CN109305760A - The coating method of energy-saving glass mechanical coating - Google Patents

The coating method of energy-saving glass mechanical coating Download PDF

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Publication number
CN109305760A
CN109305760A CN201710624097.7A CN201710624097A CN109305760A CN 109305760 A CN109305760 A CN 109305760A CN 201710624097 A CN201710624097 A CN 201710624097A CN 109305760 A CN109305760 A CN 109305760A
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CN
China
Prior art keywords
coating
glass
energy
coating method
functional layer
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710624097.7A
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Chinese (zh)
Inventor
刘旺林
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Sperm Membrane Polytron Technologies Inc
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Sperm Membrane Polytron Technologies Inc
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Filing date
Publication date
Application filed by Sperm Membrane Polytron Technologies Inc filed Critical Sperm Membrane Polytron Technologies Inc
Priority to CN201710624097.7A priority Critical patent/CN109305760A/en
Publication of CN109305760A publication Critical patent/CN109305760A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00Surface treatment of glass, not in the form of fibres or filaments, by coating
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C27/00Joining pieces of glass to pieces of other inorganic material; Joining glass to glass other than by fusing
    • C03C27/06Joining glass to glass by processes other than fusing
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2217/00Coatings on glass
    • C03C2217/70Properties of coatings
    • C03C2217/73Anti-reflective coatings with specific characteristics
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2218/00Methods for coating glass
    • C03C2218/10Deposition methods
    • C03C2218/11Deposition methods from solutions or suspensions
    • C03C2218/117Deposition methods from solutions or suspensions by ultrasonic methods

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Ceramic Engineering (AREA)
  • Joining Of Glass To Other Materials (AREA)

Abstract

A kind of coating method of energy-saving glass mechanical coating includes: step A, and glass to be processed is carried out cleaning, drying by cleaning and drying.Step B is coated with functional layer in glass surface in a manner of ultrasonic wave coating, and used ultrasonic spray nozzle vibration frequency is in 20kHz~130kHz.Step C, sizing allow be coated with functional layer to be cured sizing in the surface of the glass.Step D, nature examination carry out the detection of the thickness and coating uniformity of functional layer, and together in detection, numerical value person is then finished product.

