CN109331075A - A kind of preparation method reducing the flower concrete from generation to generation that fragrance is lost - Google Patents
A kind of preparation method reducing the flower concrete from generation to generation that fragrance is lost Download PDFInfo
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- 239000003205 fragrance Substances 0.000 title claims abstract description 49
- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 47
- 244000183685 Citrus aurantium Species 0.000 claims abstract description 36
- 235000007716 Citrus aurantium Nutrition 0.000 claims abstract description 36
- 239000012141 concentrate Substances 0.000 claims abstract description 28
- 238000001223 reverse osmosis Methods 0.000 claims abstract description 24
- 239000007788 liquid Substances 0.000 claims abstract description 16
- 239000006071 cream Substances 0.000 claims abstract description 15
- 239000012528 membrane Substances 0.000 claims abstract description 14
- 238000000034 method Methods 0.000 claims abstract description 11
- 230000008569 process Effects 0.000 claims abstract description 9
- 238000001816 cooling Methods 0.000 claims abstract description 8
- 238000001914 filtration Methods 0.000 claims abstract description 7
- 238000005374 membrane filtration Methods 0.000 claims abstract description 7
- 238000005119 centrifugation Methods 0.000 claims abstract description 6
- 239000000843 powder Substances 0.000 claims description 14
- 238000000605 extraction Methods 0.000 claims description 13
- 239000000706 filtrate Substances 0.000 claims description 12
- 238000011084 recovery Methods 0.000 claims description 7
- 239000000126 substance Substances 0.000 claims description 7
- 239000004744 fabric Substances 0.000 claims description 6
- 238000004519 manufacturing process Methods 0.000 claims description 6
- 239000000284 extract Substances 0.000 abstract description 3
- 230000009467 reduction Effects 0.000 abstract description 3
- 230000000694 effects Effects 0.000 abstract description 2
- 230000036571 hydration Effects 0.000 abstract description 2
- 238000006703 hydration reaction Methods 0.000 abstract description 2
- 238000009833 condensation Methods 0.000 abstract 1
- 230000005494 condensation Effects 0.000 abstract 1
- 235000013305 food Nutrition 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 239000002994 raw material Substances 0.000 description 3
- GLZPCOQZEFWAFX-UHFFFAOYSA-N Geraniol Chemical compound CC(C)=CCCC(C)=CCO GLZPCOQZEFWAFX-UHFFFAOYSA-N 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- QMVPMAAFGQKVCJ-UHFFFAOYSA-N citronellol Chemical compound OCCC(C)CCC=C(C)C QMVPMAAFGQKVCJ-UHFFFAOYSA-N 0.000 description 2
- 235000013399 edible fruits Nutrition 0.000 description 2
- XMGQYMWWDOXHJM-UHFFFAOYSA-N limonene Chemical compound CC(=C)C1CCC(C)=CC1 XMGQYMWWDOXHJM-UHFFFAOYSA-N 0.000 description 2
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 description 2
- 210000004185 liver Anatomy 0.000 description 2
- 230000001105 regulatory effect Effects 0.000 description 2
- 210000002784 stomach Anatomy 0.000 description 2
- NQPDZGIKBAWPEJ-UHFFFAOYSA-N valeric acid Chemical compound CCCCC(O)=O NQPDZGIKBAWPEJ-UHFFFAOYSA-N 0.000 description 2
- 239000000341 volatile oil Substances 0.000 description 2
- 239000001490 (3R)-3,7-dimethylocta-1,6-dien-3-ol Substances 0.000 description 1
- QMVPMAAFGQKVCJ-SNVBAGLBSA-N (R)-(+)-citronellol Natural products OCC[C@H](C)CCC=C(C)C QMVPMAAFGQKVCJ-SNVBAGLBSA-N 0.000 description 1
- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 description 1
- 239000001606 7-[(2S,3R,4S,5S,6R)-4,5-dihydroxy-6-(hydroxymethyl)-3-[(2S,3R,4R,5R,6S)-3,4,5-trihydroxy-6-methyloxan-2-yl]oxyoxan-2-yl]oxy-5-hydroxy-2-(4-hydroxyphenyl)chroman-4-one Substances 0.000 description 1
- 208000030090 Acute Disease Diseases 0.000 description 1
- 206010001497 Agitation Diseases 0.000 description 1
- 241000207199 Citrus Species 0.000 description 1
- 235000005976 Citrus sinensis Nutrition 0.000 description 1
- GLZPCOQZEFWAFX-YFHOEESVSA-N Geraniol Natural products CC(C)=CCC\C(C)=C/CO GLZPCOQZEFWAFX-YFHOEESVSA-N 0.000 description 1
- 239000005792 Geraniol Substances 0.000 description 1
- 206010019280 Heart failures Diseases 0.000 description 1
