CN109293391A - A kind of Ruyao Zijin glaze and preparation method thereof - Google Patents
A kind of Ruyao Zijin glaze and preparation method thereof Download PDFInfo
- Publication number
- CN109293391A CN109293391A CN201811174384.3A CN201811174384A CN109293391A CN 109293391 A CN109293391 A CN 109293391A CN 201811174384 A CN201811174384 A CN 201811174384A CN 109293391 A CN109293391 A CN 109293391A
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- glaze
- kiln
- ruyao
- green body
- temperature
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Classifications
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Inorganic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Glass Compositions (AREA)
- Compositions Of Oxide Ceramics (AREA)
Abstract
The present invention relates to a kind of Ruyao Zijin glaze and preparation method thereof, the glaze is made according to the following weight ratio by each component: 30-40 parts of dark stone, red iron-stone 10-20 parts, 5-10 parts of calcite, 20-26 parts of wind scoop soil, each raw material successively by ball mill ball milling and is sieved by reasonable quality proportioning, leaching glaze and finishing are carried out to biscuit, green body is put into kiln to fire in oxidizing atmosphere and reducing atmosphere respectively your porcelain of Ruyao Zijin glaze can be obtained；Your ceramic handiwork that formula mentioned in the present invention and manufacture craft burn out, glaze paint are smooth and glossy.
Description
Technical field
The invention belongs to enamel frit makeing technical fields, and in particular to a kind of Ruyao Zijin glaze and preparation method thereof.
Background technique
Your porcelain is one of five big porcelain in China, and manufacturing process was once once lost, is diligently studied by technical staff,
It resumes production, Ruyao enamel key colour is a kind of light Celeste, is commonly called as " Ovum Anas domestica putamina cyan ", glaze layer is not thick, with moulding
Transition variation, be presented the layer variability of the deep or light depth, glaze paint Crack piece, mostly in picturesque disorder superfine line piece, be commonly called as
" crab claw line ", glaze colours changes with light, and glaze paint taste has obvious butter to feel that glaze is slightly bright, is in milkiness or crystalloid, like " rain more
Cross and become a fine day cloud tear " it is beautiful, gentle simple and unsophisticated, Zijin glaze is a kind of high temperature color glaze, and color is beautiful, ornamental value is strong, but due to
Glaze formula difference, the control of sintering procedure atmosphere, temperature are inaccurate, so that ideal effect is not achieved in glaze face color, gloss；Cause
This, provides that a kind of glaze paint is smooth and glossiness Ruyao Zijin glaze and preparation method thereof is very important.
Summary of the invention
The purpose of the invention is to overcome the deficiencies in the prior art, and provide that a kind of glaze paint is smooth and glossiness Ruyao
Tea-dust glaze and preparation method thereof.
The object of the present invention is achieved like this: a kind of Ruyao Zijin glaze, it is by each component according to following weight proportion
It is made: 30-40 parts of dark stone, red iron-stone 10-20 parts, 5-10 parts of calcite, 20-26 parts of wind scoop soil.
A kind of preparation method of Ruyao Zijin glaze, it the following steps are included:
Step 1: ball milling is mixed according to certain weight ratio and is put into ball mill, in ball mill after crushing all raw materials
Water-wet is added to grind 22-30 hours, wet-grinded slurry crosses 300 meshes, stands 12 hours, spare；
Step 2: glazing carries out wiping dedusting to biscuit with water, and wiping is simultaneously by step 1 gained slurry by clockwise or counterclockwise
Direction is stirred, when stirring since the center of slurry, and it is gradually mobile to circumference, mixing time is 20 minutes, has been stirred
Biscuit is put into glaze slurry after, leaching glaze is carried out to biscuit outer surface, after the completion of soaking glaze, modifies green body；
Step 3: kiln is burnt, and the green body trimmed in step 2 is put into kiln, ventilation in kiln burns green body in oxidizing atmosphere
System controls the firing temperature in kiln, and temperature is made to be ramped up 1100 ° -1200 ° in 7-8 hours；Reduce the ventilation of kiln
Amount, makes combustion atmosphere in kiln gradually switch to reducing atmosphere, and green body keeps the temperature 40-50 minutes under 1200 ° -1220 °, controls kiln
Interior firing temperature was gradually warmed up with 3 minutes 1 ° of temperature, and green body is kept the temperature under conditions of 1250 ° -1280 ° fires half an hour, was stopped
Fire is taken out after being cooled to room temperature to get to your porcelain of Ruyao Zijin glaze.
In the step 1, the weight for the water being added in ball mill is the 70%-80% of each raw material gross weight.
In the step 1, water content after being stood using moisture teller detection in obtained slurry, and by water content
It is adjusted to 60%-80%.
Beneficial effects of the present invention: the present invention uses dark stone, red iron-stone, calcite and wind scoop soil for raw material, each raw material
Between by reasonable quality proportioning, successively by ball mill ball milling, carry out leaching glaze to biscuit, green body be put into kiln and is fired
It can be obtained your porcelain of Ruyao Zijin glaze, ball milling method is arranged by reasonably rotating the raw material and proportion relation of glaze in the present invention
With the temperature of time, glazing mode and time and kiln burning, time, your ceramic glaze surface obtained can be made smooth and glossy.