Description

The coating method of energy-saving glass mechanical coating
Technical field
The present invention is related with the processing technology of glass surface coating, especially the coating side of an energy-saving glass mechanical coating Method.
Background technique
It can make glass that there is a variety of different functions and characteristic with being coated with or attaching different materials in glass surface, Such as ultraviolet resistant, infrared resistant coating, antimicrobial coating or anti-scraping coating etc., especially energy-saving glass using upper, It namely is coated with the part of uvioresistant, infrared resistant in glass surface, because can be sun-proof and penetrating for thermal energy be avoided, and Reach energy-efficient effect so current this mechanical glass is referred to as energy-saving glass and is also widely used.
The heat-insulating and energy-saving data of glass are industry with Shading Coefficient (abbreviation SC) and U-Value (abbreviation U) Standard.SC measure radiant heat energy, U value measure conduction thermal energy, this two numerical value it is lower better.
With setting for surface functional layer (such as the ultraviolet resistant, infrared resistant coating) of currently marketed mechanical glass Set mode it is big it is supreme be divided into hard plating and two kinds (especially shading heat-protecting glass) of soft plating, the mode plated firmly is mainly to use thermosol Functional layer is arranged to the surface of glass the mode of solution, and U value is about in 1.84W/m2K, SC value are about 0.78.Such way advantage is At low cost, handling ease can directly carry out online in the production of bare glass plate, but can only monolithic monolithic manufacture and also only It can single side.The mode of soft plating is then that functional layer is set to the surface of glass by the way of vacuum splashing and plating, and U value is about in 1.4W/ m2K, SC value are about 0.52.The advantages of such way is that the harder plating mode of optical property is good, but the disadvantage is that since it is desired that vacuum is set It is standby so equipment cost is too high, and this coated glass post-processing it is effective on limitation.
Summary of the invention
The purpose of the present invention is to provide a kind of coating methods of energy-saving glass mechanical coating, can be with continuous production and nothing Need too high equipment cost.
In order to achieve the above objectives, the present invention provides the coating method of an energy-saving glass mechanical coating, includes: step A, Glass to be processed is carried out cleaning, drying by cleaning and drying.Step B, with ultrasonic wave coating method coating functional layer in glass Surface, used ultrasonic spray nozzle vibration frequency is in 20kHz~130kHz.Step C, sizing, makes be coated with functional layer can With the sizing that is cured in the surface of the glass.Step D, nature examination carry out the inspection of the thickness and coating uniformity of functional layer It surveys, together in detection, numerical value person is then finished product, does not strike off functional layer then together in testing number value person and is coated with again.
Detailed description of the invention
Fig. 1 is flow chart of the invention.
Fig. 2 is the manufacturing flow chart of double glazing of the present invention.
Specific embodiment
The coating method of energy-saving glass mechanical coating of the invention, as shown in Figure 1, its method are as follows:
Step A, cleaning and drying, glass to be processed are cleaned, to remove the greasy dirt and impurity of glass surface, so After dry, with remove cleaning when moisture.
Step B, with ultrasonic wave coating method coating functional layer in glass surface, used ultrasonic spray nozzle vibration frequency In 20kHz~130kHz, the spraying atomization angle of nozzle is formed by drop size at 10~80 μm at 20~80 degree.Because Material properties used in the functional layer of coating are different, therefore corresponding used ultrasonic spray nozzle vibration frequency, nozzle Spraying atomization angle and be formed by drop size also can be different.The present embodiment is applied with being coated with uvioresistant and infrared resistant Layer is illustrates example, and but not limited to this, and ultrasonic spray nozzle vibration frequency used in the present embodiment is in 60kHz, the spray of nozzle Applying atomization angle is 70 degree, is formed by drop size at 33 μm.Same coating method can also be used to coating uvioresistant The functional layer of layer, antimicrobial coating or anti-scraping coating etc. different function, but because of the functional layer of different function, its material property is had Difference, therefore the vibration frequency of ultrasonic spray nozzle, the atomization angle of nozzle and are formed by drop size and can also be changed.
Step C, sizing allow be coated with functional layer to be cured sizing in the surface of the glass, and according to being coated with The difference of functional layer type and use different sizing modes, if functional layer be coated be UV dosage form if irradiated with ultraviolet light it is fixed Type, if functional layer be coated be heat curing type if be formed using the mode of heated baking.Uvioresistant in the present embodiment and Infrared resistant coating is formed in a manner of heated baking.
Step D, nature examination carry out the detection of the thickness and coating uniformity of functional layer, then together in detection numerical value person For finished product, functional layer is not struck off then together in testing number value person and be coated with again.The present embodiment is examined in a manner of detecting light transmittance The thickness of functional layer and the uniformity of coating are surveyed, but not limited to this, and material properties difference is with regard to necessary used in functional layer Cooperation uses different detection modes.
Being formed by mechanical glass if to be coated with uvioresistant and IR resisting layer via aforementioned coating method can reach To effect listed in Table.(detection thickness of glass is 6mm)
Test equipment: DETM WP4500
Single-glass in upper table refers to being coated with uvioresistant and infrared coating in the side of simple layer glass, and Double glazing is that can have air or inert gas or vacuum, two sheet glass in an interval, the interval between two sheet glass Respectively there is side to be coated with uvioresistant and infrared coating.The comparison numerical value as listed by upper table is it is known that with side of the invention Its U value of mechanical glass made by method is about in 1.4~2.65W/m2K, SC value are about 0.45.With better ultraviolet light and red The protection effect of outside line.
Other than it monolithic glass can be made or it is made double glazing with the inventive method, method is preceding It is further added by a step E after stating the step D of embodiment, is combined:
Equally for being coated with the single-glass of uvioresistant and infrared resistant, as shown in Fig. 2, step E, take two it is aforementioned Two glass is respectively arranged at the two sides of a frame by monolithic glass made by embodiment, makes the frame by two glass clamp Set on therebetween.It can be filled with inert gas between two glass or vacuumize or be only filled with general air and be general Air pressure (atmospheric pressure).Manufactured double glazing has the effect of good uvioresistant and heat-insulated in this approach.

