CN109332693A - A kind of three-phase Ti of laser gain material manufacture2The heat treatment process of AlNb based alloy - Google Patents
A kind of three-phase Ti of laser gain material manufacture2The heat treatment process of AlNb based alloy Download PDFInfo
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- CN109332693A CN109332693A CN201811325719.7A CN201811325719A CN109332693A CN 109332693 A CN109332693 A CN 109332693A CN 201811325719 A CN201811325719 A CN 201811325719A CN 109332693 A CN109332693 A CN 109332693A
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B22F10/00—Additive manufacturing of workpieces or articles from metallic powder
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F10/00—Additive manufacturing of workpieces or articles from metallic powder
- B22F10/20—Direct sintering or melting
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
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- B22F10/00—Additive manufacturing of workpieces or articles from metallic powder
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- B22F10/64—Treatment of workpieces or articles after build-up by thermal means
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- B22F3/00—Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
- B22F3/24—After-treatment of workpieces or articles
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B33—ADDITIVE MANUFACTURING TECHNOLOGY
- B33Y—ADDITIVE MANUFACTURING, i.e. MANUFACTURING OF THREE-DIMENSIONAL [3-D] OBJECTS BY ADDITIVE DEPOSITION, ADDITIVE AGGLOMERATION OR ADDITIVE LAYERING, e.g. BY 3-D PRINTING, STEREOLITHOGRAPHY OR SELECTIVE LASER SINTERING
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- B22F3/00—Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
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Abstract
The invention discloses a kind of three-phase Ti of laser gain material manufacture2The heat treatment process of AlNb based alloy comprising following steps: laser gain material step 1: is manufactured into three-phase Ti2AlNb based alloy thin wall product, the thin wall product is put into heating furnace, with stove heating to 1100 DEG C, is kept the temperature 0.5-1h, is then cooled to room temperature;Step 2: being put into heating furnace for the thin wall product Jing Guo step 1, with stove heating to 920 DEG C, keeps the temperature 2h, is then cooled to room temperature;Step 3: the thin wall product Jing Guo step 2 is put into heating furnace, with stove heating to 800 DEG C, is kept the temperature 18-24h, is then cooled to room temperature.Present invention process makes material while keeping some strength, and plasticity, intensity and plasticity excellent combination property greatly improved, and manufactures three-phase Ti for laser gain material2The engineer application of AlNb based alloy provides technical foundation.
Description
Technical field
The invention belongs to metal material and preparation technical fields, and in particular to a kind of three-phase of laser gain material manufacture
Ti2The heat treatment process of AlNb based alloy.
Background technique
With the fast development of aeronautical and space technology, the demand of lightening fire resistant structural material increasingly increases.Ti2AlNb base
Alloy has the excellent property such as high specific strength, high-fracture toughness, high temperature and creep resistance as a kind of novel light high-temperature structural material
Can, compared to traditional nickel base superalloy (such as GH4169 alloy) can loss of weight 35% or so, have in fields such as aerospaces wide
Wealthy application prospect.
The part forming of the material is needed by multiple alloy melting, β phase region hammer cogging, threephase region or two-phase section at present
Forging or the multiple hot-working such as rolling, solid-solution and aging heat treatment, machining and welding and post weld heat treatment and heat treated
Journey causes the raw material of the alloy part and processing cost sufficiently expensive, and the development and production period is long, seriously constrains such high property
The application of energy material.
Laser gain material manufacturing technology has short development and production period, short route, quick response, formed flexible degree and integrated level
High technical characterstic and advantage obtain application breakthrough in terms of the direct forming of Ti alloy with high performance material parts in recent years, draw
Play extensive concern both domestic and external.With laser gain material manufacturing technology near-net forming Ti2AlNb based alloy components, are able to solve
Traditional molding methods bring a series of problems.
But the deposited Ti of laser gain material manufacturing technology preparation2AlNb based alloy tissue is markedly different from traditional forging
Tissue is made, coarse B2 phase crystal grain (more than 200 μm) leads to deposited Ti2AlNb based alloy plasticity is poor, is not able to satisfy reality
The demand of border application, it is therefore desirable to which one kind manufactures deposited three-phase Ti for laser gain material2The heat treatment process of AlNb based alloy,
Under the premise of meeting strength character, its plasticity is improved.
