CN109317072A - Phosphate dihydrogen aluminum solution Preparation equipment - Google Patents

Phosphate dihydrogen aluminum solution Preparation equipment Download PDF

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Publication number
CN109317072A
CN109317072A CN201811218758.7A CN201811218758A CN109317072A CN 109317072 A CN109317072 A CN 109317072A CN 201811218758 A CN201811218758 A CN 201811218758A CN 109317072 A CN109317072 A CN 109317072A
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China
Prior art keywords
container
ring body
outer ring
lifting
shaft
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Granted
Application number
CN201811218758.7A
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Chinese (zh)
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CN109317072B (en
Inventor
张国栋
侯永建
崔维坤
冯延春
魏培文
郑训峰
王书言
王书志
于占军
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Shandong Yaohua Refractory Material Science & Technology Co Ltd
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Shandong Yaohua Refractory Material Science & Technology Co Ltd
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Priority to CN201811218758.7A priority Critical patent/CN109317072B/en
Publication of CN109317072A publication Critical patent/CN109317072A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B08CLEANING
    • B08BCLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
    • B08B9/00Cleaning hollow articles by methods or apparatus specially adapted thereto 
    • B08B9/02Cleaning pipes or tubes or systems of pipes or tubes
    • B08B9/023Cleaning the external surface
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00092Tubes

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Accessories For Mixers (AREA)

Abstract

Phosphate dihydrogen aluminum solution Preparation equipment belongs to the preparation technical field of chemical material solution.It is characterized by comprising rack, two cylindrical reaction vessels are set, and two reaction vessels are respectively the first container and second container, and first and second are respectively set in the first container and second container and stirs evenly device in the rack;The first container and the setting of the bottom sides of second container pass through the mutual connection of connection transverse tube;The first and second deflector holes are opened up respectively in the bottom of the first and second containers, are connected between first and second deflector hole by heat cycles pipe, series circulation power device and heating device on heat cycles pipe.Phosphate dihydrogen aluminum solution evenness made from equipment of the present invention is splendid and temperature control is accurate during heating, is not susceptible to dry pot phenomenon;And scale formation will not occur for equipment long-time service, enable following process process that can accurately hold the concentration of allotment solution, promote product goes out quality.

Description

Phosphate dihydrogen aluminum solution Preparation equipment
Technical field
The invention belongs to the preparation technical fields of chemical material solution, and in particular to a kind of preparation of phosphate dihydrogen aluminum solution is set It is standby.
Background technique
Phosphate dihydrogen aluminum solution is often used as the adhesive of refractory material, is mainly used for electrical industry, high temperature kiln, Re Chu Manage resistance furnace and electric insulation.It is also used for petroleum, chemical industry, shipbuilding and space technology etc.;It is alternatively arranged as inorganic coating with Organic coating is used cooperatively.The preparation process of traditional phosphate dihydrogen aluminum solution is as follows: in the reaction vessel of solution-preparation device Phosphoric acid is added, then adds water while stirring, then after heating heating, is slow added into aluminium hydroxide, adjusts pH value and control object The phosphate dihydrogen aluminum solution of normal concentration is made in the addition specific gravity of material.
The Preparation equipment of phosphate dihydrogen aluminum solution generally heats tanning, evenness difference and temperature control using traditional cooking stove type crucible Difficulty, the careless slightly easy dry pot phenomenon of generation;And traditional equipment long-time service fouling is serious, and following process process is enabled to be difficult to accurately The concentration for holding allotment solution, influence product goes out quality.
Summary of the invention
Technical problem to be solved by the invention is to provide a kind of phosphate dihydrogen aluminum solution Preparation equipment, can assist efficiently High-quality prepares phosphate dihydrogen aluminum solution.
The technical solution adopted by the present invention to solve the technical problems is: providing a kind of preparation of phosphate dihydrogen aluminum solution and sets It is standby, it is characterised in that including rack, two cylindrical reaction vessels to be set, and two reaction vessels are respectively first in the rack First and second are respectively set in the first container and second container and stirs evenly device for container and second container;The first container and The bottom sides setting of two containers passes through the mutual connection of connection transverse tube;The first He is opened up respectively in the bottom of the first and second containers Second deflector hole is connected between first and second deflector hole by heat cycles pipe, connects and follow on heat cycles pipe Ring power device and heating device.