Specific embodiment
Embodiment 1
A kind of Ruyao Zijin glaze, it is made according to the following weight ratio by each component: 30-40 parts of dark stone, red iron-stone 10-20
Part, 5-10 parts of calcite, 20-26 parts of wind scoop soil.
A kind of preparation method of Ruyao Zijin glaze, it the following steps are included:
Step 1: ball milling is mixed according to certain weight ratio and is put into ball mill, in ball mill after crushing all raw materials
Water-wet is added to grind 22-30 hours, wet-grinded slurry crosses 300 meshes, stands 12 hours, spare；
Step 2: glazing carries out wiping dedusting to biscuit with water, and wiping is simultaneously by step 1 gained slurry by clockwise or counterclockwise
Direction is stirred, when stirring since the center of slurry, and it is gradually mobile to circumference, mixing time is 20 minutes, has been stirred
Biscuit is put into glaze slurry after, leaching glaze is carried out to biscuit outer surface, after the completion of soaking glaze, modifies green body；
Step 3: kiln is burnt, and the green body trimmed in step 2 is put into kiln, ventilation in kiln burns green body in oxidizing atmosphere
System controls the firing temperature in kiln, and temperature is made to be ramped up 1100 ° -1200 ° in 7-8 hours；Reduce the ventilation of kiln
Amount, makes combustion atmosphere in kiln gradually switch to reducing atmosphere, and green body keeps the temperature 40-50 minutes under 1200 ° -1220 °, controls kiln
Interior firing temperature was gradually warmed up with 3 minutes 1 ° of temperature, and green body is kept the temperature under conditions of 1250 ° -1280 ° fires half an hour, was stopped
Fire is taken out after being cooled to room temperature to get to your porcelain of Ruyao Zijin glaze.
The present invention uses dark stone, red iron-stone, calcite and wind scoop soil for raw material, passes through reasonable quality between each raw material
Proportion, successively by ball mill ball milling, biscuit is carried out leaching glaze, by green body be put into kiln fire Ruyao Zijin glaze can be obtained
Your porcelain, the present invention by reasonably rotating the raw material and proportion relation of glaze, be arranged ball milling method and time, glazing mode and when
Between and kiln burn temperature, the time, your obtained ceramic glaze surface can be made smooth and glossy.
Embodiment 2
A kind of Ruyao Zijin glaze, it is made according to the following weight ratio by each component: 30-40 parts of dark stone, red iron-stone 10-20
Part, 5-10 parts of calcite, 20-26 parts of wind scoop soil.
A kind of preparation method of Ruyao Zijin glaze, it the following steps are included:
Step 1: ball milling is mixed according to certain weight ratio and is put into ball mill, in ball mill after crushing all raw materials
Water-wet is added to grind 22-30 hours, wet-grinded slurry crosses 300 meshes, stands 12 hours, spare；
Step 2: glazing carries out wiping dedusting to biscuit with water, and wiping is simultaneously by step 1 gained slurry by clockwise or counterclockwise
Direction is stirred, when stirring since the center of slurry, and it is gradually mobile to circumference, mixing time is 20 minutes, has been stirred
Biscuit is put into glaze slurry after, leaching glaze is carried out to biscuit outer surface, after the completion of soaking glaze, modifies green body；
Step 3: kiln is burnt, and the green body trimmed in step 2 is put into kiln, ventilation in kiln burns green body in oxidizing atmosphere
System controls the firing temperature in kiln, and temperature is made to be ramped up 1100 ° -1200 ° in 7-8 hours；Reduce the ventilation of kiln
Amount, makes combustion atmosphere in kiln gradually switch to reducing atmosphere, and green body keeps the temperature 40-50 minutes under 1200 ° -1220 °, controls kiln
Interior firing temperature was gradually warmed up with 3 minutes 1 ° of temperature, and green body is kept the temperature under conditions of 1250 ° -1280 ° fires half an hour, was stopped
Fire is taken out after being cooled to room temperature to get to your porcelain of Ruyao Zijin glaze.
In the step 1, the weight for the water being added in ball mill is the 70%-80% of each raw material gross weight.
In the step 1, water content after being stood using moisture teller detection in obtained slurry, and by water content
It is adjusted to 60%-80%.
The present invention uses dark stone, red iron-stone, calcite and wind scoop soil for raw material, passes through reasonable quality between each raw material
Proportion, successively by ball mill ball milling, biscuit is carried out leaching glaze, by green body be put into kiln fire Ruyao Zijin glaze can be obtained
Your porcelain, the present invention by reasonably rotating the raw material and proportion relation of glaze, be arranged ball milling method and time, glazing mode and when
Between and kiln burn temperature, the time, your obtained ceramic glaze surface can be made smooth and glossy.
Claims (4)
1. a kind of Ruyao Zijin glaze, which is characterized in that it is made according to the following weight ratio by each component: dark stone 30-40
Part, red iron-stone 10-20 parts, 5-10 parts of calcite, 20-26 parts of wind scoop soil.