Claims (10)

1. a kind of coating method of energy-saving glass mechanical coating, it includes have:
Step A, cleaning and drying, glass to be processed is cleaned, to remove the greasy dirt and impurity of glass surface, is then dried It is dry;
Step B, with ultrasonic wave coating method coating functional layer in the surface of the glass, used ultrasonic spray nozzle vibration frequency In 20kHz~130kHz;
Step C, sizing allow be coated with functional layer to be cured sizing in the surface of the glass;
Step D, nature examination carry out the detection of the thickness and coating uniformity of functional layer, and together in detection, numerical value person is then into Product do not strike off functional layer then together in testing number value person and are coated with again.
2. wherein step B ultrasound sound wave coating is used according to the coating method of energy-saving glass mechanical coating described in claim 1 Nozzle its spray atomization angle at 20~80 degree.
3. wherein step B ultrasound sound wave coating is formed according to the coating method of energy-saving glass mechanical coating described in claim 1 Drop size at 10~80 μm.
4. wherein step B ultrasound sound wave coating is formed according to the coating method of energy-saving glass mechanical coating described in claim 2 Drop size at 10~80 μm.
5. according to the coating method of energy-saving glass mechanical coating described in claim 1, wherein solidification side used in step C Method is heated baking solidifying and setting.
6. according to the coating method of energy-saving glass mechanical coating described in claim 4, wherein solidification side used in step C Method is heated baking solidifying and setting.
7. according to the coating method of energy-saving glass mechanical coating described in claim 1, wherein solidification side used in step C Method is ultraviolet light irradiation sizing.
8. according to the coating method of energy-saving glass mechanical coating described in claim 4, wherein solidification side used in step C Method is ultraviolet light irradiation sizing.
9. the coating method according to energy-saving glass mechanical coating described in claim 1 takes two wherein having further included a step E Two glass is respectively arranged at the two sides of a frame by monolithic glass made by piece abovementioned steps, makes the frame by two glass Glass sandwiched is therebetween.
10. being wherein filled between two glass lazy according to the coating method of energy-saving glass mechanical coating described in claim 9 Property gas.
CN201710624097.7A 2017-07-27 2017-07-27 The coating method of energy-saving glass mechanical coating Pending CN109305760A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710624097.7A CN109305760A (en) 2017-07-27 2017-07-27 The coating method of energy-saving glass mechanical coating

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710624097.7A CN109305760A (en) 2017-07-27 2017-07-27 The coating method of energy-saving glass mechanical coating

Publications (1)

Publication Number Publication Date
CN109305760A true CN109305760A (en) 2019-02-05

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0486393A1 (en) * 1990-11-16 1992-05-20 Centre National De La Recherche Scientifique Sol-gel deposition process for thin layers by ultrasonic spraying
KR20120013559A (en) * 2010-08-05 2012-02-15 주식회사 젠트로 Coating method and coating device using ultrasonics wave
KR20140006135A (en) * 2012-06-25 2014-01-16 한국생산기술연구원 Pyrolytic low-e glass manufacturing device and pyrolytic low-e glass manufacturing method using the same
CN104353572A (en) * 2014-10-17 2015-02-18 南开大学 Device for realizing large-area uniform film coating without movement parts
CN105439469A (en) * 2015-12-04 2016-03-30 太仓市建兴石英玻璃厂 Method for chemically plating nickel-copper alloy on quartz glass surface
KR20160102783A (en) * 2015-02-23 2016-08-31 한국교통대학교산학협력단 Method for preparing flexible transparent conductive film and flexible transparent conductive film manufactured thereby

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0486393A1 (en) * 1990-11-16 1992-05-20 Centre National De La Recherche Scientifique Sol-gel deposition process for thin layers by ultrasonic spraying
KR20120013559A (en) * 2010-08-05 2012-02-15 주식회사 젠트로 Coating method and coating device using ultrasonics wave
KR20140006135A (en) * 2012-06-25 2014-01-16 한국생산기술연구원 Pyrolytic low-e glass manufacturing device and pyrolytic low-e glass manufacturing method using the same
CN104353572A (en) * 2014-10-17 2015-02-18 南开大学 Device for realizing large-area uniform film coating without movement parts
KR20160102783A (en) * 2015-02-23 2016-08-31 한국교통대학교산학협력단 Method for preparing flexible transparent conductive film and flexible transparent conductive film manufactured thereby
CN105439469A (en) * 2015-12-04 2016-03-30 太仓市建兴石英玻璃厂 Method for chemically plating nickel-copper alloy on quartz glass surface

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
白振中等: "《工程玻璃深加工技术手册》", 30 April 2014, 中国建材工业出版社 *

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