CN109351172A - A kind of preform tail gas collection system - Google Patents

A kind of preform tail gas collection system Download PDF

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Publication number
CN109351172A
CN109351172A CN201811534308.9A CN201811534308A CN109351172A CN 109351172 A CN109351172 A CN 109351172A CN 201811534308 A CN201811534308 A CN 201811534308A CN 109351172 A CN109351172 A CN 109351172A
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CN
China
Prior art keywords
tail gas
cushion chamber
collection system
pressure measuring
air
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Pending
Application number
CN201811534308.9A
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Chinese (zh)
Inventor
汤剑波
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SHANGHAI ZHENGFAN TECHNOLOGY Co Ltd
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SHANGHAI ZHENGFAN TECHNOLOGY Co Ltd
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Priority to CN201811534308.9A priority Critical patent/CN109351172A/en
Publication of CN109351172A publication Critical patent/CN109351172A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34Chemical or biological purification of waste gases
    • B01D53/46Removing components of defined structure
    • B01D53/68Halogens or halogen compounds
    • B01D53/685Halogens or halogen compounds by treating the gases with solids
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B23/00Noble gases; Compounds thereof
    • C01B23/001Purification or separation processes of noble gases
    • C01B23/0036Physical processing only
    • C01B23/0052Physical processing only by adsorption in solids
    • C01B23/0057Physical processing only by adsorption in solids characterised by the adsorbent
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B37/00Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
    • C03B37/01Manufacture of glass fibres or filaments
    • C03B37/012Manufacture of preforms for drawing fibres or filaments
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2251/00Reactants
    • B01D2251/30Alkali metal compounds
    • B01D2251/304Alkali metal compounds of sodium
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2251/00Reactants
    • B01D2251/40Alkaline earth metal or magnesium compounds
    • B01D2251/404Alkaline earth metal or magnesium compounds of calcium
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2251/00Reactants
    • B01D2251/60Inorganic bases or salts
    • B01D2251/602Oxides
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2210/00Purification or separation of specific gases
    • C01B2210/0029Obtaining noble gases
    • C01B2210/0031Helium
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2210/00Purification or separation of specific gases
    • C01B2210/0043Impurity removed
    • C01B2210/0098Other impurities

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Health & Medical Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Biomedical Technology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Waste-Gas Treatment And Other Accessory Devices For Furnaces (AREA)

Abstract

The invention discloses a kind of preform tail gas collection systems, belong to light manufacturing technology field, including main line and pressure measuring piece, flow direction on main line along tail gas is disposed with flow controller, the first cushion chamber, chlorine remover, the second cushion chamber, regulating valve, air-supply assembly and concentration detector, and main line is provided with flow controller one end and is connected to prefabricated rods sintering furnace;There are two pressure measuring piece is set, wherein a pressure measuring piece is set on the first cushion chamber, and it is electrically connected to regulating valve, another pressure measuring piece is set on the second cushion chamber, and is electrically connected to air-supply assembly.Light prefabricated rods tail gas collection system proposed by the present invention, by chlorine remover by chlorine remove, avoid the storage or processing equipment of the subsequent tail gas of chlorine corrosion.By setting the range of flow of flow controller according to the air inflow of helium and chlorine, and then the amount for entering the air of prefabricated rods sintering furnace is controlled, avoids the air capacity in tail gas excessive and concentrations of helium is reduced.

