CN109260749A - Distilling filled tower is used in a kind of separation of chemical material - Google Patents
Distilling filled tower is used in a kind of separation of chemical material Download PDFInfo
- Publication number
- CN109260749A CN109260749A CN201811439046.8A CN201811439046A CN109260749A CN 109260749 A CN109260749 A CN 109260749A CN 201811439046 A CN201811439046 A CN 201811439046A CN 109260749 A CN109260749 A CN 109260749A
- Authority
- CN
- China
- Prior art keywords
- partition
- cylinder
- chemical material
- side wall
- cooling
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000463 material Substances 0.000 title claims abstract description 102
- 239000000126 substance Substances 0.000 title claims abstract description 101
- 238000000926 separation method Methods 0.000 title claims abstract description 28
- 238000005192 partition Methods 0.000 claims abstract description 144
- 238000001816 cooling Methods 0.000 claims abstract description 101
- 230000007246 mechanism Effects 0.000 claims abstract description 34
- 238000009434 installation Methods 0.000 claims abstract description 18
- 238000001704 evaporation Methods 0.000 claims abstract description 16
- 230000008020 evaporation Effects 0.000 claims abstract description 16
- 238000009527 percussion Methods 0.000 claims abstract description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 25
- 238000010438 heat treatment Methods 0.000 claims description 10
- 239000007789 gas Substances 0.000 abstract description 77
- 230000033001 locomotion Effects 0.000 abstract description 15
- 239000012535 impurity Substances 0.000 abstract description 8
- 238000005373 pervaporation Methods 0.000 abstract description 4
- 239000007788 liquid Substances 0.000 description 46
- 239000002826 coolant Substances 0.000 description 17
- 239000000110 cooling liquid Substances 0.000 description 3
- 238000010586 diagram Methods 0.000 description 3
- 230000008859 change Effects 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000013016 damping Methods 0.000 description 2
- 239000000945 filler Substances 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 239000007790 solid phase Substances 0.000 description 1
- 230000032258 transport Effects 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/16—Fractionating columns in which vapour bubbles through liquid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/32—Other features of fractionating columns ; Constructional details of fractionating columns not provided for in groups B01D3/16 - B01D3/30
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The present invention relates to chemical material separation field, specifically a kind of chemical material separation distilling filled tower, including cylinder, cooling body, drainage conduit, evaporation device, partition, collecting mechanism, percussion mechanism and bellows；The bottom end of cylinder is installed by evaporation device, the inside installation partition and cooling body of cylinder run through partition, when the inside for needing chemical material to be separated to enter cylinder after pervaporation, the inside sinuous movement of chemical material gas and other gases in partition, contact chemical material gas and other gases uniformly with cooling body, make chemical material gas and other gas liquefactions, the inside of cylinder is separated into multiple units by partition, making a part is that chemical material gas and other gases liquefy in the inner bottom of partition, most chemical material gas liquefies in the inner tip of cylinder, remove impurity, guarantee the quality of chemical material after separating.
Description
Technical field
The present invention relates to chemical material separation field, distilling filled tower is used in specifically a kind of chemical material separation.
Background technique
Packed tower refers to that fluid resistance is small, and process that amount of liquid small big suitable for gas treatment amount.Liquid is along filler table
Face is flowed from up to down, and gas and liquid are at countercurrent or cocurrent, depending on specific reaction.Packed tower memory liquid measure is smaller.No matter
Gas phase or liquid phase, the flow problem in tower is all close to piston flow.If there is solid phase generation in reaction process, it should not use and fill out
Expect tower.
When being separated chemical material using packed tower, the gas of other substances of chemical material gas inclusions is in filler
A certain amount of impurity is contained in the internal coolant of tower, the inside of the chemical material after distilling, and reduces the matter of chemical material
Amount.In consideration of it, the present invention provides a kind of chemical material separation distilling filled tower, have the following characteristics that
(1) a kind of chemical material separation distilling filled tower of the present invention, evaporation device, cylinder are installed in the bottom end of cylinder
The inside installation partition and cooling body of body run through partition, when need chemical material to be separated enters after pervaporation
The inside of cylinder, chemical material gas and other gases make chemical material gas and its in the inside sinuous movement of partition
He uniformly contacts gas with cooling body, makes chemical material gas and other gas liquefactions, and partition is by the inside of cylinder
Multiple units are separated into, making a part is that chemical material gas and other gases liquefy in the inner bottom of partition, big portion
The chemical material gas divided liquefies in the inner tip of cylinder, removes impurity, guarantees the quality of chemical material after separation.
