CN109330909A - Change colour lip gloss and preparation method thereof - Google Patents

Change colour lip gloss and preparation method thereof Download PDF

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Publication number
CN109330909A
CN109330909A CN201811505049.7A CN201811505049A CN109330909A CN 109330909 A CN109330909 A CN 109330909A CN 201811505049 A CN201811505049 A CN 201811505049A CN 109330909 A CN109330909 A CN 109330909A
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parts
discoloration
lip gloss
acid
unchanged
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不公告发明人
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Shenzhen Ou Keli Technology Co Ltd
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Shenzhen Ou Keli Technology Co Ltd
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
    • A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/31—Hydrocarbons
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36—Carboxylic acids; Salts or anhydrides thereof
    • A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
    • A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9789—Magnoliopsida [dicotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/001—Preparations for care of the lips
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/08—Anti-ageing preparations
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/42—Colour properties
    • A61K2800/43—Pigments; Dyes
    • A61K2800/438—Thermochromatic; Photochromic; Phototropic
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59—Mixtures
    • A61K2800/592—Mixtures of compounds complementing their respective functions
    • A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18

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  • Cosmetics (AREA)

Abstract

The present invention provides a kind of discoloration lip gloss, comprising: 65-90 parts of emollient, 13-18 parts of excipient, 0.3-2 parts of colorant, 0.02-1.0 parts of stabilizer, 0.5-6 parts of additive；Emollient is isohexadecane, octyl dodecanol, tridecanol trimellitate, two isostearic acid malates, ethylhexyl palmitate, isopropyl myristate, octanoic acid/certain herbaceous plants with big flowers acid glycerol three ester, three isostearate of polyglycereol -2-, pentaerythritol tetraoctyl stearate, isopropyl isostearate, jojoba ester, hydrogenation isobutene, any several combination in C30-45 alkyl cetearyl Dimethicone Crosspolymer；Colorant anthocyanidin；Stabilizer is any several combination in malic acid, natrium malicum, potassium malate, glutamic acid and lysine.The discoloration lip gloss has the characteristics that safe, obvious using stabilization, colourshifting process.The present invention also provides a kind of preparation methods of lip gloss that changes colour.

Description

Change colour lip gloss and preparation method thereof
Technical field
The present invention relates to cosmetic technical fields more particularly to a kind of discoloration lip gloss and preparation method thereof.
Background technique
Compared with facial skin, the skin of lip has the characteristics that: 1, than relatively thin；2, there is no sweat gland；3, there is no sebaceous glands；4, Poor barrier function.Since lip has the characteristics that these, so it is easy to drying, aging rate faster, is easy to lose bullet Property, lip profile become unintelligible, and lip is thinning, aging and tarnishes.Lip gloss is change indispensable in people's daily life Cosmetic can make the soft and moist gloss of lip after use, can not only make one lips and persistently keep moist and wet, while maintenance lip of releiving The bad phenomenons such as portion's skin and prevention lip are dry, peel, crack.The appearance and function of lip gloss are sent out constantly all the time Exhibition and variation, in order to meet the growing individual demand of people, the lip gloss with color changeable effect slowly enters people's The visual field.But its discoloration is mostly bromic acid red dye in currently marketed discoloration lip gloss, while discoloration, is had Certain dyeing effect, makeup removing is inconvenient, and entering in oral cavity accidentally also can cause adverse effect to body.On the other hand, at present The discoloration lip gloss problem unstable there is also color in the market, after use after a period of time, lotion appearance face Color can change, and colourshifting process can also fade away.
Summary of the invention
The present invention provides the discoloration lip gloss of a kind of safety, colour stable.
To solve the above-mentioned problems, the present invention provides a kind of discoloration lip gloss, press following mass parts group by following components At: 65-90 parts of emollient, 13-18 parts of excipient, 0.3-2 parts of colorant, 0.02-1.0 parts of stabilizer, 0.5-6 parts of additive； The emollient is isohexadecane, octyl dodecanol, tridecanol trimellitate, two isostearic acid malates, palmitinic acid Ethylhexyl, isopropyl myristate, octanoic acid/certain herbaceous plants with big flowers acid glycerol three ester, three isostearate of polyglycereol -2-, pentaerythrite four are different Stearate, isopropyl isostearate, jojoba ester, hydrogenation isobutene, C30-45 alkyl cetearyl polydimethylsiloxanes Any several combination in alkane cross-linked polymer；
The colorant is anthocyanidin；
The stabilizer is any several group in malic acid, natrium malicum, potassium malate, glutamic acid and lysine It closes.
The discoloration lip gloss realizes color changeable effect using anthocyanidin as colorant, makes the use of the discoloration lip gloss It is more safe and healthy；The discoloration of the discoloration lip gloss is controlled using organic acid, acylate or amino acid as stabilizer Journey makes the lotion colour stable of the discoloration lip gloss keep stablizing, quickly discoloration after smearing；Using polarity oil bigger than normal Rouge disperses the colorant and the stabilizer as emollient, forms stable oil-based system.
Further, the excipient be polyethylene, it is beeswax, microwax, candelila wax, paint pericarp wax, any in ceresine Several mixing.The excipient makes the discoloration lip gloss have certain shape.