- 235000010254 Jasminum officinale Nutrition 0.000 description 1
- 240000005385 Jasminum sambac Species 0.000 description 1
- 241001093501 Rutaceae Species 0.000 description 1
- 241000270666 Testudines Species 0.000 description 1
- 244000269722 Thea sinensis Species 0.000 description 1
- 206010047700 Vomiting Diseases 0.000 description 1
- 210000001015 abdomen Anatomy 0.000 description 1
- JGQFVRIQXUFPAH-UHFFFAOYSA-N beta-citronellol Natural products OCCC(C)CCCC(C)=C JGQFVRIQXUFPAH-UHFFFAOYSA-N 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 230000017531 blood circulation Effects 0.000 description 1
- 230000001684 chronic effect Effects 0.000 description 1
- 235000000484 citronellol Nutrition 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 238000007596 consolidation process Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 229940113087 geraniol Drugs 0.000 description 1
- 235000001510 limonene Nutrition 0.000 description 1
- 229940087305 limonene Drugs 0.000 description 1
- 229930007744 linalool Natural products 0.000 description 1
- 239000012263 liquid product Substances 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- DFPMSGMNTNDNHN-ZPHOTFPESA-N naringin Chemical compound O[C@@H]1[C@H](O)[C@@H](O)[C@H](C)O[C@H]1O[C@H]1[C@H](OC=2C=C3O[C@@H](CC(=O)C3=C(O)C=2)C=2C=CC(O)=CC=2)O[C@H](CO)[C@@H](O)[C@@H]1O DFPMSGMNTNDNHN-ZPHOTFPESA-N 0.000 description 1
- 229940052490 naringin Drugs 0.000 description 1
- 229930019673 naringin Natural products 0.000 description 1
- ARGKVCXINMKCAZ-UZRWAPQLSA-N neohesperidin Chemical compound C1=C(O)C(OC)=CC=C1[C@H]1OC2=CC(O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O3)O[C@H]3[C@@H]([C@H](O)[C@@H](O)[C@H](C)O3)O)=CC(O)=C2C(=O)C1 ARGKVCXINMKCAZ-UZRWAPQLSA-N 0.000 description 1
- ARGKVCXINMKCAZ-UHFFFAOYSA-N neohesperidine Natural products C1=C(O)C(OC)=CC=C1C1OC2=CC(OC3C(C(O)C(O)C(CO)O3)OC3C(C(O)C(O)C(C)O3)O)=CC(O)=C2C(=O)C1 ARGKVCXINMKCAZ-UHFFFAOYSA-N 0.000 description 1
- 210000000653 nervous system Anatomy 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 230000005180 public health Effects 0.000 description 1
- 230000011514 reflex Effects 0.000 description 1
- 230000004206 stomach function Effects 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
- 210000002700 urine Anatomy 0.000 description 1
- 229940005605 valeric acid Drugs 0.000 description 1
- 230000008673 vomiting Effects 0.000 description 1
Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/75—Rutaceae (Rue family)
- A61K36/752—Citrus, e.g. lime, orange or lemon
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/51—Concentration
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/53—Liquid-solid separation, e.g. centrifugation, sedimentation or crystallization
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Botany (AREA)
- Mycology (AREA)
- Nutrition Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Medical Informatics (AREA)
- Animal Behavior & Ethology (AREA)
- Alternative & Traditional Medicine (AREA)
- Medicinal Chemistry (AREA)
- Microbiology (AREA)
- Pharmacology & Pharmacy (AREA)
- Epidemiology (AREA)
- Biotechnology (AREA)
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Abstract
The invention discloses a kind of preparation methods of flower concrete from generation to generation that reduction fragrance is lost, comprising the following steps: 1) crushes；2) it extracts, collects extracting solution and fragrance recycle-water；3) by extracting solution filtering, centrifugation, cooling；4) centrifugate after cooling, standing is collected into feed liquid using smart membrane filtration；5) feed liquid is subjected to reverse osmosis concentration, the RO water generated when collecting concentrate and reverse osmosis concentration；6) concentrate is concentrated in vacuo to obtain condensed cream, is collected simultaneously concentration condensed water；7) fragrance concentrate is concentrated to get using reverse osmosis membrane after fragrance recycle-water, RO water and concentration condensation hydration；8) fragrance concentrate is merged with the condensed cream of step 6), obtains flower concrete from generation to generation.The present invention reduces the fragrance loss in bitter orange flower process to greatest extent, improves the aroma effect of product.
