CN109181929A - One kind removing heavy metal preparation of wine - Google Patents
One kind removing heavy metal preparation of wine Download PDFInfo
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- CN109181929A CN109181929A CN201811379994.7A CN201811379994A CN109181929A CN 109181929 A CN109181929 A CN 109181929A CN 201811379994 A CN201811379994 A CN 201811379994A CN 109181929 A CN109181929 A CN 109181929A
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12G—WINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
- C12G1/00—Preparation of wine or sparkling wine
- C12G1/02—Preparation of must from grapes; Must treatment and fermentation
- C12G1/0203—Preparation of must from grapes; Must treatment and fermentation by microbiological or enzymatic treatment
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- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Biotechnology (AREA)
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- Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
Abstract
The invention discloses one kind to remove heavy metal preparation of wine, and include the following steps: S1, choose raw material: selection maturity is good, and fruit is complete, nothing is broken, without green sick mildew and rot grape, and standing time was no more than 7 days;S2, destemming are broken: the new fresh grape chosen in S1 being cleaned up rear destemming and is crushed, is then added Chinese medical extract cryo-conservation 4-8 days;S3, alcoholic fermentation: broken grape is pumped into tank, and yeast liquid is added, and is fermented 6-12 days, and keeping temperature is 26-30 DEG C, and when specific gravity is down between 0.9995~0.992, is less than 4g/L containing sugar, alcoholic fermentation terminates.Compared with other preparation methods; the preparation method is suitable for industrialization and large-scale production; biggish economic results in society can be brought; and resulting wine quality is stablized; preparation process is not influenced by metal ion; improve the production control of grape wine, establishment of standard easy to produce and quality control.
Description
Technical field
The present invention relates to food processing fields, more specifically more particularly to a kind of preparation side for removing heavy metal grape wine
Method.
Background technique
Grape wine is the fermented wine for containing certain alcoholic strength made of brewing through grape.The raw material generally used is fresh
Grape or grape juice, to make grape wine rich in a variety of chemical beneficiating ingredients, such as amino acid, vitamin, organic acid, polysaccharide
Substance and total phenol substance (such as tannin, anthocyanidin, resveratrol).Often appropriateness drinks grape wine, can enhance human body blood
Liquid circulation reduces cholesterol level and promotes body metabolism, while can stimulate liver function and anti-aging, prevents angle
Film inflammation, anemia, reinforces digestive function at scurvy, is beneficial to alleviate cardiac conditions.
But most of grape wine is brewed by civil workshop or personal group at present, fermentation technique and product quality
Unstable, especially in brewing process, metal ion has a significant impact to the finished product tool of grape wine, and then leads to the steady of grape wine
Qualitative difference, mouthfeel are bad, it is difficult to realize real industrialization and scale, and in the brewing process for carrying out grape wine,
Its process of alcoholic fermentation the step is relatively simple, and fermentation liquid cannot be made to be uniformly mixed, and leads to the quality for influencing grape wine,
For this purpose, it is proposed that one kind removes heavy metal preparation of wine.
Summary of the invention
The purpose of the present invention is to solve disadvantages existing in the prior art, and the one kind proposed removes heavy metal grape wine
Preparation method.
To achieve the above object, the invention provides the following technical scheme: one kind removes heavy metal preparation of wine, packet
Include following steps:
S1, choose raw material: selection maturity is good, and fruit is complete, nothing is broken, without green sick mildew and rot grape, and when placement
Between be no more than 7 days;
S2, destemming are broken: the new fresh grape chosen in S1 being cleaned up rear destemming and is crushed, Chinese medical extract is then added
Cryo-conservation 4-8 days;
S3, alcoholic fermentation: broken grape is pumped into tank, and yeast liquid is added, and is fermented 6-12 days, and holding temperature is
26-30 DEG C, when specific gravity is down between 0.9995~0.992, is less than 4g/L containing sugar, alcoholic fermentation terminates;
S4, separation squeezing: carrying out separation squeezing for the grape solidliquid mixture after alcoholic fermentation, collects the liquid that squeezing obtains
Body, keeping temperature is 18-20 DEG C;
S5, lactic fermentation: will be added lactobacillus suspension in liquid obtained in S4, ferment 6-12 days, and holding temperature is 15-25
DEG C, then it is filtered again;
S6, ageing: in filtrate plus cation exchange resin, closed placement 60-120 days are kept for 10-15 DEG C of environment temperature,
Finally it is filtered.
Preferably, the Chinese medical extract additional amount in S2 is 0.05-0.1 times of the grape quality after stalk.
Preferably, grape avoids making grape when picking by that should be picked fine daytime in weather based on manually picking
Fruit is broken, and picking container is avoided using irony and copper utensil.
