upper and lower position of 2 the second through-hole 9 and 2 first through hole
Accordingly;7 upper end of outlet tube passes through the top that the second corresponding through-hole 9 extends to seal closure 201.
Inlet opening 3 is located at the position on filler cap 202 far from all second through-holes 9, and upright projection falls in cone tank
On 2021 inner walls.
In use, difference from Example 2 is, the sample reagent for entering bottle body 1 is drained to from 2 outlet tubes 7
2 or 2 or more outside bottle body (when for 2 or more, can be located at the connection of the pipeline section outside filler cap 202 three in outlet tube 7
Siphunculus or triple valve) mobile phase in.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention
Within mind and principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.