CN109200974A - A kind of Chemical Manufacture reaction kettle with flow-disturbing function - Google Patents
A kind of Chemical Manufacture reaction kettle with flow-disturbing function Download PDFInfo
- Publication number
- CN109200974A CN109200974A CN201710520347.2A CN201710520347A CN109200974A CN 109200974 A CN109200974 A CN 109200974A CN 201710520347 A CN201710520347 A CN 201710520347A CN 109200974 A CN109200974 A CN 109200974A
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- CN
- China
- Prior art keywords
- flow
- disturbing
- fixedly connected
- autoclave body
- reaction kettle
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
- B01J19/1806—Stationary reactors having moving elements inside resulting in a turbulent flow of the reactants, such as in centrifugal-type reactors, or having a high Reynolds-number
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
- B01J19/1868—Stationary reactors having moving elements inside resulting in a loop-type movement
- B01J19/1875—Stationary reactors having moving elements inside resulting in a loop-type movement internally, i.e. the mixture circulating inside the vessel such that the upwards stream is separated physically from the downwards stream(s)
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
- B01J2219/332—Details relating to the flow of the phases
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
Abstract
A kind of Chemical Manufacture reaction kettle with flow-disturbing function, including autoclave body, middle is fixedly connected with motor on the upside of the autoclave body, active rotating shaft is fixedly connected on motor output shaft, active rotating shaft is located inside autoclave body, and active rotating shaft bottom end is fixedly connected with flow-disturbing cylinder, flow-disturbing cylinder upper end is open-like shape, is uniformly provided with several first through hole on flow-disturbing cylinder side wall；The active rotating shaft top is fixedly connected with driving gear, driving gear two sides are symmetrically engaged with driven gear, driven spindle is fixedly connected on driven gear, it is rotatablely connected at the top of driven spindle top and autoclave body, the driven spindle lower part is located in flow-disturbing cylinder, and several flow-disturbing protrusions are uniformly fixedly connected on driven spindle side wall；It is symmetrically fixedly connected on the flow-disturbing cylinder lateral wall there are two spoiler, is uniformly provided with several flow-disturbing holes on spoiler.The present invention has many advantages, such as that reasonable in design, easy to use and flow-disturbing effect is good, has certain application value.
Description
Technical field
The present invention relates to chemical equipment technical fields, and in particular to a kind of Chemical Manufacture reaction with flow-disturbing function
Kettle.
Background technique
The broad understanding of reaction kettle has the container physically or chemically reacted, is designed by the structure to container and is matched with parameter
It sets, realizes the mixed function for heating, evaporation, cooling and the low high speed that technique requires.Reaction kettle be widely used in petroleum, chemical industry,
Rubber, pesticide, dyestuff, medicine, food, for completing the pressure of the technical process such as vulcanization, nitrification, hydrogenation, hydrocarbonylation, polymerization, condensation
Force container, such as reactor, reaction pot, decomposition pot, polymeric kettle etc.；Material generally has carbon manganese steel, stainless steel, zirconium, Ni-based (Kazakhstan
Family name, Monel, inconel) alloy and other composite materials.
And stirring apparatus for reaction kettle in the prior art is generally to drive stirring blade to be stirred using shaft,
But its stirring range is very limited, is only stirred under normal circumstances to the material in fixed area, so as to cause reaction
Mixed effect between object is poor, and reaction is not thorough.
Summary of the invention
The purpose of the present invention is to provide a kind of Chemical Manufacture reaction kettles with flow-disturbing function, to solve above-mentioned background
The problem of being proposed in technology.
To achieve the above object, the invention provides the following technical scheme:
A kind of Chemical Manufacture reaction kettle with flow-disturbing function, including autoclave body, autoclave body upside middle are fixedly connected with
Motor is fixedly connected with active rotating shaft on motor output shaft, and active rotating shaft is located inside autoclave body, and active rotating shaft bottom end is fixed connects
It is connected to flow-disturbing cylinder, flow-disturbing cylinder upper end is open-like shape, is uniformly provided with several first through hole on flow-disturbing cylinder side wall；The active rotating shaft
Top is fixedly connected with driving gear, and driving gear two sides are symmetrically engaged with driven gear, be fixedly connected on driven gear from
It is rotatablely connected at the top of turn axis, driven spindle top and autoclave body, the driven spindle lower part is located in flow-disturbing cylinder, and driven spindle
Several flow-disturbing protrusions are uniformly fixedly connected on side wall；It is symmetrically fixedly connected on the flow-disturbing cylinder lateral wall there are two spoiler,
Several flow-disturbing holes are uniformly provided on spoiler；It is provided with circulation pipe on the autoclave body bottom side wall, is disposed with and follows on circulation pipe
Ring pump, the upper end of the circulation pipe are connected with autoclave body top, and circulation pipe upper end outlet is located at right above flow-disturbing cylinder.
It is as a further solution of the present invention: is provided with feed opening at the top of the autoclave body.
As the present invention, further scheme is: the autoclave body bottom is equipped with discharge port, and discharge outlet is equipped with valve.
