CN109198493A - It is a kind of to freeze instant halogen squid and its processing method - Google Patents

It is a kind of to freeze instant halogen squid and its processing method Download PDF

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Publication number
CN109198493A
CN109198493A CN201811274006.2A CN201811274006A CN109198493A CN 109198493 A CN109198493 A CN 109198493A CN 201811274006 A CN201811274006 A CN 201811274006A CN 109198493 A CN109198493 A CN 109198493A
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Prior art keywords
squid
parts
halogen
freezing
temperature
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邓立青
林春强
林春宝
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Fujian Kun Xing Marine Ltd By Share Ltd
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Fujian Kun Xing Marine Ltd By Share Ltd
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Priority to CN201811274006.2A priority Critical patent/CN109198493A/en
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L17/00Food-from-the-sea products; Fish products; Fish meal; Fish-egg substitutes; Preparation or treatment thereof
    • A23L17/50Molluscs
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L5/00Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
    • A23L5/10General methods of cooking foods, e.g. by roasting or frying
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

Abstract

The present invention relates to a kind of processing methods for freezing instant halogen squid, comprising the following specific steps S1, immersion: cuing open after the squid after killing is cleaned and impregnate 2 ~ 4 hours;S2, stew in soy sauce: by stew in soy sauce in the squid investment thick gravy after draining;S3, drying: the good squid of halogen carries out heat pump drying processing after draining thick gravy, and the heat pump temperature of heat pump drying processing is 35-40 DEG C, and dry humidity is 45 ~ 50%, and wind speed is 2 ~ 4m/s, 1 ~ 2h of drying time;S4, secondary seasoning: heat pump drying treated halogen squid is subjected to secondary seasoning;S5, packaging freezing: using the freezing of double helix mono-frozen machine is sent into after vacuum packaging, -18 DEG C are refrigerated to.The processing method is under the premise of guaranteeing that the leisure of squid product is convenient edible, nutrition and the health efficacy of squid product can be effectively kept again, it can also ensure that the flavor and shelf life of squid product simultaneously, consumer can feel at ease and relievedly enjoy deliciousness and the nutrition of squid.

Description

It is a kind of to freeze instant halogen squid and its processing method
Technical field
The invention belongs to food processing technology fields, and in particular to a kind of to freeze instant halogen squid and its processing method.
Background technique
Squid, also referred to as squid are a kind of software Brachiopoda marine products of high nutritive value, rich in protein, needed by human The elements such as amino acid, taurine and calcium, iron, phosphorus, this to skeleton develop, prevention anaemia and adult disease, relieve fatigue, Improving liver function etc. can all play a role, and whole 50% is promised to fight in squid trunk part, and cephalopodium part accounts for about whole 30%, squid edible part is higher by 20% or so up to 80% or more, than general fish, is excellent processing of aquatic products raw material.It is existing The present, process on the market since category is more, such as squid dried product, soaked chili squids, baked squid.
The fast pace life of modern, for leisure convenience food increasingly by their favor, flavor squid is one Kind leisure, delicious Speciality Foods, it is deep to be liked by public group, still, with the gradual improvement of people's living standard, to certainly The hard bright attention rate of body is also constantly promoted, and selected edible food requires also increasingly to be particular about, and existing squid fish products are big Only focus on taste, such as soaked chili squids, such eating method just has ignored the nutrition of squid and health more;Even if there is part production Product consider the nutrition problem of squid product, and such as room temperature of various flavors seasons squid, and room temperature seasoning squid just needs emphasis Quality, mouthfeel and the shelf-life of squid are protected, but in order to extend the shelf life and organoleptic quality of room temperature seasoning squid, in room temperature In the process of squid, antisepsis antistaling agent is added with being just frequently considered that, the Excess free enthalpy of this kind of food additives certainly will be to people The health care belt of body endangers.In addition, room temperature seasoning squid product is in the process of production and processing, need by high-temperature sterilization treatment, After high-temperature sterilization treatment, quality, brittleness and the flavor substance of squid product all can be destroyed significantly.
Summary of the invention
In view of above-mentioned deficiencies of the prior art, the present invention is intended to provide a kind of freeze instant halogen squid and its processing method, Under the premise of guaranteeing that the leisure of squid product is convenient edible, and nutrition and the health efficacy of squid product can be effectively kept, together When can also ensure that the flavor and shelf life of squid product, allow consumer can feel at ease and relievedly enjoy squid deliciousness and battalion It supports.
