CN109342257A - The measurement device of moisture in bromine - Google Patents
The measurement device of moisture in bromine Download PDFInfo
- Publication number
- CN109342257A CN109342257A CN201811361522.9A CN201811361522A CN109342257A CN 109342257 A CN109342257 A CN 109342257A CN 201811361522 A CN201811361522 A CN 201811361522A CN 109342257 A CN109342257 A CN 109342257A
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- tube
- phosphorus pentoxide
- measurement device
- bromine
- calcium oxide
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N5/00—Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid
- G01N5/04—Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid by removing a component, e.g. by evaporation, and weighing the remainder
- G01N5/045—Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid by removing a component, e.g. by evaporation, and weighing the remainder for determining moisture content
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
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Abstract
The invention discloses the measurement devices of moisture in bromine, including measurement device shell and hose, the measurement device shell is internally provided with partition, one end of the partition is provided with thermal insulative board, inside one end of the measurement device shell is surrounded with concentrated sulfuric acid chamber by partition, the concentrated sulfuric acid chamber is internally provided with injection pipe, the side of the concentrated sulfuric acid chamber is provided with calcium oxide U-tube A, one end of the calcium oxide U-tube A is provided with phosphorus pentoxide U-tube A, one end of the phosphorus pentoxide U-tube A is provided with bromine evaporative flask, the measurement device shell and thermal insulative board are surrounded by water-bath room, the bromine evaporative flask is placed on the inside of water-bath room, one end of the measurement device shell is provided with filler pipe；By the measurement device shell of design, each element that measurement device needs is become one, it is convenient to take when in use, it is more convenient when moisture is measured in bromine, and measurement is more accurate.
Description
Technical field
The invention belongs to measurement device technical fields, and in particular to the measurement device of moisture in bromine.
Background technique
Bromine is a kind of liquid of reddish brown, irritant smell and strong corrosive.Bromine is the weight to involve the interests of the state and the people
Industrial chemicals is wanted, it is widely used, it is mainly used in flame-retarding fire-extinguishing, oil exploitation, sterilizing, chemicals, military project space flight, changes
Learn the synthesis and manufacture of the related industries such as the fields, and medicine, pesticide, dyestuff intermediate, membrane material, photosensitive material such as protection.
Bromine resource is primarily present in seawater, subsurface brine and fossil sea floor and deposits in salt mine and salt lake saline, industrialization
Production technology has steam distillation and air blowout enrichment-steam distillation.The production technology of bromine causes in bromine not
It is evitable to be mixed with partial moisture.Moisture in bromine easily caused in bromine use process catalyst inactivation, reaction be difficult into
Row, directly affects the production of bromine fine chemical product, therefore, has strict requirements to moisture content in bromine both at home and abroad.Water
Point content height is the key factor for distinguishing bromine superiority and inferiority, and China studied in terms of determination of moisture in bromine it is less, lack compared with
For outstanding measurement device.
The measurement device of moisture when in use, since each element disperses, is assembled in existing bromine
Use, in this way carry out using when be easy to cause bromine to be revealed because poorly sealed, cause damages to environment and the person, simultaneously
Be easy to happen and implement damage and the problem of error occur, thus it is proposed that in bromine moisture measurement device.
Summary of the invention
The purpose of the present invention is to provide the measurement devices of moisture in bromine, mentioned above in the background art existing to solve
The measurement device of moisture when in use, since each element disperses, needs to carry out assembling use, exist in this way in some bromines
Carry out using when be easy to happen damage and the problem of error occur.