As the present invention, further scheme is: the contact position of the active rotating shaft and driven spindle and autoclave body is respectively provided with
There is bearing.
As the present invention, further scheme is: the flow-disturbing protrusion is in tetrapyamid shape.
As the present invention, further scheme is: flow-disturbing cylinder bottom is uniformly provided with several second through-holes, and the
Two through-hole diameters are less than first through hole diameter.
As the present invention, further scheme is: second through-hole diameter is 1.0mm-2.5mm.
The beneficial effects of the invention are as follows the solution in flow-disturbing cylinder to be flowed out under the action of the centrifugal force by first through hole, is passing through
Certain immixture is obtained during first through hole, between solution；After active rotating shaft rotation, driving gear rotation is driven,
The driven gear being meshed with driving gear rotates, and driven spindle rotation is driven after driven gear rotation, to make driven
The steering of shaft and flow-disturbing cylinder further improves between solution on the contrary, thus carry out flow-disturbing effect to the solution in flow-disturbing cylinder
Reaction effect；Flow-disturbing cylinder drives spoiler rotation in rotation, and the flow-disturbing hole on spoiler carries out perturbation action to solution.This hair
It is bright to have many advantages, such as that reasonable in design, easy to use and flow-disturbing effect is good, there is certain application value.
Detailed description of the invention
Fig. 1 is the structural diagram of the present invention.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other
Embodiment shall fall within the protection scope of the present invention.
Referring to Fig. 1, in the embodiment of the present invention, a kind of Chemical Manufacture reaction kettle with flow-disturbing function, including autoclave body
1, the 1 upside middle of autoclave body is fixedly connected with motor 4, and active rotating shaft 5 is fixedly connected on 4 output shaft of motor, is actively turned
Axis 5 is located inside autoclave body 1, and 5 bottom end of active rotating shaft is fixedly connected with flow-disturbing cylinder 11, and 11 upper end of flow-disturbing cylinder is open-like shape, flow-disturbing
Several first through hole 12 are uniformly provided on 11 side walls of cylinder, motor 4 drives active rotating shaft 5 to rotate, and active rotating shaft 5 drives flow-disturbing cylinder
11 rotate, and the solution in flow-disturbing cylinder 11 passes through first through hole 12 under the action of the centrifugal force and flows out, in the mistake for passing through first through hole 12
Cheng Zhong obtains certain immixture between solution；
5 top of active rotating shaft is fixedly connected with driving gear 6, and 6 two sides of driving gear are symmetrically engaged with driven gear 8, from
It is fixedly connected with driven spindle 7 on moving gear 8, is rotatablely connected at the top of 7 top of driven spindle and autoclave body 1, under the driven spindle 7
Portion is located in flow-disturbing cylinder 11, and several flow-disturbing protrusions 10 are uniformly fixedly connected on 7 side wall of driven spindle, and active rotating shaft 5 rotates
Afterwards, driving gear 5 is driven to rotate, the driven gear 8 being meshed with driving gear 5 rotates, and driven gear 8 drives after rotating
Driven spindle 7 rotates, to make the steering of driven spindle 7 and flow-disturbing cylinder 11 on the contrary, thus carrying out to the solution in flow-disturbing cylinder 11
Flow-disturbing effect, further improves the reaction effect between solution；
Spoiler 16 there are two being symmetrically fixedly connected on 11 lateral wall of flow-disturbing cylinder, if being uniformly provided with interference on spoiler 16
Discharge orifice 17, flow-disturbing cylinder 11 drive spoiler 16 to rotate in rotation, and the flow-disturbing hole 17 on spoiler 16 carries out disturbance work to solution
With；
Be provided with circulation pipe 9 in 1 bottom sidewall of autoclave body, be disposed with circulating pump 18 on circulation pipe 9, the circulation pipe 9 it is upper
End is connected with 1 top of autoclave body, and 9 upper end outlet of circulation pipe is located at the surface of flow-disturbing cylinder 11, using circulating pump 18 by autoclave body bottom
The material in portion is extracted into flow-disturbing cylinder 11 by circulation pipe 9, and flow-disturbing effect is carried out in flow-disturbing cylinder 11, makes mixing between solution more
Uniformly, reaction effect is effectively increased.
Feed opening 2 is provided at the top of the autoclave body 1.
1 bottom of autoclave body is equipped with discharge port 15, is equipped with valve 14 at discharge port 15.
The contact position of the active rotating shaft 5 and driven spindle 7 and autoclave body 1 is provided with bearing 3.
The flow-disturbing protrusion 10 is in tetrapyamid shape.
11 bottom of flow-disturbing cylinder is uniformly provided with several second through-holes 13, and 13 diameter of the second through-hole is less than first through hole
12 diameters, 13 diameter of the second through-hole is smaller, can prevent the solution entered in flow-disturbing cylinder 11 from quickly leaking from 11, flow-disturbing cylinder
Out, flow-disturbing effect is thereby reduced；Meanwhile when after reaction, the solution of 11 bottom of flow-disturbing cylinder can also pass through the second through-hole
13 all discharges, not will cause the generation that discharge is not thorough phenomenon.