Technical scheme is as follows:
A kind of processing method freezing instant halogen squid, comprising the following specific steps
S1, immersion: it cuts open after the squid after killing is cleaned and impregnates 2~4 hours;
S2, stew in soy sauce: by stew in soy sauce in the squid investment thick gravy after draining;
S3, drying: the good squid of halogen carries out heat pump drying processing after draining thick gravy, and the heat pump temperature of heat pump drying processing is 35-40 DEG C, dry humidity is 45~50%, and wind speed is 2~4m/s, 1~2h of drying time;
S4, secondary seasoning: heat pump drying treated halogen squid is subjected to secondary seasoning;
S5, packaging freezing: using the freezing of double helix mono-frozen machine is sent into after vacuum packaging, -18 DEG C are refrigerated to.
Further, in the step S1 impregnate process use immersion complex liquid include it is following by weight percentage Ingredient:
Component A: sodium carbonate 0.8~2.2%;Sodium citrate 1.5~5%;Sorbierite 2~4%;Trehalose 0.5~1.5% With edible salt 1~1.5%;
B component: green onion 3~8%;Ginger 3-8%;Cooking wine 2-4% and beer 8-12%;The ice water temperature is maintained at 5~8 DEG C, soaking time is 2~4 hours;Component A and B component are added surplus ice water and put into squid after being mixed evenly;
Further, the thick gravy that stew in soy sauce process uses in the step S2 is according to the weight for putting into squid 3000-3500 parts Ratio prepares the component of following parts by weight: 800~1500 parts of bone soup, 500~800 parts of drinking water, dark soy sauce 300~340 It is part, 280~350 parts of spices bag, 250~300 parts of light soy sauce, 75~80 parts of refined salt, 45~50 parts of white sugar, 35~50 parts of cooking wine, red 30~35 parts of drum oil, 15~20 parts of chicken paste, 10~15 parts of monosodium glutamate, 8~12 parts of fish sauce, 5~8 parts of chicken fine powder and ethyl malt 0.8~1.2 part of phenol.
Further, the spices bag is made of following weight: southern ginger 120-150 parts, 30-35 parts of lemongrass, 30-35 parts of garlic, 25-35 parts of coriander head, 15-20 parts of capsicum, 12-17 parts of tsaoko, 10-15 parts of illiciumverum, 8-12 parts of zingiber kawagoii, osmanthus 8-12 parts of skin, 8-10 parts of Radix Glycyrrhizae, 8-10 parts of Siraitia grosvenorii, 8-10 parts of dried orange peel, 5-8 parts of fennel seeds and 3-5 parts of cloves.
Further, the formula of the step S4 secondary seasoning is according to 100~120 parts of squid of weight after heat pump drying Ratio prepares the component of following parts by weight: 0.2~0.7 part of cumin powder, 0.5~part of sweet plum powder 1, meat flavour essence cream 0.1~0.5 Part, 0.2~0.7 part of sesame oil, 0.3~1 part of sweet fermented flour sauce, 0.2~0.6 part of tremella polysaccharides, 0.3~0.8 part of trehalose.
Further, in secondary seasoning under the action of before step S5 packaging freezes in cryogenic high pressure fluidisation compression Halogen squid surface is formed with the preservative protective film of trehalose composite solution composition;The trehalose composite solution is by trehalose, sea Mosanom and exogenous protease are constituted;Squid after secondary seasoning is sent into low temperature fluidized equipment, so that mass concentration is 0.1~0.5% aqueous trehalose low speed flows uniformly through squid surface, forms stable fluidisation liquid film, and temperature maintains 1~ 5 DEG C, pressure maintains 0.2~0.5MPa, so that trehalose composite solution is in squid surface homogeneous condensation film-forming.
Further, before step S5 vacuum packaging, first halogen squid is carried out using vacuum pre-cooling to product Pre-cooling, allow, allow the temperature of halogen squid from room temperature fast precooling, the pressure of vacuum pre-cooling is 0.6kPa, the final temperature of product pre-cooling It is 3~5 DEG C.
Further, double helix mono-frozen machine freezes halogen squid in the step S5, and temperature need to be operated by following freezing curve:
(1) -15~-10 DEG C are cooled to from 1~5 DEG C, cool down 5~8min, and rate of temperature fall is 1.5~4 DEG C/min (fast speed Cross zone of a crystal);
(2) -35~-30 DEG C are cooled to from -15~-10 DEG C, cool down 25~30min, and rate of temperature fall is 0.5~1 DEG C/min;
(3) -20~-18 DEG C are warming up to from -35~-30 DEG C, heat up 5~10min, and heating rate is 1~3 DEG C/min.
Further, the fish oil in enzymolysis and extraction squid, the condition of extraction are as follows: enzyme are carried out using alkali protease enzymatic isolation method Amount is 850u/g, solid-to-liquid ratio 1:8, enzymolysis time 3.8h, 48 DEG C of hydrolysis temperature and enzymolysis liquid pH are 7.9, is mentioned what enzymatic hydrolysis obtained Liquid is taken to be added in the step S4 secondary seasoning.