(2) a kind of chemical material separation distilling filled tower of the present invention, the connection of cooling body and partition
Place's installation percussion mechanism, when internal motion cooling liquid of the coolant liquid in cooling body, coolant liquid drives cooling body to shake,
It falls the liquefied chemical material of cooling body side wall quickly from the side wall of cooling body, facilitates collection.
Summary of the invention
For the problems of the prior art, the present invention provides a kind of chemical material separation distilling filled tower, cylinder
Evaporation device is installed in bottom end, and the inside installation partition and cooling body of cylinder run through partition, when need to be separatedization
Work material enters the inside of cylinder, chemical material gas and other gases after pervaporation and transports in the inside complications of partition
It is dynamic, it contacts chemical material gas and other gases uniformly with cooling body, makes chemical material gas and other gas liquefactions,
The inside of cylinder is separated into multiple units by partition, and making a part is chemical material gas and other gases in partition
Inner bottom liquefaction, most chemical material gas cylinder inner tip liquefy, remove impurity, guarantee separation after change
Percussion mechanism is installed in the junction of the quality of work material, cooling body and partition, when coolant liquid is in the inside of cooling body
When moving cooling liquid, coolant liquid drives cooling body to shake, and makes the liquefied chemical material of cooling body side wall quickly from cooling
The side wall of mechanism is fallen, and facilitates collection.
The technical solution adopted by the present invention to solve the technical problems is: a kind of chemical material separation distilling filled tower,
Including cylinder, cooling body, drainage conduit, evaporation device, partition, collecting mechanism, percussion mechanism and bellows；The cylinder
Bottom end the evaporation device is installed, the partition is installed in the inside of the cylinder；The internal symmetry of the cylinder is installed
The cooling body, and the cooling body runs through the partition, the connection of the partition and the cooling body
Place is installed by the percussion mechanism；The side wall of the cylinder installs multiple drainage conduits, and the drainage conduit contradicts the separation
The side wall of mechanism；The collecting mechanism is installed, and the collecting mechanism contradicts the separation machine at the interior central of the cylinder
The bellows is installed in the bottom end of the side wall of structure, the cylinder, and the bellows is connected to the bottom end of the cooling body.
Specifically, the evaporation device includes evaporative cylinder, feed pipe and heating coil, the bottom end of the cylinder is fixedly connected
The evaporative cylinder, the feed pipe is installed on the top of the evaporative cylinder, and the inside installation of the evaporative cylinder is spiral described
Heating coil.
Specifically, the partition includes first partition, communicating pipe, the first strainer and second partition, the cylinder
The first partition is installed in inner tip and bottom end respectively, and the side wall of the first partition locates the installation communicating pipe between two parties；Institute
It states and the second partition is installed at the interior central of cylinder, and institute is installed in the internal connection of the second partition and the cylinder
State the first strainer, the top surface of the first partition and the second partition is tilted from from placed in the middle to both ends, and a partition and
The bottom surface of the second partition is arcuate structure.
Specifically, the cooling body includes cooling tube, connecting tube and water storage cylinder, the storage is installed in the top surface of the cylinder
The connecting tube is installed in the top inside of water drum, the cylinder, and the connecting tube is connected to the water storage cylinder；The connecting tube
Bottom end is symmetrically installed multiple cooling tubes, and the cooling tube runs through the first partition and the second partition；It is described cold
But the bellows is installed in the bottom end of pipe, and the cylinder is run through in one end of the bellows.
Specifically, the collecting mechanism includes fixed ring, the second strainer, water pipe, groove, connection ring and connecting plate, it is described
The top surface of second partition is fixedly connected with the fixed ring, and funnel shaped second strainer is installed on the top of the fixed ring；Institute
The connection ring is installed on the top for stating the second strainer, and the top surface installation side wall of the connection ring is the connecting plate of triangle,
And the connecting plate and the side wall of the connection ring contradict the inner sidewall of the cylinder；The top surface of the connection ring is equipped with annular
The groove, the water pipe is installed in the bottom end of the groove, and the water pipe protrudes into the fixed ring through second strainer
Inside.