Summary of the invention
The purpose of the present invention is to provide one kind to manufacture three-phase Ti based on laser gain material2The heat treatment work of AlNb based alloy
Skill makes moulding material on the basis of proof strength performance, improves plasticity, manufactures three-phase Ti for laser gain material2AlNb based alloy
Practical application establish technical foundation.
To achieve the above object, the present invention takes following technical scheme:
A kind of laser gain material manufacture three-phase Ti2The heat treatment process of AlNb based alloy.The technique is in Ti2AlNb based alloy
The solid solution of the monophase field B2, eliminates the α in B2 matrix2Mutually and O phase, crystal boundary and transgranular there is a small amount of α in cooling procedure2Mutually generate;Subsequent B2
+ O two-phase section is kept the temperature, crystal boundary and transgranular α2It mutually remains, and part α in heat treatment process2Phase transition is O phase, the phase
Change process forms O phase in rich Nb element area along with the diffusion of Nb element.The concrete form of phase transformation is α2Mutually wrapped with B2 phase
Analysis reaction is changed into O phase.After heat treatment, B2 is transgranular in addition to α2Phase, there are also largely in grayish lath-shaped O phase, O phase size is big
It is small different.Large scale O phase is to retain after B2+O two-phase section high-temperature process, can be also precipitated after B2+O two-phase section low-temperature treatment a large amount of small
Size O phase forms double size tissues.Compared with deposited, matrix precipitate is grown up obviously, and Grain Boundary Precipitates width is suitable.
In the present invention, the three-phase Ti of laser gain material manufacture2The heat treatment process of AlNb based alloy the following steps are included:
Step 1: laser gain material is manufactured into three-phase Ti2The thin wall product is put into heating by AlNb based alloy thin wall product
In furnace, with stove heating to 1100 DEG C, 0.5-1h is kept the temperature, room temperature is then cooled to;
Step 2: the thin wall product Jing Guo step 1 is put into heating furnace, with stove heating to 920 DEG C, keeps the temperature 2h,
It is then cooled to room temperature;
Step 3: the thin wall product Jing Guo step 2 is put into heating furnace, with stove heating to 800 DEG C, keeps the temperature 18-
For 24 hours, then it is cooled to room temperature.
Further, the three-phase Ti2AlNb based alloy thin wall product has the Ti of laser gain material manufacture2AlNb based alloy
Deposited α2+ B2+O three-phase contexture.
Further, heating furnace used is chamber type electric resistance furnace in step 1, accuracy of temperature control ± 5 DEG C, heating rate is 10 DEG C/
Min, the type of cooling are air-cooled.
It being further limited as of the invention, heating furnace used is chamber type electric resistance furnace in step 2, accuracy of temperature control ± 5 DEG C,
Heating rate is 10 DEG C/min, and the type of cooling is air-cooled.
It being further limited as of the invention, heating furnace used is chamber type electric resistance furnace in step 3, accuracy of temperature control ± 5 DEG C,
Heating rate is 10 DEG C/min, and the type of cooling is air-cooled.
The beneficial effects of the present invention are:
A kind of laser gain material manufacture three-phase Ti is provided2The heat treatment process of AlNb based alloy, laser gain material manufacture three-phase
Ti2AlNb based alloy is after monophase field solution treatment, α2With O phase back dissolving into matrix, large scale O is formed after the processing of B2+O two-phase section
The double size tissues mutually coexisted with small size O phase.The α retained in alloy2Mutually be conducive to the promotion of alloy strength;Transgranular O phase is sent out
Apparent roughening is given birth to, phase interface reduces, weakens the strengthening effect of precipitated phase, increase passability when dislocation motion, make
Material is obtained while keeping some strength, plasticity, intensity and plasticity excellent combination property greatly improved.
Detailed description of the invention
Fig. 1 is the three-phase Ti of laser gain material manufacture2The heat treatment process flow chart of AlNb based alloy.