To achieve the above object, the invention provides the following technical scheme: in bromine moisture measurement device, including measurement dress
Shell and hose are set, the measurement device shell is internally provided with partition, and one end of the partition is provided with thermal insulative board, described
Inside one end of measurement device shell is surrounded with concentrated sulfuric acid chamber by partition, and the concentrated sulfuric acid chamber is internally provided with injection
Pipe, the side of the concentrated sulfuric acid chamber are provided with calcium oxide U-tube A, and one end of the calcium oxide U-tube A is provided with five oxidations
Two phosphorus U-tube A, one end of the phosphorus pentoxide U-tube A is provided with bromine evaporative flask, the measurement device shell and thermal insulative board
It is surrounded by water-bath room, the bromine evaporative flask is placed on the inside of water-bath room, and one end of the measurement device shell is provided with plus water
Pipe, the filler pipe are connected with water-bath room, and one end of the bromine evaporative flask is provided with phosphorus pentoxide U-tube B, five oxygen
The one end for changing two phosphorus U-tube B is provided with phosphorus pentoxide U-tube C, and one end of the phosphorus pentoxide U-tube C is provided with oxidation
Calcium U-tube B, one end of the calcium oxide U-tube B are provided with surge chamber, and the side of the surge chamber is provided with sodium hydroxide room,
The sodium hydroxide room and surge chamber are by connection U-tube connection, and the both ends for connecting U-tube are connected to surge chamber and hydrogen
The bottom of sodium oxide molybdena room, the other end of the measurement device shell are provided with bleeding point, the bleeding point and sodium hydroxide room phase
Connection.
Preferably, the concentrated sulfuric acid chamber, calcium oxide U-tube A, phosphorus pentoxide U-tube A, bromine evaporative flask, five oxidations two
Phosphorus U-tube B, phosphorus pentoxide U-tube C, calcium oxide U-tube B and surge chamber are attached by bindiny mechanism and hose, described
Bindiny mechanism includes fixture nut and pressing plate, and the hose is fixed on calcium oxide U-tube A, phosphorus pentoxide U-tube A, bromine evaporation
The outside of bottle, phosphorus pentoxide U-tube B, phosphorus pentoxide U-tube C and the connecting pin calcium oxide U-tube B, and one end peace of hose
Mounted in the inside of pressing plate, the fixture nut screw connecting with pressing plate by screw thread, the calcium oxide U-tube A, five oxidations
Two phosphorus U-tube A, phosphorus pentoxide U-tube B, phosphorus pentoxide U-tube C and calcium oxide U-tube B side be provided with fixation
Anchor ear, one end of the fixed anchor ear are provided with fixing bolt, and one end of the fixing bolt is provided with butterfly nut.
Preferably, the side of the measurement device shell is provided with cover board, and the lower end of the cover board is provided with inserted link, described
The side of measurement device shell corresponds to the position setting jack of inserted link, and the side of the cover board is provided with fixing buckle, the cover board
It is fixedly connected with measurement device shell by fixing buckle, and the junction of cover board and measurement device shell is provided with sealing
Circle.
Preferably, the phosphorus pentoxide U-tube B, phosphorus pentoxide U-tube C and bromine evaporative flask are installed in by thermal insulation
In the water-bath room that plate surrounds, and concentrated sulfuric acid chamber, calcium oxide U-tube A, phosphorus pentoxide U-tube A, water-bath room, phosphorus pentoxide
U-tube B, phosphorus pentoxide U-tube C, calcium oxide U-tube B and the lower end of sodium hydroxide room are provided with drainpipe.
Preferably, the upper end of the water-bath room is provided with flip lid, and calcium oxide U-tube A and phosphorus pentoxide U-tube A, five
It aoxidizes and is provided with cover board on the outside of two phosphorus U-tube B and phosphorus pentoxide U-tube C and calcium oxide U-tube B.
Compared with prior art, the beneficial effects of the present invention are:
(1) by the measurement device shell of design, each element that measurement device needs is become one, it is convenient to make
Used time takes, more convenient when moisture is measured in bromine, and measurement is more accurate；
(2) it by the bindiny mechanism of design, when connecting and dismantled between each measurement element, need to only can be manually rotated
Connection and disassembly can be completed in fixture nut, more convenient, facilitates and is overhauled and replaced；
Detailed description of the invention
Fig. 1 is measurement device positive structure diagram of the invention；
Fig. 2 is measurement device backsight structural representation of the invention；
Fig. 3 is measurement device overlooking structure diagram of the invention；
Fig. 4 is fixation hooping structure schematic diagram of the invention；
Fig. 5 is fixed plate structure schematic diagram of the invention；
Fig. 6 is attachment structure schematic diagram of the invention；
Fig. 7 is connection pressure plate structure schematic diagram of the invention；
In figure: 1, measurement device shell；2, concentrated sulfuric acid chamber；3, injection pipe；4, partition；5, calcium oxide U-tube A；6, five
Aoxidize two phosphorus U-tube A；7, fixed anchor ear；8, thermal insulative board；9, bromine evaporative flask；10, water-bath room；11, drainpipe；12, filler pipe；
13, phosphorus pentoxide U-tube B；14, phosphorus pentoxide U-tube C；15, calcium oxide U-tube B；16, surge chamber；17, sodium hydroxide
Room；18, bleeding point；19, cover board；20, it renovates；21, fixing buckle；22, butterfly nut；23, fixing bolt；24, inserted link；25, solid
Determine nut；26, pressing plate；27, hose.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other
Embodiment shall fall within the protection scope of the present invention.