Further, the additive includes preservative, essence and functional component, wherein the preservative is Ni Bo Tortoise beetle ester, propylben, any one or any several mixing in tocopherol acetate, for preventing the infection of microorganism And breeding, so that the discoloration lip gloss has certain shelf-life；The essence is bouquet type composition, Fruity type essence and food Any one in product type essence or any several mixing assign the discoloration lip gloss pleasant fragrance as flavouring agent； The functional component be allantoin, hydrolytic collagen, saualane, oriental cherry flower extract, ginseng root extract, calendula extract, Any one in apple seed extract, oil-soluble Sodium Hyaluronate or any several mixing, the addition of the functional component make Obtaining the discoloration lip gloss has the function of whitening, moisturizing, anti-aging, crease-resistant etc..
Further, the discoloration lip gloss includes following components:
Emollient: octyl dodecanol, tridecanol trimellitate, two isostearic acid malates, palm acid ethyl oneself Ester, isopropyl myristate, octanoic acid/certain herbaceous plants with big flowers acid glycerol three ester, three isostearate of polyglycereol -2-, hydrogenation isobutene, C30-45 alkane Base cetearyl Dimethicone Crosspolymer；
Excipient: polyethylene, beeswax, microwax；
Colorant: anthocyanidin；
Stabilizer: malic acid, natrium malicum, glutamic acid；
Additive: methylparaben, grape essence, oriental cherry flower extract, saualane.
Further, the discoloration lip gloss includes 80 parts of emollient, 1 part of colorant and 0.1 part of stabilizer,
The emollient includes 3 parts of octyl dodecanol, 2 parts of tridecanol trimellitate, two isostearic acid malates 10 parts, 7 parts of ethylhexyl palmitate, 25 parts of isopropyl myristate, octanoic acid/10 parts of certain herbaceous plants with big flowers acid glycerol three ester, polyglycereol -2- three 9 parts of isostearate, hydrogenation 8 parts of isobutene, 6 parts of Dimethicone Crosspolymer of C30-45 alkyl cetearyl；
The stabilizer includes 0.03 part of malic acid, 0.04 part of natrium malicum, 0.03 part of glutamic acid.
Further, the discoloration lip gloss includes 16 parts of excipient, and the excipient includes 9 parts of polyethylene, beeswax 4 Part, 3 parts of microwax.
Further, the discoloration lip gloss includes 4 parts of additive, and the additive includes 0.5 part of methylparaben, Portugal 0.5 part of grape essence, 2 parts of saualane, 1 part of oriental cherry flower extract.
The present invention also provides a kind of preparation methods of lip gloss that changes colour, comprising the following steps:
Step S1: being divided into two parts for emollient, and a part therein is mixed with stabilizer, is warming up to 85-90 DEG C, side Heating side is stirred to the stabilizer dissolved clarification, and about 30-40min obtains the first mixture；
Step S2: extracting anthocyanidin from purple sweet potato, and anthocyanidin is added in first mixture, and temperature keeps 75-80 DEG C, it heats while stirring to anthocyanidin dissolved clarification, about 30-40min, obtains the second mixture；
Step S3: being warming up to 100-110 DEG C for excipient, heats while stirring to dissolved clarification, about 15-20min, obtains Three mixtures；Emollient described in remaining another part and second mixture are mixed with the third mixture, temperature It is kept for 95-100 DEG C, heated while stirring to homogeneous, more 15-20min obtains the 4th mixture；
Step S4: the 4th mixture is cooled to 90-95 DEG C, and additive is added thereto, is heated while stirring To homogeneous, about 10-15min obtains the 5th mixture；
Step S5: the 5th mixture is injected in mold, is taken off after cooling 3-5min under the conditions of -10 DEG C Mould obtains the discoloration lip gloss.
Emollient is divided into two parts by the preparation method of the discoloration lip gloss, and a part therein is mixed with stabilizer It closes, it is pre-dispersed to stabilizer progress to obtain the first mixture, pre-dispersed obtain is carried out to anthocyanidin with first mixture To the second mixture, overcomes the stabilizer and the anthocyanidin is insoluble in the problems in grease.
Further, in step S1, that a part of described emollient mixed with the stabilizer includes the emollient The polarity of the middle biggish component of polarity, the stabilizer and anthocyanidin is larger, mixed with the stabilizer according to similar compatibility principle That a part of described emollient closed includes biggish group of timesharing of polarity in the emollient, it is easier to quickly be dispersed described steady Determine agent and anthocyanidin.
Further, in step S2, from purple sweet potato extract anthocyanidin method the following steps are included:
Step S2a: extractant being added into purple sweet potato powder, and mass fraction shared by ethyl alcohol is 60% in the extractant； The mass ratio of the purple sweet potato powder and extractant is 1:15-1:35；
Step S2b: the mixed solution of purple sweet potato powder and extractant is placed in 60 DEG C of environment and stands 2-3h；
Step S2c: the mixed solution after standing is filtered, and takes filtrate through being concentrated in vacuo to obtain after UF membrane Anthocyanidin powder.