Fig. 2 is the three-phase Ti of laser gain material manufacture2The primary deposit state microstructure picture of AlNb based alloy.
Fig. 3 is the three-phase Ti of laser gain material manufacture2The heat treatment state optical microstructure photo of AlNb based alloy.
Fig. 4 is the three-phase Ti of laser gain material manufacture2The heat treatment state scanning electron microscope microstructure picture of AlNb based alloy.
Specific embodiment
The present invention will be further described in detail below with reference to the embodiments and the accompanying drawings.
Embodiment 1
A kind of three-phase Ti of laser gain material manufacture2The heat treatment process of AlNb based alloy, raw material use increasing material manufacturing α2+B2+
O three-phase Ti2AlNb based alloy thin-walled, having a size of 45mm (width) × 45mm (height) × 4mm (thickness).
The three-phase Ti of laser gain material manufacture2The heat treatment process of AlNb based alloy the following steps are included:
Step 1: the three-phase Ti that laser gain material is manufactured2AlNb based alloy thin-walled is put into heating furnace, extremely with stove heating
1100 DEG C, heating rate is 10 DEG C/min, keeps the temperature 1h, is then air-cooled to room temperature;
Step 2: the thin-walled Jing Guo step 1 is put into heating furnace, with stove heating to 920 DEG C, heating rate is 10 DEG C/
Min keeps the temperature 2h, is then air-cooled to room temperature;
Step 3: the thin-walled Jing Guo step 2 is put into heating furnace, with stove heating to 800 DEG C, heating rate is 10 DEG C/
Min, heat preservation for 24 hours, are then air-cooled to room temperature.
Embodiment 2
A kind of three-phase Ti of laser gain material manufacture2The heat treatment process of AlNb based alloy, raw material use increasing material manufacturing α2+B2+
O three-phase Ti2AlNb based alloy thin-walled, having a size of 50mm (width) × 50mm (height) × 4mm (thickness).
The three-phase Ti of laser gain material manufacture2The heat treatment process of AlNb based alloy the following steps are included:
Step 1: the three-phase Ti that laser gain material is manufactured2AlNb based alloy thin-walled is put into heating furnace, extremely with stove heating
1100 DEG C, heating rate is 10 DEG C/min, keeps the temperature 0.5h, is then air-cooled to room temperature;
Step 2: the thin-walled Jing Guo step 1 is put into heating furnace, with stove heating to 920 DEG C, heating rate is 10 DEG C/
Min keeps the temperature 2h, is then air-cooled to room temperature;
Step 3: the thin-walled Jing Guo step 2 is put into heating furnace, with stove heating to 800 DEG C, heating rate is 10 DEG C/
Min keeps the temperature 18h, is then air-cooled to room temperature.
Embodiment 3
A kind of three-phase Ti of laser gain material manufacture2The heat treatment process of AlNb based alloy, raw material use increasing material manufacturing α2+B2+
O three-phase Ti2AlNb based alloy thin-walled, having a size of 50mm (width) × 50mm (height) × 3mm (thickness).
The three-phase Ti of laser gain material manufacture2The heat treatment process of AlNb based alloy the following steps are included:
Step 1: the three-phase Ti that laser gain material is manufactured2AlNb based alloy thin-walled is put into heating furnace, extremely with stove heating
1100 DEG C, heating rate is 10 DEG C/min, keeps the temperature 0.5h, is then air-cooled to room temperature;
Step 2: the thin-walled Jing Guo step 1 is put into heating furnace, with stove heating to 920 DEG C, heating rate is 10 DEG C/
Min keeps the temperature 2h, is then air-cooled to room temperature;
Step 3: the thin-walled Jing Guo step 2 is put into heating furnace, with stove heating to 800 DEG C, heating rate is 10 DEG C/
Min, heat preservation for 24 hours, are then air-cooled to room temperature.