Specifically, the drainage conduit is installed in the top surface of the first partition and the second partition respectively, it is located at the cylinder
The inside of the evaporative cylinder is protruded into one end of a piece drainage conduit of the side wall lowermost end of body, is located at the second partition top surface
The drainage conduit run through the fixed ring.
Specifically, the percussion mechanism includes spring, rubber stopper, sliding slot and convex block, spiral shell is installed in the inside of the cooling tube
The convex block for revolving shape, installs the rubber stopper between the cooling tube and the first partition and the second partition, described
Cooling tube runs through the rubber stopper；The inside of the first partition and the second partition is equipped with the sliding slot, the sliding slot
Internal slide connects the cooling tube, and the spring is staggered installation of between the cooling tube and the side wall of the sliding slot.
Beneficial effects of the present invention:
(1) a kind of chemical material separation distilling filled tower of the present invention, evaporation device, cylinder are installed in the bottom end of cylinder
The inside installation partition and cooling body of body run through partition, when need chemical material to be separated enters after pervaporation
The inside of cylinder, chemical material gas and other gases make chemical material gas and its in the inside sinuous movement of partition
He uniformly contacts gas with cooling body, makes chemical material gas and other gas liquefactions, and partition is by the inside of cylinder
Multiple units are separated into, making a part is that chemical material gas and other gases liquefy in the inner bottom of partition, big portion
The chemical material gas divided liquefies in the inner tip of cylinder, removes impurity, guarantees the quality of chemical material after separation.
(2) a kind of chemical material separation distilling filled tower of the present invention, the connection of cooling body and partition
Place's installation percussion mechanism, when internal motion cooling liquid of the coolant liquid in cooling body, coolant liquid drives cooling body to shake,
It falls the liquefied chemical material of cooling body side wall quickly from the side wall of cooling body, facilitates collection.
Detailed description of the invention
Present invention will be further explained below with reference to the attached drawings and examples.
Fig. 1 is that a kind of structure of a kind of preferred embodiment of chemical material separation distilling filled tower provided by the invention is shown
It is intended to；
Fig. 2 is inner barrel structural schematic diagram shown in FIG. 1；
Fig. 3 is collecting mechanism schematic diagram of internal structure shown in Fig. 2；
Fig. 4 is cooling tube schematic diagram of internal structure shown in FIG. 1.
In figure: 1, cylinder, 2, cooling body, 21, cooling tube, 22, connecting tube, 23, water storage cylinder, 3, drainage conduit, 4, evaporation
Mechanism, 41, evaporative cylinder, 42, feed pipe, 43, heating coil, 5, partition, 51, first partition, 52, communicating pipe, 53, first
Strainer, 54, second partition, 6, collecting mechanism, 61, fixed ring, the 62, second strainer, 63, water pipe, 64, groove, 65, connection ring,
66, connecting plate, 7, percussion mechanism, 71, spring, 72, rubber stopper, 73, sliding slot, 74, convex block, 8, bellows.
Specific embodiment
In order to be easy to understand the technical means, the creative features, the aims and the efficiencies achieved by the present invention, tie below
Specific embodiment is closed, the present invention is further explained.
As Figure 1-Figure 4, a kind of chemical material separation distilling filled tower of the present invention, including cylinder 1, cooling
Mechanism 2, drainage conduit 3, evaporation device 4, partition 5, collecting mechanism 6, percussion mechanism 7 and bellows 8；The bottom of the cylinder 1
The evaporation device 4 is installed at end, and the partition 5 is installed in the inside of the cylinder 1；The internal symmetry of the cylinder 1 is installed
The cooling body 2, and the cooling body 2 runs through the partition 5, the partition 5 and the cooling body 2
Junction is installed by the percussion mechanism 7；The side wall of the cylinder 1 installs multiple drainage conduits 3, and the drainage conduit 3 contradicts
The side wall of the partition 5；The collecting mechanism 6 is installed, and the collecting mechanism 6 supports at the interior central of the cylinder 1
The side wall of the partition 5 is touched, the bellows 8 is installed in the bottom end of the cylinder 1, and the bellows 8 is connected to the cooling
The bottom end of mechanism 2.
Specifically, the evaporation device 4 includes evaporative cylinder 41, feed pipe 42 and heating coil 43, the bottom end of the cylinder 1
It is fixedly connected with the evaporative cylinder 41, the feed pipe 42, and the inside of the evaporative cylinder 41 are installed in the top of the evaporative cylinder 41
The spiral heating coil 43 is installed, the evaporative cylinder 41 is entered by the feed pipe 42 in order to facilitate chemical material
Inside, the heating coil 43 generate heat, and the chemical material inside the evaporative cylinder 41 is made to evaporate into the inside of the cylinder 1.
