CN109181907A - A kind of high hair conditioning natural liquid essential oil soap and preparation method thereof - Google Patents
A kind of high hair conditioning natural liquid essential oil soap and preparation method thereof Download PDFInfo
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- CN109181907A CN109181907A CN201810861403.3A CN201810861403A CN109181907A CN 109181907 A CN109181907 A CN 109181907A CN 201810861403 A CN201810861403 A CN 201810861403A CN 109181907 A CN109181907 A CN 109181907A
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
- C11D9/262—Organic compounds, e.g. vitamins containing oxygen containing carbohydrates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/30—Organic compounds, e.g. vitamins containing nitrogen
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
Abstract
The invention discloses a kind of high hair conditioning natural liquid essential oil soaps and preparation method thereof, it is saponified by the vegetable fat of 22-28%, the sucrose of 7.0%-20%, the polyalcohol of the C3-C6 of 7.0%-14%, the fragrant plant of 3.0%-6.0% impregnates oil and the water-soluble carrier of surplus forms.Finished product is sucrose ester micro emulsion transparent under room temperature, significantly improves the hair conditioning to hair and skin.The present invention improves the hair conditioning of soap lye using sucrose ester micro emulsion preparation process principle, avoids damage of the strong basicity soap base product to hair and skin；And provide a kind of liquid form for being more suitable for quantitative fetching；Its transparent appearance, the natural origin of formula material and suitable volume production condition are kept simultaneously.
Description
Technical field
The present invention relates to a kind of essential oil soap, in particular to the transparent type liquid natural essential oil soap of a kind of high hair conditioning.
Background technique
Soap base product is as traditional cleaning products, since it forms the ionization property of fatty acid salt, pH all meta-alkalescences,
Therefore its cleaning force and degreasing power are all relatively strong, also relatively obvious to the damage of skin and hair.Nowadays people wash individual
The requirement of shield product is not only basic cleaning, and is more the use feeling and functionality for paying attention to product, simple soap base
Product has been unable to meet consumer demand.A kind of faintly acid essential oil soap of the patent of invention for being application No. is 201510131076 and
Preparation method improves the hair conditioning of soap by changing pH；Application No. is a kind of conditionings of 201710780506.2 patent of invention
Type solid-state hair soap uses the common prescription system of liquid shampoo, such as increases mild cosurfactant, and adjust with cation
The mode of reason agent and silicone oil compounding improves hair conditioning.
And people for soap product dote on be more due to its natural raw material sources, good biological degradability and
It is easy the characteristic rinsed.The preparation process of handmade soap is complicated, at high cost, is not suitable for volume production.It is (a kind of that essential oil soap then more focuses on fragrant atmosphere
Osmanthus essential oil soap, 201610714378.7；Essential oil soap of extract containing lemon grass and preparation method thereof, 201711140247.3)
With transparent appearance (essential oil soap -201730260122.9；Essential oil soap (lavender anti-acne) 201730377652.1.Using conjunction
At branched fatty acid or short chain fatty acids (US3793214), or by addition ethyl alcohol etc. clarifiers (transparent solid perfumed soap,
200880018983.4) or the crystal form of punching press change soap can produce solid transparent soap product.But this solid product
It is always not easy to rationed and safety and sanitation storages, and the product of the strong basicity of usually complete neutralization in use,
It is also undesirable to the hair conditioning of skin and hair.And traditional alkalescent Soap-base facial cleanser cannot then form transparent appearance, and
And formula usually requires addition stabilizer, the hair conditioning applied on hair is also required to improve.
Summary of the invention
The technical problem to be solved by the present invention is to overcome the defects of the hair conditioning difference of soap base product in the prior art, provide
A kind of high hair conditioning natural liquid essential oil soap composition and preparation method thereof.
In order to solve the above-mentioned technical problems, the present invention provides the following technical solutions:
A kind of high hair conditioning natural liquid essential oil soap, the vegetable fat containing weight percent 22-28% is saponified, also contains:
(a) sucrose of composition weight percentage 7.0%-20% is accounted for；
(b) polyalcohol of the C3-C6 of composition weight percentage 7.0%-14% is accounted for；
(c) fragrant plant for accounting for composition weight percentage 3.0%-6.0% impregnates oil；
(d) the water-soluble carrier of surplus；
The sum of the saponified middle stearate of the vegetable fat and palmitate content < 10%(w/w)；The C3-C6's is more
First alcohol contains the propylene glycol for accounting for its 50% or more weight, and the fragrant plant impregnates oil for basic vegetable fat and volatile aromatic
The mixture of oil, contains the fatty glyceride for accounting for its 95% or more weight；The sucrose and fragrant plant impregnate mole of oil
Than > 3；Content >=20%(w/w of natural surfactant in the water-soluble carrier).And without containing any type of
Polymer viscosifier.
