CN109307781A - Adjustable full-automatic sample injector, the elemental analyser for varying position - Google Patents

Adjustable full-automatic sample injector, the elemental analyser for varying position Download PDF

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Publication number
CN109307781A
CN109307781A CN201811523142.0A CN201811523142A CN109307781A CN 109307781 A CN109307781 A CN 109307781A CN 201811523142 A CN201811523142 A CN 201811523142A CN 109307781 A CN109307781 A CN 109307781A
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CN
China
Prior art keywords
sample
hole location
telescopic rod
rotation axis
power system
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Application number
CN201811523142.0A
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Chinese (zh)
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CN109307781B (en
Inventor
林丽
李以康
樊博
郭小伟
柯浔
曹广民
李玉林
李茜
杜岩功
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Northwest Institute of Plateau Biology of CAS
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Northwest Institute of Plateau Biology of CAS
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N35/00Automatic analysis not limited to methods or materials provided for in any single one of groups G01N1/00 - G01N33/00; Handling materials therefor
    • G01N35/10Devices for transferring samples or any liquids to, in, or from, the analysis apparatus, e.g. suction devices, injection devices

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  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

The present invention provides a kind of adjustable full-automatic sample injectors for varying position, comprising: disk body, N number of hole location, N root telescopic rod, sample running track, electromagnetic power system and rotation axis;Wherein, disk body is for carrying electromagnetic power system and rotation axis;N number of hole location arranges to form at least two injection annulus, and in the operating condition, all hole locations of one of injection annulus are located in sample running track, and all hole locations of other injection annulus are located on respective sample position;For every telescopic rod, one end of telescopic rod and rotation axis connection, the other end are fixedly connected with a hole location, and telescopic rod drives hole location rotation when rotating around rotation axis;Under the action of electromagnetic power system, telescopic rod can be stretched or be shunk, and realize position switching of the hole location between sample position and sample running track.The present invention can guarantee 24 hours whole day automatic runnings of elemental analyser, meet the timeliness of sample measurement, improve work efficiency.