Specifically, the partition 5 includes first partition 51, communicating pipe 52, the first strainer 53 and second partition 54, institute
It states the inner tip of cylinder 1 and the first partition 51 is installed in bottom end respectively, the side wall of the first partition 51 is located to install between two parties
The communicating pipe 52；The second partition 54, and the second partition 54 and the cylinder are installed at the interior central of the cylinder 1
First strainer 53 is installed in the internal connection of body 1, and the top surface of the first partition 51 and the second partition 54 is from placed in the middle
Place is tilted to both ends, and the bottom surface of a partition 51 and the second partition 54 is arcuate structure, for convenience described in two
The inside of the cylinder 1 is separated into three units by first partition 51 and the second partition 54, enters chemical material gas
The inside of three units is cooled down, and chemical material gas runs through the communicating pipe that a first partition 51 is located between two parties
52 enter between the first partition 51 and the second partition 54, and chemical material gas is from the interior central of the cylinder 1
Two end motions to the cylinder 1, make chemical material gas through 54 side wall of second partition first strainer 53 into
Enter between the second partition 54 and another described first partition 51, chemical material gas is again from the inside two of the cylinder 1
It holds to movement at the interior central of the cylinder 1, to make chemical material gas in the inside sinuous movement of the cylinder 1, increases
Add chemical material gas in the 1 internal motion time of cylinder, facilitates the liquefaction separation of chemical material gas cooling.
Specifically, the cooling body 2 includes cooling tube 21, connecting tube 22 and water storage cylinder 23, the top surface of the cylinder 1 is pacified
The water storage cylinder 23 is filled, the connecting tube 22 is installed inside the top of the cylinder 1, and the connecting tube 22 is connected to the water storage
Cylinder 23；The bottom end of the connecting tube 22 is symmetrically installed multiple cooling tubes 21, and the cooling tube 21 through described first every
Plate 51 and the second partition 54；The bellows 8 is installed in the bottom end of the cooling tube 21, and one end of the bellows 8 is passed through
The cylinder 1 is worn, the coolant liquid inside the water storage cylinder 23 enters the cooling tube 21 through the connecting tube 22 for convenience
Inside, reduce the side wall temperatures of the cooling tube 21, and for convenience chemical material gas in 51 He of first partition
Between the second partition 54 when sinuous movement, chemical material gas is contacted with the cooling tube 21, meets chemical material gas
Cold rapid cooling.
Specifically, the collecting mechanism 6 includes fixed ring 61, the second strainer 62, water pipe 63, groove 64,65 and of connection ring
Connecting plate 66, the top surface of the second partition 54 are fixedly connected with the fixed ring 61, and funnel is installed on the top of the fixed ring 61
Second strainer 62 of shape；The top of second strainer 62 is installed by the connection ring 65, the top surface peace of the connection ring 61
The connecting plate 66 that side wall is triangle is filled, and the connecting plate 66 and the side wall of the connection ring 65 contradict the cylinder 1
Inner sidewall；The top surface of the connection ring 65 is equipped with the groove 64 of annular, and the water pipe is installed in the bottom end of the groove 64
63, and the water pipe 63 protrudes into the inside of the fixed ring 61 through second strainer 62, on the top of the second partition 54
Between 51 bottom surface of the first partition on 1 top of face and the cylinder when cooling chemical material gas, a part of chemical material
Gas liquefaction is located between two parties in 1 internal side wall of cylinder, and chemical material liquid enters the company in the side walls of the cylinder 1
The side wall of fishplate bar 66, chemical material liquid slide downward into the connection ring 65 and described recessed in the side wall of the connecting plate 66
The inside of slot 64, chemical material liquid enter the inside of the fixed ring 61, making through the water pipe 63 from the groove 64
Work feed liquid stays in the top surface of the second partition 54, and described is installed between the connection ring 65 and the fixed ring 61
Two strainers 62 facilitate chemical material gas through first strainer 53 and second strainer 62 in the second partition 54
It is moved between 51 bottom surface of the first partition on 1 top of top surface and the cylinder.