Specific embodiment
It is clear in order to be more clear the purpose of the present invention, technical scheme and beneficial effects, below in conjunction with of the invention real The subordinate list in mode is applied, the technical solution in embodiment of the present invention is clearly and completely described, it is clear that described Embodiment is only some embodiments of the invention, rather than whole embodiments.Based on the embodiment party in the present invention Formula, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all belongs to In the scope of protection of the invention.
First embodiment
A kind of discoloration lip gloss is made of following components by following mass parts: 65-90 parts of emollient, excipient 13-18 Part, 0.3-2 parts of colorant, 0.02-1.0 parts of stabilizer, 0.5-6 parts of additive；It is characterized in that,
The emollient is isohexadecane, octyl dodecanol, tridecanol trimellitate, two isostearic acid malic acid Ester, ethylhexyl palmitate, isopropyl myristate, octanoic acid/certain herbaceous plants with big flowers acid glycerol three ester, three isostearate of polyglycereol -2-, season penta Tetrol pentaerythritol tetraisostearate, isopropyl isostearate, jojoba ester, hydrogenation isobutene, C30-45 alkyl cetearyl poly- two Any several combination in methylsiloxane cross-linked polymer；
The colorant is anthocyanidin；
The stabilizer is any several group in malic acid, natrium malicum, potassium malate, glutamic acid and lysine It closes.
The discoloration lip gloss realizes color changeable effect using anthocyanidin as colorant, makes the use of the discoloration lip gloss It is more safe and healthy；The discoloration of the discoloration lip gloss is controlled using organic acid, acylate or amino acid as stabilizer Journey makes the lotion colour stable of the discoloration lip gloss keep stablizing, quickly discoloration after smearing；Using polarity oil bigger than normal Rouge disperses the colorant and the stabilizer as emollient, forms stable oil-based system.
The excipient includes all wax.In the present embodiment, the excipient be polyethylene, beeswax, microwax, Candelila wax, paint pericarp wax, any several mixing in ceresine.
The additive includes preservative, essence and functional component.In the present embodiment, the preservative is Ni Bo Tortoise beetle ester, propylben, any one or any several mixing in tocopherol acetate, for preventing the infection of microorganism And breeding, so that the discoloration lip gloss has certain preservation term；The essence is bouquet type composition, Fruity type essence and food Any one in product type essence or any several mixing assign the discoloration lip gloss pleasant fragrance as flavouring agent； The functional component be allantoin, hydrolytic collagen, saualane, oriental cherry flower extract, ginseng root extract, calendula extract, Any one in apple seed extract, oil-soluble Sodium Hyaluronate or any several mixing, the addition of the functional component make Obtaining the discoloration lip gloss has the function of whitening, moisturizing, anti-aging, crease-resistant etc..
Specifically, in the present embodiment, the discoloration lip gloss is grouped as by the group of following mass parts:
80 parts of emollient: including 3 parts of octyl dodecanol, 2 parts of tridecanol trimellitate, two isostearic acid malates 10 parts, 7 parts of ethylhexyl palmitate, 25 parts of isopropyl myristate, octanoic acid/10 parts of certain herbaceous plants with big flowers acid glycerol three ester, polyglycereol -2- three 9 parts of isostearate, hydrogenation 8 parts of isobutene, 6 parts of Dimethicone Crosspolymer of C30-45 alkyl cetearyl；
1 part of colorant: including 1 part of anthocyanidin；
0.1 part of stabilizer: including 0.03 part of malic acid, 0.04 part of natrium malicum, 0.03 part of glutamic acid.
16 parts of excipient: including 9 parts of polyethylene, 4 parts of beeswax, 3 parts of microwax；
4 parts of additive: including 0.5 part of methylparaben, 0.5 part of grape essence, 2 parts of saualane, oriental cherry flower extract 1 Part.
The preparation method of the discoloration lip gloss, comprising the following steps:
Step S1: being divided into two parts for emollient, and a part therein is mixed with stabilizer, is warming up to 85-90 DEG C, side Heating side is stirred to the stabilizer dissolved clarification, and about 30-40min obtains the first mixture.
Preferably, that a part of described emollient mixed with the stabilizer include in the emollient polarity it is biggish The polarity of component, the stabilizer and anthocyanidin is larger, and according to similar compatibility principle, that mixed with the stabilizer is a part of The emollient includes biggish group of timesharing of polarity in the emollient, it is easier to quickly disperse the stabilizer and cyanine Element.Specifically, in the present embodiment, that a part of described emollient mixed with the stabilizer includes two isostearic acid apples 10 parts of tartaric acid ester, 3 parts of octyl dodecanol, 10 parts of isopropyl myristate.
Step S2: extracting anthocyanidin from purple sweet potato, and anthocyanidin is added in first mixture, and temperature keeps 75-80 DEG C, it heats while stirring to anthocyanidin dissolved clarification, about 30-40min, obtains the second mixture.
Specifically, from the method for extracting anthocyanidin in purple sweet potato the following steps are included: first into purple sweet potato powder extractant is added, Mass fraction shared by ethyl alcohol is 60% in the extractant, and the mass ratio of the purple sweet potato powder and extractant is 1:15 to 1: 25, in the present embodiment, the mass ratio of the purple sweet potato powder and extractant is 1:20；Secondly, by purple sweet potato powder and extractant Mixed solution be placed in 60 DEG C of environment and stand 2-3h；Finally, the mixed solution after standing is filtered, filtrate is taken to pass through It is concentrated in vacuo to obtain anthocyanidin powder after UF membrane.
