CN109234031A - A kind of washing cloth grass washing powder - Google Patents
A kind of washing cloth grass washing powder Download PDFInfo
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- CN109234031A CN109234031A CN201811113763.1A CN201811113763A CN109234031A CN 109234031 A CN109234031 A CN 109234031A CN 201811113763 A CN201811113763 A CN 201811113763A CN 109234031 A CN109234031 A CN 109234031A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/38—Cationic compounds
- C11D1/65—Mixtures of anionic with cationic compounds
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/046—Salts
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/10—Carbonates ; Bicarbonates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
- C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
- C11D3/1246—Silicates, e.g. diatomaceous earth
- C11D3/1253—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite
- C11D3/1266—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite in liquid compositions
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
- C11D3/14—Fillers; Abrasives ; Abrasive compositions; Suspending or absorbing agents not provided for in one single group of C11D3/12; Specific features concerning abrasives, e.g. granulometry or mixtures
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/18—Hydrocarbons
- C11D3/184—Hydrocarbons unsaturated
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2003—Alcohols; Phenols
- C11D3/2006—Monohydric alcohols
- C11D3/2017—Monohydric alcohols branched
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2003—Alcohols; Phenols
- C11D3/2041—Dihydric alcohols
- C11D3/2044—Dihydric alcohols linear
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/22—Carbohydrates or derivatives thereof
- C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
- C11D3/38609—Protease or amylase in solid compositions only
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/123—Sulfonic acids or sulfuric acid esters; Salts thereof derived from carboxylic acids, e.g. sulfosuccinates
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/38—Cationic compounds
- C11D1/62—Quaternary ammonium compounds
Abstract
The present invention relates to articles for washing technical fields, and in particular to a kind of washing cloth grass washing powder.The washing powder includes 13~22 parts of dioctyl sodium sulfosuccinate, 3~5 parts of methyl anyl alcohol, 4~7 parts of softener, 4~8 parts of ethohexadiol, 3~5 parts of sodium alginate, 5~8 parts of papain, 10~20 parts of sodium bicarbonate, 8~16 parts of sodium carbonate, modified 5~9 parts of river sand, neutral 1~3 part of kaolin, 3~5 parts of jasmine pollen, 2~4 parts of lycopene；Make softener by adding glucose ester based quaternary ammonium salt, effectively overcome the problems, such as existing washing powder pollution on the environment, cloth grass jaundice after washing is prevented to be hardened；Meanwhile the present invention makees defoaming agent by adding higher alcohols, effectively reduces the foam that finished product washing powder is generated in washing, readily volatilized, environmental sound will not also inhibit washing effect；Furthermore the present invention makees carrier by modified river sand, reaches and helps suspension effect, improves the washing effect of washing powder.
Description
Technical field
The present invention relates to articles for washing technical fields, and in particular to a kind of washing cloth grass washing powder.
Background technique
Washing powder is a kind of synthetic detergent of alkalinity, be for do washing clothes chemicals, earliest by Henkel KGaA in
It is in 1907 primary raw material invention with borate and silicate.
The main component of washing powder is anionic surfactant, sodium alkyl benzene sulfonate, a small amount of nonionic surfactant,
Again plus some auxiliary agents, phosphate, silicate, anhydrous sodium sulphate, fluorescer, enzyme etc., it the techniques such as mixed, dusted to be made.
With the reinforcement of environmental consciousness, gradually attention of the whole people to environmental protection, Powdered Detergent Containing Phosphate is to gradually eliminating, or even forbids
It produces and sells；Meanwhile with the continuous improvement of people's health consciousness, the cleaning requirement of the articles such as clothing is increasingly stringenter,
Traditional washing powder is to reach decontamination purpose by adding chemicals mostly, and such washing powder can not only remain in clothing
On, there is side effects, the waste liquids such as certain stimulation also to have due to containing chemicals, to environment centainly the skin of human body
Pollution.
Summary of the invention
For the status for overcoming existing washing powder to pollute the environment, solve after existing washing powder washing clothing to skin
Stimulation problem, the present invention provides a kind of washing cloth grass washing powder.