A kind of instant halogen squid of freezing according to made from above-mentioned processing method.
The invention has the following beneficial effects:
1, immersion treatment is used in the present invention, promotes squid brittleness mouthfeel and removal squid fishy smell;Using heat pump low temperature It is dried, thick gravy squid is carried out after suitably air-drying, obtained product appearance is splendid, and crisp;In combination with two Taste manufacturing process is assigned in secondary seasoning, and obtained pot-stewed fowl squid may be implemented flavor diversification, meet the taste demand of different crowd, most Eventually again in conjunction with frozen step, by product quick freezing, effectively inhibit the multiplication products of microorganism, without adding any anti-corrosion Agent extends the shelf life of product;The mutually coordinated cooperation of above-mentioned operation is related to high-temperature sterilization instead of tradition addition preservative Step avoids the quality, brittleness and flavor substance of squid product from all mutually being assisted by the destruction of big degree by these processes Allotment is closed, and the shelf life of product can be both extended, and also be can achieve the fresh purpose with nutrition of latching of product in the application, is allowed Consumer can really enjoy the leisure flavor halogen squid of delicious health.
2, sorbierite, tremella polysaccharides, sodium carbonate and lemon be joined in impregnating the soak that process uses in the present invention Sour sodium, wherein sorbierite can be used for the extraction of protein as a kind of nonionic surfactant, and tremella polysaccharides have fine Lubricity and film forming, Heat-resistant stable, be suitable for various acid or alkali environments, external action can be resisted, be effectively protected in squid Protein invariance, and the flavor substance of squid is kept not to be lost, while passing through the coordination reciprocation of batch part, adjusts leaching Liquid pH value is steeped between 6.6-7.0, can promote squid water retention property, squid water retention property is better, then the quality of squid is crisp Tender property is better;Tremella polysaccharides and trehalose ingredient are added in secondary seasoning process, tremella polysaccharides, which have, surmounts hyaluronic acid Water holding capacity, can there is up to 500 times of water-retaining propertys, at the same trehalose can the surface layer of protein molecule formed one layer it is special Protective film can further keep the antitypy of squid frost resistance and squid albumen, utilize seaweed by the coordinative role of the two Sugared film technique and low temperature fluidized pressurization compression processing can either play substitution in secondary halogen squid surface formation preservative protective film Preservative plays anti-corrosion effect, while the nutritional ingredient that squid can be avoided using protective film and the flavor by having after seasoning It is lost.
3, the cryogenic temperature of packaging freezing halogen squid has been carried out and its stringent planning and control in the present invention, first Biggish rate of temperature fall is carried out when secondary cooling, makes squid product in frozen step quickly through (- 5 DEG C of zone of maximum ice crystal formation ~0 DEG C), interiors of products ice crystal is minimum, so that the quick-frozen process organization structure of squid be effectively reduced by freeze injury, further avoids The loss of juice and nutriment;Later, rate of temperature fall is reduced, prevents lasting fast cooling from halogen squid surface being caused to be formed There is cracking phenomena since rate of temperature fall is too fast in preservative protective film;Finally, temperature is quickly risen to the center temperature of squid product Degree, prevents lasting low temperature from making the nutritional ingredient activity in squid weaker, guarantees the nutritional ingredient of squid product.
4, the application is after cuing open and killing squid, appearance is bad or the leftover bits and pieces and internal organ that cut down from squid, single Enzymolysis and extraction fish oil therein (EPA, DHA) is solely carried out using alkali protease enzymatic isolation method, the extracting solution for later obtaining enzymatic hydrolysis It is added in secondary seasoning, further improves the nutriment ingredient of squid product, meanwhile, also fully utilize squid by-product Product improve the added value of product processing.
Specific embodiment
Below with reference to preferred embodiment, the present invention is further illustrated.
A kind of processing method freezing instant halogen squid, production technology route are as follows: raw material examination → defrosting cut open kill → it is clear It washes → impregnates → stew in soy sauce → and air-dry → secondary seasoning → packaging → quick-frozen → excessively golden spy → vanning → storage, wherein raw material examination, Defrosting, which is cutd open, kills and cleans to pre-process, and the specific operation method is as follows:
Raw material is checked and accepted: the squid of selection is preferred with Argentinian squid, can select true squid, local squid etc., squid is former Material requires a problem that freshness is good, meat turns to be yellow without nigrescence, and accomplishes in the same size uniform, the bad squid of rejecting freshness as far as possible Fish;
Defrosting, which is cutd open, kills: squid raw material being taken out in frozen storehouse, in 15 DEG C of room temperature thawing room natural thaw 7h below or is put Defrosting 1.5h is impregnated in flowing clear water, between -1 DEG C~3 DEG C, the squid thawed is gone donor center temperature after defrosting The non-edible portion such as internal organ, eyeball, mouth.