Description
Technical field
The present invention relates to bitter orange flower field of deep, and in particular to a kind of preparation for reducing the flower concrete from generation to generation that fragrance is lost
Method.
Background technique
Bitter orange flower, alias: bitter orange, turn green orange, turtle turtle belong to Rutaceae, citrus plant.Dungarunga, branches and leaves are dense, thorn
It is more.It is dark green at the beginning of the fruit of bitter orange flower, it shows orange-yellow after mature, does not fall off to next year spring and summer and become dark green again, therefore have and " return
The title of green orange ".If maintenance is done in the proper way, fruit can harbor third year, and it is also known as " from generation to generation ".Bitter orange flower bud contain volatile oil, oil in
Mainly containing limonene, linalool, Geraniol, citronellol, valeric acid etc., still contain neohesperidin and naringin, there is heart tonifying, benefit
Urine, calm and reducing heart rate function, can reduce the excitability and spinal reflex hyperfunction of nervous system, for acute disease and
Chronic cardiac insufficiency.In Chinese medicine, bitter orange flower is sweet in flavor, slight bitter, soothing liver and harmonizing stomach, regulating the flow of vital energy and dispeling melancholy, cures mainly in the heart that ruffian is bored, stomach duct and abdomen is swollen
Bitterly, the few food of vomiting.It purifies the blood, promotes blood circulation, relax liver, stomach function regulating, qi-regulating have very high medical value.
2 months in 2002, it is both food and pharmaceutical raw material that the Ministry of Public Health, which formally announces bitter orange flower,.The application of bitter orange flower can be joined
It is executed according to the relevant criterion of food, market obviously rises the demand of bitter orange flower.
The application of China bitter orange flower, which is mainly still embodied in raw material as jasmine tea and brews and refine essential oil, at present uses, and deposits
In higher application limitation, application range is relatively narrow, improper a wide range of, food industrialization, scale utilization.Generation in the market
The deep processing of seville orange flower and the correlative study of extract also more lack.So developing a kind of good flower concrete from generation to generation of fragrance
Market demand degree with higher and wide application prospect.
Summary of the invention
It is existing for solving the purpose of the present invention is to provide a kind of preparation method of flower concrete from generation to generation that reduction fragrance is lost
There is the market vacancy of flower concrete from generation to generation, to improve the bitter orange flower related derivative competitiveness of product in market.
To achieve the goals above, the invention adopts the following technical scheme:
A kind of preparation method reducing the flower concrete from generation to generation that fragrance is lost comprising following steps:
1) bitter orange flower is crushed, is sieved, obtains bitter orange flower powder；
2) bitter orange flower powder investment three-level tank group extractor is extracted, every grade of extraction time is 30-35min, Extracting temperature
It is 93-95 DEG C, three-level obtains extracting solution after extracting；
Condensing recovery is carried out to the aroma substance of extraction process release simultaneously, obtains fragrance recycle-water；
3) extracting solution is filtered to and collected filtrate, then filtrate is centrifuged, then collect centrifugate and is cooled to not higher than 15
DEG C, it stands；
4) it uses membrane aperture for 20-25 μm of smart membrane filtration the centrifugate after cooling, standing, collects feed liquid；
5) above-mentioned feed liquid is subjected to reverse osmosis concentration, is concentrated into the concentrate of refractive power > 30%, production when being collected simultaneously reverse osmosis concentration
Raw RO water；
6) concentrate is concentrated in vacuo, is concentrated into the condensed cream of refractive power > 80%, be collected simultaneously vacuum Concentrating Process generation
Condensed water is concentrated；
7) by the fragrance recycle-water in step 2, the RO water in step 5) and the concentration condensed water in step 6) merge, and obtain
Mixed liquor, the mixed liquor are concentrated to get fragrance concentrate using reverse osmosis membrane；
8) the fragrance concentrate in step 7) is merged with the condensed cream of step 6), obtains flower concrete from generation to generation.
In step 1), the partial size of the bitter orange flower powder is 20-30 mesh.