Specifically, the drainage conduit 3 is installed in the top surface of the first partition 51 and the second partition 54 respectively, it is located at institute
The inside of the evaporative cylinder 41 is protruded into the one end for stating a drainage conduit 3 of the side wall lowermost end of cylinder 1, is located at described second
The drainage conduit 3 of 54 top surface of partition runs through the fixed ring 61, and the first partition 51 and described second are discharged for convenience
The liquefied gas in the top surface of partition 54, and between the first partition 51 and the second partition 52 of 1 bottom end of cylinder
Tentatively cooling chemical material liquid, the gas of other substances in 1 bottom end of cylinder the first partition 51 with it is described
It liquefies between second partition 52, chemical material liquid internal is caused to contain a large amount of impurities, the chemical material liquid contained a large amount of impurities
Body enters the inside of the evaporative cylinder 41 by a drainage conduit 3, is processed again.
Specifically, the percussion mechanism 7 includes spring 71, rubber stopper 72, sliding slot 73 and convex block 74, the cooling tube 21
The spiral convex block 74 is installed in inside, pacifies between the cooling tube 21 and the first partition 51 and the second partition 54
The rubber stopper 72 is filled, the cooling tube 21 runs through the rubber stopper 72；The first partition 51 and the second partition 54
Inside is equipped with the sliding slot 73, and the internal slide of the sliding slot 73 connects the cooling tube 21, and the cooling tube 21 with it is described
The spring 71 is staggered installation of between the side wall of sliding slot 73, in order to facilitate coolant liquid in the internal motion of the cooling tube 21,
Coolant liquid screw between the spiral convex block 74, makes the inside of coolant liquid impinging cooling pipe 21, makes the cooling
Pipe 21 shakes, and the liquid after facilitating 21 surface of cooling tube to liquefy is fallen downwards, and when the shaking of the cooling tube 21, described cold
But pipe 21 drives the rubber stopper 72 to shake, and the rubber stopper 72 is closed at both ends by the sliding slot 73, prevents liquid from entering institute
The inside of sliding slot 73 is stated, and is staggered installation of the spring 71 between the cooling tube 21 and the side wall of the sliding slot 73, it is described cold
But the spring 71 is squeezed when pipe 21 moves, makes the spring 71 21 damping of cooling tube, avoids the cooling tube 21
Shaking degree is excessive.
When in use, be added by feed pipe 42 to the inside of evaporative cylinder 41 needs chemical material to be separated in right amount, then will
Water storage cylinder 23 connects coolant liquid, and the coolant liquid inside water storage cylinder 23 enters the inside of cooling tube 21 through connecting tube 22, makes to cool down
The side wall temperatures of pipe 21 reduce, the inside discharge of coolant liquid bellows 8 again.The present apparatus is accessed into power supply, opens heating coil
43, heating coil 43 generates heat, and evaporates the chemical material inside evaporative cylinder 41 and moves upwards into the inside of cylinder 1.First
The bottom surface of partition 51 is the funnel-shaped structure of back-off, and the gas into 1 bottom end of cylinder moves convergence in the bottom surface of first partition 51
Moved to the interior central of cylinder 1, make gas through the connecting tube 52 of 1 bottom end of cylinder enter 51 top surface of first partition with
Between 52 bottom surface of second partition, two end motions from the inner bottom of chemical material gas from cylinder 1 is placed in the middle to cylinder 1, chemical industry
Material gas is contacted with the lower cooling tube 21 of temperature, and a part of makes chemical material gas and other gas fast liquefyings, is made
The chemical material liquid and other liquid of a part are moved in the top surface of the first partition 51 of 1 bottom end of cylinder, and first partition 51
Top surface tilted from from placed in the middle to both ends, facilitate the chemical material liquid of a part and other liquid to enter drainage conduit 3
Inside, the inside for making the chemical material liquid of a part and other liquid be again introduced into evaporative cylinder 41 are processed again.One is small
Other partial gases and most chemical material gas continue to move, and the bottom surface of second partition 54 is infundibulate, convenient
Gas enters between 54 top surface of second partition and another first partition 51 through the first strainer 53 and the second strainer 62, makes gas
Mobile at interior central of the inside both ends of cylinder 1 to cylinder 1, gas lengthens gas and exists in the inside sinuous movement of cylinder 1
1 internal motion time of cylinder, other gases of sub-fraction and most chemical material gas are contacted again with cooling tube 21,
Other gases and the chemical material gas of a part are made to liquefy again.In the top surface and the first of 1 top of cylinder of second partition 54
Between 51 bottom surface of partition when cooling chemical material gas, a part of chemical material gas liquefaction is placed in the middle in 1 internal side wall of cylinder