Second through-hole, 13 diameter is 1.0mm-2.5mm.
The course of work of the invention is: motor 4 drives active rotating shaft 5 to rotate, and active rotating shaft 5 drives flow-disturbing cylinder 11 to rotate,
Solution in flow-disturbing cylinder 11 passes through first through hole 12 under the action of the centrifugal force and flows out, molten during passing through first through hole 12
Certain immixture is obtained between liquid；After active rotating shaft 5 rotates, drives driving gear 5 to rotate, be meshed with driving gear 5
Driven gear 8 rotate, driven gear 8 rotate after drive driven spindle 7 rotate, to make driven spindle 7 and flow-disturbing cylinder
11 steering further improves the reaction effect between solution on the contrary, thus to the solution progress flow-disturbing effect in flow-disturbing cylinder 11；
Flow-disturbing cylinder 11 drives spoiler 16 to rotate in rotation, and the flow-disturbing hole 17 on spoiler 16 carries out perturbation action to solution；It utilizes
The material of autoclave body bottom is extracted into flow-disturbing cylinder 11 by circulating pump 18 by circulation pipe 9, and flow-disturbing effect is carried out in flow-disturbing cylinder 11, is made
Mixing between solution is more uniform, effectively increases reaction effect；Second through-hole, 13 diameter is smaller, can prevent from entering flow-disturbing
Solution in cylinder 11 is quickly leaked out from 11, flow-disturbing cylinder, thereby reduces flow-disturbing effect；Meanwhile when after reaction, flow-disturbing
The solution of 11 bottoms of cylinder can also be all discharged by the second through-hole 13, not will cause the generation that discharge is not thorough phenomenon.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims
Variation is included within the present invention.Any reference signs in the claims should not be construed as limiting the involved claims.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiments being understood that.
Claims (7)
1. a kind of Chemical Manufacture reaction kettle with flow-disturbing function, including autoclave body, which is characterized in that intermediate on the upside of the autoclave body
Place is fixedly connected with motor, and active rotating shaft is fixedly connected on motor output shaft, and active rotating shaft is located inside autoclave body, and actively turns
Axis bottom end is fixedly connected with flow-disturbing cylinder, and flow-disturbing cylinder upper end is open-like shape, is uniformly provided with several first through hole on flow-disturbing cylinder side wall；
The active rotating shaft top is fixedly connected with driving gear, and driving gear two sides are symmetrically engaged with driven gear, on driven gear
It is fixedly connected with driven spindle, is rotatablely connected at the top of driven spindle top and autoclave body, the driven spindle lower part is located at flow-disturbing cylinder
It is interior, and several flow-disturbing protrusions are uniformly fixedly connected on driven spindle side wall；It is symmetrically fixedly connected on the flow-disturbing cylinder lateral wall
There are two spoiler, several flow-disturbing holes are uniformly provided on spoiler；It is provided with circulation pipe on the autoclave body bottom side wall, is recycled
Circulating pump is disposed on pipe, the upper end of the circulation pipe is connected with autoclave body top, and circulation pipe upper end outlet is located at flow-disturbing cylinder
Surface.
2. a kind of Chemical Manufacture reaction kettle with flow-disturbing function according to claim 1, which is characterized in that the kettle
Feed opening is provided at the top of body.
3. a kind of Chemical Manufacture reaction kettle with flow-disturbing function according to claim 1 or 2, which is characterized in that institute
Autoclave body bottom is stated equipped with discharge port, discharge outlet is equipped with valve.
4. a kind of Chemical Manufacture reaction kettle with flow-disturbing function according to claim 3, which is characterized in that the master
The contact position of turn axis and driven spindle and autoclave body is provided with bearing.
5. a kind of Chemical Manufacture reaction kettle with flow-disturbing function according to claim 1, which is characterized in that described to disturb
Stream protrusion is in tetrapyamid shape.
6. a kind of Chemical Manufacture reaction kettle with flow-disturbing function according to claim 1, which is characterized in that described to disturb
Flow cartridge bottom is uniformly provided with several second through-holes, and the second through-hole diameter is less than first through hole diameter.
7. a kind of Chemical Manufacture reaction kettle with flow-disturbing function according to claim 6, which is characterized in that described
Two through-hole diameters are 1.0mm-2.5mm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710520347.2A CN109200974A (en) | 2017-06-30 | 2017-06-30 | A kind of Chemical Manufacture reaction kettle with flow-disturbing function |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710520347.2A CN109200974A (en) | 2017-06-30 | 2017-06-30 | A kind of Chemical Manufacture reaction kettle with flow-disturbing function |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109200974A true CN109200974A (en) | 2019-01-15 |
Family
ID=64977076
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710520347.2A Pending CN109200974A (en) | 2017-06-30 | 2017-06-30 | A kind of Chemical Manufacture reaction kettle with flow-disturbing function |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109200974A (en) |
-
2017
- 2017-06-30 CN CN201710520347.2A patent/CN109200974A/en active Pending
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20190115 |
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| WD01 | Invention patent application deemed withdrawn after publication |