Step S3: being warming up to 100-110 DEG C for excipient, heats while stirring to dissolved clarification, about 15-20min, obtains Three mixtures；Emollient described in remaining another part and second mixture are mixed with the third mixture, temperature It is kept for 95-100 DEG C, heated while stirring to homogeneous, more 15-20min obtains the 4th mixture.
Step S4: the 4th mixture is cooled to 90-95 DEG C, and additive is added thereto, is heated while stirring To homogeneous, about 10-15min obtains the 5th mixture.
Step S5: the 5th mixture is injected in mold, is taken off after cooling 3-5min under the conditions of -10 DEG C Mould obtains the discoloration lip gloss.
Emollient is divided into two parts by the preparation method of the discoloration lip gloss, and a part therein is mixed with stabilizer It closes, it is pre-dispersed to stabilizer progress to obtain the first mixture, pre-dispersed obtain is carried out to anthocyanidin with first mixture To the second mixture, overcomes the stabilizer and the anthocyanidin is insoluble in the problems in grease.
Second embodiment
A kind of discoloration lip gloss is grouped as by the group of following mass parts:
80 parts of emollient: including 3 parts of octyl dodecanol, 2 parts of tridecanol trimellitate, two isostearic acid malates 10 parts, 7 parts of ethylhexyl palmitate, 25 parts of isopropyl myristate, octanoic acid/10 parts of certain herbaceous plants with big flowers acid glycerol three ester, polyglycereol -2- three 9 parts of isostearate, hydrogenation 8 parts of isobutene, 6 parts of Dimethicone Crosspolymer of C30-45 alkyl cetearyl；
1 part of colorant: including 1 part of anthocyanidin；
0.1 part of stabilizer: including 0.1 part of malic acid.
16 parts of excipient: including 9 parts of polyethylene, 4 parts of beeswax, 3 parts of microwax；
4 parts of additive: including 0.5 part of methylparaben, 0.5 part of grape essence, 2 parts of saualane, oriental cherry flower extract 1 Part.
In the present embodiment, the preparation method of the discoloration lip gloss is identical with first embodiment.
Third embodiment
A kind of discoloration lip gloss is grouped as by the group of following mass parts:
80 parts of emollient: including 3 parts of octyl dodecanol, 2 parts of tridecanol trimellitate, two isostearic acid malates 10 parts, 7 parts of ethylhexyl palmitate, 25 parts of isopropyl myristate, octanoic acid/10 parts of certain herbaceous plants with big flowers acid glycerol three ester, polyglycereol -2- three 9 parts of isostearate, hydrogenation 8 parts of isobutene, 6 parts of Dimethicone Crosspolymer of C30-45 alkyl cetearyl；
1 part of colorant: including 1 part of anthocyanidin；
0.2 part of stabilizer: including 0.06 part of malic acid, 0.08 part of natrium malicum, 0.06 part of glutamic acid.
16 parts of excipient: including 9 parts of polyethylene, 4 parts of beeswax, 3 parts of microwax；
4 parts of additive: including 0.5 part of methylparaben, 0.5 part of grape essence, 2 parts of saualane, oriental cherry flower extract 1 Part.
In the present embodiment, the preparation method of the discoloration lip gloss is identical with first embodiment.
4th embodiment
A kind of discoloration lip gloss is grouped as by the group of following mass parts:
80 parts of emollient: including 3 parts of octyl dodecanol, 2 parts of tridecanol trimellitate, two isostearic acid malates 10 parts, 7 parts of ethylhexyl palmitate, 25 parts of isopropyl myristate, octanoic acid/10 parts of certain herbaceous plants with big flowers acid glycerol three ester, polyglycereol -2- three it is different 9 parts of stearate, hydrogenation 8 parts of isobutene, 6 parts of Dimethicone Crosspolymer of C30-45 alkyl cetearyl；
1 part of colorant: including 1 part of anthocyanidin；
16 parts of excipient: including 9 parts of polyethylene, 4 parts of beeswax, 3 parts of microwax；
4 parts of additive: including 0.5 part of methylparaben, 0.5 part of grape essence, 2 parts of saualane, oriental cherry flower extract 1 Part.
In the present embodiment, it is described discoloration lip gloss preparation method and first embodiment the difference is that: In present embodiment, the preparation method of the discoloration lip gloss does not include step S2.
5th embodiment
A kind of discoloration lip gloss is grouped as by the group of following mass parts:
80 parts of emollient: including 3 parts of octyl dodecanol, 2 parts of tridecanol trimellitate, two isostearic acid malates 10 parts, 7 parts of ethylhexyl palmitate, 25 parts of isopropyl myristate, octanoic acid/10 parts of certain herbaceous plants with big flowers acid glycerol three ester, polyglycereol -2- three 9 parts of isostearate, hydrogenation 8 parts of isobutene, 6 parts of Dimethicone Crosspolymer of C30-45 alkyl cetearyl；
1 part of colorant: including 1 part of anthocyanidin；
0.1 part of stabilizer: including 0.03 part of malic acid, 0.04 part of natrium malicum, 0.03 part of glutamic acid.