Description

A kind of preform tail gas collection system
Technical field
The present invention relates to optic fibre manufacturing technology field more particularly to a kind of preform tail gas collection systems.
Background technique
Optical fiber production manufacture each technique in need to use a large amount of helium, especially preform production and Using helium as cooling and protectiveness atmosphere gas in drawing optical fibers technique, since helium is rare gas, valence in nature Lattice are expensive, and the use cost of helium accounts for 25% or more of manufacture preform cost, it is therefore desirable to be recycled again to helium It utilizes.
Currently, preform is sintered in optical fiber sintering furnace, due to the particularity of optical fiber sintering furnace, in sintering It can be passed through helium and chlorine, chlorine has strong corrosive, can corrode the storage or processing equipment of subsequent tail gas, and agglomerating plant It is communicated with atmosphere, a large amount of air can be contained by being sintered in tail gas, so that the concentration of helium reduces in tail gas, be not easy to collect.
Summary of the invention
The purpose of the present invention is to provide a kind of preform tail gas collection systems, realize the chlorine in removal tail gas, It avoids the amount of air in tail gas excessive simultaneously, reduces the concentration of helium.
As above design, the technical scheme adopted by the invention is that:
A kind of preform tail gas collection system, comprising:
Main line is disposed with flow controller, the first cushion chamber, chlorine remover, along the flow direction of tail gas thereon Two cushion chambers, regulating valve, air-supply assembly and concentration detector, and the main line is provided with flow controller one end connection In prefabricated rods sintering furnace;
Pressure measuring piece, if there are two, wherein a pressure measuring piece is set on first cushion chamber, and it is electrically connected to described Regulating valve, another pressure measuring piece is set on second cushion chamber, and is electrically connected to the air-supply assembly.
Further, further include two bye-passes, two bye-passes be all connected to the main line be provided with it is described One end of concentration detector.
Further, wherein being provided with first switch part and gas storage packet on a bye-pass, on another bye-pass It is provided with second switch part.
Further, the first switch part and the second switch part are pneumatic operated valve.
It further, further include controller, the controller is electrically connected in the flow controller, regulating valve, send Wind component, concentration detector and two pressure measuring pieces.
It further, further include third switch member, the third switch member is set on the main line, and is located at described Between prefabricated rods sintering furnace and the flow controller.
Further, the chlorine remover includes cavity, and dry adsorption agent is provided in the cavity.
Further, the air-supply assembly is blower.
The invention has the benefit that
Light prefabricated rods tail gas collection system proposed by the present invention can be by the chlorine in tail gas by the way that chlorine remover is arranged Removal, avoids the storage or processing equipment of the subsequent tail gas of chlorine corrosion.By the way that flow controller is arranged, according to helium and chlorine Air inflow set the range of flow of flow controller, and then control the amount for the air for entering prefabricated rods sintering furnace, because As soon as when the timing of the range of flow of flow controller, the amount of chlorine and helium also a timing can limit entrance air amount, And then it avoids the air capacity in tail gas excessive and concentrations of helium is reduced.
Detailed description of the invention
Fig. 1 is the schematic diagram of preform tail gas collection system provided by the invention.
In figure:
1, main line;11, third switch member;12, flow controller;13, the first cushion chamber;14, chlorine remover;15, second Cushion chamber;16, regulating valve;17, air-supply assembly;18, concentration detector;191, the first pressure measuring piece;192, the second pressure measuring piece;
2, the first bye-pass;21, first switch part;22, gas storage packet;
3, the second bye-pass;31, second switch part;
4, prefabricated rods sintering furnace.
Specific embodiment
To keep the technical problems solved, the adopted technical scheme and the technical effect achieved by the invention clearer, below In conjunction with attached drawing and pass through specific embodiment to further illustrate the technical scheme of the present invention.It is understood that this place is retouched The specific embodiment stated is used only for explaining the present invention rather than limiting the invention.It also should be noted that in order to just Only the parts related to the present invention are shown in description, attached drawing and it is not all.
Fig. 1 is the schematic diagram of preform tail gas collection system in the present embodiment.As shown in Figure 1, the present embodiment provides A kind of preform tail gas collection system, including main line 1, pressure measuring piece and controller, main line 1 and pressure measuring piece are by resistance to The material of chlorine corrosion is made, such as nickel-base alloy, engineering plastics etc..
Wherein, on main line 1 along the direction of the flowing of tail gas be disposed with third switch member 11, flow controller 12, First cushion chamber 13, chlorine remover 14, the second cushion chamber 15, regulating valve 16, air-supply assembly 17 and concentration detector 18, and main line 1 one end for being provided with third switch member 11 is connected to the offgas outlet of prefabricated rods sintering furnace 4, and in the present embodiment, third is opened Pass part 11 is pneumatic operated valve, and flow controller 12 is flowmeter, and regulating valve 16 is ratio adjusting valve, and air-supply assembly 17 is blower, dense Degree detector 18 is concentrations of helium instrument, and certainly in other embodiments, third switch member 11 can also be the structures such as shut-off valve, dense Spending detector 18 can also be the structures such as gas sensor.
There are two pressure measuring piece is set, respectively the first pressure measuring piece 191 and the second pressure measuring piece 192, the first pressure measuring piece 191 are set to On first cushion chamber 13, the second pressure measuring piece 192 is set on the second cushion chamber 15, in the present embodiment, 191 He of the first pressure measuring piece Second pressure measuring piece 192 is pressure gauge.Controller (not shown) is electrically connected to flow controller 12, regulating valve 16, air-supply Organize 17, Concentration Testing 18, the first pressure measuring piece 192 and the second pressure measuring piece 192.