Fig. 1-7 is please referred to, the present invention provides a kind of technical solution: the measurement device of moisture in bromine, including measurement device
Shell 1 and hose 27, measurement device shell 1 are internally provided with partition 4, and one end of partition 4 is provided with thermal insulative board 8, measurement dress
It sets inside one end of shell 1 and concentrated sulfuric acid chamber 2 is surrounded with by partition 4, concentrated sulfuric acid chamber 2 is internally provided with injection pipe 3, dense
The side of sulfuric acid chamber 2 is provided with calcium oxide U-tube A5, and one end of calcium oxide U-tube A5 is provided with phosphorus pentoxide U-tube
A6, one end of phosphorus pentoxide U-tube A6 are provided with bromine evaporative flask 9, and measurement device shell 1 and thermal insulative board 8 are surrounded by water-bath room
10, bromine evaporative flask 9 is placed on the inside of water-bath room 10, and one end of measurement device shell 1 is provided with filler pipe 12, filler pipe 12 with
Water-bath room 10 is connected, and one end of bromine evaporative flask 9 is provided with phosphorus pentoxide U-tube B13, and the one of phosphorus pentoxide U-tube B13
End is provided with phosphorus pentoxide U-tube C14, and one end of phosphorus pentoxide U-tube C14 is provided with calcium oxide U-tube B15, oxidation
One end of calcium U-tube B15 is provided with surge chamber 16, and the side of surge chamber 16 is provided with sodium hydroxide room 17, sodium hydroxide room 17
With surge chamber 16 by connection U-tube connection, and the both ends for connecting U-tube are connected to surge chamber 16 and sodium hydroxide room 17
Bottom, the other end of measurement device shell 1 is provided with bleeding point 18, and bleeding point 18 is connected with sodium hydroxide room 17.
Disassembly maintenance is carried out in order to facilitate measurement device, in the present embodiment, it is preferred that concentrated sulfuric acid chamber 2, calcium oxide U
Type pipe A5, phosphorus pentoxide U-tube A6, bromine evaporative flask 9, phosphorus pentoxide U-tube B13, phosphorus pentoxide U-tube C14, oxidation
Calcium U-tube B15 and surge chamber 16 are attached by bindiny mechanism and hose 27, and bindiny mechanism includes fixture nut 25 and pressing plate
26, hose 27 be fixed on calcium oxide U-tube A5, phosphorus pentoxide U-tube A6, bromine evaporative flask 9, phosphorus pentoxide U-tube B13,
The outside of phosphorus pentoxide U-tube C14 and the connecting pin calcium oxide U-tube B15, and one end of hose 27 is mounted on the interior of pressing plate 26
Side, fixture nut 25 screw connecting with pressing plate 26 by screw thread, calcium oxide U-tube A5, phosphorus pentoxide U-tube A6, five
The side for aoxidizing two phosphorus U-tube B13, phosphorus pentoxide U-tube C14 and calcium oxide U-tube B15 is provided with fixed anchor ear 7, Gu
The one end for determining anchor ear 7 is provided with fixing bolt 23, and one end of fixing bolt 23 is provided with butterfly nut 22.
In order to keep measurement device easy to use, in the present embodiment, it is preferred that the side of measurement device shell 1 is provided with lid
Plate 19, the lower end of cover board 19 are provided with inserted link 24, and the side of measurement device shell 1 corresponds to the position setting jack of inserted link 24, lid
The side of plate 19 is provided with fixing buckle 21, and cover board 19 is fixedly connected with measurement device shell 1 by fixing buckle 21, and cover board
19 are provided with sealing ring with the junction of measurement device shell 1.