16 parts of excipient: including 9 parts of polyethylene, 4 parts of beeswax, 3 parts of microwax；
4 parts of additive: including 0.5 part of methylparaben, 0.5 part of grape essence, 2 parts of saualane, oriental cherry flower extract 1 Part.
In the present embodiment, it is described discoloration lip gloss preparation method be different from the first embodiment, specifically include with Lower step:
Step S1: being warming up to 100-110 DEG C for excipient, heats while stirring to dissolved clarification, about 15-20min；Thereto Emollient is added, temperature is kept for 95-100 DEG C, heats while stirring to clarification, about 15-20min, obtain the first mixture；
Step S2: extracting anthocyanidin from purple sweet potato, and anthocyanidin and stabilizer are added in first mixture, and temperature is protected 80-85 DEG C is held, is heated while stirring to anthocyanidin and stabilizer dissolved clarification, about 7-8h, the second mixture is obtained；
Step S3: second mixture is warming up to 90-95 DEG C, and additive is added thereto, is heated while stirring Until homogeneous, about 10-15min obtains third mixture；
Step S4: the third mixture is injected in mold, is taken off after 3-5 minutes cooling under the conditions of -10 DEG C Mould obtains the discoloration lip gloss.
The preparation method used time of discoloration lip gloss described in present embodiment is too long, not can guarantee in actual production process Production efficiency is not presently preferred embodiments of the present invention.
Comparative example
Certain commercially available discoloration lip gloss, composed of the following components:
Emollient: including C10-30 acid cholesterine/lanosterol mixed ester, diisooctadecanol malate, double-two glycerol More acyl group adipate esters -2, phytosterol/octyl dodecanol lauroyl glutamate ester, dimerization Asia oleyl alcohol dimerized linoleic acid ester, C20-40 alcohol, three isostearate of polyglycereol -2；
Colorant: including titanium dioxide, red 21, yellow 6 color lakes, bromic acid red；
Excipient: including beeswax, ceresine, polyethylene；
Additive: including tocopherol, decyl oxazolidone, Butylated Hydroxytoluene, essence, vanillic aldehyde, mango seed rouge, Seeds of Luffa cylindrica Oil.
Stability test
Take discoloration lip gloss prepared by first embodiment to the 5th embodiment and the commercially available discoloration lip gloss each 30；In 50 DEG C of high temperature, 45 DEG C of high temperature, -10 DEG C of low temperature, room temperature, LED light photograph, high/low temperature circulation (45 DEG C of high temperature and low temperature -10 DEG C each alternate cycles for 24 hours, the test under the test condition only carry out two weeks) etc. test in 8 weeks by a definite date is carried out under the conditions of six, often Lower 5 of a test condition, checks steadiness every other week.The steadiness is from lotion appearance color, lotion appearance Shape, lotion are smeared three dimensions such as color and are considered, if lotion appearance color is kept without significant change, lotion face shaping Completely there is apparent colourshifting process after (no to scratch), smearing, then has good stability.Due in daily life, the storage of lip gloss Deposit temperature generally at 0-35 DEG C or so, the low temperature of the rarely possible high temperature and -10 DEG C that can reach 50 DEG C.If by survey in one month It after examination, has good stability, then can guarantee the lower 1 year stability of routine use state；If after bimestrial test, It has good stability, then can guarantee the stability of 2-3 under routine use state.
1 first embodiment stability test result (lotion appearance color) of table
50 DEG C of high temperature 45 DEG C of high temperature - 10 DEG C of low temperature Room temperature LED light is shone High/low temperature circulation
1 week It is unchanged It is unchanged It is unchanged It is unchanged It is unchanged It is unchanged
2 weeks It is unchanged It is unchanged It is unchanged It is unchanged It is unchanged It is unchanged
3 weeks It is unchanged It is unchanged It is unchanged It is unchanged It is unchanged —
4 weeks It is unchanged It is unchanged It is unchanged It is unchanged It is unchanged —
6 weeks It is unchanged It is unchanged It is unchanged It is unchanged It is unchanged —
8 weeks It is unchanged It is unchanged It is unchanged It is unchanged It is unchanged —
2 first embodiment stability test result (lotion face shaping) of table
50 DEG C of high temperature 45 DEG C of high temperature - 10 DEG C of low temperature Room temperature LED light is shone High/low temperature circulation
1 week Completely Completely Completely Completely Completely Completely
2 weeks Completely Completely Completely Completely Completely Completely
3 weeks Completely Completely Completely Completely Completely —
4 weeks Completely Completely Completely Completely Completely —
6 weeks Completely Completely Completely Completely Completely —
8 weeks Slightly scratch Slightly scratch Completely Completely Completely —
3 first embodiment stability test result of table (smears color)
50 DEG C of high temperature 45 DEG C of high temperature - 10 DEG C of low temperature Room temperature LED light is shone High/low temperature circulation
1 week 3s discoloration 3s discoloration 3s discoloration 3s discoloration 3s discoloration 3s discoloration
2 weeks 3s discoloration 3s discoloration 3s discoloration 3s discoloration 3s discoloration 3s discoloration