Description

Adjustable full-automatic sample injector, the elemental analyser for varying position
Technical field
The present invention relates to organic element analysis technical field, more particularly to a kind of adjustable full-automatic sample injector for varying position, Elemental analyser.
Background technique
In terrestrial ecosystems, soil organic matter and nitrogen are the important components of the soil organism, it is the ecosystem Connect soil, plant, animal and microorganism important tie, for promote plant growth, increase soil fertility, protect environment, Promote the sustainable development of agricultural environment to play a significant role, is to pay close attention to one of highest index of power in current agrology research.
Organic carbon is measured in agrology and the conventional method of total nitrogen content is respectively potassium bichromate titrimetric method and kjeldahl determination Method, its advantage is that at low cost, the disadvantage is that it is cumbersome, expend it is a large amount of it is artificial, random error is big, be unfavorable for the quick of great amount of samples Measurement.With the fast development of analysis instrument, carbon nitrogen schema elements analyzer is increasingly used in SOIL CARBON AND NITROGEN content Measurement, existing elemental analyser are limited (80 hole locations) by sample introduction position on sample injection disc, and the time of continuous automatic running has Limit, data output efficiency is limited, cannot achieve the quick measurement requirement of high-volume, variable quality sample on instrument line.
Summary of the invention
(1) technical problems to be solved
In view of above-mentioned technical problem, the present invention provides a kind of adjustable full-automatic sample injector, elemental analysers for varying position. The present invention improves the sample injector of sample, meets the timeliness of sample measurement, provides working efficiency.
(2) technical solution
According to an aspect of the invention, there is provided a kind of adjustable full-automatic sample injector for varying position, comprising: disk body, N number of Hole location, N root telescopic rod, sample running track, electromagnetic power system and rotation axis;Wherein,
Disk body is for carrying electromagnetic power system and rotation axis;
N number of hole location arranges to form at least two injection annulus, in the operating condition, all hole location positions of one of injection annulus In sample running track, all hole locations of other injection annulus are located on respective sample position;
For every telescopic rod, one end of telescopic rod and rotation axis connection, the other end are fixedly connected with a hole location, telescopic rod Hole location rotation is driven when around rotation axis rotation;
Under the action of electromagnetic power system, telescopic rod can be stretched or be shunk, and realize that hole location is transported in sample position and sample Position switching between row track.
In certain embodiments of the present invention, electromagnetic power system includes 2N electromagnetic coil, solenoid valve and controller, Wherein each electromagnetic coil has electric current access point, and every two electromagnetic coil is located in the inner cavity of a telescopic rod, and sets relatively It sets, the stretching, extension or contraction of solenoid valve control telescopic rod, controller controls the operation of electromagnetic power system.
In certain embodiments of the present invention, telescopic rod includes outer bar and interior bar, and outer bar and rotation axis connection, outer bar have One cavity, two electromagnetic coils are located in the inner cavity, and one end of interior bar is socketed in the inner cavity, and the end of interior bar connects it In an electromagnetic coil, the other end of interior bar connects hole location, and interior bar can be reciprocating along the inner cavity.
In certain embodiments of the present invention, outer bar also has a bar portion, one end of bar portion and rotation axis connection, the other end It is socketed in the inner cavity, and the end of bar portion connects another electromagnetic coil.
In certain embodiments of the present invention, N number of hole location arranges to form two injection annulus.
According to another aspect of the present invention, additionally provide a kind of elemental analyser, including as described above automatically into Sample device, each injection annulus are in turn located in sample running track in different time sections, and the hole location in each injection annulus, which surrounds, to be turned Moving axis rotation, so that the sample in hole location enters in elemental analyser.
In certain embodiments of the present invention, elemental analyser continues 24 hours automatic runnings incessantly.
(3) beneficial effect
It can be seen from the above technical proposal that the adjustable full-automatic sample injector for varying position of the present invention, elemental analyser are at least Have the advantages that the present invention by the way that multiple injection annulus are arranged, enables elemental analyser to complete 24 hours whole days automatic Operation meets the timeliness of sample measurement, improves work efficiency.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the adjustable full-automatic sample injector for varying position of the embodiment of the present invention.
Fig. 2 is the structural schematic diagram of electromagnetic coil of the embodiment of the present invention and telescopic rod.
[main element]
10- disk body;
20- telescopic rod;
21- first segment;
22- second segment;
23- interconnecting piece;
30- sample running track;
40- electromagnetic power system;
50- rotation axis;
60- electromagnetic coil;
70- hole location.
Specific embodiment
To make the objectives, technical solutions, and advantages of the present invention clearer, below in conjunction with specific embodiment, and reference Attached drawing, the present invention is described in more detail.
First embodiment:
In the present embodiment, a kind of adjustable full-automatic sample injector for varying position is provided.As shown in Figure 1, the present invention is adjustable The full-automatic sample injector for varying position includes: disk body 10, N number of hole location 70, N number of telescopic rod 20, sample running track 30, electromagnetic power System 40 and a rotation axis 50.
N number of arrangement of hole location 70 forms two injection annulus, is divided into the first ring and the second ring, and all hole locations are located at same put down On face, such as each injection annulus has 80 hole locations, and what the stain in Fig. 1 represented is unillustrated hole location, is filled in hole location 70 There is sample, when hole location 70 rotates in sample running track 30, the sample in hole location 70, which is admitted in elemental analyser, to be carried out Elemental analysis.One end of telescopic rod 20 is connect with rotation axis 50, and the other end is fixedly connected with a hole location 70, and telescopic rod 20, which surrounds, to be turned The rotation of hole location 70 is driven when moving axis 50 rotates;Under the action of electromagnetic power system 40, realize hole location 70 in sample position and sample Switching between running track 30, also, all hole locations 70 of the first ring are located at respective sample position or sample running track simultaneously 30, all hole locations 70 of the second ring are located at respective sample position or sample running track 30 simultaneously.As hole location 70 in the first ring When in sample running track 30, the hole location 70 of the second ring is located on respective sample position;When the hole location 70 of the second ring is located at sample When in running track 30, the hole location 70 of the first ring is located on respective sample position.