Preferably, for the Chinese medical extract in S2 the preparation method is as follows: taking Chinese honey locust pod appropriate, addition is equivalent to Chinese honey locust pod
2-4 times of the fruit water measured impregnates 2-4 days, and adjusting pH value is 7-9, and the cellulose for being equivalent to Chinese honey locust pod quality 0.5-1.5% is added
Complex enzyme digests 2-6 hours, and hydrolysis temperature is 40-60 DEG C, and enzyme is killed in water-bath, and temperature is 95-100 DEG C, and the time is 5-15 minutes,
Filtering, obtains enzymolysis liquid;It is 1.1-1.2 (50-60 DEG C of detection) that enzymolysis liquid, which is concentrated into relative density, and ethanol solution is added, makes entire
System concentration of alcohol reaches 60-80%, 12-24 hours static, filtering, and concentration filtrate to relative density is 1.15-1.25 (50-
60 DEG C of detections) to get.
Preferably, in the fermentation time in S3, reverse irrigation processing should be carried out, the grape liquid of fermenter base is pumped to
Fermentor top.
Preferably, the lactobacillus suspension additional amount in S5 is the 0.001-0.01% of entire fermentation liquid.
Technical effect and advantage of the invention:
1, the present invention controls the preparation process of grape wine using the characteristic of Chinese herbal medicine Chinese honey locust pod, and Chinese honey locust pod passes through enzyme
After solution is separated with alcohol precipitation, a large amount of gleditsin is obtained, the space structure energy polymer/metallic ionization well of gleditsin can
The metal ion generated in polymerized glucose and in fermentation process, guarantees going on smoothly for fermentation, traditional aging process be added sun from
Sub-exchange resin, after gleditsin resin-bonded, after the section of space in metal ion exchanged with the hydrogen ion in resin, mistake
It filters off and removes metal ion.
2, the grape liquid of fermenter base can be pumped to hair by carrying out reverse irrigation processing in alcoholic fermentation by the present invention
Fermentation tank top can then be such that fermentation liquid is uniformly mixed, and reinforce maceration, be dissolved in wine conducive to pigment and tannin, aroma substance,
It can be fermentation liquid ventilation oxygen supply, be conducive to yeast activity, keep fermentation more thorough, flavor is purer.
3, the resulting wine quality of the present invention is stablized, and preparation process is not influenced by metal ion, improves grape wine
Production control, establishment of standard easy to produce and quality control.
Specific embodiment
In order to make the objectives, technical solutions, and advantages of the present invention clearer, below in conjunction with specific embodiment, to this
Invention is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, not
For limiting the present invention.Based on the embodiments of the present invention, those of ordinary skill in the art are not before making creative work
Every other embodiment obtained is put, shall fall within the protection scope of the present invention.
Embodiment
One kind removing heavy metal preparation of wine, includes the following steps:
S1, choose raw material: selection maturity is good, and fruit is complete, nothing is broken, without green sick mildew and rot grape, and when placement
Between be no more than 7 days;
S2, destemming are broken: the new fresh grape chosen in S1 being cleaned up rear destemming and is crushed, Chinese medical extract is then added
Cryo-conservation 4-8 days;
S3, alcoholic fermentation: broken grape is pumped into tank, and yeast liquid is added, and is fermented 6-12 days, and holding temperature is
26-30 DEG C, when specific gravity is down between 0.9995~0.992, is less than 4g/L containing sugar, alcoholic fermentation terminates;
S4, separation squeezing: carrying out separation squeezing for the grape solidliquid mixture after alcoholic fermentation, collects the liquid that squeezing obtains
Body, keeping temperature is 18-20 DEG C;
S5, lactic fermentation: will be added lactobacillus suspension in liquid obtained in S4, ferment 6-12 days, and holding temperature is 15-25
DEG C, then it is filtered again;
S6, ageing: in filtrate plus cation exchange resin, closed placement 60-120 days are kept for 10-15 DEG C of environment temperature,
Finally it is filtered.
In summary: one kind provided by the invention removes heavy metal preparation of wine, compared with other preparation methods,
The preparation method is suitable for industrialization and large-scale production, can bring biggish economic results in society, and resulting grape wine
Quality is stablized, and preparation process do not influenced by metal ion, improves the production control of grape wine, establishment of standard easy to produce and
Quality control.
Finally, it should be noted that the foregoing is only a preferred embodiment of the present invention, it is not intended to restrict the invention,
Although the present invention is described in detail referring to the foregoing embodiments, for those skilled in the art, still may be used
To modify the technical solutions described in the foregoing embodiments or equivalent replacement of some of the technical features,
All within the spirits and principles of the present invention, any modification, equivalent replacement, improvement and so on should be included in of the invention
Within protection scope.