Preferably, described first and second to stir evenly device include interior stirring wheel apparatus, magnetcisuspension lifting drive loop device and several The high patience silica gel of root stirs rope, it is described in stir wheel apparatus include shaft, rotating wheel wing is installed in the upper end of shaft intercalation reaction container, In the external installation settings lower ring body of rotating wheel wing, several lower part rope end fixation holes are set on lower ring body, the shaft is worn Driven pulley is installed in the lower end of reaction vessel out;Described first and second driven pulleies for stirring evenly device are connected by belt Drive pulley is connect, the drive pulley is mounted on runner driving motor.
Preferably, the magnetcisuspension lifting drive loop device includes inner ring body, outer ring body and left and right lifting guide pillar, it is described on Ring body is arranged in the reaction vessel, several top rope end fixation holes is arranged on inner ring body, the high patience silica gel stirs rope Both ends are separately fixed in the rope end fixation hole of upper and lower part;The left and right lifting guide pillar is vertically arranged in reaction vessel respectively In the rack of the left and right sides, the left and right arc-shaped guide rail frame that section is in " Contraband " shape is installed respectively in the lifting guide pillar of left and right, in left and right Outer ring body is installed in arc-shaped guide rail frame;The chamber wall of the reaction vessel is made of the non magnetic material of thin-walled;The inner ring body and It is respectively embedded into inside and outside magnetite in outer ring body, can be attracted each other by magnetic force between inner ring body and outer ring body;In left arc-shaped guide rail Outer ring switch motor and outer ring lifting motor are installed on frame or right arc-shaped guide rail frame;Pacify on the motor shaft of the outer ring switch motor Fill active friction wheel, the outer wall of the active friction wheel and outer ring body contacts with each other setting, when outer ring switch motor drives active When friction pulley rotates, it is able to drive outer ring body synchronous rotation, then drives inner ring body to rotate synchronously by magnetic attraction;The outer ring Installation lifting driving gear on the motor shaft of lifting motor, the longitudinally disposed rack gear on left riser guide or right riser guide, when When outer ring lifting motor drives lifting driving gear rotation, it is able to drive outer ring body and is moved up and down along left and right riser guide, simultaneously Drive inner ring body synchronization lifting mobile by magnetic attraction.
Preferably, the cycle power device is resistance to hot recycle pump.
Preferably, the cycle power device is arranged on the heat cycles pipe between the first container and heating device;Institute Heat cycles pipe is stated to be made of flexible material.
Preferably, the heating device includes high-performance heat exchanger, and the high-performance heat exchanger includes outer housing, in outer housing Inlet is arranged in left upper portion, and liquid outlet is arranged in the left lower of outer housing, diaphragm plate, the tabula are arranged in outer housing The inner space of outer housing is divided into mutually independent upper heat exchanging chamber and lower heat exchanging chamber by plate, is led on the right side of the setting of the right side of diaphragm plate Hole, the upper heat exchanging chamber and lower heat exchanging chamber pass through the mutual connection of right side through-hole;It is arranged in several " " shapes in outer housing and changes Heat pipe, the interior heat exchanger tube include upper lateral tube and lower transverse tubule, and the left side of upper lower transverse tubule is connected by arc cross over pipe, in diaphragm plate Left side open up several threading holes, the middle part of the arc cross over pipe passes through the left side that threading hole is fixed on diaphragm plate;It is described The right end of upper lateral tube is pierced by outer housing by outlet tube and connects medium storage tank, and the right end of lower transverse tubule is pierced by shell by inlet tube Body is simultaneously connected to medium storage tank by medium circulation pump.
Preferably, the heating device further includes upper and lower apparatus for eliminating sludge, and the upper and lower apparatus for eliminating sludge is separately mounted to On lower transverse tubule;The apparatus for eliminating sludge up and down respectively includes upper and lower drive shaft, and the upper and lower drive shaft passes through above and below respectively Mounting rack is mounted in inlet and liquid outlet;Installation settings is distinguished on driving upside down shaft drives runner;It is driving upside down Annular wave channel is set on the periphery wall of axis, caulking groove sliding block, hinged first folding of caulking groove sliding block are set in annular wave channel The front end of bar, the front end of hinged second pole in the rear end of first pole;Several cleaning sleeves are set on upper and lower transverse tube Tin, it is hinged by connecting rod between the cleaning sleeve of coaxial arrangement, it is arranged along the periphery wall bus of one of cleaning sleeve and is oriented to Sliding slot, the guide chute is interior to be arranged guide runner, and guide rod jack, the rear end of second pole is arranged on the guide runner It is inserted into guide rod jack;It is able to drive driving runner rotation by the liquid stream of inlet and liquid outlet, and drives to drive upside down and turn Axis rotation enables caulking groove sliding block move up and down along annular wave channel, and then the first pole is driven to bob and weave, and leads to season second Pole is bobbed and woven, thus enable cleaning sleeve can vertically transverse tube outer wall move back and forth cleaning tube wall incrustation.