In step 3), the filtering uses the filter cloth of 280-300 mesh, and the centrifugation uses tube centrifuge, centrifuge RPMs
For 4500-5500r/min, the time of repose is 25-35min.
In step 6), the temperature of the vacuum concentration is not higher than 80 DEG C.
In step 7), the mixed liquor is concentrated into the 10-15% of secondary concentration liquid product.
The invention has the following advantages: 1, bitter orange flower can become very soft very consolidation after extracting, it is easy to sink to the bottom and is compacted,
The present invention is extracted using three-level tank group extractor, is then slagged tap using horizontal centrifuge, and bitter orange flower raw material can be prevented stifled
Firmly liquid outlet helps preferably to go out liquid and improves the yield of product.2, the aroma substance that step 2 discharges extraction process
Condensing recovery is carried out, as far as possible reduction fragrance loss.3, the present invention uses secondary concentration mode, pre- dense using RO for the first time
For the second time using vacuum concentration thickening efficiency can be improved, and reduce total concentration time and high temperature section concentration time in contracting.4, originally
In invention preparation process, step 2 collects fragrance recycle-water, the RO water generated when collecting reverse osmosis concentration in step 5), step 7)
The middle concentration condensed water collecting vacuum Concentrating Process and generating, and condense fragrance recycle-water, RO water and concentration in final stage
Hydration simultaneously, is backfilled in condensed cream after reverse osmosis membrane is concentrated, obtains product flower concrete from generation to generation, the present invention is reduced to greatest extent
Fragrance loss in bitter orange flower process, improves the aroma effect of product.
Specific embodiment
A kind of preparation method reducing the flower concrete from generation to generation that fragrance is lost, comprising the following steps:
1) bitter orange flower is crushed, crosses -30 mesh screen of 20 mesh, obtains bitter orange flower powder；
2) bitter orange flower powder investment three-level tank group extractor is extracted, every grade of extraction time is 30-35min, Extracting temperature
It is 93-95 DEG C, three-level obtains extracting solution after extracting；
Condensing recovery is carried out to the aroma substance of extraction process release simultaneously, obtains fragrance recycle-water；
3) extracting solution by the filter-cloth filtering of 280-300 mesh and is collected into filtrate, then filtrate is centrifuged using tube centrifuge, from
Heart revolution is 4500-5500r/min, then collects centrifugate and is cooled to not higher than 15 DEG C, stands 25-35min；
4) it uses membrane aperture for 20-25 μm of smart membrane filtration the centrifugate after cooling, standing, collects feed liquid；
5) above-mentioned feed liquid is subjected to reverse osmosis concentration, is concentrated into the concentrate of refractive power > 30%, production when being collected simultaneously reverse osmosis concentration
Raw RO water (reverse osmosis water)；
6) concentrate is concentrated in vacuo under the conditions of being not higher than 80 DEG C, is concentrated into the condensed cream of refractive power > 80%, is collected simultaneously
The concentration condensed water that vacuum Concentrating Process generates；
7) by the fragrance recycle-water in step 2, the RO water in step 5) and the concentration condensed water in step 6) merge, and obtain
Mixed liquor, the mixed liquor are concentrated into the 10-15% of concentration paste volume using reverse osmosis membrane, obtain fragrance concentrate；
8) the fragrance concentrate in step 7) is merged with the condensed cream of step 6), obtains flower concrete from generation to generation.
Embodiment 1
A kind of preparation method reducing the flower concrete from generation to generation that fragrance is lost, comprising the following steps:
1) bitter orange flower is crushed, crosses 20 mesh screens, obtains bitter orange flower powder；
2) bitter orange flower powder investment three-level tank group extractor is extracted, every grade of extraction time is 30min, extracts duration in total
For 90min, Extracting temperature is 95 DEG C, and three-level obtains extracting solution after extracting；
Condensing recovery is carried out to the aroma substance of extraction process release simultaneously, obtains fragrance recycle-water；
3) extracting solution by the filter-cloth filtering of 300 mesh and is collected into filtrate, then filtrate is centrifuged using tube centrifuge, centrifugation turns
Number is 5000r/min, then collects centrifugate and is cooled to not higher than 15 DEG C, stands 30min；
4) it uses membrane aperture for 20 μm of smart membrane filtration the centrifugate after cooling, standing, collects feed liquid；
5) above-mentioned feed liquid is subjected to reverse osmosis concentration, is concentrated into the concentrate of refractive power > 30%, production when being collected simultaneously reverse osmosis concentration
Raw RO water；
6) concentrate is concentrated in vacuo under the conditions of being not higher than 80 DEG C, is concentrated into the condensed cream of refractive power > 80%, is collected simultaneously
The concentration condensed water that vacuum Concentrating Process generates；
7) by the fragrance recycle-water in step 2, the RO water in step 5) and the concentration condensed water in step 6) merge, and obtain
Mixed liquor, the mixed liquor are concentrated into the 10% of concentration paste volume using reverse osmosis membrane, obtain fragrance concentrate；
8) the fragrance concentrate in step 7) is merged with the condensed cream of step 6), obtains flower concrete from generation to generation.