Disk body 10 can be column structure, for carrying electromagnetic power system 40.
Electromagnetic power system 40 includes 2N electromagnetic coil 60, solenoid valve and controller, and every 2 electromagnetic coils 60 are located at In one telescopic rod 20, the hole location 70 of the first ring of solenoid valve control or the hole location 70 of the second ring are stretched or are shunk simultaneously, control The operation of device control electromagnetic power system 40 processed.
It should be noted that two electromagnetic coils 60 in each telescopic rod 20 are oppositely arranged, i.e. two electromagnetic wires The axis of circle 60 is parallel to each other, it is preferable that the axis of two electromagnetic coils 60 is located on the same line.
As shown in Fig. 2, telescopic rod 20 includes first segment 21, second segment 22, and first segment 21 is connect with second segment 22 Interconnecting piece 23, one end of first segment 21 connect with rotation axis 50, and the other end connects an electromagnetic coil 60, one end of second segment 22 Another electromagnetic coil 60 is connected, the other end connects a hole location 70, and two electromagnetic coils 60 are opposite, and respectively connect with electric current Access point, interconnecting piece 23 is between first segment 21 and second segment 22, and second segment 22 can back and forth be transported along interconnecting piece 23 It is dynamic.For example, interconnecting piece 23 is a box-shaped shell, two electromagnetic coils 60 are located in shell, and second segment 22 passes through the hole on shell It is inserted into shell.
The magnetic pole for changing two electromagnetic coils 60 by changing the current direction in electromagnetic coil 60, using identical charges repel each other There is a natural attraction between the sexes, realizes the reciprocating motion of each telescopic rod 20.For example, in the first state, all hole locations 70 of the first ring are located at In sample running track 30, all hole locations 70 of the second ring are located on respective sample position, and in the second condition, the first ring owns Hole location 70 is located on respective sample position, and all hole locations 70 of the second ring are located in sample running track 30, when needs are by the first shape When state is switched over to the second state, the controller of electromagnetic power system 40 changes the current direction in electromagnetic coil 60, a side The magnetic pole for two electromagnetic coils 60 in telescopic rod 20 that face connects the hole location 70 of the first ring is identical, at this time the hole of the first ring All telescopic rods 20 that position 70 is connected stretch, so that hole location 70 is released sample running track 30;On the other hand make the second ring The telescopic rod 20 that is connected of hole location 70 in the magnetic poles of two electromagnetic coils 60 repel each other, the hole location 70 of the second ring is connected at this time All telescopic rods 20 shrink, so that hole location 70 is retracted sample running track 30.
It should be noted that being above exemplary illustration, the present embodiment is not limited to this.N number of hole location, which is arranged, to be formed Injection annulus can be two incessantly, and the hole location 70 of one of injection annulus is retracted sample operation rail using electromagnetic power system 70 Road, other injection annulus hole locations 70 are respectively positioned on respective sample position.Telescopic rod 20 can not have first segment 21, interconnecting piece 23 and electromagnetism The rotation axis connection of dynamical system 40, is not especially limited this, as long as it is reciprocating to can be realized second segment 22.
By above structure, under the action of electromagnetic power system 40, realize the hole location 70 in each injection annulus in sample position With the switching between sample running track 30 so that each injection annulus is in turn located at sample running track 30 in different time sections In, the hole location 70 in each injection annulus is rotated around rotation axis 50, so that the sample in hole location 70 enters in elemental analyser, by Can guarantee 24 hours whole day automatic runnings of elemental analyser in the position of sample in total of multiple injection annulus, meet sample measurement when Effect property, improves work efficiency.
So far, attached drawing is had been combined the present embodiment is described in detail.According to above description, those skilled in the art There should be clear understanding to adjustable full-automatic sample injector, the elemental analyser for varying position of the present invention.
It should be noted that in attached drawing or specification text, the implementation for not being painted or describing is affiliated technology Form known to a person of ordinary skill in the art, is not described in detail in field.In addition, the above-mentioned definition to each element and method is simultaneously It is not limited only to various specific structures, shape or the mode mentioned in embodiment, those of ordinary skill in the art can carry out letter to it It singly changes or replaces.
It should also be noted that, the direction term mentioned in embodiment, for example, "upper", "lower", "front", "rear", " left side ", " right side " etc. is only the direction with reference to attached drawing, the protection scope being not intended to limit the invention.
It should be noted that the above-mentioned embodiments illustrate rather than limit the invention, and ability Field technique personnel can be designed alternative embodiment without departing from the scope of the appended claims.In the claims, Any reference symbol between parentheses should not be configured to limitations on claims.Word "comprising" does not exclude the presence of not Element or step listed in the claims.Word "a" or "an" located in front of the element does not exclude the presence of multiple such Element.The present invention can be by means of including the hardware of several different elements and being come by means of properly programmed computer real It is existing.In the unit claims listing several devices, several in these devices can be through the same hardware branch To embody.The use of word first, second, and third does not indicate any sequence.These words can be explained and be run after fame Claim.
It should be noted that running through attached drawing, identical element is indicated by same or similar appended drawing reference.In the following description, Some specific embodiments are used for description purposes only, and should not be construed to the present invention has any restrictions, and only the present invention is real Apply the example of example.When may cause the understanding of the present invention and cause to obscure, conventional structure or construction will be omitted.It should be noted that figure In the shape and size of each component do not reflect actual size and ratio, and only illustrate the content of the embodiment of the present invention.
Particular embodiments described above has carried out further in detail the purpose of the present invention, technical scheme and beneficial effects It describes in detail bright, it should be understood that the above is only a specific embodiment of the present invention, is not intended to restrict the invention, it is all Within the spirit and principles in the present invention, any modification, equivalent substitution, improvement and etc. done should be included in guarantor of the invention Within the scope of shield.