The present invention is achieved by the following technical solutions:
A kind of washing cloth grass washing powder, including following raw material:
13~22 parts of dioctyl sodium sulfosuccinate, there is building action, be used as active constituent；
3~5 parts of methyl anyl alcohol, it is used as dispersing agent；
It is 4~7 parts of softener, soft for cloth grass after guaranteeing washing, it is smooth；
4~8 parts of ethohexadiol, it is used as defoaming agent, reduces foams of washing powder, but do not inhibit washing effect；
3~5 parts of sodium alginate, ingredient is washed as helping；
5~8 parts of papain, it is used as synergistic component, weakens the electrostatic efficiency of cloth grass after washing, reach the mesh of antistatic
's；
10~20 parts of sodium bicarbonate, it is used as active constituent；
8~16 parts of sodium carbonate, ingredient is washed as helping；
Modified 5~9 parts of river sand, as buffer composition, helps and washes ingredient, the carrier as washing powder；
1~3 part of neutral kaolin is used as auxiliary element；
3~5 parts of jasmine pollen, it is used as synergistic component, so that finished product washing powder is fragrant with jasmine, while reaches antibiotic and sterilizing
Effect；
2~4 parts of lycopene, it is used as synergistic component, increases the sun-proof and ultraviolet ray preventing effect of cloth grass after washing, weakens
Stimulation of the cloth grass to human body after washing；
Wherein, Jasmine Powder Particle Size≤0.5 μm；The modified river sand and kaolinic granularity≤0.5 μm.
Preferably, the washing cloth grass washing powder includes following raw material:
18 parts of dioctyl sodium sulfosuccinate, 3 parts of methyl anyl alcohol, 5 parts of softener, 5 parts of ethohexadiol, 5 parts of sodium alginate, wood
7 parts of melon protease, 14 parts of sodium bicarbonate, 12 parts of sodium carbonate, modified 6 parts of river sand, neutral 1 part of kaolin, 3 parts of jasmine pollen, west
4 parts of red persimmon red pigment；
Wherein, 5 μm of the Jasmine Powder Particle Size；The modified river sand and 3 μm of kaolinic granularity.
Preferably, the jasmine pollen is prepared using following methods:
Take new fresh jasmine, be placed in clear water and rinse 1~2 time, shut down each petal, be put into concentration be 85% it is anhydrous
In ethyl alcohol, the amount ratio of the Jasmine and ethyl alcohol is 1:8, hot 10~12min of reflow treatment at 65~70 DEG C, terminates heat and returns
Stream process, constant temperature impregnate 35~40min, and dehydrated alcohol is recycled in filtering, obtain dehydrated alcohol S, the dehydrated alcohol S and acidity
The dehydrated alcohol of the hot reflow treatment of river sand is identical；
It taking jasmine petal to be placed in clear water to eluriate 2~3 times, air-dried moisture is dried to water content≤8%, it crushed 5 μm of sieves,
Jasmine pollen is made.
Preferably, the modified river sand is prepared using following methods:
A large amount of river sands are taken, is placed in clear water and eluriates completely, drain, cross 1mm sieve, takes sieve is upper partially to cross 3mm sieve, takes lower part of screen
The deionized water for dividing 3~5 times of addition stirs 15~20min at a temperature of 28~32 DEG C, and the concentrated sulfuric acid that concentration is 80% is added
62~65ml stirs 20~25min, is heated to 45~50 DEG C in draught cupboard, continues 1.2~1.5h of stirring, be cooled to room temperature,
Liquid out, it is 6.8~6.9 that river sand group, which selects clear water to wash to pH, is dried to water content≤11% in 85~95 DEG C of dryer,
It crushed 5 μm of sieves, it is spare to obtain acid river sand；
Acid river sand is taken, the kaolin for accounting for acid river sand gross weight 1/10 is added, kaolinite soil granularity≤5 μm add
The deionized water for accounting for 3~5 times of acid river sand, in 25~30 DEG C of temperature, stir stirring 25 under conditions of 120~125r/min of speed~
30min stands 2~3h, and 15~20min is centrifuged in the centrifuge of 3500~3800r/min, removes supernatant, bottom object is through 5
μm the screen to filtrate, 1~3 layer of gauze of pad on strainer；Solid is taken to pour into the dehydrated alcohol S of 3~5 times of quality, hot reflow treatment
10~12min recycles dehydrated alcohol S, and solid is dried to water content≤9%, grinds, and crosses 3 μm of sieves, obtains modified river sand.