Embodiment 2
A kind of preparation method reducing the flower concrete from generation to generation that fragrance is lost, comprising the following steps:
1) bitter orange flower is crushed, crosses 30 mesh screens, obtains bitter orange flower powder；
2) bitter orange flower powder investment three-level tank group extractor is extracted, every grade of extraction time is 35min, a length of when always extracting
105min, Extracting temperature are 93 DEG C, and three-level obtains extracting solution after extracting；
Condensing recovery is carried out to the aroma substance of extraction process release simultaneously, obtains fragrance recycle-water；
3) extracting solution by the filter-cloth filtering of 280 mesh and is collected into filtrate, then filtrate is centrifuged using tube centrifuge, centrifugation turns
Number is 4500r/min, then collects centrifugate and is cooled to not higher than 15 DEG C, stands 25min；
4) it uses membrane aperture for 25 μm of smart membrane filtration the centrifugate after cooling, standing, collects feed liquid；
5) above-mentioned feed liquid is subjected to reverse osmosis concentration, is concentrated into the concentrate of refractive power > 30%, production when being collected simultaneously reverse osmosis concentration
Raw RO water；
6) concentrate is concentrated in vacuo under the conditions of being not higher than 80 DEG C, is concentrated into the condensed cream of refractive power > 80%, is collected simultaneously
The concentration condensed water that vacuum Concentrating Process generates；
7) by the fragrance recycle-water in step 2, the RO water in step 5) and the concentration condensed water in step 6) merge, and obtain
Mixed liquor, the mixed liquor are concentrated into the 12.5% of concentration paste volume using reverse osmosis membrane, obtain fragrance concentrate；
8) the fragrance concentrate in step 7) is merged with the condensed cream of step 6), obtains flower concrete from generation to generation.
Embodiment 3
A kind of preparation method reducing the flower concrete from generation to generation that fragrance is lost, comprising the following steps:
1) bitter orange flower is crushed, crosses 20 mesh screens, obtains bitter orange flower powder；
2) bitter orange flower powder investment three-level tank group extractor is extracted, every grade of extraction time is 30min, a length of when always extracting
90min, Extracting temperature are 95 DEG C, and three-level obtains extracting solution after extracting；
Condensing recovery is carried out to the aroma substance of extraction process release simultaneously, obtains fragrance recycle-water；
3) extracting solution by the filter-cloth filtering of 280 mesh and is collected into filtrate, then filtrate is centrifuged using tube centrifuge, centrifugation turns
Number is 5500r/min, then collects centrifugate and is cooled to not higher than 15 DEG C, stands 35min；
4) it uses membrane aperture for 25 μm of smart membrane filtration the centrifugate after cooling, standing, collects feed liquid；
5) above-mentioned feed liquid is subjected to reverse osmosis concentration, is concentrated into the concentrate of refractive power > 30%, production when being collected simultaneously reverse osmosis concentration
Raw RO water；
6) concentrate is concentrated in vacuo under the conditions of being not higher than 80 DEG C, is concentrated into the condensed cream of refractive power > 80%, is collected simultaneously
The concentration condensed water that vacuum Concentrating Process generates；
7) by the fragrance recycle-water in step 2, the RO water in step 5) and the concentration condensed water in step 6) merge, and obtain
Mixed liquor, the mixed liquor are concentrated into the 15% of concentration paste volume using reverse osmosis membrane, obtain fragrance concentrate；
8) the fragrance concentrate in step 7) is merged with the condensed cream of step 6), obtains flower concrete from generation to generation.