Claims (6)
1. one kind removes heavy metal preparation of wine, characterized by the following steps:
S1, choose raw material: selection maturity is good, and fruit is complete, nothing is broken, without green sick mildew and rot grape, and standing time is not
More than 7 days;
S2, destemming are broken: the new fresh grape chosen in S1 being cleaned up rear destemming and is crushed, Chinese medical extract low temperature is then added
It saves 4-8 days;
S3, alcoholic fermentation: broken grape is pumped into tank, and yeast liquid is added, and is fermented 6-12 days, and holding temperature is 26-
30 DEG C, when specific gravity is down between 0.9995~0.992, is less than 4g/L containing sugar, alcoholic fermentation terminates;
S4, separation squeezing: carrying out separation squeezing for the grape solidliquid mixture after alcoholic fermentation, collects the liquid that squeezing obtains,
Keeping temperature is 18-20 DEG C;
S5, lactic fermentation: will be added lactobacillus suspension in liquid obtained in S4, ferment 6-12 days, and keeping temperature is 15-25 DEG C,
Then it is filtered again;
S6, ageing: in filtrate plus cation exchange resin, closed placement 60-120 days are kept for 10-15 DEG C of environment temperature, finally
It is filtered.
2. one kind according to claim 1 removes heavy metal preparation of wine, it is characterised in that: the Chinese medicine in S2
Extract additional amount is 0.05-0.1 times of the grape quality after stalk.
3. one kind according to claim 1 removes heavy metal preparation of wine, it is characterised in that: grape is by manually adopting
It based on plucking, should be picked fine daytime in weather, avoid making grape fruit broken when picking, picking container is avoided using iron
Matter and copper utensil.
4. one kind according to claim 1 removes heavy metal preparation of wine, it is characterised in that: the Chinese medicine in S2
Method for preparing extractive is as follows: taking Chinese honey locust pod appropriate, addition is equivalent to the water that 2-4 times of Chinese honey locust pod is measured, and impregnates 2-4 days, adjusts
Section pH value is 7-9, and the cellulose complex enzyme for being equivalent to Chinese honey locust pod quality 0.5-1.5% is added, and is digested 2-6 hours, enzymatic hydrolysis temperature
Degree is 40-60 DEG C, and enzyme is killed in water-bath, and temperature is 95-100 DEG C, and the time is 5-15 minutes, and filtering obtains enzymolysis liquid;Enzymolysis liquid is concentrated into
Relative density is 1.1-1.2 (50-60 DEG C of detection), and ethanol solution is added, whole system concentration of alcohol is made to reach 60-80%, quiet
Only 12-24 hours, filtering, concentration filtrate to relative density be 1.15-1.25 (50-60 DEG C detection) to get.
5. one kind according to claim 1 removes heavy metal preparation of wine, it is characterised in that: the fermentation in S3
In time, reverse irrigation processing should be carried out, the grape liquid of fermenter base is pumped to fermentor top.
6. one kind according to claim 1 removes heavy metal preparation of wine, it is characterised in that: the lactic acid in S5
Bacterium solution additional amount is the 0.001-0.01% of entire fermentation liquid.
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CN201811379994.7A CN109181929A (en) | 2018-11-20 | 2018-11-20 | One kind removing heavy metal preparation of wine |
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CN201811379994.7A CN109181929A (en) | 2018-11-20 | 2018-11-20 | One kind removing heavy metal preparation of wine |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113801758A (en) * | 2021-09-22 | 2021-12-17 | 劲牌有限公司 | Method for reducing total saponin loss and delaying total saponin attenuation in shelf life in production process of health-care wine |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107937192A (en) * | 2018-01-23 | 2018-04-20 | 胡江宇 | A kind of preparation of wine |
CN107937202A (en) * | 2018-01-23 | 2018-04-20 | 胡江宇 | Remove heavy metal preparation of wine |
CN108018146A (en) * | 2018-01-23 | 2018-05-11 | 胡江宇 | Remove heavy metal grape wine and preparation method thereof |
CN108018147A (en) * | 2018-01-23 | 2018-05-11 | 胡江宇 | Ultrasonic washing prepares the method for removing heavy metal grape wine |
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2018
- 2018-11-20 CN CN201811379994.7A patent/CN109181929A/en not_active Withdrawn
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107937192A (en) * | 2018-01-23 | 2018-04-20 | 胡江宇 | A kind of preparation of wine |
CN107937202A (en) * | 2018-01-23 | 2018-04-20 | 胡江宇 | Remove heavy metal preparation of wine |
CN108018146A (en) * | 2018-01-23 | 2018-05-11 | 胡江宇 | Remove heavy metal grape wine and preparation method thereof |
CN108018147A (en) * | 2018-01-23 | 2018-05-11 | 胡江宇 | Ultrasonic washing prepares the method for removing heavy metal grape wine |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113801758A (en) * | 2021-09-22 | 2021-12-17 | 劲牌有限公司 | Method for reducing total saponin loss and delaying total saponin attenuation in shelf life in production process of health-care wine |
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Application publication date: 20190111 |
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