Preferably, the neutral kaolin is prepared using following methods:
Take kaolin, be dried to water content≤11%, ground 5 μm of sieves, lower part of screen pour in separately into mass fraction be 15% it is white
In vinegar, control light-coloured vinegar is totally submerged kaolin；In 30~32 DEG C of temperature, stir stirring 15 under conditions of 350~400r/min of speed~
20min, filtering, filter residue pour into clear water, until clear water submerges filter residue, the sodium hydroxide 35ml that mass concentration is 8% is added, in
120~130r/min's stirs 15~20min of stirring at normal temperature under speed, and filtering is selected clear water to wash filter residue pH to 7.0, is dried to aqueous
3 μm of sieves are crossed in amount≤9%, grinding, and neutrality kaolin is made.
Preferably, the softener is purification glucose ester based quaternary ammonium salt, is processed into using following methods:
Glucose ester based quaternary ammonium salt is taken, is poured into the deionized water for accounting for 3~5 times of glucose ester based quaternary ammonium salt gross weight, Yu Wen
45~50 DEG C of degree, stir 1350~1500r/min of speed stir under speed 30~35min of stirring, 60~90min of standing, with 4500~
The rate of 6000r/min is centrifuged 10~12min, removes supernatant, takes slurries, through 5 μm of the screen to filtrates, on strainer 2~3 layers of pad it is clean
Net gauze, takes solid powder to be dried to water content≤5%, and purification glucose ester based quaternary ammonium salt is made in ground 1 μm of sieve.
In the technical solution provided by the present invention, the washing cloth grass is the white powder of granularity≤5 μm with washing powder shape
End.
The beneficial effects of the present invention are:
Compared with prior art, the present invention selects environment-friendly materials to make each raw material of washing powder, passes through addition glucose ester
Based quaternary ammonium salt makees softener, and softness is stablized, and dosage is small, and prominent biological degradability is environmentally protective, more with anti-yellowing
The multiple functions such as change, sterilizing effectively overcome the problems, such as existing washing powder pollution on the environment, prevent cloth grass after washing from sending out
Xanthochromia is hard；Meanwhile high-carbon is pure makees defoaming agent by addition by the present invention, effectively reduces the bubble that finished product washing powder is generated in washing
Foam, readily volatilized, environmental sound will not also inhibit washing effect；Furthermore the present invention makees carrier by modified river sand, reaches
Suspension effect is helped, the washing effect of washing powder is improved；Secondly, the present invention by addition papain, effectively inhibits after washing
The electrostatic effect of cloth grass reduces injury of the cloth grass to human body after washing；Finally, the present invention is red by natural-plant-essence-tomato
The addition of element reduces stimulation of the washing powder to body, reduces injury of the washing powder to human body, improves cloth grass after washing powder washs
Sun-proof, ultraviolet ray preventing effect.
Specific embodiment
The present invention is further described in detail With reference to embodiment, but technical solution provided by the invention
It not only include the content showed in embodiment.
Embodiment 1
Present embodiments provide a kind of washing powder for washing cloth grass, including following raw material:
18 parts of dioctyl sodium sulfosuccinate, there is building action, be used as active constituent；
3 parts of methyl anyl alcohol, it is used as dispersing agent；
It is 5 parts of softener, soft for cloth grass after guaranteeing washing, it is smooth；
5 parts of ethohexadiol, it is used as defoaming agent, reduces foams of washing powder, but do not inhibit washing effect；
5 parts of sodium alginate, ingredient is washed as helping；
7 parts of papain, it is used as synergistic component, weakens the electrostatic efficiency of cloth grass after washing, achieve the purpose that antistatic；
14 parts of sodium bicarbonate, it is used as active constituent；
12 parts of sodium carbonate, ingredient is washed as helping；
Modified 6 parts of river sand, as buffer composition, helps and washes ingredient, the carrier as washing powder；
1 part of neutral kaolin is used as auxiliary element；
3 parts of jasmine pollen, it is used as synergistic component, so that finished product washing powder is fragrant with jasmine, while reaches antibiotic and sterilizing
Effect；
4 parts of lycopene, it is used as synergistic component, increases the sun-proof and ultraviolet ray preventing effect of cloth grass after washing, decrease is washed
Rear cloth grass is washed to the stimulation of human body；
Wherein, 5 μm of the Jasmine Powder Particle Size；The modified river sand and 3 μm of kaolinic granularity.