Place, chemical material liquid enter the side wall of connecting plate 66 in the side walls of cylinder 1, and chemical material liquid is in the side of connecting plate 66
Wall slides downward into the inside of connection ring 65 and groove 64, and chemical material liquid enters fixed ring from groove 64 through water pipe 63
61 inside makes chemical material liquid stay in the top surface of second partition 54, makes most chemical material liquid and on a small quantity miscellaneous
Matter liquid is discharged by the drainage conduit 3 of 54 top surface of second partition.After saying that the chemical material gas being filtered for multiple times removed impurity, change
Connecting tube 22 of the work material through 1 top of cylinder enters between the first partition 51 on 1 top of cylinder and the inside top surface of cylinder 1,
Chemical material gas contacts liquefaction with cooling tube 21 between the first partition 51 and the inside top surface of cylinder 1 on 1 top of cylinder, makes
The chemical material liquid of high-purity stays on the top surface of the first partition 51 on 1 top of cylinder, makes the chemical material liquid of high-purity
It is discharged from the inside of drainage conduit 3.In internal motion of the coolant liquid in cooling tube 21, coolant liquid is between spiral convex block 74
Screw makes the inside of coolant liquid impinging cooling pipe 21, shakes cooling tube 21, the liquid after facilitating 21 surface of cooling tube to liquefy
Body is fallen downwards, so that liquid is fallen on the top surface of first partition 51 and second partition 54, and when the shaking of cooling tube 21,21 band of cooling tube
Dynamic rubber stopper 72 shakes, and rubber stopper 72 is closed at both ends by sliding slot 73, prevents liquid from entering the inside of sliding slot 73, and cooling tube 21
It is staggered installation of spring 71 between the side wall of sliding slot 73, spring 71 is squeezed when cooling tube 21 moves, makes 71 cooling tube 21 of spring
Damping avoids the shaking degree of cooling tube 21 excessive, prevents cooling tube 21 from falling from the bottom end of connecting tube 22.
The basic principles, main features and advantages of the invention have been shown and described above.The technical staff of the industry should
Understand, the present invention is not limited to the above embodiments, and the description in above embodiment and specification only illustrates the present invention
Principle, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these variation and
Improvement is both fallen in the scope of protection of present invention.The claimed scope of the invention is by appended claims and its equivalent
Object defines.
Claims (7)
1. a kind of chemical material separation distilling filled tower, it is characterised in that: including cylinder (1), cooling body (2), drainage conduit
(3), evaporation device (4), partition (5), collecting mechanism (6), percussion mechanism (7) and bellows (8)；The cylinder (1)
The evaporation device (4) is installed in bottom end, and the partition (5) is installed in the inside of the cylinder (1)；The cylinder (1) it is interior
Portion is symmetrically installed the cooling body (2), and the cooling body (2) runs through the partition (5), the partition
(5) percussion mechanism (7) is installed with the junction of the cooling body (2)；The side wall installation of the cylinder (1) is multiple described
Drainage conduit (3), and the drainage conduit (3) contradicts the side wall of the partition (5)；Pacify at the interior central of the cylinder (1)
It fills the collecting mechanism (6), and the collecting mechanism (6) contradicts the side wall of the partition (5), the bottom of the cylinder (1)
The bellows (8) is installed at end, and the bellows (8) is connected to the bottom end of the cooling body (2).
2. a kind of chemical material separation distilling filled tower according to claim 1, it is characterised in that: the evaporation device
It (4) include evaporative cylinder (41), feed pipe (42) and heating coil (43), the bottom end of the cylinder (1) is fixedly connected with the evaporation
Cylinder (41), the feed pipe (42) is installed on the top of the evaporative cylinder (41), and spiral is installed in the inside of the evaporative cylinder (41)
The heating coil (43) of shape.
3. a kind of chemical material separation distilling filled tower according to claim 2, it is characterised in that: the partition
It (5) include first partition (51), communicating pipe (52), the first strainer (53) and second partition (54), the inside top of the cylinder (1)
End is installed the first partition (51) respectively with bottom end, and the side wall of the first partition (51) locates the installation communicating pipe between two parties
(52)；The second partition (54), and the second partition (54) and the cylinder are installed at the interior central of the cylinder (1)
(1) internal connection is installed by first strainer (53), the top surface of the first partition (51) and the second partition (54)
It is tilted from from placed in the middle to both ends, and the bottom surface of a partition (51) and the second partition (54) is arcuate structure.