Under the action of blower, tail gas is flowed along main line 1, and chlorine when by chlorine remover 14 in tail gas is gone It removes.Above-mentioned chlorine remover 14 includes cavity, is provided with dry adsorption agent in cavity, and in the present embodiment, dry adsorption agent is alkali stone Ash or soda lime can occur chemical reaction with chlorine and remove chlorine, avoid the storage of the subsequent tail gas of chlorine corrosion Or processing equipment.
Moreover, set the range of flow of flow controller 12 according to the air inflow of helium and chlorine, so come control into Enter the amount of the air to prefabricated rods sintering furnace 4, this is because when the timing of range of flow one of flow controller 12, due to chlorine and The amount of helium is also certain, then can come limit entrance air amount, and then avoid air capacity in tail gas excessive and So that concentrations of helium reduces.
When carrying out exhaust collection, 13 inner exhaust gas of the first cushion chamber is set according to the operating pressure in prefabricated rods sintering furnace 4 Pressure limit negative pressure state is in the first cushion chamber 13, when the first pressure measuring piece 191 detects first in the present embodiment When the absolute value of 13 inner exhaust gas pressure of cushion chamber is greater than the maximum value of pressure in the pressure limit of setting, subtracted by controller The aperture of small scale regulating valve slows down the flowing velocity of tail gas;When the first pressure measuring piece 191 detects the pressure in the first cushion chamber 13 When the absolute value of power is less than the least absolute value of pressure in the pressure limit of setting, pass through opening for controller scaling up regulating valve Degree, increases the flowing velocity of tail gas.Make 13 inner exhaust gas of the first cushion chamber by the first manometric module 191 and ratio adjusting valve Pressure maintains in a certain range, controls the tube pressure in prefabricated rods sintering furnace 4 with this, guarantees the preform tail Gas collection system will not influence the pressure in prefabricated rods sintering furnace 4, and then avoid damaging prefabricated rods sintering furnace 4.
In addition, the effect of the second cushion chamber 15 is the pressure stablized in the preform tail gas collection system, according to reality Border needs to set the pressure limit of 15 inner exhaust gas of the second cushion chamber.In the present embodiment, the second cushion chamber 15 is similarly in negative pressure State, when the second pressure measuring piece 192 detects that the absolute value of 15 inner exhaust gas pressure of the second cushion chamber is greater than in the pressure limit of setting When the maximum value of pressure, reduces the frequency of blower by controller, slow down the flowing velocity of tail gas;When the second pressure measuring piece 192 detect the pressure in the second cushion chamber 15 absolute value be less than setting pressure limit in pressure least absolute value when, The frequency for increasing blower by controller, increases the flowing velocity of tail gas.Pass through the second manometric module 192 and blower collective effect So that the second cushion chamber 15 is maintained in certain pressure limit, so that the preform tail gas collection system maintains In certain pressure limit.
In addition, the first pressure measuring piece 191 and ratio adjusting valve, the second pressure measuring piece 192 and blower collective effect, so that the optical fiber Pressure in prefabricated rods tail gas collection system is stablized, and does not influence the pressure in prefabricated rods sintering furnace 4, guarantees preform Sintering process is normally carried out.
As shown in Figure 1, the preform tail gas collection system further includes two bye-passes, two bye-passes are all connected to Main line 1 is provided with one end of concentration detector 18.Two bye-passes are respectively designated as the first bye-pass 2 and the second bye-pass 3.Wherein, it is provided with first switch part 21 and gas storage packet 22 on the first bye-pass 2, is provided with second switch on the second bye-pass 3 Part 31.In the present embodiment, first switch part 21 and second switch part 31 are pneumatic operated valve, by solenoid valve control, and electromagnetism Valve is connected to controller.
When carrying out exhaust collection, when concentration detector 18 detects the concentration of helium less than preset value, controller control First switch part 21 processed is closed, and controls the opening of second switch part 31, and tail gas is discharged to exhaust treatment system and is handled;When When concentration detector 18 detects that the concentration of helium is more than or equal to preset value, controller controls second switch part 31 and closes, and the One switch member 21 is opened, and by exhaust collection into gas storage packet 22, is then carried out the extraction of helium by tail gas treatment device and is mentioned Pure, wherein the preset value of concentrations of helium is configured according to actual needs.
The course of work of the tail gas collection system to the preform is described in detail below.
Controller controls third switch member 11, blower and second switch part 31 are opened, the tail gas that prefabricated rods sintering generates according to It is secondary through third switch member 11, flow controller 12, the first cushion chamber 13, chlorine remover 14, the second cushion chamber 15, ratio adjusting valve, Blower and concentration detector 18, chlorine remover 14 remove the chlorine in tail gas, and in 18 real-time monitoring tail gas of concentration detector The concentration of helium, when the concentration of helium is more than or equal to preset value, controller closes second switch part 31, opens first switch part 21, tail gas enters in gas storage packet 22 through first switch part 21.
In the process, the amount of air in tail gas is controlled by setting the range of flow of flow controller 12.Pass through One manometric module 191 and ratio adjusting valve keep the pressure of 13 inner exhaust gas of the first cushion chamber in a certain range.Pass through Two manometric modules 192 and blower keep the pressure of 15 inner exhaust gas of the second cushion chamber in a certain range.
Embodiment of above only elaborates that the basic principles and features of the invention, the present invention are not limited by above embodiment System, without departing from the spirit and scope of the present invention, the invention also has various changes and changes, and these changes and changes are all It falls into scope of the claimed invention.The claimed scope of the invention is by appended claims and its equivalent circle It is fixed.