It is heated to facilitate measurement device, in the present embodiment, it is preferred that phosphorus pentoxide U-tube B13, five oxygen
Change two phosphorus U-tube C14 and bromine evaporative flask 9 is installed in the water-bath room 10 surrounded by thermal insulative board 8, and concentrated sulfuric acid chamber 2, oxidation
Calcium U-tube A5, phosphorus pentoxide U-tube A6, water-bath room 10, phosphorus pentoxide U-tube B13, phosphorus pentoxide U-tube C14, oxygen
The lower end for changing calcium U-tube B15 and sodium hydroxide room 17 is provided with drainpipe 11.
In order to keep water-bath room 10 easy to use, in the present embodiment, it is preferred that the upper end of water-bath room 10 is provided with flip lid 20,
And calcium oxide U-tube A5 and phosphorus pentoxide U-tube A6, phosphorus pentoxide U-tube B13 and phosphorus pentoxide U-tube C14 and oxygen
Change and is provided with cover board 19 on the outside of calcium U-tube B15.
The working principle of the invention and process for using: it after the present invention installs, first checks for installation of the invention and fixes
And security protection, it then can use, bleeding point 18 connects aspiration pump, the oxidation of phosphorus pentoxide U-tube B13 and five two
The quality of phosphorus U-tube C14 is fixed, and the concentrated sulfuric acid is put into concentrated sulfuric acid chamber 2, sodium hydroxide is put into sodium hydroxide room 17, in oxygen
Calcium oxide is placed in the inside for changing calcium U-tube A5 and calcium oxide U-tube B15, U-shaped in phosphorus pentoxide U-tube A6, phosphorus pentoxide
It is put into the phosphorus pentoxide of fixed weight in pipe B13 and phosphorus pentoxide U-tube C14, and is passed through hot water in water-bath room 10, it is right
Phosphorus pentoxide U-tube B13, phosphorus pentoxide U-tube C14 and bromine evaporative flask 9 carry out water-bath, and the temperature of bromine evaporative flask 9 is
Between 50 DEG C~70 DEG C, the temperature of phosphorus pentoxide U-tube B13 and phosphorus pentoxide U-tube C14 is between 50 DEG C~70 DEG C,
Without bromine vapor in the bromine and water of noresidue in bromine evaporative flask 9, phosphorus pentoxide U-tube B13 and phosphorus pentoxide U-tube C14
When, aspiration pump is closed, then water in water-bath room 10 is released by drainpipe 11, under cover board 19 is dismantled by fixing buckle 21
Come, rotation butterfly nut 22 opens fixed anchor ear 7, then rotary fixing screw mother 25 unclamps pressing plate 26 from hose 27, then
Hose 27 is extracted, make phosphorus pentoxide U-tube B13 and phosphorus pentoxide U-tube C14 disassemble carry out and by piston into
Then phosphorus pentoxide U-tube B13 and phosphorus pentoxide U-tube C14 are placed in cooling in drier by row sealing, right after cooling
Phosphorus pentoxide U-tube B13 and phosphorus pentoxide U-tube C14 weigh, phosphorus pentoxide U-tube B13 and phosphorus pentoxide
The increased quality of U-tube C14 is the quality of moisture in bromine, and this completes to use process of the invention, the present invention
Structure is simple, safe and convenient to use.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (5)
1. the measurement device of moisture in bromine, including measurement device shell (1) and hose (27), it is characterised in that: the measurement
Crust of the device (1) is internally provided with partition (4), and one end of the partition (4) is provided with thermal insulative board (8), the measurement device
Inside one end of shell (1) is surrounded with concentrated sulfuric acid chamber (2) by partition (4), and concentrated sulfuric acid chamber (2) are internally provided with
Injection pipe (3), the side of the concentrated sulfuric acid chamber (2) are provided with calcium oxide U-tube A (5), the calcium oxide U-tube A (5)
One end is provided with phosphorus pentoxide U-tube A (6), and one end of the phosphorus pentoxide U-tube A (6) is provided with bromine evaporative flask (9),
The measurement device shell (1) and thermal insulative board (8) are surrounded by water-bath room (10), and the bromine evaporative flask (9) is placed on water-bath room
(10) one end of inside, the measurement device shell (1) is provided with filler pipe (12), the filler pipe (12) and water-bath room
(10) it is connected, one end of the bromine evaporative flask (9) is provided with phosphorus pentoxide U-tube B (13), and the phosphorus pentoxide is U-shaped
One end of pipe B (13) is provided with phosphorus pentoxide U-tube C (14), and one end of the phosphorus pentoxide U-tube C (14) is provided with
One end of calcium oxide U-tube B (15), the calcium oxide U-tube B (15) are provided with surge chamber (16), the surge chamber (16)
Side is provided with sodium hydroxide room (17), and the sodium hydroxide room (17) and surge chamber (16) are connected by connection U-tube connection
The both ends for connecing U-tube are connected to the bottom of surge chamber (16) and sodium hydroxide room (17), the measurement device shell (1)
The other end is provided with bleeding point (18), and the bleeding point (18) is connected with sodium hydroxide room (17).