In the present embodiment, the jasmine pollen is prepared using following methods:
New fresh jasmine is taken, is placed in clear water and rinses 1 time, shut down each petal, is put into the anhydrous second that concentration is 85%
In alcohol, the amount ratio of the Jasmine and ethyl alcohol is 1:8, and the hot reflow treatment 10min at 70 DEG C terminates hot reflow treatment, permanent
Temperature impregnates 35min, and filtering recycles dehydrated alcohol, obtains dehydrated alcohol S, at the hot reflux of the dehydrated alcohol S and acid river sand
The dehydrated alcohol of reason is identical；
It takes jasmine petal to be placed in clear water to eluriate 2 times, air-dried moisture, being dried to water content is 8%, crushed 5 μm of sieves, is made
Jasmine pollen.
In the present embodiment, the modified river sand is prepared using following methods:
A large amount of river sands are taken, is placed in clear water and eluriates completely, drain, cross 1mm sieve, takes sieve is upper partially to cross 3mm sieve, takes lower part of screen
The deionized water for dividing 5 times of addition stirs 15min at a temperature of 32 DEG C, and the concentrated sulfuric acid 65ml that concentration is 80% is added, stirring
25min is heated to 50 DEG C in draught cupboard, continues to stir 1.2h, be cooled to room temperature, and pours out liquid, and river sand group selects clear water washing
It is 6.9 to pH, it is 11% that water content is dried in 95 DEG C of dryer, crushed 5 μm of sieves, it is spare to obtain acid river sand；
Acid river sand is taken, the kaolin for accounting for acid river sand gross weight 1/10 is added, the kaolinite soil granularity is 5 μm, is added
The deionized water for accounting for 3 times of acid river sand, in 30 DEG C of temperature, stir fast 120r/min under conditions of stir 25min, stand 3h, in
It is centrifuged 20min in the centrifuge of 3500r/min, removes supernatant, bottom object pads 1 layer of cleaning on strainer through 5 μm of the screen to filtrate
Gauze；Solid is taken to pour into the dehydrated alcohol S of 5 times of quality, hot reflow treatment 10min recycles dehydrated alcohol S, and solid, which is dried to, to be contained
Water is 9%, grinding, crosses 3 μm of sieves, obtains modified river sand.
In the present embodiment, the neutral kaolin is prepared using following methods:
Take kaolin, be dried to water content be 11%, it is ground 5 μm sieve, lower part of screen pour in separately into mass fraction be 15% it is white
In vinegar, control light-coloured vinegar is totally submerged kaolin；In 30 DEG C of temperature, stir fast 400r/min under conditions of stir 15min, filter, filter
Slag pours into clear water, until clear water submerges filter residue, the sodium hydroxide 35ml that mass concentration is 8% is added, stirs speed in 120r/min
Lower stirring at normal temperature 20min, filtering select clear water to wash filter residue pH to 7.0, and being dried to water content is 9%, and 3 μm of sieves are crossed in grinding,
Neutrality kaolin is made.
In the present embodiment, the softener is purification glucose ester based quaternary ammonium salt, is processed into using following methods:
Glucose ester based quaternary ammonium salt is taken, is poured into the deionized water for accounting for 5 times of glucose ester based quaternary ammonium salt gross weight, in temperature 45
DEG C, stir stirring under speed for fast 1350r/min and stir 35min, stand 90min, 12min be centrifuged with the rate of 4500r/min, in removal
Clear liquid takes slurries, and through 5 μm of the screen to filtrates, 2 layers of pad clean gauze on strainer, taking solid powder to be dried to water content is 5%, grinding
1 μm of sieve is crossed, purification glucose ester based quaternary ammonium salt is made.
Embodiment 2
The washing powder for present embodiments providing a kind of cloth grass washing, specifically includes following raw material:
22 parts of dioctyl sodium sulfosuccinate, there is building action, be used as active constituent；
3 parts of methyl anyl alcohol, it is used as dispersing agent；
It is 7 parts of softener, soft for cloth grass after guaranteeing washing, it is smooth；
4 parts of ethohexadiol, it is used as defoaming agent, reduces foams of washing powder, but do not inhibit washing effect；
5 parts of sodium alginate, ingredient is washed as helping；
5 parts of papain, it is used as synergistic component, weakens the electrostatic efficiency of cloth grass after washing, achieve the purpose that antistatic；
20 parts of sodium bicarbonate, it is used as active constituent；
8 parts of sodium carbonate, ingredient is washed as helping；
Modified 9 parts of river sand, as buffer composition, helps and washes ingredient, the carrier as washing powder；
3 parts of neutral kaolin is used as auxiliary element；
5 parts of jasmine pollen, it is used as synergistic component, so that finished product washing powder is fragrant with jasmine, while reaches antibiotic and sterilizing
Effect；
2 parts of lycopene, it is used as synergistic component, increases the sun-proof and ultraviolet ray preventing effect of cloth grass after washing, decrease is washed
Rear cloth grass is washed to the stimulation of human body；
Wherein, 3 μm of the Jasmine Powder Particle Size；The modified river sand and 1 μm of kaolinic granularity.
In the present embodiment, the jasmine pollen is prepared using following methods:
New fresh jasmine is taken, is placed in clear water and rinses 2 times, shut down each petal, is put into the anhydrous second that concentration is 85%
In alcohol, the amount ratio of the Jasmine and ethyl alcohol is 1:8, and the hot reflow treatment 12min at 65 DEG C terminates hot reflow treatment, permanent
Temperature impregnates 40min, and filtering recycles dehydrated alcohol, obtains dehydrated alcohol S, at the hot reflux of the dehydrated alcohol S and acid river sand
The dehydrated alcohol of reason is identical；
It takes jasmine petal to be placed in clear water to eluriate 3 times, air-dried moisture, being dried to water content is 6%, crushed 3 μm of sieves, is made
Jasmine pollen.
Preferably, the modified river sand is prepared using following methods:
A large amount of river sands are taken, is placed in clear water and eluriates completely, drain, cross 1mm sieve, takes sieve is upper partially to cross 3mm sieve, takes lower part of screen
The deionized water for dividing 3 times of addition stirs 20min at a temperature of 30 DEG C, and the concentrated sulfuric acid 62ml that concentration is 80% is added, stirring
25min is heated to 45 DEG C in draught cupboard, continues to stir 1.5h, be cooled to room temperature, and pours out liquid, and river sand group selects clear water washing
It is 6.8 to pH, it is 9% that water content is dried in 85 DEG C of dryer, crushed 5 μm of sieves, it is spare to obtain acid river sand；
Acid river sand is taken, the kaolin for accounting for acid river sand gross weight 1/10 is added, the kaolinite soil granularity is 3 μm, is added
The deionized water for accounting for 3 times of acid river sand, in 30 DEG C of temperature, stir fast 130r/min under conditions of stir 20min, stand 2h, in
It is centrifuged 15min in the centrifuge of 3800r/min, removes supernatant, bottom object pads 3 layers of yarn on strainer through 5 μm of the screen to filtrate
Cloth；Solid is taken to pour into the dehydrated alcohol S of 3 times of quality, hot reflow treatment 15min recycles dehydrated alcohol S, and solid is dried to aqueous
Amount is 5%, grinding, crosses 1 μm of sieve, obtains modified river sand.
In the present embodiment, the neutral kaolin is prepared using following methods:
Kaolin is taken, being dried to water content is 9%, ground 5 μm of sieves, the light-coloured vinegar that it is 15% into mass fraction that lower part of screen, which is poured in separately,
In, control light-coloured vinegar is totally submerged kaolin；In 32 DEG C of temperature, stir fast 350r/min under conditions of stir 20min, filter, filter residue
It pours into clear water, until clear water submerges filter residue, the sodium hydroxide 35ml that mass concentration is 8% is added, stirs speed in~130r/min
Lower stirring at normal temperature 15min, filtering select clear water to wash filter residue pH to 7.0, and being dried to water content is 7%, and 1 μm of sieve is crossed in grinding,
Neutrality kaolin is made.
In the present embodiment, the softener is purification glucose ester based quaternary ammonium salt, is processed into using following methods:
Glucose ester based quaternary ammonium salt is taken, is poured into the deionized water for accounting for 3 times of glucose ester based quaternary ammonium salt gross weight, in temperature 50
DEG C, stir stirring under speed for fast 1500r/min and stir 30min, stand 60min, 10min be centrifuged with the rate of 6000r/min, in removal
Clear liquid takes slurries, and through 5 μm of the screen to filtrates, 3 layers of pad clean gauze on strainer, taking solid powder to be dried to water content is 3%, grinding
1 μm of sieve is crossed, purification glucose ester based quaternary ammonium salt is made.
Implement 3
A kind of washing methods of hotel's cloth grass is present embodiments provided, the washing powder is what embodiment 1 produced
Cloth grass washing washing powder, the white powder that the washing powder shape is 3 μm of granularity, specific washing process are as follows:
A, prewashing: by sheet investment washing machine to be washed, sheet 40kg to be washed is put into, the processing life of embodiment 1 is added
The cloth grass washing washing powder 45g of output, injects after 140kg water and washs 3min with 31r/min, water is completely exhausted out in 50s；
B, master washes: after water is completely exhausted out, the cloth grass washing laundry that embodiment 1 produces being added into washing machine
Powder 520g injects 100kg water, and setting temperature is 75 DEG C and is washed, in 50s that water is complete after washing 15min with 31r/min
Full discharge；
C, cross in water and take off: injection 320kg water washs 2min with 31r/min, water is completely exhausted out in 50s, is reinjected
320kg water, washs 2min with 31r/min, is dehydrated 4min with 310r/min；
D, cross water draining: injection 320kg water washs 2min with 31r/min, water is completely exhausted out in 50s, is reinjected
320kg water washs 2min with 31r/min, water is completely exhausted out in 50s；
E, neutralize: neutralizer 120g is added in injection 100kg water, and setting temperature is 40 DEG C, in 31r/min and 5min,
Water is completely exhausted out in 50s；
F, high de-: to fill 320kg water, 2min is washed with 31r/min, 5min is dehydrated with 680r/min；
G, it dries: dewatered sheet is taken out, be put into standing suspension type drying unit the dry 10min at 75 DEG C,
Obtain the sheet of washes clean.
In the present embodiment, it tests to the sheet washed out, the sheet after discovery drying is fragrant with light jasmine
Taste, it is soft smooth, it slowly generates heat under rubbing action, and generated without electrostatic.
In the present embodiment, component content measurement also being carried out with water to after washing, discovery phosphorus content is 0.0012mg/L,
Content of beary metal is 0.003mg/L.
The above described is only a preferred embodiment of the present invention, being not intended to limit the present invention in any form, appoint
What without departing from technical solution of the present invention content, according to the technical essence of the invention any modification to the above embodiments, etc.
With variation and modification, all of which are still within the scope of the technical scheme of the invention.
Claims (6)
1. a kind of washing cloth grass washing powder, which is characterized in that including following raw material:
13~22 parts of dioctyl sodium sulfosuccinate, 3~5 parts of methyl anyl alcohol, 4~7 parts of softener, 4~8 parts of ethohexadiol, seaweed
3~5 parts of sour sodium, 5~8 parts of papain, 10~20 parts of sodium bicarbonate, 8~16 parts of sodium carbonate, modified 5~9 parts of river sand, in
Property 1~3 part of kaolin, 3~5 parts of jasmine pollen, 2~4 parts of lycopene；
Wherein, Jasmine Powder Particle Size≤0.5 μm；The modified river sand and kaolinic granularity≤0.5 μm.
2. a kind of washing cloth grass washing powder according to claim 1, which is characterized in that including following raw material:
18 parts of dioctyl sodium sulfosuccinate, 3 parts of methyl anyl alcohol, 5 parts of softener, 5 parts of ethohexadiol, 5 parts of sodium alginate, pawpaw egg
7 parts of white enzyme, 14 parts of sodium bicarbonate, 12 parts of sodium carbonate, modified 6 parts of river sand, neutral 1 part of kaolin, 3 parts of jasmine pollen, tomato
4 parts of red pigment；
Wherein, 5 μm of the Jasmine Powder Particle Size；The modified river sand and 3 μm of kaolinic granularity.
3. a kind of washing cloth grass washing powder according to claim 1 or 2, which is characterized in that the jasmine pollen uses
Following methods are prepared:
New fresh jasmine is taken, is placed in clear water and rinses 1~2 time, shut down each petal, is put into the dehydrated alcohol that concentration is 85%
In, the amount ratio of the Jasmine and ethyl alcohol is 1:8, and hot 10~12min of reflow treatment, terminates at hot reflux at 65~70 DEG C
Reason, constant temperature impregnate 35~40min, and filtering recycles dehydrated alcohol, obtains dehydrated alcohol S；
It takes jasmine petal to be placed in clear water to eluriate 2~3 times, air-dried moisture is dried to water content≤8%, crushed 5 μm of sieves, is made
Jasmine pollen.
4. a kind of washing cloth grass washing powder according to claim 1 or 2, which is characterized in that the modified river sand uses
Following methods are prepared:
A large amount of river sands are taken, elutriation in clear water is placed in and completely, drains, cross 1mm sieve, take sieve above partially to cross 3mm sieve, lower part of screen point is taken to add
The deionized water for entering 3~5 times, 15~20min of stirring at a temperature of 28~32 DEG C, the concentrated sulfuric acid 62 that addition concentration is 80%~
65ml stirs 20~25min, is heated to 45~50 DEG C in draught cupboard, continues 1.2~1.5h of stirring, be cooled to room temperature, pour out liquid
Body, it is 6.8~6.9 that river sand group, which selects clear water to wash to pH, and water content≤11% is dried in 85~95 DEG C of dryer, is crushed
5 μm of sieves are crossed, it is spare to obtain acid river sand；
Acid river sand is taken, the kaolin for accounting for acid river sand gross weight 1/10 is added, kaolinite soil granularity≤5 μm add and account for acid
Property 3~5 times of river sand of deionized water, in 25~30 DEG C of temperature, stir 120~125r/min of speed under conditions of stir 25~30min,
2~3h is stood, 15~20min is centrifuged in the centrifuge of 3500~3800r/min, removes supernatant, bottom object is through 5 μm of sieve
Net filtration, 1~3 layer of gauze of pad on strainer；Solid is taken to pour into the dehydrated alcohol S of 3~5 times of quality, hot reflow treatment 10~
12min recycles dehydrated alcohol S, and solid is dried to water content≤9%, grinds, and crosses 3 μm of sieves, obtains modified river sand.
5. a kind of washing cloth grass washing powder according to claim 1 or 2, which is characterized in that the neutrality kaolin is adopted
It is prepared with following methods:
Kaolin is taken, water content≤11%, ground 5 μm of sieves are dried to, lower part of screen pours in separately in the light-coloured vinegar that mass fraction is 15%,
Control light-coloured vinegar is totally submerged kaolin；In 30~32 DEG C of temperature, stirs and stirs 15~20min under conditions of 350~400r/min of speed,
Filtering, filter residue pours into clear water, until clear water submerges filter residue, the sodium hydroxide 35ml that mass concentration is 8% is added, in 120~
130r/min's stirs 15~20min of stirring at normal temperature under speed, and filtering selects clear water to wash filter residue pH to 7.0, be dried to water content≤
9%, 3 μm of sieves are crossed in grinding, and neutrality kaolin is made.
6. a kind of washing cloth grass washing powder according to claim 1 or 2, which is characterized in that the softener is purification
Glucose ester based quaternary ammonium salt, is processed into using following methods:
Glucose ester based quaternary ammonium salt is taken, is poured into the deionized water for accounting for 3~5 times of glucose ester based quaternary ammonium salt gross weight, in temperature 45
~50 DEG C, stir 1350~1500r/min of speed stir under speed 30~35min of stirring, 60~90min is stood, with 4500~6000r/
The rate of min is centrifuged 10~12min, removes supernatant, takes slurries, through 5 μm of the screen to filtrates, 2~3 layers of pad clean yarn on strainer
Cloth, takes solid powder to be dried to water content≤5%, and purification glucose ester based quaternary ammonium salt is made in ground 1 μm of sieve.
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Application publication date: 20190118 |