Claims (8)

1. a kind of preform tail gas collection system, which is characterized in that including;
Main line (1) is disposed with flow controller (12) along the flow direction of tail gas thereon, the first cushion chamber (13), removes Chlorine device (14), the second cushion chamber (15), regulating valve (16), air-supply assembly (17) and concentration detector (18), and the main line (1) one end for being provided with the flow controller (12) is connected to prefabricated rods sintering furnace (4);
Pressure measuring piece, if there are two, wherein a pressure measuring piece is set on first cushion chamber (13), and it is electrically connected to described Regulating valve (16), another pressure measuring piece is set on second cushion chamber (15), and is electrically connected to the air-supply assembly (17)。
2. preform tail gas collection system according to claim 1, which is characterized in that it further include two bye-passes, Two bye-passes are all connected to one end that the main line (1) is provided with the concentration detector (18).
3. preform tail gas collection system according to claim 2, which is characterized in that wherein on a bye-pass It is provided with first switch part (21) and gas storage packet (22), second switch part (31) are provided on another bye-pass.
4. preform tail gas collection system according to claim 3, which is characterized in that the first switch part (21) It is pneumatic operated valve with the second switch part (31).
5. preform tail gas collection system according to claim 1, which is characterized in that it further include controller, it is described Controller be electrically connected in the flow controller (12), regulating valve (16), air-supply assembly (17), concentration detector (18) and Two pressure measuring pieces.
6. preform tail gas collection system according to claim 1, which is characterized in that further include third switch member (11), the third switch member (11) is set on the main line (1), and is located at the prefabricated rods sintering furnace (4) and described Between flow controller (12).
7. preform tail gas collection system according to claim 1, which is characterized in that the chlorine remover (14) includes Cavity is provided with dry adsorption agent in the cavity.
8. preform tail gas collection system according to claim 1, which is characterized in that the air-supply assembly (17) is Blower.
CN201811534308.9A 2018-12-14 2018-12-14 A kind of preform tail gas collection system Pending CN109351172A (en)