Cleaning: cuing open the squid after killing and rinsed, and removes the impurity foreign matter etc. adhered on squid.
Embodiment 1
A kind of processing method freezing instant halogen squid, specifically comprises the following steps:
S1, the squid rinsed clean after pretreatment, are impregnated;When immersion, component A and B component are uniformly mixed, A Component includes following component by weight percentage: sodium carbonate 0.8%, sodium citrate 1.5%, sorbierite 2%, trehalose 0.5% With edible salt 1%, sodium carbonate, sodium citrate, sorbierite, trehalose and edible salt are contained in component A, passes through the coordination of batch part Reciprocation adjusts soak pH value between 6.6~7.0, can promote squid water retention property, squid albumen is avoided to become Property.Squid water retention property is better, then the tender and crisp property of the quality of squid is better;B component includes following component by weight percentage: containing green onion 3%, ginger 3%, cooking wine 2% and beer 8%;Contain green onion, ginger and cooking wine in B component, is mainly used for deodorization;Component A and B component are mixed It closes liquid and is added to ice water 78.2%, ice water temperature is maintained between 5 DEG C, squid is immersed in mixed liquor, soaking time 2h;
S2, the soaked squid of water conservation, carry out stew in soy sauce after draining away the water.It is as follows that brine makes formula meter: squid 3000 parts of fish, 900 parts of pig bone soup, 550 parts of drinking water, 300 parts of dark soy sauce, 296 parts of spices bag, 260 parts of light soy sauce, 75 parts of refined salt, 50 parts of white sugar, 40 parts of cooking wine, 32 parts of red soy sauce, 16 parts of chicken paste, 10 parts of monosodium glutamate, 11 parts of fish sauce, 8 parts of chicken fine powder, ethyl wheat 0.8 part of bud phenol;The spices bag is by following weight component: 120 parts of southern ginger, 31 parts of lemongrass, 30 parts of garlic, coriander head 25 parts of (caraway head), 17 parts of capsicum, 15 parts of tsaoko, 10 parts octagonal, 8 parts of zingiber kawagoii, 8 parts of cassia bark, 8 parts of Radix Glycyrrhizae, 8 parts of Siraitia grosvenorii, 8 parts of dried orange peel, 5 parts of fennel seeds, 3 parts of cloves.
After the good squid of S3, halogen drains thick gravy, using hot pump in low temp dry technology, the good squid of stew in soy sauce is carried out to air-dry work Industry, heat pump drying technological parameter are as follows: 35 DEG C of heat pump temperature, drying time 2h, dry humidity is 45%, wind speed 3m/s;Using This technological parameter treated squid product, moisture content improve brittleness mouthfeel between 55~60%;
S4, can be to the secondary tax taste of halogen squid according to taste demand, the formula of secondary seasoning is according to the squid after heat pump drying The weight ratio that 100 parts of fish prepares the component of following parts by weight: 0.2 part of cumin powder, 0.5 part of sweet plum powder, meat flavour essence cream 0.1 Part, 0.2 part of sesame oil, 0.3 part of sweet fermented flour sauce, 0.2 part of tremella polysaccharides, 0.3 part of trehalose;The tremella polysaccharides that are added in secondary seasoning and Trehalose can further keep the antitypy of squid frost resistance and squid albumen by the coordinative role of the two.
Further, stew in soy sauce process is as follows: 1, all spices being packed into gauze bag, and tighten sack, spices bag not fill Must be too tight, otherwise it is unfavorable for the infusion of flavor component;2, after bone soup and drinking water height being burnt boiling, other tune are put into Material, and stirring and dissolving is uniform, is then placed in spices bag, after moderate heat infusion to soup stock water boiling, switchs to small fire, keeps in container Soup stock is in slight boiling condition, persistently keeps 1.5h, the fragrance component in spices bag is allowed to be fully dissolved out, be then turned off fire source and take out perfume (or spice) Material packet;3, it will be put into brine after the squid metering after draining, open fire source and held with small fight is switched to after the boiled brine of high fire After continuous 10min, fire source is closed, can be taken the dish out of the pot after allowing squid to impregnate 2h in thick gravy, halogen squid is made.