3 weeks 3s discoloration 3s discoloration 3s discoloration 3s discoloration 3s discoloration —
4 weeks 3s discoloration 3s discoloration 3s discoloration 3s discoloration 3s discoloration —
6 weeks 3s discoloration 3s discoloration 3s discoloration 3s discoloration 3s discoloration —
8 weeks 3s discoloration 3s discoloration 3s discoloration 3s discoloration 3s discoloration —
4 second embodiment stability test result (lotion appearance color) of table
50 DEG C of high temperature 45 DEG C of high temperature - 10 DEG C of low temperature Room temperature LED light is shone High/low temperature circulation
1 week It is unchanged It is unchanged It is unchanged It is unchanged It is unchanged It is unchanged
2 weeks It is unchanged It is unchanged It is unchanged It is unchanged It is unchanged Slightly purpling
3 weeks It is unchanged It is unchanged It is unchanged It is unchanged It is unchanged —
4 weeks Slightly purpling It is unchanged It is unchanged It is unchanged It is unchanged —
6 weeks Purpling Slightly purpling It is unchanged It is unchanged It is unchanged —
8 weeks Purpling Purpling It is unchanged It is unchanged It is unchanged —
5 second embodiment stability test result (lotion face shaping) of table
50 DEG C of high temperature 45 DEG C of high temperature - 10 DEG C of low temperature Room temperature LED light is shone High/low temperature circulation
1 week Completely Completely Completely Completely Completely Completely
2 weeks Completely Completely Completely Completely Completely Completely
3 weeks Completely Completely Completely Completely Completely —
4 weeks Completely Completely Completely Completely Completely —
6 weeks Completely Completely Completely Completely Completely —
8 weeks Slightly scratch Slightly scratch Completely Completely Completely —
6 second embodiment stability test result of table (smears color)
7 third embodiment stability test result (lotion appearance color) of table
50 DEG C of high temperature 45 DEG C of high temperature - 10 DEG C of low temperature Room temperature LED light is shone High/low temperature circulation
1 week It is unchanged It is unchanged It is unchanged It is unchanged It is unchanged It is unchanged
2 weeks It is unchanged It is unchanged It is unchanged It is unchanged It is unchanged It is unchanged
3 weeks It is unchanged It is unchanged It is unchanged It is unchanged It is unchanged —
4 weeks It is unchanged It is unchanged It is unchanged It is unchanged It is unchanged —
6 weeks It is unchanged It is unchanged It is unchanged It is unchanged It is unchanged —
8 weeks It is unchanged It is unchanged It is unchanged It is unchanged It is unchanged —
8 third embodiment stability test result (lotion face shaping) of table
50 DEG C of high temperature 45 DEG C of high temperature - 10 DEG C of low temperature Room temperature LED light is shone High/low temperature circulation
1 week Completely Completely Completely Completely Completely Completely
2 weeks Completely Completely Completely Completely Completely It scratches
3 weeks Completely Completely Completely Completely Completely —
4 weeks Slightly scratch Completely Completely Completely Completely —
6 weeks It scratches Slightly scratch Completely Completely Completely —
8 weeks It scratches It scratches Completely Completely Completely —
9 third embodiment stability test result of table (smears color)
50 DEG C of high temperature 45 DEG C of high temperature - 10 DEG C of low temperature Room temperature LED light is shone High/low temperature circulation
1 week 10s discoloration 10s discoloration 10s discoloration 10s discoloration 10s discoloration 10s discoloration
2 weeks 10s discoloration 10s discoloration 10s discoloration 10s discoloration 10s discoloration 10s discoloration
3 weeks 10s discoloration 10s discoloration 10s discoloration 10s discoloration 10s discoloration —
4 weeks 10s discoloration 10s discoloration 10s discoloration 10s discoloration 10s discoloration —
6 weeks 10s discoloration 10s discoloration 10s discoloration 10s discoloration 10s discoloration —
8 weeks 10s discoloration 10s discoloration 10s discoloration 10s discoloration 10s discoloration —
The 4th embodiment stability test result (lotion appearance color) of table 10
50 DEG C of high temperature 45 DEG C of high temperature - 10 DEG C of low temperature Room temperature LED light is shone High/low temperature circulation
1 week It is unchanged It is unchanged It is unchanged It is unchanged It is unchanged Slightly purpling
2 weeks Slightly purpling It is unchanged It is unchanged It is unchanged It is unchanged Purpling
3 weeks Purpling Slightly purpling It is unchanged It is unchanged It is unchanged —
4 weeks Purpling Purpling Slightly purpling Slightly purpling Slightly purpling —
6 weeks Purpling Purpling Slightly purpling Slightly purpling Slightly purpling —
8 weeks Purpling Purpling Purpling Purpling Purpling —
The 4th embodiment stability test result (lotion face shaping) of table 11
50 DEG C of high temperature 45 DEG C of high temperature - 10 DEG C of low temperature Room temperature LED light is shone High/low temperature circulation
1 week Completely Completely Completely Completely Completely Completely
2 weeks Completely Completely Completely Completely Completely Completely
3 weeks Completely Completely Completely Completely Completely —
4 weeks Completely Completely Completely Completely Completely —
6 weeks Completely Completely Completely Completely Completely —