2. a kind of preparation method of Ruyao Zijin glaze according to claim 1, which is characterized in that it the following steps are included:
Step 1: ball milling is mixed according to certain weight ratio and is put into ball mill, in ball mill after crushing all raw materials
Water-wet is added to grind 22-30 hours, wet-grinded slurry crosses 300 meshes, stands 12 hours, spare；
Step 2: glazing carries out wiping dedusting to biscuit with water, and wiping is simultaneously by step 1 gained slurry by clockwise or counterclockwise
Direction is stirred, when stirring since the center of slurry, and it is gradually mobile to circumference, mixing time is 20 minutes, has been stirred
Biscuit is put into glaze slurry after, leaching glaze is carried out to biscuit outer surface, after the completion of soaking glaze, modifies green body；
Step 3: kiln is burnt, and the green body trimmed in step 2 is put into kiln, ventilation in kiln burns green body in oxidizing atmosphere
System controls the firing temperature in kiln, and temperature is made to be ramped up 1100 ° -1200 ° in 7-8 hours；Reduce the ventilation of kiln
Amount, makes combustion atmosphere in kiln gradually switch to reducing atmosphere, and green body keeps the temperature 40-50 minutes under 1200 ° -1220 °, controls kiln
Interior firing temperature was gradually warmed up with 3 minutes 1 ° of temperature, and green body is kept the temperature under conditions of 1250 ° -1280 ° fires half an hour, was stopped
Fire is taken out after being cooled to room temperature to get to your porcelain of Ruyao Zijin glaze.
3. a kind of Ruyao Zijin glaze preparation method as claimed in claim 2, it is characterised in that: in the step 1, in ball milling
The weight for the water being added in machine is the 70%-80% of each raw material gross weight.
4. a kind of Ruyao Zijin glaze preparation method as claimed in claim 2, it is characterised in that: in the step 1, use water
The water content in slurry obtained after dividing analyzer detection to stand, and water content is adjusted to 60%-80%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811174384.3A CN109293391A (en) | 2018-10-09 | 2018-10-09 | A kind of Ruyao Zijin glaze and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811174384.3A CN109293391A (en) | 2018-10-09 | 2018-10-09 | A kind of Ruyao Zijin glaze and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109293391A true CN109293391A (en) | 2019-02-01 |
Family
ID=65162011
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811174384.3A Pending CN109293391A (en) | 2018-10-09 | 2018-10-09 | A kind of Ruyao Zijin glaze and preparation method thereof |
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| CN (1) | CN109293391A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110668697A (en) * | 2019-11-15 | 2020-01-10 | 汝州市宣和坊汝瓷有限公司 | Non-open-piece inner glaze for Ru porcelain wine bottles and preparation method thereof |
| CN111943638A (en) * | 2020-08-19 | 2020-11-17 | 金华市婺窑小镇文化发展有限公司 | Preparation method of high-hardness gem diamond violet glaze |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101058476A (en) * | 2007-03-27 | 2007-10-24 | 王振芳 | Antiseep glaze material and glair for Ruyao kiln package container and preparing method thereof |
| CN102898121A (en) * | 2012-08-24 | 2013-01-30 | 王振宇 | Ru-kiln celadon ware and preparation process thereof |
| CN105565789A (en) * | 2015-12-24 | 2016-05-11 | 河南廷怀汝瓷科技有限公司 | Active magnetizing glaze ceramic |
| CN105753323A (en) * | 2016-03-23 | 2016-07-13 | 杨云超 | Method for preparing jade green glaze porcelain |
| CN108314319A (en) * | 2018-04-18 | 2018-07-24 | 黄俊龙 | Zijin glaze and its method for cooking |
-
2018
- 2018-10-09 CN CN201811174384.3A patent/CN109293391A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101058476A (en) * | 2007-03-27 | 2007-10-24 | 王振芳 | Antiseep glaze material and glair for Ruyao kiln package container and preparing method thereof |
| CN102898121A (en) * | 2012-08-24 | 2013-01-30 | 王振宇 | Ru-kiln celadon ware and preparation process thereof |
| CN105565789A (en) * | 2015-12-24 | 2016-05-11 | 河南廷怀汝瓷科技有限公司 | Active magnetizing glaze ceramic |
| CN105753323A (en) * | 2016-03-23 | 2016-07-13 | 杨云超 | Method for preparing jade green glaze porcelain |
| CN108314319A (en) * | 2018-04-18 | 2018-07-24 | 黄俊龙 | Zijin glaze and its method for cooking |
Non-Patent Citations (1)
| Title |
|---|
| 远宏等: "《汝窑》", 30 June 2018, 黑龙江美术出版社 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110668697A (en) * | 2019-11-15 | 2020-01-10 | 汝州市宣和坊汝瓷有限公司 | Non-open-piece inner glaze for Ru porcelain wine bottles and preparation method thereof |
| CN111943638A (en) * | 2020-08-19 | 2020-11-17 | 金华市婺窑小镇文化发展有限公司 | Preparation method of high-hardness gem diamond violet glaze |
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Application publication date: 20190201 |
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