Embodiment 2
S1, the squid rinsed clean after pretreatment, are impregnated;When immersion, component A and B component are uniformly mixed, A Component includes following component by weight percentage: sodium carbonate 2.2%, sodium citrate 5%, sorbierite 4%, 1.5% and of trehalose Edible salt 1.5% contains sodium carbonate, sodium citrate, sorbierite, trehalose and edible salt in component A, passes through the coordination of batch part Reciprocation adjusts soak pH value between 6.6~7.0, can promote squid water retention property, squid albumen is avoided to become Property.Squid water retention property is better, then the tender and crisp property of the quality of squid is better;B component includes following component by weight percentage: containing green onion 8%, ginger 8%, cooking wine 4% and beer 12%;Contain green onion, ginger and cooking wine in B component, is mainly used for deodorization;Component A and B component Mixed liquor is added to ice water 53.8%, and ice water temperature is maintained between 8 DEG C, squid is immersed in mixed liquor, soaking time 4h;
S2, the soaked squid of water conservation, carry out stew in soy sauce, it is as follows that brine makes formula meter: squid after draining away the water 3500 parts of fish, 1500 parts of pig bone soup, 800 parts of drinking water, 320 parts of dark soy sauce, 328 parts of spices bag, 295 parts of light soy sauce, 80 parts of refined salt, 48 parts of white sugar, 42 parts of cooking wine, red drum oily 30 parts, 18 parts of chicken paste, 14 parts of monosodium glutamate, 8 parts of fish sauce, 7 parts of chicken fine powder, ethyl malt 0.9 part of phenol;The spices bag is by following weight component: 130 parts of southern ginger, 33 parts of lemongrass, 35 parts of garlic, coriander head 28 parts of (caraway head), 18 parts of capsicum, 16 parts of tsaoko, octagonal 13 parts, 10 parts of zingiber kawagoii, 10 parts of cassia bark, 9 parts of Radix Glycyrrhizae, Siraitia grosvenorii 9 Part, 8 parts of dried orange peel, 6 parts of fennel seeds, 3 parts of cloves.
After the good squid of S3, halogen drains thick gravy, using hot pump in low temp dry technology, the good squid of stew in soy sauce is carried out to air-dry work Industry, heat pump drying technological parameter are as follows: 38 DEG C of heat pump temperature, drying time 1.8h, dry humidity is 46%, and wind speed 2m/s is adopted With this technological parameter treated squid product, moisture content improves brittleness mouthfeel between 55~60%;
S4, can be to the secondary tax taste of halogen squid according to taste demand, the formula of secondary seasoning is according to the squid after heat pump drying The weight ratio that 120 parts of fish, prepares the component of following parts by weight: 0.7 part of cumin powder, 1 part of sweet plum powder, 0.5 part of meat flavour essence cream, 0.7 part of sesame oil, 1 part of sweet fermented flour sauce, 0.6 part of tremella polysaccharides, 0.8 part of trehalose;The tremella polysaccharides added in secondary seasoning and seaweed Sugar can further keep the antitypy of squid frost resistance and squid albumen by the coordinative role of the two.
Further, stew in soy sauce process is as follows: being packed into gauze bag first, by all spices, and tightens sack, spices bag should not It fills too tight, is otherwise unfavorable for the infusion of flavor component;Secondly, after bone soup and drinking water height being burnt boiling, it is put into Its condiment, and stirring and dissolving is uniform, is then placed in spices bag, after moderate heat infusion to soup stock water boiling, switchs to small fire, keeps container Interior soup stock is in slight boiling condition, persistently keeps 2h, the fragrance component in spices bag is allowed to be fully dissolved out, be then turned off fire source and take out Spices bag;Finally, it will be put into brine after the squid metering after draining, open fire source and with switching to small fire after the boiled brine of high fire And after continuing 20min, fire source is closed, can be taken the dish out of the pot after allowing squid to impregnate 1h in thick gravy, halogen squid is made.
Embodiment 3
S1, the squid rinsed clean after pretreatment, are impregnated;When immersion, component A and B component are uniformly mixed, A Component includes following component by weight percentage: sodium carbonate 1.6%, sodium citrate 3.5%, sorbierite 3%, 1% and of trehalose Edible salt 1.2% contains sodium carbonate, sodium citrate, sorbierite, trehalose and edible salt in component A, passes through the coordination of batch part Reciprocation adjusts soak pH value between 6.6~7.0, can promote squid water retention property, squid albumen is avoided to become Property.Squid water retention property is better, then the tender and crisp property of the quality of squid is better;B component includes following component by weight percentage: containing green onion 5%, ginger 5%, cooking wine 3% and beer 10%;Contain green onion, ginger and cooking wine in B component, is mainly used for deodorization;Component A and B component Mixed liquor is added to ice water 66.7%, and ice water temperature is maintained between 6 DEG C, squid is immersed in mixed liquor, soaking time 3h;
S2, the soaked squid of water conservation, carry out stew in soy sauce, it is as follows that brine makes formula meter: squid after draining away the water 3200 parts of fish, 1300 parts of pig bone soup, 750 parts of drinking water, 340 parts of dark soy sauce, 350 parts of spices bag, 280 parts of light soy sauce, 75 parts of refined salt, 45 parts of white sugar, 50 parts of cooking wine, red drum oily 35 parts, 20 parts of chicken paste, 13 parts of monosodium glutamate, 10 parts of fish sauce, 7 parts of chicken fine powder, ethyl wheat 1.2 parts of bud phenol;The spices bag is by following weight component: 150 parts of southern ginger, 31 parts of lemongrass, 30 parts of garlic, coriander head 30 parts of (caraway head), 18 parts of capsicum, 15 parts of tsaoko, octagonal 13 parts, 11 parts of zingiber kawagoii, 11 parts of cassia bark, 10 parts of Radix Glycyrrhizae, Siraitia grosvenorii 10 Part, 9 parts of dried orange peel, 6 parts of fennel seeds, 5 parts of cloves.