Preferably, the funnel type strainer of the middle and lower part setting inversed taper platform shape open topped in reaction vessel, the funnel Several rectification holes are opened up on type strainer;The funnel type strainer is co-axially mounted with shaft, but funnel type strainer does not turn with shaft It is dynamic.
The innovation of the invention consists in that:
1, phosphate dihydrogen aluminum solution evenness made from equipment of the present invention is splendid and temperature control is accurate during heating, is not easy to send out Raw dry pot phenomenon;And scale formation will not occur for equipment long-time service, enable following process process that can accurately hold allotment molten The concentration of liquid, promote product goes out quality.
2, the present invention and dedicated unit achieve significant beneficial effect by experiment and batch lab scale, are suitable in the industry cycle It popularizes.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of solution-preparation device;
Fig. 2 is the portion the A enlarged drawing of Fig. 1;
Fig. 3 is the structural schematic diagram of high-performance heat exchanger;
Fig. 4 is the portion the B enlarged drawing of Fig. 3;
Fig. 5 is the interior structural schematic diagram for stirring wheel apparatus;
Wherein: 1, the first container;2, funnel type strainer;3, rotating wheel wing;4, lower ring body;5, shaft;6, driven pulley;7, Resistance to hot recycle pump;8, inlet tube;9, upper lateral tube;10, outer housing;11, outlet tube;12, threading hole;13, lower transverse tubule;14, tabula Plate;15, liquid outlet;16, lower apparatus for eliminating sludge;17, upper apparatus for eliminating sludge;18, arc cross over pipe;19, heat cycles pipe;20, rack; 21, inlet;22, right lifting guide pillar;23, initiative driver;24, runner driving motor;25, connection transverse tube;26, second holds Device;27, high patience silica gel stirs rope;28, inner ring body;29, left lifting guide pillar;30, the chamber wall of reaction vessel;31, right arc is led Rail gantry;32, active friction wheel;33, outer ring switch motor;34,;35, outer ring lifting motor;36, driving gear is gone up and down;37, outer Ring body;38, connecting rod;39, sleeve is cleaned;40, annular wave channel;41, upper drive shaft;42, runner is driven;43, the first pole; 44, the second pole;45, guide runner;46, guide chute;47, lower part rope end fixation hole.
Specific embodiment
As shown in Figure 1, a kind of phosphate dihydrogen aluminum solution Preparation equipment of the present invention, including rack, in the rack Two cylindrical reaction vessels are set, and two reaction vessels are respectively the first container and second container, in the first container and second First and second are respectively set in container and stirs evenly device;The first container and the setting of the bottom sides of second container pass through connection transverse tube Mutual connection;The first and second deflector holes, first and second deflector hole are opened up respectively in the bottom of the first and second containers Between be connected by heat cycles pipe, series circulation power device and heating device on heat cycles pipe.
Described first and second, which stir evenly device, stirs wheel apparatus, magnetcisuspension lifting drive loop device and several high patience including interior Silica gel stirs rope, it is described in stir wheel apparatus include shaft, rotating wheel wing is installed in the upper end of shaft intercalation reaction container, in rotating wheel The external installation settings lower ring body of wing, is arranged several lower part rope end fixation holes on lower ring body, and the shaft is pierced by reaction and holds The lower end of device is installed by driven pulley;Described first and second driven pulleies for stirring evenly device connect active skin by belt Belt wheel, the drive pulley are mounted on runner driving motor;
As shown in Fig. 2, the magnetcisuspension lifting drive loop device includes inner ring body, outer ring body and left and right lifting guide pillar, the upper ring Body is arranged in the reaction vessel, several top rope end fixation holes is arranged on inner ring body, the high patience silica gel stirs the two of rope End is separately fixed in the rope end fixation hole of upper and lower part;The left and right lifting guide pillar is vertically arranged in a left side for reaction vessel respectively In the rack of right two sides, the left and right arc-shaped guide rail frame that section is in " Contraband " shape is installed respectively in the lifting guide pillar of left and right, in left and right arc Outer ring body is installed in shape guide rail bracket;The chamber wall of the reaction vessel is made of the non magnetic material of thin-walled;The inner ring body and outer It is respectively embedded into inside and outside magnetite in ring body, can be attracted each other by magnetic force between inner ring body and outer ring body;In left arc-shaped guide rail frame Or outer ring switch motor and outer ring lifting motor are installed on right arc-shaped guide rail frame;It is installed on the motor shaft of the outer ring switch motor The outer wall of active friction wheel, the active friction wheel and outer ring body contacts with each other setting, actively rubs when outer ring switch motor drives When wiping wheel rotation, it is able to drive outer ring body synchronous rotation, then drives inner ring body to rotate synchronously by magnetic attraction;The outer ring liter Installation lifting driving gear, the longitudinally disposed rack gear on left riser guide or right riser guide, when outer on the motor shaft of motor drop When ring lifting motor drives lifting driving gear rotation, it is able to drive outer ring body and is moved up and down along left and right riser guide, led to simultaneously Crossing magnetic attraction drives inner ring body synchronization lifting mobile.
The cycle power device is resistance to hot recycle pump.
It is arranged on the heat cycles pipe between the first container and heating device in the cycle power device;The heating Circulation pipe is made of flexible material.
As shown in figure 3, the heating device includes high-performance heat exchanger, the high-performance heat exchanger includes outer housing, in shell Inlet is arranged in the left upper portion of body, and liquid outlet is arranged in the left lower of outer housing, diaphragm plate is arranged in outer housing, described The inner space of outer housing is divided into mutually independent upper heat exchanging chamber and lower heat exchanging chamber by diaphragm plate, is arranged on the right side of diaphragm plate right Side through hole, the upper heat exchanging chamber and lower heat exchanging chamber pass through the mutual connection of right side through-hole;Several " " shapes are set in outer housing Interior heat exchanger tube, the interior heat exchanger tube include upper lateral tube and lower transverse tubule, and the left side of upper lower transverse tubule is connected by arc cross over pipe, in cross Several threading holes are opened up on the left of partition, the middle part of the arc cross over pipe passes through the left side that threading hole is fixed on diaphragm plate; The right end of the upper lateral tube is pierced by outer housing by outlet tube and connects medium storage tank, and the right end of lower transverse tubule is pierced by by inlet tube Outer housing is simultaneously connected to medium storage tank by medium circulation pump.
As shown in figure 4, the heating device further includes upper and lower apparatus for eliminating sludge, the upper and lower apparatus for eliminating sludge is separately mounted to On upper lower transverse tubule;The apparatus for eliminating sludge up and down respectively includes upper and lower drive shaft, the upper and lower drive shaft pass through respectively it is upper, Lower mounting rack is mounted in inlet and liquid outlet;Installation settings is distinguished on driving upside down shaft drives runner;It is driving up and down Annular wave channel is set on the periphery wall of moving axis, caulking groove sliding block, the caulking groove sliding block hinged first are set in annular wave channel The front end of pole, the front end of hinged second pole in the rear end of first pole;Several cleaning sleeves are set on upper and lower transverse tube Tin, it is hinged by connecting rod between the cleaning sleeve of coaxial arrangement, it is arranged along the periphery wall bus of one of cleaning sleeve and is oriented to Sliding slot, the guide chute is interior to be arranged guide runner, and guide rod jack, the rear end of second pole is arranged on the guide runner It is inserted into guide rod jack;It is able to drive driving runner rotation by the liquid stream of inlet and liquid outlet, and drives to drive upside down and turn Axis rotation enables caulking groove sliding block move up and down along annular wave channel, and then the first pole is driven to bob and weave, and leads to season second Pole is bobbed and woven, thus enable cleaning sleeve can vertically transverse tube outer wall move back and forth cleaning tube wall incrustation.
The funnel type strainer of middle and lower part setting inversed taper platform shape open topped in reaction vessel, on the funnel type strainer Open up several rectification holes;The funnel type strainer is co-axially mounted with shaft, but funnel type strainer is not rotated with shaft.