4. a kind of chemical material separation distilling filled tower according to claim 3, it is characterised in that: the cooling body
It (2) include cooling tube (21), connecting tube (22) and water storage cylinder (23), the water storage cylinder (23) is installed in the top surface of the cylinder (1),
The connecting tube (22) is installed, and the connecting tube (22) is connected to the water storage cylinder (23) inside the top of the cylinder (1)；Institute
The bottom end for stating connecting tube (22) is symmetrically installed multiple cooling tubes (21), and the cooling tube (21) runs through the first partition
(51) and the second partition (52)；The bottom end of the cooling tube (21) is installed by the bellows (8), and the bellows (8)
One end run through the cylinder (1).
5. a kind of chemical material separation distilling filled tower according to claim 4, it is characterised in that: the collecting mechanism
It (6) include fixed ring (61), the second strainer (62), water pipe (63), groove (64), connection ring (65) and connecting plate (66), it is described
The top surface of second partition (54) is fixedly connected the fixed ring (61), and the top installation of the fixed ring (61) is funnel shaped described
Second strainer (62)；The top of second strainer (62) is installed by the connection ring (65), the top surface peace of the connection ring (61)
The connecting plate (66) that side wall is triangle is filled, and described in the connecting plate (66) and the conflict of the side wall of the connection ring (65)
The inner sidewall of cylinder (1)；The top surface of the connection ring (65) is equipped with the groove (64) of annular, the bottom end of the groove (64)
It installs the water pipe (63), and the water pipe (63) protrudes into the inside of the fixed ring (61) through second strainer (62).
6. a kind of chemical material separation distilling filled tower according to claim 5, it is characterised in that: the first partition
(51) and the drainage conduit (3) are installed in the top surface of the second partition (54) respectively, are located at the side wall lowermost end of the cylinder (1)
One end of a drainage conduit (3) protrude into the inside of the evaporative cylinder (41), be located at the second partition (54) top surface
The drainage conduit (3) runs through the fixed ring (61).
7. a kind of chemical material separation distilling filled tower according to claim 5, it is characterised in that: the percussion mechanism
It (7) include spring (71), rubber stopper (72), sliding slot (73) and convex block (74), spiral shape is installed in the inside of the cooling tube (21)
The convex block (74), between the cooling tube (21) and the first partition (51) and the second partition (54) installation described in
Rubber stopper (72), the cooling tube (21) run through the rubber stopper (72)；The first partition (51) and the second partition
(54) inside is equipped with the sliding slot (73), and the internal slide of the sliding slot (73) connects the cooling tube (21), and described cold
But it manages between (21) and the side wall of the sliding slot (73) and is staggered installation of the spring (71).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811439046.8A CN109260749B (en) | 2018-11-29 | 2018-11-29 | Chemical material separation is with rectification packed tower |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811439046.8A CN109260749B (en) | 2018-11-29 | 2018-11-29 | Chemical material separation is with rectification packed tower |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109260749A true CN109260749A (en) | 2019-01-25 |
| CN109260749B CN109260749B (en) | 2021-04-27 |
Family
ID=65185861
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811439046.8A Expired - Fee Related CN109260749B (en) | 2018-11-29 | 2018-11-29 | Chemical material separation is with rectification packed tower |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109260749B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114196430A (en) * | 2021-12-20 | 2022-03-18 | 刘德民 | Petroleum is refined with petroleum distillation plant |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1486771A (en) * | 2002-08-02 | 2004-04-07 | 株式会社日本触媒 | Method for recorering sublimates |
| JP2009240895A (en) * | 2008-03-31 | 2009-10-22 | Chugoku Electric Power Co Inc:The | Carbon dioxide recovery apparatus |