After the good squid of S3, halogen drains thick gravy, using hot pump in low temp dry technology, the good squid of stew in soy sauce is carried out to air-dry work Industry, heat pump drying technological parameter are as follows: 40 DEG C of heat pump temperature, drying time 1.5h, dry humidity is 50%, wind speed 4m/s;It adopts With this technological parameter treated squid product, moisture content improves brittleness mouthfeel between 55~60%;
S4, can be to the secondary tax taste of halogen squid according to taste demand, the formula of secondary seasoning is according to the squid after heat pump drying The weight ratio that 100~120 parts of fish prepares the component of following parts by weight: 0.5 part of cumin powder, 0.7 part of sweet plum powder, meat flavour essence 0.3 part of cream, 0.5 part of sesame oil, 0.6 part of sweet fermented flour sauce, 0.4 part of tremella polysaccharides, 0.6 part of trehalose;The tremella added in secondary seasoning Polysaccharide and trehalose can further keep the antitypy of squid frost resistance and squid albumen by the coordinative role of the two.
Further, stew in soy sauce process is as follows: 1, all spices being packed into gauze bag, and tighten sack, spices bag not fill Must be too tight, otherwise it is unfavorable for the infusion of flavor component;2, after bone soup and drinking water height being burnt boiling, other tune are put into Material, and stirring and dissolving is uniform, is then placed in spices bag, after moderate heat infusion to soup stock water boiling, switchs to small fire, keeps in container Soup stock is in slight boiling condition, persistently keeps 1.5h, the fragrance component in spices bag is allowed to be fully dissolved out, be then turned off fire source and take out perfume (or spice) Material packet.3, it will be put into brine after the squid metering after draining, open fire source and held with small fight is switched to after the boiled brine of high fire After continuous 12min, fire source is closed, can be taken the dish out of the pot after allowing squid to impregnate 4h in thick gravy, halogen squid is made.
It is also needed after halogen squid made from above-described embodiment 1-3 by packaging freezing, excessively gold spy, vanning and storage, it is specific to grasp It is as follows to make method:
Packaging freezing: the halogen squid after air-drying is packed by specification requirement, vacuumizes packaging, vacuum parameters: when vacuum Between 8s, hot-air mouth time 3s, require in packaging sealing it is tight, smooth, without broken bag;Packaged product crosses double helix mono-frozen machine, The central temperature of squid is allowed to drop to -18 DEG C and less;
Cross gold spy: the squid product freezed crosses metal detector by bag, it is desirable that Fe ∮ >=1.5mm, SUS ∮ >=2.2mm are not It must detect;
Vanning: after visiting by the excessively complete gold of bag, qualified product is cased by production specification requirement, is neatly stacked;
Storage: the product whole plate installed is placed in -18 DEG C of warehouse for finished products below and stores.
Wherein, it is formed under the action of cryogenic high pressure is fluidized and compressed on the halogen squid surface of secondary seasoning before packaging freezing The preservative protective film for having trehalose composite solution to constitute, the trehalose composite solution is by trehalose, sodium alginate and external source egg White enzyme is constituted;Squid after secondary seasoning is sent into low temperature fluidized equipment, so that the sea that mass concentration is 0.1~0.5% Algae sugar juice low speed flows uniformly through squid surface, forms stable fluidisation liquid film, and temperature maintains 1~5 DEG C, and pressure maintains 0.2~0.5MPa, so that trehalose composite solution solidifies homogeneous film formation in squid surface condensation.