2. the measurement device of moisture in bromine according to claim 1, it is characterised in that: the concentrated sulfuric acid chamber (2), oxygen
Change calcium U-tube A (5), phosphorus pentoxide U-tube A (6), bromine evaporative flask (9), phosphorus pentoxide U-tube B (13), phosphorus pentoxide
U-tube C (14), calcium oxide U-tube B (15) and surge chamber (16) are attached by bindiny mechanism and hose (27), the company
Connection mechanism includes fixture nut (25) and pressing plate (26), and the hose (27) is fixed on calcium oxide U-tube A (5), phosphorus pentoxide
U-tube A (6), bromine evaporative flask (9), phosphorus pentoxide U-tube B (13), phosphorus pentoxide U-tube C (14) and calcium oxide U-tube B
(15) outside of connecting pin, and one end of hose (27) is mounted on the inside of pressing plate (26), the fixture nut (25) and pressing plate
(26) it carries out screwing connection, the calcium oxide U-tube A (5), phosphorus pentoxide U-tube A (6), phosphorus pentoxide U by screw thread
The side of type pipe B (13), phosphorus pentoxide U-tube C (14) and calcium oxide U-tube B (15) are provided with fixed anchor ear (7), institute
The one end for stating fixed anchor ear (7) is provided with fixing bolt (23), and one end of the fixing bolt (23) is provided with butterfly nut
(22)。
3. the measurement device of moisture in bromine according to claim 1, it is characterised in that: the measurement device shell (1)
Side be provided with cover board (19), the lower end of the cover board (19) is provided with inserted link (24), the one of the measurement device shell (1)
Side corresponds to the position setting jack of inserted link (24), and the side of the cover board (19) is provided with fixing buckle (21), the cover board (19)
It is fixedly connected with measurement device shell (1) by fixing buckle (21), and the connection of cover board (19) and measurement device shell (1)
Place is provided with sealing ring.
4. the measurement device of moisture in bromine according to claim 1, it is characterised in that: the phosphorus pentoxide U-tube B
(13), phosphorus pentoxide U-tube C (14) and bromine evaporative flask (9) are installed in the water-bath room (10) surrounded by thermal insulative board (8),
And concentrated sulfuric acid chamber (2), calcium oxide U-tube A (5), phosphorus pentoxide U-tube A (6), water-bath room (10), phosphorus pentoxide are U-shaped
Pipe B (13), phosphorus pentoxide U-tube C (14), calcium oxide U-tube B (15) and sodium hydroxide room (17) lower end be provided with row
Water pipe (11).
5. the measurement device of moisture in bromine according to claim 1, it is characterised in that: the upper end of the water-bath room (10)
Be provided with flip lid (20), and calcium oxide U-tube A (5) and phosphorus pentoxide U-tube A (6), phosphorus pentoxide U-tube B (13) and
Cover board (19) are provided on the outside of phosphorus pentoxide U-tube C (14) and calcium oxide U-tube B (15).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811361522.9A CN109342257A (en) | 2018-11-15 | 2018-11-15 | The measurement device of moisture in bromine |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811361522.9A CN109342257A (en) | 2018-11-15 | 2018-11-15 | The measurement device of moisture in bromine |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109342257A true CN109342257A (en) | 2019-02-15 |
Family
ID=65315790
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811361522.9A Pending CN109342257A (en) | 2018-11-15 | 2018-11-15 | The measurement device of moisture in bromine |
Country Status (1)
| Country | Link |
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| CN (1) | CN109342257A (en) |
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Application publication date: 20190215 |