Claims (7)

1. a kind of adjustable full-automatic sample injector for varying position characterized by comprising disk body (10), N number of hole location (70), N root are stretched Contracting bar (20), sample running track (30), electromagnetic power system (40) and rotation axis (50);Wherein,
The disk body (10) is for carrying the electromagnetic power system (40) and the rotation axis (50);
N number of hole location (70) arrangement forms at least two injection annulus, in the operating condition, all holes of one of injection annulus Position (70) is located in the sample running track (30), and all hole locations (70) of other injection annulus are located on respective sample position;
For every telescopic rod (20), one end of telescopic rod (20) is connect with the rotation axis (50), and the other end is fixedly connected with one A hole location (70), telescopic rod (20) drive hole location (70) rotation when rotating around the rotation axis (50);
Under the action of the electromagnetic power system (40), telescopic rod (20) can be stretched or be shunk, and realize that hole location (70) exist Position switching between the sample position and the sample running track (30).
2. full-automatic sample injector according to claim 1, which is characterized in that the electromagnetic power system (40) includes 2N Electromagnetic coil (60), solenoid valve and controller, wherein each electromagnetic coil (60) has electric current access point, every two electromagnetic wire Circle (60) is located in the inner cavity of a telescopic rod (20), and is oppositely arranged, the stretching, extension or receipts of solenoid valve control telescopic rod (20) Contracting, controller control the operation of electromagnetic power system (40).
3. full-automatic sample injector according to claim 2, which is characterized in that the telescopic rod (20) includes outer bar and interior Bar, the outer bar are connect with the rotation axis (50), and the outer bar has a cavity, and two electromagnetic coils (60) are located at the inner cavity In, one end of interior bar is socketed in the inner cavity, and the end of interior bar connects one of electromagnetic coil (60), interior bar it is another End connection hole location (70), interior bar can be reciprocating along the inner cavity.
4. full-automatic sample injector according to claim 3, which is characterized in that the outer bar also has a bar portion, bar portion One end is connect with the rotation axis (50), and the other end is socketed in the inner cavity, and the end of bar portion connects another electromagnetic wire It encloses (60).
5. full-automatic sample injector according to claim 1, which is characterized in that N number of hole location (70) arrangement forms two Injection annulus.
6. a kind of elemental analyser, which is characterized in that including full-automatic sample injector as described in any one in claim 1-5, often A injection annulus is in turn located in the sample running track (30) in different time sections, and the hole location (70) in each injection annulus is enclosed It is rotated around the rotation axis (50), so that the sample in hole location (70) enters in the elemental analyser.
7. elemental analyser according to claim 6, which is characterized in that the elemental analyser continues 24 hours uninterruptedly Ground automatic running.
CN201811523142.0A 2018-12-13 2018-12-13 Full-automatic sample injector with changeable sample position and element analyzer Active CN109307781B (en)