Further, before step S5 packaging freezing, first halogen squid is carried out using vacuum pre-cooling to product Pre-cooling allows the temperature of halogen squid from room temperature fast precooling, and the pressure of vacuum pre-cooling is 0.6kPa, and the final temperature of product pre-cooling is 3~5 ℃。
Further, halogen squid is freezed using double helix mono-frozen machine, temperature need to be operated by following freezing curve:
(1) -15~-10 DEG C are cooled to from 1~5 DEG C, cool down 5~8min, and rate of temperature fall is 1.5~4 DEG C/min;Quickly Temperature-fall period can allow squid product in frozen step quickly through zone of maximum ice crystal formation (- 5 DEG C~0 DEG C), interiors of products Ice crystal is minimum, so that the quick-frozen process organization structure of squid be effectively reduced by freeze injury, further avoids juice and nutriment Loss;
(2) -35~-30 DEG C are cooled to from -15~-10 DEG C, cool down 25~30min, and rate of temperature fall is 0.5~1 DEG C/min; Rate of temperature fall is reduced, prevents the preservative protective film for causing halogen squid surface to be formed after fast cooling from going out since rate of temperature fall is too fast Existing cracking phenomena;
(4) -20~-18 DEG C are warming up to from -35~-30 DEG C, heat up 5~10min, and heating rate is 1~3 DEG C/min;Fastly Temperature is risen to the central temperature of squid product by speed, prevents lasting low temperature from making the nutritional ingredient activity in squid weaker, is protected Demonstrate,prove the nutritional ingredient of squid product.
Meanwhile it collecting to thaw in the present invention and cuing open the squid leftover bits and pieces for killing acquisition using the progress of alkali protease enzymatic isolation method Fish oil in enzymolysis and extraction squid, the condition of extraction are as follows: enzyme amount 850u/g, solid-to-liquid ratio 1:8, enzymolysis time 3.8h, enzymatic hydrolysis temperature 48 DEG C and enzymolysis liquid pH of degree are 7.9, and the extracting solution that enzymatic hydrolysis obtains is added in the step S4 secondary seasoning, is further increased The nutriment ingredient of squid product, meanwhile, squid byproduct is also fully utilized, the added value of product processing is improved.
Test method:
The squid product obtained using processing method of the invention is compared with the similar squid product of traditional processing, quality Tender and crisp degree is effectively improved.It is tested using texture analyser, the tender and crisp degree of squid product is indicated with resistance measurement, i.e., Shearing force required when meat is cut, that is, the maximal force that blade cutting sample of popping one's head in needs.The location parameter of resistance measurement is set It is fixed: shear velocity 1.00mm/s;Speed 10.00mm/s after shearing;Shear distance 6mm.The test group and blank of each embodiment Test result is as follows for control group:
The tender and crisp degree test of 1 squid product of table
The water retention property of squid is embodied by defrosting loss late and cooking loss rate index in the present invention.
Defrosting loss late=(weight after weight-defrosting before thawing)/weight * 100% before thawing
Weight * 100% before cooking loss rate=(weight after weight-boiling before boiling)/boiling
The test of 2 squid water-retaining property of table
The above embodiment is a preferred embodiment of the present invention, but embodiments of the present invention are not by above-described embodiment Limitation, other any changes, modifications, substitutions, combinations, simplifications made without departing from the spirit and principles of the present invention, It should be equivalent substitute mode, be included in protection scope of the present invention.

Claims (10)

1. a kind of processing method for freezing instant halogen squid, which is characterized in that comprising the following specific steps
S1, immersion: it cuts open after the squid after killing is cleaned and impregnates 2 ~ 4 hours;
S2, stew in soy sauce: by stew in soy sauce in the squid investment thick gravy after draining;
S3, drying: the good squid of halogen carries out heat pump drying processing after draining thick gravy, and the heat pump temperature of heat pump drying processing is 35- 40 DEG C, dry humidity is 45 ~ 50%, and wind speed is 2 ~ 4m/s, 1 ~ 2h of drying time;
S4, secondary seasoning: heat pump drying treated halogen squid is subjected to secondary seasoning;
S5, packaging freezing: using the freezing of double helix mono-frozen machine is sent into after vacuum packaging, -18 DEG C are refrigerated to.
2. a kind of processing method for freezing instant halogen squid as described in claim 1, it is characterised in that: soaked in the step S1 Steeping the immersion complex liquid that process uses includes following components by weight percentage:
Component A: sodium carbonate 0.8 ~ 2.2%;Sodium citrate 1.5 ~ 5%;Sorbierite 2 ~ 4%;Trehalose 0.5 ~ 1.5% and edible salt 1 ~ 1.5%;
B component: green onion 3 ~ 8%;Ginger 3-8%;Cooking wine 2-4%;Beer 8-12% and surplus ice water;The ice water temperature is maintained at 5 ~ 8 DEG C, soaking time is 2 ~ 4 hours;Component A and B component will enter squid after being mixed evenly.