Three-phase deposited Ti2The microscopic structure of AlNb based alloy is as shown in Fig. 2, press the technological parameter of above three embodiments
The processed three-phase deposited Ti of method2The microscopic structure of AlNb based alloy is as shown in Figure 3, Figure 4.Its mechanical property reaches respectively
It arrives: 959MPa, 5.0%;962MPa, 4.9%;950MPa, 5.2%.Compared with deposited 1012MPa, 1.8% tensile property phase
Than intensity slightly declines, but maintains a higher level, and elongation percentage greatly improves, so that laser gain material manufactures three-phase
Ti2AlNb based alloy has the prospect of engineer application.
Technical solution of the present invention is described in detail in above-described embodiment.It is apparent that the present invention is not limited being retouched
The embodiment stated.Based on the embodiments of the present invention, those skilled in the art can also make a variety of variations accordingly, but appoint
What is equal with the present invention or similar variation shall fall within the protection scope of the present invention.
Claims (5)
1. a kind of three-phase Ti of laser gain material manufacture2The heat treatment process of AlNb based alloy, which comprises the following steps:
Step 1: laser gain material is manufactured into three-phase Ti2AlNb based alloy thin wall product, the thin wall product is put into heating furnace,
With stove heating to 1100 DEG C, 0.5-1h is kept the temperature, room temperature is then cooled to;
Step 2: being put into heating furnace for the thin wall product Jing Guo step 1, with stove heating to 920 DEG C, keeps the temperature 2h, then cold
But to room temperature;
Step 3: the thin wall product Jing Guo step 2 is put into heating furnace, with stove heating to 800 DEG C, keeps the temperature 18-24h,
Then it is cooled to room temperature.
2. technique according to claim 1, which is characterized in that the three-phase Ti2AlNb based alloy thin wall product has laser
The Ti of increasing material manufacturing2The deposited α of AlNb based alloy2+ B2+O three-phase contexture.
3. technique according to claim 1, which is characterized in that heating furnace used is chamber type electric resistance furnace, temperature control in step 1
Precision ± 5 DEG C, heating rate are 10 DEG C/min, and the type of cooling is air-cooled.
4. technique according to claim 1, which is characterized in that heating furnace used is chamber type electric resistance furnace, temperature control in step 2
Precision ± 5 DEG C, heating rate are 10 DEG C/min, and the type of cooling is air-cooled.
5. technique according to claim 1, which is characterized in that heating furnace used is chamber type electric resistance furnace, temperature control in step 3
Precision ± 5 DEG C, heating rate are 10 DEG C/min, and the type of cooling is air-cooled.
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110977108A (en) * | 2019-11-25 | 2020-04-10 | 北京理工大学 | Ti2Electric arc additive manufacturing method of AlNb-based alloy structural member and device used by same |
CN111826594A (en) * | 2020-07-30 | 2020-10-27 | 北京理工大学 | Heat treatment method for manufacturing high-strength titanium alloy through electric arc additive manufacturing and reinforced high-strength titanium alloy |
CN112410698A (en) * | 2020-11-03 | 2021-02-26 | 中国航发北京航空材料研究院 | Three-phase Ti2AlNb alloy multilayer structure uniformity control method |
CN112725712A (en) * | 2020-12-18 | 2021-04-30 | 北京钢研高纳科技股份有限公司 | Selective laser melting of Ti2Heat treatment method of AlNb-based alloy and product prepared by heat treatment method |
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110977108A (en) * | 2019-11-25 | 2020-04-10 | 北京理工大学 | Ti2Electric arc additive manufacturing method of AlNb-based alloy structural member and device used by same |
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CN112410698A (en) * | 2020-11-03 | 2021-02-26 | 中国航发北京航空材料研究院 | Three-phase Ti2AlNb alloy multilayer structure uniformity control method |
CN112725712A (en) * | 2020-12-18 | 2021-04-30 | 北京钢研高纳科技股份有限公司 | Selective laser melting of Ti2Heat treatment method of AlNb-based alloy and product prepared by heat treatment method |
CN112725712B (en) * | 2020-12-18 | 2021-09-14 | 北京钢研高纳科技股份有限公司 | Selective laser melting of Ti2Heat treatment method of AlNb-based alloy and product prepared by heat treatment method |
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Application publication date: 20190215 |