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Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201751665U (en) * 2010-07-08 2011-02-23 西北工业大学 Multi-head sample support for electromagnetic suspension
CN202093003U (en) * 2011-06-21 2011-12-28 青岛盛瀚色谱技术有限公司 Ion chromatography sample introduction device
CN102749467A (en) * 2012-07-18 2012-10-24 镡丰锦 Full-automatic inspection device of urinalysis test paper belts with batch packaging function
CN103439137A (en) * 2013-08-28 2013-12-11 中国水产科学研究院南海水产研究所 Separable type sample incoming disc mechanism used in element analyzer
CN203432985U (en) * 2013-01-23 2014-02-12 中国科学院寒区旱区环境与工程研究所 Solid sampling disc directly applied to automatic sampler of elemental analyzer
CN204374156U (en) * 2014-12-17 2015-06-03 天津市环境监测中心 A kind of chromatography of ions automatic sampler
CN205193086U (en) * 2015-12-11 2016-04-27 北京先驱威锋技术开发公司 Retractable sample transition system
CN205657573U (en) * 2016-06-02 2016-10-19 合肥京东方光电科技有限公司 Telescopic link drive structure, base plate position correction device and array substrate test equipment
CN206038706U (en) * 2016-08-04 2017-03-22 武汉埔楠量化科技有限公司 Autosampler that can adapt to multiple device interface
CN209280735U (en) * 2018-12-13 2019-08-20 中国科学院西北高原生物研究所 Adjustable full-automatic sample injector, the elemental analyser for varying position

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201751665U (en) * 2010-07-08 2011-02-23 西北工业大学 Multi-head sample support for electromagnetic suspension
CN202093003U (en) * 2011-06-21 2011-12-28 青岛盛瀚色谱技术有限公司 Ion chromatography sample introduction device
CN102749467A (en) * 2012-07-18 2012-10-24 镡丰锦 Full-automatic inspection device of urinalysis test paper belts with batch packaging function
CN203432985U (en) * 2013-01-23 2014-02-12 中国科学院寒区旱区环境与工程研究所 Solid sampling disc directly applied to automatic sampler of elemental analyzer
CN103439137A (en) * 2013-08-28 2013-12-11 中国水产科学研究院南海水产研究所 Separable type sample incoming disc mechanism used in element analyzer
CN204374156U (en) * 2014-12-17 2015-06-03 天津市环境监测中心 A kind of chromatography of ions automatic sampler
CN205193086U (en) * 2015-12-11 2016-04-27 北京先驱威锋技术开发公司 Retractable sample transition system
CN205657573U (en) * 2016-06-02 2016-10-19 合肥京东方光电科技有限公司 Telescopic link drive structure, base plate position correction device and array substrate test equipment
CN206038706U (en) * 2016-08-04 2017-03-22 武汉埔楠量化科技有限公司 Autosampler that can adapt to multiple device interface
CN209280735U (en) * 2018-12-13 2019-08-20 中国科学院西北高原生物研究所 Adjustable full-automatic sample injector, the elemental analyser for varying position

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