3. a kind of processing method for freezing instant halogen squid as described in claim 1, it is characterised in that: halogen in the step S2 The thick gravy that process processed uses prepares the component of following parts by weight: bone according to squid 3000-3500 parts of investment of weight ratio 800 ~ 1500 parts of soup, 500 ~ 800 parts of drinking water, 300 ~ 340 parts of dark soy sauce, 280 ~ 350 parts of spices bag, 250 ~ 300 parts of light soy sauce, refined salt 75 ~ 80 parts, 45 ~ 50 parts of white sugar, 35 ~ 50 parts of cooking wine, 30 ~ 35 parts of red soy sauce, 15 ~ 20 parts of chicken paste, 10 ~ 15 parts of monosodium glutamate, fish sauce 8 ~ 12 parts, 5 ~ 8 parts and 0.8 ~ 1.2 part of ethylmaltol of chicken fine powder.
4. a kind of processing method for freezing instant halogen squid as claimed in claim 3, it is characterised in that: the spices bag by Following weight composition: southern ginger 120-150 parts, 30-35 parts of lemongrass, 30-35 parts of garlic, 25-35 parts of coriander head, capsicum 15-20 parts, 12-17 parts of tsaoko, 10-15 parts of illiciumverum, 8-12 parts of zingiber kawagoii, 8-12 parts of cassia bark, 8-10 parts of Radix Glycyrrhizae, Siraitia grosvenorii 8-10 Part, 8-10 parts of dried orange peel, 5-8 parts of fennel seeds and 3-5 parts of cloves.
5. a kind of processing method for freezing instant halogen squid as described in claim 1, it is characterised in that: the step S4 bis- times The formula of seasoning prepares the component of following parts by weight: cumin according to 100 ~ 120 parts of squid of weight ratio after heat pump drying 0.2 ~ 0.7 part of powder, 0.5 ~ part of sweet plum powder 1,0.1 ~ 0.5 part of meat flavour essence cream, 0.2 ~ 0.7 part of sesame oil, 0.3 ~ 1 part of sweet fermented flour sauce, tremella 0.2 ~ 0.6 part of polysaccharide, 0.3 ~ 0.8 part of trehalose.
6. a kind of processing method for freezing instant halogen squid as described in claim 1, it is characterised in that: in the step S5 packet Trehalose composite solution is formed on the halogen squid surface of secondary seasoning under the action of cryogenic high pressure is fluidized and compressed before dress freezing The preservative protective film of composition;The trehalose composite solution is made of trehalose, sodium alginate and exogenous protease;Two will be passed through Secondary seasoned squid is sent into low temperature fluidized equipment, so that the aqueous trehalose low speed that mass concentration is 0.1 ~ 0.5% flows uniformly through Squid surface forms stable fluidisation liquid film, and temperature maintains 1 ~ 5 DEG C, and pressure maintains 0.2 ~ 0.5MPa, so that trehalose Composite solution is in squid surface homogeneous condensation film-forming.
7. a kind of processing method for freezing instant halogen squid as described in claim 1, it is characterised in that: true in the step S5 Before empty package, halogen squid is first subjected to the pre-cooling to product using vacuum pre-cooling, allows, makes the temperature of halogen squid fast from room temperature Speed pre-cooling, the pressure of vacuum pre-cooling are 0.6kPa, and the final temperature of product pre-cooling is 3 ~ 5 DEG C.
8. a kind of processing method for freezing instant halogen squid as described in claim 1, it is characterised in that: double in the step S5 Spiral mono-frozen machine freezes halogen squid, and temperature need to be operated by following freezing curve:
(1) -15 ~ -10 DEG C are cooled to from 1 ~ 5 DEG C, cool down 5 ~ 8min, and rate of temperature fall is that 1.5 ~ 4 DEG C/min(quickly spends crystallization Band);
(2) -35 ~ -30 DEG C are cooled to from -15 ~ -10 DEG C, cool down 25 ~ 30min, and rate of temperature fall is 0.5 ~ 1 DEG C/min;
(3) -20 ~ -18 DEG C are warming up to from -35 ~ -30 DEG C, heat up 5 ~ 10min, and heating rate is 1 ~ 3 DEG C/min.
9. a kind of processing method for freezing instant halogen squid as described in claim 1, it is characterised in that: use alkali protease Enzymatic isolation method carries out the fish oil in enzymolysis and extraction squid, the condition of extraction are as follows: enzyme amount 850u/g, solid-to-liquid ratio 1:8, enzymolysis time 3.8h, 48 DEG C of hydrolysis temperature and enzymolysis liquid pH are 7.9, and the extracting solution that enzymatic hydrolysis obtains is added to the step S4 secondary seasoning In.
10. the instant halogen squid of freezing made from a kind of processing method as described in claim 1 to 9 is any.
CN201811274006.2A 2018-10-30 2018-10-30 It is a kind of to freeze instant halogen squid and its processing method Pending CN109198493A (en)

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CN114946927A (en) * 2022-05-12 2022-08-30 福建省农业科学院农业工程技术研究所 Smoked goose preservation method suitable for e-commerce sales mode

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