Claims (5)
1. it is a kind of reduce fragrance be lost flower concrete from generation to generation preparation method, it is characterised in that: itself the following steps are included:
1) bitter orange flower is crushed, is sieved, obtains bitter orange flower powder；
2) bitter orange flower powder investment three-level tank group extractor is extracted, every grade of extraction time is 30-35min, Extracting temperature
It is 93-95 DEG C, three-level obtains extracting solution after extracting；
Condensing recovery is carried out to the aroma substance of extraction process release simultaneously, obtains fragrance recycle-water；
3) extracting solution is filtered to and collected filtrate, then filtrate is centrifuged, then collect centrifugate and is cooled to not higher than 15
DEG C, it stands；
4) it uses membrane aperture for 20-25 μm of smart membrane filtration the centrifugate after cooling, standing, collects feed liquid；
5) above-mentioned feed liquid is subjected to reverse osmosis concentration, is concentrated into the concentrate of refractive power > 30%, production when being collected simultaneously reverse osmosis concentration
Raw RO water；
6) concentrate is concentrated in vacuo, is concentrated into the condensed cream of refractive power > 80%, be collected simultaneously vacuum Concentrating Process generation
Condensed water is concentrated；
7) by the fragrance recycle-water in step 2, the RO water in step 5) and the concentration condensed water in step 6) merge, and obtain
Mixed liquor, the mixed liquor are concentrated to get fragrance concentrate using reverse osmosis membrane；
8) the fragrance concentrate in step 7) is merged with the condensed cream of step 6), obtains flower concrete from generation to generation.
2. a kind of preparation method for reducing the flower concrete from generation to generation that fragrance is lost according to claim 1, it is characterised in that: step
It is rapid 1) in, the partial size of the bitter orange flower powder is 20-30 mesh.
3. a kind of preparation method for reducing the flower concrete from generation to generation that fragrance is lost according to claim 1, it is characterised in that: step
It is rapid 3) in, it is described filtering use 280-300 mesh filter cloth, it is described centrifugation use tube centrifuge, centrifuge RPMs 4500-
5500r/min, the time of repose are 25-35min.
4. a kind of preparation method for reducing the flower concrete from generation to generation that fragrance is lost according to claim 1, it is characterised in that: step
It is rapid 6) in, the temperature of the vacuum concentration is not higher than 80 DEG C.
5. a kind of preparation method for reducing the flower concrete from generation to generation that fragrance is lost according to claim 1, it is characterised in that: step
It is rapid 7) in, the mixed liquor be concentrated into concentration paste volume 10-15%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811073862.1A CN109331075A (en) | 2018-09-14 | 2018-09-14 | A kind of preparation method reducing the flower concrete from generation to generation that fragrance is lost |
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| CN111053791A (en) * | 2019-12-27 | 2020-04-24 | 广东一方制药有限公司 | Method for extracting volatile components from Chinese medicinal materials |
| CN112022886A (en) * | 2019-12-27 | 2020-12-04 | 广东一方制药有限公司 | Preparation method of angelica sinensis extract, angelica sinensis formula granules and preparation method thereof |
| CN113337341A (en) * | 2021-06-07 | 2021-09-03 | 劲牌持正堂药业有限公司 | Method for comprehensively utilizing effective components and aroma of sweet osmanthus |
| CN113575723A (en) * | 2021-07-29 | 2021-11-02 | 山西振东五和健康科技股份有限公司 | Red bean and coix seed instant tea and preparation method and application thereof |
| CN114588231A (en) * | 2022-02-22 | 2022-06-07 | 山西振东五和医养堂股份有限公司 | Traditional Chinese medicine preparation with volatile aroma content and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111053791A (en) * | 2019-12-27 | 2020-04-24 | 广东一方制药有限公司 | Method for extracting volatile components from Chinese medicinal materials |
| CN112022886A (en) * | 2019-12-27 | 2020-12-04 | 广东一方制药有限公司 | Preparation method of angelica sinensis extract, angelica sinensis formula granules and preparation method thereof |
| CN113337341A (en) * | 2021-06-07 | 2021-09-03 | 劲牌持正堂药业有限公司 | Method for comprehensively utilizing effective components and aroma of sweet osmanthus |
| CN113575723A (en) * | 2021-07-29 | 2021-11-02 | 山西振东五和健康科技股份有限公司 | Red bean and coix seed instant tea and preparation method and application thereof |
| CN114588231A (en) * | 2022-02-22 | 2022-06-07 | 山西振东五和医养堂股份有限公司 | Traditional Chinese medicine preparation with volatile aroma content and preparation method thereof |
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