The present apparatus is using, and phosphoric acid is added in sequence in the first container, and aluminium hydroxide is then added successively, and starting turns Wheel drive motor enables runner driving motor is forward and reverse alternately and repeatedly to rotate 60-180 degree, thus drives lower ring body synchronization action;Together Shi Qidong outer ring switch motor enables it that active friction wheel is driven to carry out forward and reverse alternately and repeatedly rotation 60-180 degree, thus rubs Outer ring body synchronization action is driven, outer ring body passes through magnetic power drive inner ring body synchronization action.Enable lower ring body and inner ring body same as a result, Step rotates backward, and drives high patience silica gel to stir rope torsional shear formula, to stir evenly the material in the first container.Material dispensing finishes Afterwards, that is, start resistance to hot recycle pump, after enabling the liquid material in the first container heat by high-performance heat exchanger, along by heat cycles pipe Into in second container.Since the bottom of second container is connected by connection transverse tube with the first container, linker structure is formed, it can The liquid level of the two is enabled to keep horizontal consistent.
The working principle of the high-performance heat exchanger is as follows: thermal medium stores in medium storage tank, can be in medium storage tank In preset heater and temperature detector, accurately to control the temperature of thermal medium.Thermal medium by accurate temperature adjustment is along by feed liquor Pipe enters in the upper lateral tube of outer housing, and along by upper lateral tube flow simultaneously with by inlet enter upper heat exchanging chamber preparation solution into Row contact heat-exchanging enables and prepares solution realization heating heating;Solution is prepared to enter in lower heat exchanging chamber by threading hole;And thermal medium Along by arc cross over pipe entering lower transverse tubule, and enables in lower transverse tubule and to prepare solution and further exchange heat heating.By high-performance heat exchanger The configuration solution of heating is suitable to be entered in second container by heat cycles pipe, then enters the first container along by connection transverse tube, completes one A heat cycles.The thermal medium that heat exchange is completed in upper and lower heat exchanging chamber is returned in medium storage tank by outlet tube again.
It should be pointed out that above embodiment is only the preferred embodiment of the invention, for the common of the art For technical staff, under the premise of meeting working principle of the present invention, any equivalent or similar replacement each falls within of the invention In protection scope.

Claims (8)

1. a kind of phosphate dihydrogen aluminum solution Preparation equipment, it is characterised in that including rack, two cylindrical shapes are arranged in the rack Reaction vessel, two reaction vessels are respectively the first container and second container, are respectively set in the first container and second container First and second stir evenly device;The first container and the setting of the bottom sides of second container pass through the mutual connection of connection transverse tube;? One and the bottom of second container open up the first and second deflector holes respectively, followed between first and second deflector hole by heating Endless tube is connected, series circulation power device and heating device on heat cycles pipe.
2. a kind of phosphate dihydrogen aluminum solution Preparation equipment according to claim 1, it is characterised in that described first and second Stirring evenly device includes that interior wheel apparatus, magnetcisuspension lifting drive loop device and several high patience silica gel of stirring stirs rope, and the interior wheel that stirs fills It sets including shaft, rotating wheel wing, the ring under the external installation settings of rotating wheel wing is installed in the upper end of shaft intercalation reaction container Body, is arranged several lower part rope end fixation holes on lower ring body, and the shaft is pierced by the lower end installation follower belt of reaction vessel Wheel;Described first and second driven pulleies for stirring evenly device connect drive pulley, the drive pulley by belt It is mounted on runner driving motor.
3. a kind of phosphate dihydrogen aluminum solution Preparation equipment according to claim 2, it is characterised in that the magnetcisuspension lifting is dynamic Power loop device includes inner ring body, outer ring body and left and right lifting guide pillar, and the upper ring body is arranged in the reaction vessel, in inner ring body Upper several top rope end fixation holes of setting, it is solid that the both ends that the high patience silica gel stirs rope are separately fixed at upper and lower part rope end Determine in hole;In the rack for the left and right sides that the left and right lifting guide pillar is vertically arranged in reaction vessel respectively, in left and right, lifting is led The left and right arc-shaped guide rail frame that section is in " Contraband " shape is installed respectively on column, outer ring body is installed in the arc-shaped guide rail frame of left and right;It is described anti- The chamber wall of container is answered to be made of the non magnetic material of thin-walled;Inside and outside magnetite, inner ring are respectively embedded into the inner ring body and outer ring body It can be attracted each other by magnetic force between body and outer ring body;Outer ring switch is installed on left arc-shaped guide rail frame or right arc-shaped guide rail frame Motor and outer ring lifting motor;Active friction wheel is installed on the motor shaft of the outer ring switch motor, the active friction wheel with The outer wall of outer ring body contacts with each other setting, and when outer ring switch motor drives active friction wheel rotation, it is same to be able to drive outer ring body Step rotation, then drives inner ring body to rotate synchronously by magnetic attraction;Installation lifting master on the motor shaft of the outer ring lifting motor Moving gear, the longitudinally disposed rack gear on left riser guide or right riser guide, when outer ring lifting motor drives lifting driving gear It when rotation, is able to drive outer ring body and is moved up and down along left and right riser guide, while inner ring body synchronization lifting is driven by magnetic attraction It is mobile.