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CN201811534308.9A CN109351172A (en) 2018-12-14 2018-12-14 A kind of preform tail gas collection system

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Application Number Priority Date Filing Date Title
CN201811534308.9A CN109351172A (en) 2018-12-14 2018-12-14 A kind of preform tail gas collection system

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CN109351172A true CN109351172A (en) 2019-02-19

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110498401A (en) * 2019-09-02 2019-11-26 北京中科富海低温科技有限公司 Helium recovery purification device
CN110624321A (en) * 2019-10-28 2019-12-31 苏州朗道节能技术有限公司 A preceding processing apparatus for waste gas recovery purifies
CN112225448A (en) * 2020-10-22 2021-01-15 江苏亨通光导新材料有限公司 Helium-chlorine mixed gas circulation system for sintering optical fiber perform
CN114031288A (en) * 2021-11-08 2022-02-11 苏州回能环保科技有限公司 Device and method for collecting helium-containing waste gas discharged by optical fiber preform sintering furnace

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5377491A (en) * 1992-12-11 1995-01-03 Praxair Technology, Inc. Coolant recovery process
CN206089041U (en) * 2016-09-26 2017-04-12 湖北和远气体股份有限公司 Steady pressure retrieves device of rich helium tail gas
CN106744749A (en) * 2016-11-30 2017-05-31 富通集团(嘉善)通信技术有限公司 For the helium online recycling Application way and device of drawing optical fibers system
CN206872677U (en) * 2017-05-31 2018-01-12 江苏奥维信亨通光学科技有限公司 A kind of preform sinters furnace pressure automatic control system
CN209302532U (en) * 2018-12-14 2019-08-27 上海正帆科技股份有限公司 A kind of preform tail gas collection system

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5377491A (en) * 1992-12-11 1995-01-03 Praxair Technology, Inc. Coolant recovery process
CN206089041U (en) * 2016-09-26 2017-04-12 湖北和远气体股份有限公司 Steady pressure retrieves device of rich helium tail gas
CN106744749A (en) * 2016-11-30 2017-05-31 富通集团(嘉善)通信技术有限公司 For the helium online recycling Application way and device of drawing optical fibers system
CN206872677U (en) * 2017-05-31 2018-01-12 江苏奥维信亨通光学科技有限公司 A kind of preform sinters furnace pressure automatic control system
CN209302532U (en) * 2018-12-14 2019-08-27 上海正帆科技股份有限公司 A kind of preform tail gas collection system

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110498401A (en) * 2019-09-02 2019-11-26 北京中科富海低温科技有限公司 Helium recovery purification device
CN110498401B (en) * 2019-09-02 2024-05-17 北京中科富海低温科技有限公司 Helium recovery purifying device
CN110624321A (en) * 2019-10-28 2019-12-31 苏州朗道节能技术有限公司 A preceding processing apparatus for waste gas recovery purifies
CN112225448A (en) * 2020-10-22 2021-01-15 江苏亨通光导新材料有限公司 Helium-chlorine mixed gas circulation system for sintering optical fiber perform
CN114031288A (en) * 2021-11-08 2022-02-11 苏州回能环保科技有限公司 Device and method for collecting helium-containing waste gas discharged by optical fiber preform sintering furnace

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