| US20160250563A1 (en) * | 2015-02-27 | 2016-09-01 | Caloris Engineering, LLC | Compact mechanical vapor recompression evaporator system |
| CN205874349U (en) * | 2016-07-29 | 2017-01-11 | 陈思蓉 | Stills for be used for producing essence spices |
| CN206081692U (en) * | 2016-08-27 | 2017-04-12 | 嘉兴富成化工科技有限公司 | Environment -friendly distillation plant |
| CN108325225A (en) * | 2018-03-26 | 2018-07-27 | 南安初盼商贸有限公司 | A kind of evaporator that can efficiently catch juice |
| CN208081887U (en) * | 2018-01-11 | 2018-11-13 | 福建省速卖通电子商务有限公司 | A kind of efficient Petroleum Production fractionating column |
-
2018
- 2018-11-29 CN CN201811439046.8A patent/CN109260749B/en not_active Expired - Fee Related
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1486771A (en) * | 2002-08-02 | 2004-04-07 | 株式会社日本触媒 | Method for recorering sublimates |
| JP2009240895A (en) * | 2008-03-31 | 2009-10-22 | Chugoku Electric Power Co Inc:The | Carbon dioxide recovery apparatus |
| US20160250563A1 (en) * | 2015-02-27 | 2016-09-01 | Caloris Engineering, LLC | Compact mechanical vapor recompression evaporator system |
| CN205874349U (en) * | 2016-07-29 | 2017-01-11 | 陈思蓉 | Stills for be used for producing essence spices |
| CN206081692U (en) * | 2016-08-27 | 2017-04-12 | 嘉兴富成化工科技有限公司 | Environment -friendly distillation plant |
| CN208081887U (en) * | 2018-01-11 | 2018-11-13 | 福建省速卖通电子商务有限公司 | A kind of efficient Petroleum Production fractionating column |
| CN108325225A (en) * | 2018-03-26 | 2018-07-27 | 南安初盼商贸有限公司 | A kind of evaporator that can efficiently catch juice |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114196430A (en) * | 2021-12-20 | 2022-03-18 | 刘德民 | Petroleum is refined with petroleum distillation plant |
Also Published As
| Publication number | Publication date |
|---|---|
| CN109260749B (en) | 2021-04-27 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN208785826U (en) | A kind of novel demister | |
| CN109260749A (en) | Distilling filled tower is used in a kind of separation of chemical material | |
| CN107029438A (en) | Produce the integrated forced circulation crystallization evaporator and device of big crystal grain ammonium sulfate | |
| CN104556035B (en) | Preparation method and preparation device of food-grade high-purity liquid carbon dioxide | |
| CN101961562B (en) | Rectification device | |
| CN102809304A (en) | Glass cooling condenser | |
| RU2018123854A (en) | METHOD FOR REMOVING CO2 FROM A CONTAMINATED HYDROCARBON FLOW OF RAW MATERIALS | |
| CN104326485A (en) | Ammonia refining treatment process | |
| CN205473626U (en) | System for retrieve heavy hydrocarbon in liquefied natural gas production | |
| CN101071035B (en) | Method for delivering purity raised gas and purity improved overheat gas | |
| CN202315648U (en) | Cryogenic recovery system for ethylene in tail gas | |
| CN104724730B (en) | A kind of lead plaster desulfurizing byproduct sulfate crystal method and apparatus based on the quick crystallize of Local cooling | |
| CN204602153U (en) | Liquid material recycling of condensed steam utilizes device | |
| CN104830371B (en) | The apparatus and method of C2 in a kind of recovery oil refinery dry gas | |
| CN209331167U (en) | A kind of Feed Manufacturing cooling device | |
| CN207169079U (en) | A kind of rectifying column with combined type collection liquid distributor | |
| RU112840U1 (en) | ODORANT ADSORPTION DRY BLOCK | |
| CN209181388U (en) | A kind of gas-liquid separator of carbon dioxide purification | |
| CN201880386U (en) | Rectifying device | |
| CN207627966U (en) | Constant pressure distilling apparatus | |
| CN109678158A (en) | Exhaust gas treating method and system in polysilicon production process | |
| RU206853U1 (en) | FLOW DISTILLATOR | |
| CN203989929U (en) | Rectifying tower vacuum pipeline preventing clogging up device | |
| CN102675034B (en) | System and method for purifying vinyl chloride monomer | |
| CN205024118U (en) | High -purity hexane complete set rectifier unit |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20210409 Address after: 257000 dongyinggang Economic Development Zone, Dongying City, Shandong Province Applicant after: Shandong Yuetian Chemical Co.,Ltd. Address before: 610065 School of chemical engineering, Sichuan University, No. 24 south section of first ring road, Sichuan, Chengdu Applicant before: Fang Wenxing |
|
| TA01 | Transfer of patent application right | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20210427 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |