CN109206993A - A kind of environment-friendly type aqueous wooden ware sealing priming paint and preparation method thereof - Google Patents
A kind of environment-friendly type aqueous wooden ware sealing priming paint and preparation method thereof Download PDFInfo
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- CN109206993A CN109206993A CN201810765865.5A CN201810765865A CN109206993A CN 109206993 A CN109206993 A CN 109206993A CN 201810765865 A CN201810765865 A CN 201810765865A CN 109206993 A CN109206993 A CN 109206993A
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- agent
- priming paint
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- friendly type
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
Abstract
The present invention relates to a kind of environment-friendly type aqueous wooden ware sealing priming paint and preparation method thereof comprising following raw material: nanometer water acrylic resin aqueous solution, pH adjusting agent, defoaming agent, coalescing agent, grinding auxiliary agent, moistening flatting agent, deionized water, water-protected enclosure agent, thickener.The priming paint has permeability outstanding and closure, the significantly exudation of inhibition water colo(u)r or tannic acid, and moisture in upper coating is inhibited to penetrate into timber, prevents timber from rising muscle, meanwhile, also have many advantages, such as hardness height, fast drying, coating specification can be met.
Description
Technical field
The present invention relates to water-borne wood coating field more particularly to a kind of environment-friendly type aqueous wooden ware sealing priming paint and its preparations
Method.
Background technique
In recent years, with the improvement of people's environmental awareness, water-borne wood coating is constantly subjected to apply because of the advantage in terms of environmental protection
Expect the concern of manufacturer and people, but there is also many insoluble problems, such as light color to apply in construction and extension process
The main reason for the problem of material or white coating bleeding, bleeding is: water-borne wood coating is a kind of using water as the spy of decentralized medium
Different dispersion, when being coated on the wood surface with water-wet behavior, moisture is easily infiltrated through in timber, and the water in timber
The contact of dissolubility coloring matter, these coloring matters can be dissolved in the water, slowly spread then as paint film drying process, and final
It migrates to film coated surface, forms the color spot of yellow or brown, or deepen entire film colour changed into yellow.Reduce water colo(u)r or
Tannic acid exudation most simple effective method first is that coating seal coat.
In addition, the muscle problem that rises of solid wood is a water-borne wood coating the problem of not can avoid in popularization and application.
Since, containing the relationship of moisture, when coating water-borne wood coating, the non-volatile moisture of film can be from timber in timber
Surface penetration is entered, so that the original water balance of timber is destroyed, so that the conduit of wood surface and some wood thorn bulging are got up,
Original smooth of wood surface is destroyed, the muscle phenomenon that rises occurs.
Summary of the invention
For bleeding existing for aqueous wooden ware seal coat currently on the market and solid wood rise muscle the problems such as, the present invention provide
A kind of environment-friendly type aqueous wooden ware sealing priming paint.
And the present invention also provides the preparation methods of above-mentioned environment-friendly type aqueous wooden ware sealing priming paint.
To achieve the above object of the invention, the embodiment of the present invention adopts the technical scheme that
A kind of environment-friendly type aqueous wooden ware sealing priming paint, the raw material including following parts by weight proportion:
Dispersion degree is high in water for the nanometer water acrylic resin aqueous solution that the present invention is added in formula, and partial size exists
Nanometer range has permeability more outstanding and closure, it is easier to which the pore filled up in substrate is allowed to close, and reduces substrate
Middle open hole number improves integrally closed performance, to inhibit the exudation of water colo(u)r or tannic acid significantly, and inhibits upper layer
Moisture in coating penetrates into timber, prevents timber from rising muscle.In addition, nanometer water acrylic resin also have hardness height, fast drying,
The advantages that transparency is high can make coating become that uniformly, coating specification can be met.The water-protected enclosure agent of addition can prevent moisture
Intrusion, can be cooperateed under optimum ratio with nanometer water acrylic resin performance prevent moisture immerse timber effect, solution
Certainly bleeding and the muscle problem that rises, while can also prevent from damaging by worms and mould breeds, are effectively protected timber, improve the durability of wood and
Anti-corrosive properties.
Preferably, the nanometer water acrylic resin aqueous solution includes nanometer water emulsion acrylic resin, nanometer
Water-based acrylic resin aqueous dispersion or nanometer water acrylic resin aqueous solution.Lotion, aqueous dispersion or aqueous solution easily exist
Rapid dispersion in water keeps the production technology of the priming paint more convenient, and volatile organic solvent (VOCs) content is extremely low, has higher
Safety and the feature of environmental protection.Such as the HD2535 of Hua Jinsi company of the U.S..
Preferably, the water-protected enclosure agent is infiltration type wood preservation sealer.Such water-protected enclosure agent is a kind of nontoxic
Substance, biodegradable, environmental sound can prevent moisture content from corroding, and play sealing to timber and enhance the density of timber
With the effect of hardness, moreover it is possible to protect the connectivity between sealing wax and timber, extending the service life of coating can also prevent up to 3 times, and simultaneously
It only damages by worms and is bred with mould.If France first creates the tannic acid sealer SYNTHRON-STAIN 473 of chemistry, which is inorganic
Metallic solution is free of zinc, VOC and helium.
Preferably, the grinding auxiliary agent is water-based calcium stearate suspension.Water-based calcium stearate suspension have it is easy to polish,
Fast drying, the advantage that defoaming is easy, thermal denaturation resistant is good, fillibility is good, and can be improved coating surface hydrophobicity, improve paint film hand
Sense, as Guangzhou paulownia reaches the YZS-043 of chemical engineering Co., Ltd.
Preferably, the moistening flatting agent is Siloxane-Oxyalkylene Copolymers class wetting agent, can play and increase sliding, levelling work
With, make priming paint film forming after-vision effect it is plentiful, so that upper coating is easier to coating.
Preferably, the pH adjusting agent is amine neutralizer, not only has the effect of adjusting pH value, and be organic in itself
Substance has the characteristic of certain auxiliary film forming.
Preferably, the defoaming agent is organic oils defoaming agent, such defoaming agent removes foam, the pin hole that can be gone in priming paint
And the air being mingled with is without generating surface defect, such as U.S. aerochemistry defoaming agent Airase4500.
Preferably, the coalescing agent be waterborne film-forming auxiliary agent, such coalescing agent have higher boiling, low evaporation rate,
Extremely low smell, extremely low VOC, the advantages that APE, hydrolysis-stable, energy biodegrade is free of, such as the DIB coalescing agent of Luo Diya, boiling point
Up to 275-295 DEG C
The thickener is polyurethane-type water-based thickener, has strong false rheological properties, excellent shearing dilute
The characteristics of change and high sag resistance can use within the scope of very wide pH, such as the bright icepro of GermanyPUR
65。
Further, the present invention also provides the preparation methods of above-mentioned environment-friendly type aqueous wooden ware sealing priming paint.The preparation method
It at least includes the following steps:
Step a, weigh each raw material component by the formula of above-mentioned environment-friendly type aqueous wooden ware sealing priming paint, under stirring to
PH adjusting agent, defoaming agent, coalescing agent, grinding auxiliary agent, wetting stream are successively added in nanometer water acrylic resin aqueous solution
Flat agent, deionized water, water-protected enclosure agent are uniformly mixed；
Step b, it is 90s~110s with -4 glasss of viscosity of painting that mixture viscosity obtained by step a is adjusted to 25 DEG C by thickener, stirs
Mix to be uniformly mixed to get.
The preparation method of environment-friendly type aqueous wooden ware sealing priming paint provided by the invention is easy to operate, is suitable for mass production behaviour
Make.
Preferably, the speed stirred in step a is 900~1200r/min, and mixing is carried out under low whipping speed can make respectively
Raw material is faster evenly dispersed in nanometer water acrylic resin aqueous solution, avoids agglomerating in adition process.It is described mixed
It closes uniformly as with the speed of 400~600r/min stirring 15~25 minutes.Preferably mixing speed and time can make raw material group
Point mix more evenly, be unlikely to that speed is excessively slow or the time is too short and mix uneven or excessive velocities, overlong time and stir into gas
Bubble.
Preferably, it is uniformly mixed described in step b as with the speed of 700~900r/min stirring 15~25 minutes.It is preferred that
Ground mixing speed and time can be such that thickener and mixture is sufficiently mixed uniformly, avoid being layered.
Specific embodiment
In order to make the objectives, technical solutions, and advantages of the present invention clearer, below in conjunction with specific embodiment, to this
Invention is further elaborated.It should be appreciated that specific embodiment described herein is used only for explaining the present invention, not
For limiting the present invention.
Embodiment 1
The embodiment of the present invention provides a kind of environment-friendly type aqueous wooden ware sealing priming paint and preparation method thereof, including following parts by weight
The raw material of number proportion:
Wherein, nanometer water emulsion acrylic resin is the HD2535 of U.S. Hua Jinsi company, and pH adjusting agent is U.S.'s pottery
The AMP-95 of family name, defoaming agent are U.S.'s aerochemistry defoaming agent Airase4500, and coalescing agent is that the DIB film forming of Rhodia helps
Agent, grinding auxiliary agent are the YZS-043 that Guangzhou paulownia reaches chemical engineering Co., Ltd, and moistening flatting agent is the BYK331 of Germany Bi Ke,
Water-protected enclosure agent is the tannic acid sealer SYNTHRON-STAIN 473 that France first creates chemistry, and thickener is the bright icepro of GermanyPUR 65。
The priming paint the preparation method comprises the following steps:
Step a, each raw material component is weighed according to above-mentioned formula, to nanometer water propylene under the stirring of 900r/min
Successively added in acid resin lotion amine neutralizer, organic oils defoaming agent, waterborne film-forming auxiliary agent, water-based calcium stearate suspension,
Siloxane-Oxyalkylene Copolymers class wetting agent, deionized water, infiltration type wood preservation sealer stir 25 with the speed of 400r/min
Minute, it is allowed to uniformly mixed；
Step b, it is by -4 glasss of viscosity of painting that mixture viscosity obtained by step a is adjusted to 25 DEG C with polyurethane aqueous thickener
90s, with the speed of 700r/min stir 25 minutes to be uniformly mixed to get.
Embodiment 2
The embodiment of the present invention provides a kind of environment-friendly type aqueous wooden ware sealing priming paint and preparation method thereof, including following parts by weight
The raw material of number proportion:
Wherein, nanometer water emulsion acrylic resin is the HD2535 of U.S. Hua Jinsi company, and pH adjusting agent is U.S.'s pottery
The AMP-95 of family name, defoaming agent are U.S.'s aerochemistry defoaming agent Airase4500, and coalescing agent is that the DIB film forming of Rhodia helps
Agent, grinding auxiliary agent are the YZS-043 that Guangzhou paulownia reaches chemical engineering Co., Ltd, and moistening flatting agent is the BYK331 of Germany Bi Ke,
Water-protected enclosure agent is the tannic acid sealer SYNTHRON-STAIN 473 that France first creates chemistry, and thickener is the bright icepro of GermanyPUR 65。
The priming paint the preparation method comprises the following steps:
Step a, each raw material component is weighed according to above-mentioned formula, to nanometer water third under the stirring of 1200r/min
Amine neutralizer, organic oils defoaming agent, waterborne film-forming auxiliary agent, water-based calcium stearate is successively added in olefin(e) acid resin emulsion to suspend
Liquid, Siloxane-Oxyalkylene Copolymers class wetting agent, deionized water, infiltration type wood preservation sealer, are stirred with the speed of 600r/min
It mixes 15 minutes, is allowed to uniformly mixed；
Step b, it is by -4 glasss of viscosity of painting that mixture viscosity obtained by step a is adjusted to 25 DEG C with polyurethane aqueous thickener
110s, with the speed of 900r/min stir 15 minutes to be uniformly mixed to get.
Embodiment 3
The embodiment of the present invention provides a kind of environment-friendly type aqueous wooden ware sealing priming paint and preparation method thereof, including following parts by weight
The raw material of number proportion:
Wherein, nanometer water emulsion acrylic resin is the HD2535 of U.S. Hua Jinsi company, and pH adjusting agent is U.S.'s pottery
The AMP-95 of family name, defoaming agent are U.S.'s aerochemistry defoaming agent Airase4500, and coalescing agent is that the DIB film forming of Rhodia helps
Agent, grinding auxiliary agent are the YZS-043 that Guangzhou paulownia reaches chemical engineering Co., Ltd, and moistening flatting agent is the BYK331 of Germany Bi Ke,
Water-protected enclosure agent is the tannic acid sealer SYNTHRON-STAIN 473 that France first creates chemistry, and thickener is the bright icepro of GermanyPUR 65。
The priming paint the preparation method comprises the following steps:
Step a, each raw material component is weighed according to above-mentioned formula, to nanometer water third under the stirring of 1000r/min
Amine neutralizer, organic oils defoaming agent, waterborne film-forming auxiliary agent, water-based calcium stearate is successively added in olefin(e) acid resin emulsion to suspend
Liquid, Siloxane-Oxyalkylene Copolymers class wetting agent, deionized water, infiltration type wood preservation sealer, are stirred with the speed of 500r/min
It mixes 20 minutes, is allowed to uniformly mixed；
Step b, it is by -4 glasss of viscosity of painting that mixture viscosity obtained by step a is adjusted to 25 DEG C with polyurethane aqueous thickener
100s, with the speed of 800r/min stir 20 minutes to be uniformly mixed to get.
Embodiment 4
Using it is commercially available using nanometer water emulsion acrylic resin as the aqueous wooden ware seal coat of principal component as a comparison case,
By the environment-friendly type aqueous wooden ware sealing priming paint in the above various embodiments and performance comparison is carried out, the results are shown in Table 1.
Table 1
| Project | The method of inspection | Embodiment 1 | Embodiment 2 | Embodiment 3 | Comparative example |
| Water resistance | GB/T 4893.1 | 400 hours | 400 hours | 400 hours | 200 hours |
| Alkali resistance | GB/T 23999 | 12 hours | 12 hours | 12 hours | 6 hours |
| Alcohol resistance | GB/T 23999 | 24 hours | 24 hours | 24 hours | 16 hours |
| Surface drying time | 1728 second method of GB/T | 20 minutes | 17 minutes | 18 minutes | 30 minutes |
| Do solid work the time | 1728 first method of GB/T | 6 hours | 5.5 hour | 5.5 hour | 18 hours |
| Grinability | GB/T 23999 | Easily polish | Easily polish | Easily polish | It is easy to polish |
| Hardness | GB/T 6739 | 2H | 2H | 2H | H |
| Adhesive force | GB/T 9286 | 1 grade | 1 grade | 1 grade | 2 grades |
| Wearability | GB/T 1768 | 0.015 | 0.015 | 0.015 | 0.025 |
| It is bleed | ISO 787-22 | Not bleeding | Not bleeding | Not bleeding | Slight bleeding |
| The anti-muscle that rises | Spray the range estimation of pine substrate | Do not rise muscle | Do not rise muscle | Do not rise muscle | Slightly rise muscle |
In GB/T23999-2009 standard, it is desirable that paint film meet it is water-fast >=24 hours, alkaline-resisting >=1 hour, resistance to alcohol >=1 is small
When, wearability≤0.03, the environment-friendly type aqueous wooden ware sealing priming paint of various embodiments of the present invention is much higher than standard after forming a film
It is required that having excellent water resistance, alkali resistance, alcohol resistance and wearability, and it is substantially better than comparative example.By other examinations in table 1
Result is tested as it can be seen that the product of each embodiment also has the surface drying time more shorter than comparative example and does solid work the time.Therefore, by tying above
Fruit can unambiguously infer, the environment-friendly type aqueous wooden ware sealing priming paint of each embodiment can reach preferably prevent bleeding and
Solid wood rises the effect of muscle.Also, each embodiment product also has better grinability, hardness and adhesive force, can preferably protect
Guard timber material, and be conducive to the coating of upper coating.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention
Made any modification, equivalent replacement or improvement etc., should all be included in the protection scope of the present invention within mind and principle.
Claims (9)
1. a kind of environment-friendly type aqueous wooden ware sealing priming paint, it is characterised in that: the raw material including following weight percent:
2. environment-friendly type aqueous wooden ware sealing priming paint according to claim 1, it is characterised in that: the nanometer water acrylic acid
Resin aqueous solution includes nanometer water emulsion acrylic resin, nanometer water aqueous acrylic resin dispersion or nanometer water third
Olefin(e) acid resin aqueous solution.
3. environment-friendly type aqueous wooden ware sealing priming paint according to claim 1, it is characterised in that: the water-protected enclosure agent is to seep
Saturating formula wood preservation sealer.
4. environment-friendly type aqueous wooden ware sealing priming paint according to claim 1, it is characterised in that: the grinding auxiliary agent is aqueous
Calcium stearate suspension.
5. environment-friendly type aqueous wooden ware sealing priming paint according to claim 1, it is characterised in that: the moistening flatting agent is poly-
Ether modified polyorganosiloxane class wetting agent.
6. environment-friendly type aqueous wooden ware sealing priming paint according to claim 1, it is characterised in that: the pH adjusting agent is amine
Neutralizer；And/or
The defoaming agent is organic oils defoaming agent；And/or
The coalescing agent is waterborne film-forming auxiliary agent；And/or
The thickener is polyurethane aqueous thickener.
7. a kind of preparation method of environment-friendly type aqueous wooden ware sealing priming paint, which comprises the following steps:
Step a, each raw material group is weighed according to the formula of any one of the claim 1-6 environment-friendly type aqueous wooden ware sealing priming paint
Point, pH adjusting agent, defoaming agent, film forming, which are successively added, into nanometer water acrylic resin aqueous solution under stirring helps
Agent, grinding auxiliary agent, moistening flatting agent, deionized water, water-protected enclosure agent are uniformly mixed；
It step b, is 90s~110s with -4 glasss of viscosity of painting that mixture viscosity obtained by step a is adjusted to 25 DEG C by thickener, stirring is extremely
Be uniformly mixed to get.
8. preparation method according to claim 7, it is characterised in that: the speed of stirring described in step a be 900~
1200r/min；And/or
It is uniformly mixed described in step a as with the speed of 400~600r/min stirring 15~25 minutes.
9. preparation method according to claim 7, it is characterised in that: be uniformly mixed described in step b for 700~
The speed of 900r/min stirs 15~25 minutes.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810765865.5A CN109206993A (en) | 2018-07-12 | 2018-07-12 | A kind of environment-friendly type aqueous wooden ware sealing priming paint and preparation method thereof |
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| CN201810765865.5A CN109206993A (en) | 2018-07-12 | 2018-07-12 | A kind of environment-friendly type aqueous wooden ware sealing priming paint and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112980235A (en) * | 2021-04-25 | 2021-06-18 | 广东安捷伦新材料科技有限公司 | Water-based nano sealing coating for automobile wood interior and preparation method thereof |
| CN114276726A (en) * | 2021-11-16 | 2022-04-05 | 赣州市博品家具有限公司 | Water-based nanoscale anion seal primer for preventing tannin bleeding and preparation method thereof |
| CN115160875A (en) * | 2022-06-22 | 2022-10-11 | 江苏海田技术有限公司 | Water-based dip-coating white base coat for brush wooden handle and preparation method thereof |
| WO2023077518A1 (en) * | 2021-11-08 | 2023-05-11 | Dow Global Technologies Llc | Aqueous coating composition and process for preparing the same |
| CN116493230A (en) * | 2023-04-28 | 2023-07-28 | 新盛世机电制品(中山)有限公司 | Fan blade production and processing method |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112980235A (en) * | 2021-04-25 | 2021-06-18 | 广东安捷伦新材料科技有限公司 | Water-based nano sealing coating for automobile wood interior and preparation method thereof |
| WO2023077518A1 (en) * | 2021-11-08 | 2023-05-11 | Dow Global Technologies Llc | Aqueous coating composition and process for preparing the same |
| CN114276726A (en) * | 2021-11-16 | 2022-04-05 | 赣州市博品家具有限公司 | Water-based nanoscale anion seal primer for preventing tannin bleeding and preparation method thereof |
| CN115160875A (en) * | 2022-06-22 | 2022-10-11 | 江苏海田技术有限公司 | Water-based dip-coating white base coat for brush wooden handle and preparation method thereof |
| CN116493230A (en) * | 2023-04-28 | 2023-07-28 | 新盛世机电制品(中山)有限公司 | Fan blade production and processing method |
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Application publication date: 20190115 |
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