8 weeks Slightly scratch Slightly scratch Completely Completely Completely —
The 4th embodiment stability test result of table 12 (smears color)
13 comparative example stability test result (lotion appearance color) of table
50 DEG C of high temperature 45 DEG C of high temperature - 10 DEG C of low temperature Room temperature LED light is shone High/low temperature circulation
1 week It is unchanged It is unchanged It is unchanged It is unchanged It is unchanged It is unchanged
2 weeks It is unchanged It is unchanged It is unchanged It is unchanged It is unchanged It is unchanged
3 weeks It is unchanged It is unchanged It is unchanged It is unchanged It is unchanged —
4 weeks Slightly turn yellow Slightly turn yellow It is unchanged It is unchanged It is unchanged —
6 weeks Slightly turn yellow Slightly turn yellow It is unchanged It is unchanged It is unchanged —
8 weeks Turn yellow Turn yellow Slightly turn yellow Slightly turn yellow Slightly turn yellow —
14 comparative example stability test result (lotion face shaping) of table
50 DEG C of high temperature 45 DEG C of high temperature - 10 DEG C of low temperature Room temperature LED light is shone High/low temperature circulation
1 week Completely Completely Completely Completely Completely Completely
2 weeks Completely Completely Completely Completely Completely Slightly scratch
3 weeks Completely Completely Completely Completely Completely —
4 weeks Completely Completely Completely Completely Completely —
6 weeks Slightly scratch Slightly scratch Completely Completely Completely —
8 weeks It scratches It scratches Slightly scratch Completely Completely —
15 comparative example stability test result of table (smears color)
From table 1 and table 13 as can be seen that discoloration lip gloss provided by first embodiment of the invention is bimestrial in experience After test, the stabilization of lotion appearance color is still maintained；From table 3 and table 15 as can be seen that first embodiment of the invention is mentioned After undergoing bimestrial test apparent colourshifting process still can occur within 3s for the discoloration lip gloss of confession；To sum up, originally Discoloration lip gloss provided by invention first embodiment has good colour stability.
Contrast table 1, table 4 and 10, table 2, table 5 and table 11, table 3, table 6 and table 12, it can be seen that the stabilizer apple The compounding of acid, natrium malicum and glutamic acid has vital influence to the stability of the discoloration lip gloss.
Contrast table 1 and table 7, table 2 and table 8, table 3 and table 9, it can be seen that when the amount of the stabilizer is excessive, will lead to Coloring Time is too long, lotion face shaping bad stability.
The above content is just an example and description of the concept of the present invention, affiliated those skilled in the art Various modifications or additions are done to described specific embodiment or are substituted in a similar manner, without departing from hair Bright design or beyond the scope defined by this claim, is within the scope of protection of the invention.

Claims (10)

1. a kind of discoloration lip gloss is made of following components by following mass parts: 65-90 parts of emollient, 13-18 parts of excipient, 0.3-2 parts of colorant, 0.02-1.0 parts of stabilizer, 0.5-6 parts of additive；It is characterized in that,
The emollient is isohexadecane, octyl dodecanol, tridecanol trimellitate, two isostearic acid malates, palm fibre Palmitic acid acid ethylhexyl, isopropyl myristate, octanoic acid/certain herbaceous plants with big flowers acid glycerol three ester, three isostearate of polyglycereol -2-, pentaerythrite Pentaerythritol tetraisostearate, isopropyl isostearate, jojoba ester, hydrogenation isobutene, C30-45 alkyl cetearyl poly dimethyl Any several combination in Dimethicone Crosspolymer；
The colorant is anthocyanidin；
The stabilizer is any several combination in malic acid, natrium malicum, potassium malate, glutamic acid and lysine.
2. discoloration lip gloss according to claim 1, which is characterized in that the excipient is polyethylene, beeswax, crystallite Wax, candelila wax, paint pericarp wax, any several mixing in ceresine.
3. discoloration lip gloss according to claim 2, which is characterized in that the additive include preservative, essence and Functional component, wherein the preservative be methylparaben, propylben, in tocopherol acetate any one or appoint It anticipates several mixing；The essence be in bouquet type composition, Fruity type essence and food type essence any one or it is any several Mixing；The functional component is allantoin, hydrolytic collagen, saualane, oriental cherry flower extract, ginseng root extract, pot marigold Extract, apple seed extract, any one in oil-soluble Sodium Hyaluronate or any several mixing.
4. discoloration lip gloss according to claim 3, which is characterized in that composed of the following components:
Emollient: octyl dodecanol, tridecanol trimellitate, two isostearic acid malates, ethylhexyl palmitate, meat Isopropyl myristate, octanoic acid/certain herbaceous plants with big flowers acid glycerol three ester, three isostearate of polyglycereol -2-, hydrogenation isobutene, C30-45 alkyl whale Wax Stearyl dimethicone cross-linked polymer；
Excipient: polyethylene, beeswax, microwax；
Colorant: including anthocyanidin；
Stabilizer: malic acid, natrium malicum, glutamic acid；
Additive: methylparaben, grape essence, oriental cherry flower extract, saualane.