4. a kind of phosphate dihydrogen aluminum solution Preparation equipment according to claim 3, it is characterised in that the circulation power dress It is set to resistance to hot recycle pump.
5. a kind of phosphate dihydrogen aluminum solution Preparation equipment according to claim 4, it is characterised in that the circulation power dress It installs on the heat cycles pipe between the first container and heating device;The heat cycles pipe is made of flexible material.
6. a kind of phosphate dihydrogen aluminum solution Preparation equipment according to claim 5, it is characterised in that the heating device packet High-performance heat exchanger is included, the high-performance heat exchanger includes outer housing, inlet is arranged in the left upper portion of outer housing, in outer housing Liquid outlet is arranged in left lower, diaphragm plate is arranged in outer housing, the inner space of outer housing is divided into mutually by the diaphragm plate Independent upper heat exchanging chamber and lower heat exchanging chamber, the through-hole on the right side of the setting of the right side of diaphragm plate, the upper heat exchanging chamber and lower heat exchanging chamber are logical Cross the right side mutual connection of through-hole;Heat exchanger tube in several " " shapes is set in outer housing, and the interior heat exchanger tube includes upper lateral tube And lower transverse tubule, the left side of upper lower transverse tubule are connected by arc cross over pipe, several threading holes are opened up on the left of diaphragm plate, it is described The middle part of arc cross over pipe passes through the left side that threading hole is fixed on diaphragm plate;The right end of the upper lateral tube is pierced by outer by outlet tube Shell connects medium storage tank, and the right end of lower transverse tubule is pierced by outer housing by inlet tube and is connected to medium storage by medium circulation pump Deposit tank.
7. a kind of phosphate dihydrogen aluminum solution Preparation equipment according to claim 6, it is characterised in that the heating device is also Including upper and lower apparatus for eliminating sludge, the upper and lower apparatus for eliminating sludge is separately mounted on lower transverse tubule;The apparatus for eliminating sludge difference up and down Including upper and lower drive shaft, the upper and lower drive shaft passes through upper and lower mounting rack respectively and is mounted in inlet and liquid outlet; Installation settings is distinguished on driving upside down shaft drives runner;Annular wave channel is set on the periphery wall for drive upside down axis, Caulking groove sliding block, the front end of hinged first pole of caulking groove sliding block, the rear end hinge of first pole are set in annular wave channel Connect the front end of the second pole;It is set with several cleaning sleeves on upper and lower transverse tube, passes through company between the cleaning sleeve of coaxial arrangement Bar is hinged, and guide chute is arranged along the periphery wall bus of one of cleaning sleeve, guide runner is arranged in the guide chute, Guide rod jack is set on the guide runner, and the rear end of second pole is inserted into guide rod jack;Pass through inlet and liquid out The liquid stream of mouth is able to drive driving runner rotation, and drives and drive upside down shaft rotation, enables along the annular wave channel in caulking groove sliding block edge Lower movement, and then the first pole is driven to bob and weave, logical the second pole of season is bobbed and woven, to enable cleaning sleeve Can vertically transverse tube outer wall move back and forth cleaning tube wall incrustation.
8. a kind of phosphate dihydrogen aluminum solution Preparation equipment according to claim 7, it is characterised in that in reaction vessel The funnel type strainer of inversed taper platform shape open topped is arranged in middle and lower part, opens up several rectification holes on the funnel type strainer;It is described Funnel type strainer is co-axially mounted with shaft, but funnel type strainer is not rotated with shaft.
CN201811218758.7A 2018-10-19 2018-10-19 Aluminum dihydrogen phosphate solution preparation equipment Active CN109317072B (en)

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