5. discoloration lip gloss according to claim 4, which is characterized in that including 80 parts of emollient, 1 part of colorant and steady Determine 0.1 part of agent,
The emollient include 3 parts of octyl dodecanol, 2 parts of tridecanol trimellitate, 10 parts of two isostearic acid malate, 7 parts of ethylhexyl palmitate, 25 parts of isopropyl myristate, octanoic acid/10 parts of certain herbaceous plants with big flowers acid glycerol three ester, the different tristearin of polyglycereol -2- three 9 parts of acid esters, hydrogenation 8 parts of isobutene, 6 parts of Dimethicone Crosspolymer of C30-45 alkyl cetearyl；
The stabilizer includes 0.03 part of malic acid, 0.04 part of natrium malicum, 0.03 part of glutamic acid.
6. discoloration lip gloss according to claim 4, which is characterized in that including 16 parts of excipient, the excipient includes 9 parts of polyethylene, 4 parts of beeswax, 3 parts of microwax.
7. discoloration lip gloss according to claim 4, which is characterized in that including 4 parts of additive, the additive includes Buddhist nun Moor 0.5 part of tortoise beetle ester, 0.5 part of grape essence, 2 parts of saualane, 1 part of oriental cherry flower extract.
8. a kind of preparation method for the lip gloss that changes colour, which comprises the following steps:
Step S1: being divided into two parts for emollient, and a part therein is mixed with stabilizer, is warming up to 85-90 DEG C, side heating While stirring to the stabilizer dissolved clarification, about 30-40min obtains the first mixture；
Step S2: extracting anthocyanidin from purple sweet potato, and anthocyanidin is added in first mixture, and temperature is kept for 75-80 DEG C, side Heating side is stirred to anthocyanidin dissolved clarification, about 30-40min, and the second mixture is obtained；
Step S3: being warming up to 100-110 DEG C for excipient, heats while stirring to dissolved clarification, about 15-20min, obtains third mixing Object；Emollient described in remaining another part and second mixture are mixed with the third mixture, temperature keeps 95- It 100 DEG C, heats while stirring to homogeneous, more 15-20min obtains the 4th mixture；
Step S4: the 4th mixture is cooled to 90-95 DEG C, and additive is added thereto, is heated while stirring to equal Phase, about 10-15min obtain the 5th mixture；
Step S5: the 5th mixture is injected in mold, is demoulded, is obtained after cooling 3-5min under the conditions of -10 DEG C To the discoloration lip gloss.
9. the preparation method of discoloration lip gloss according to claim 8, which is characterized in that in step S1, with the stabilization That a part of described emollient of agent mixing includes the biggish component of polarity in the emollient.
10. the preparation method of discoloration lip gloss according to claim 9, which is characterized in that in step S2, mentioned from purple sweet potato Take the method for anthocyanidin the following steps are included:
Step S2a: extractant being added into purple sweet potato powder, and mass fraction shared by ethyl alcohol is 60% in the extractant；It is described The mass ratio of purple sweet potato powder and extractant is 1:15-1:35；
Step S2b: the mixed solution of purple sweet potato powder and extractant is placed in 60 DEG C of environment and stands 2-3h；
Step S2c: the mixed solution after standing is filtered, and takes filtrate through being concentrated in vacuo to obtain cyanine after UF membrane Plain powder.
CN201811505049.7A 2018-12-10 2018-12-10 Change colour lip gloss and preparation method thereof Withdrawn CN109330909A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109953907A (en) * 2019-04-17 2019-07-02 中山市美源化妆品有限公司 A kind of temperature sensing color changing lipstick
CN113397995A (en) * 2021-05-25 2021-09-17 上海达尔威生物技术研发有限公司 Lip balm containing color-changing pigment and preparation method thereof

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Publication number Priority date Publication date Assignee Title
CN103181544A (en) * 2011-12-30 2013-07-03 深圳劲创生物技术有限公司 Stable anthocyanidin prepared by novel membrane separation technology and method
CN106806161A (en) * 2017-03-29 2017-06-09 珠海京工检测技术有限公司 One kind extracts kapok anthocyanidin and prepares color-changing lipstick and preparation method thereof
CN108888528A (en) * 2018-08-31 2018-11-27 广州铭泽恒基生物科技有限公司 A kind of color-changing lipstick and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103181544A (en) * 2011-12-30 2013-07-03 深圳劲创生物技术有限公司 Stable anthocyanidin prepared by novel membrane separation technology and method
CN106806161A (en) * 2017-03-29 2017-06-09 珠海京工检测技术有限公司 One kind extracts kapok anthocyanidin and prepares color-changing lipstick and preparation method thereof
CN108888528A (en) * 2018-08-31 2018-11-27 广州铭泽恒基生物科技有限公司 A kind of color-changing lipstick and preparation method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109953907A (en) * 2019-04-17 2019-07-02 中山市美源化妆品有限公司 A kind of temperature sensing color changing lipstick
CN113397995A (en) * 2021-05-25 2021-09-17 上海达尔威生物技术研发有限公司 Lip balm containing color-changing pigment and preparation method thereof

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