Further, saponified 50-80 parts of the preferred lauric acid soap compound of the vegetable fat, oleic acid is 20-50 parts saponified,
0-20 parts of palmitic acid soap compound and stearic acid are 0-8 parts saponified.Or preferably coconut oil is 50-80 parts saponified, olive oleate soap
20-50 parts of compound, saponified 20-50 parts of ricinoleic acid and palmitoleic acid are 0-20 parts saponified.
Further, viscosity 3,000-8,000cps.
Further, the fragrant plant impregnates oil for unsaturated fatty acid content > 65%(w/ in basic vegetable fat
W), and stearic acid content < 10%(w/w) functional plants grease.
Further, it is the quality of fragrant plant and base plants grease according to 0.1%-2% that the fragrant plant, which impregnates oil,
Volume ratio (g/ml) is than preparation；Base plants grease preferably refines fruit oil and embryo oil, can be rose hip oil, Morocco's nut
Oil, macadimia nut oil, tattoo fruit oil, wheat-germ oil, any one or more in maize germ oil.Volatile aromatic oil mentions
Take Cajeputtree Leaf, lavender, rosemary aerial part, chamomile, Mai Luka, honeysuckle, roseleaf or grapefruit peel.
Further, the polyalcohol can be propylene glycol, sorbierite, pentanediol composition, and the polyalcohol both can be with
The assistant for emulsifying agent that micro emulsion is formed in production technology can also be done as the cosolvent for promoting sucrose and emulsifying vegetable fat
The moisturizer and transparencizing agent of product.It is preferred that propylene glycol can disappear because propylene glycol has dissolution for fatty acid and its salt
Except the pearly-lustre of saturated fatty acid, promotes the emulsification of sucrose and vegetable fat, be effective clarifier and visbreaking agent in system.It is polynary
Alcohol can also be sorbierite, and pentanediol reinforces moisturizing or facilitates dissolved fat hydrochlorate, and reaction is accelerated to carry out；Pentanediol is also
With enhancing antibacterial action.Preferred propylene glycol 50-80 parts of the glycol composition, 20-50 parts of pentanediol, sorbierite 0-30
Part.
Further, 50-80 parts of natural surfactant optimizing alkyl glucosides in the water-soluble carrier, fatty acyl
0-50 parts of amino-acid salt, 0-50 parts of saponin.The natural surfactant has buffered alkaline to fatty acid salt soap base system,
Reduce irritation and hard water resistance, foam enhancing or the different role of foam stabilizing；Also there is solubilising to alkalescent soap base system of the invention
Fatty acid maintains the effect of transparency.
The alkyl glucoside surfactant synthesizes non-ionic surface by renewable resource natural fatty alcohol and glucose and lives
Property agent, compatibility are good；Without cloud point；Dissolubility is good, high temperature resistant, resistance to highly basic and resisting high-concentration electrolyte.It can assist in the present invention
The hair conditioning of soap base product is improved, and improves hard water resistance property.The alkyl glycosides can be but be not limited to Decyl Polyglucoside, lauryl
Glucosides, cocoyl glucosides.
The fatty acyl amino-acid salt is had by amino acid and fatty acyl anionic surfactant dimerous
Good skin-friendly and lubricious wash shield effect.The hair conditioning of raising soap base product can be assisted in the present invention.The fatty acyl ammonia
Base hydrochlorate can be but be not limited to cocounut oil acyl glycinate, cocoyl sarcosine salt.
The saponin is a kind of special glucoside for being widely present in plant kingdom, for oral administration that there is different adjustings to be immunized
Physiological activity.It is for oral administration that plasma testosterone level can be improved if total saponins of tribulus is a kind of galenical of original non-hormone, enhance muscle
Strength, external application can be anti-oxidant and pre- anti-aging.In weak basic condition, saponin can balance the hair conditioning of soap base, and enhancing is thin
Born of the same parents' vigor.The saponin can be but be not limited to total saponins of tribulus, ginsenoside, Tea Saponin, gleditsia sinensis saponin(e, notoginsenoside,
Yucconin, sapindoside.The water-soluble carrier can also include day that other cosmetics allow to add, water-soluble
Right functional component.The water-soluble natural functional component can be but be not limited to moisturizing ingredient, whitening composition, anti-acne ingredient
And the water-soluble natural functional component of antibacterial, anti-inflammatory and other effects.The water-soluble natural functional component preferably clear matter acid, bee
Sweet extract, polysaccharide, dipotassium glycyrrhizinate, D-pantothenyl aleohol, functional polypeptide and other effect plant extracts.
The preparation method of above-mentioned high hair conditioning natural liquid essential oil soap, comprising the following steps:
(1) it after mixing each component in proportion, is stirred at low speed at 65-70 DEG C molten to uniform；
(2) stop stirring, temperature is increased to 85-95 DEG C, keeps the temperature 3.0-6.0h, carries out ester exchange reaction；
(3) water-solubility carrier is added, adding appropriate organic acid to be neutralized to pH is 7.5-8.5, and it is saturating to lotion to stir at low speed 10-30min
It is bright uniform；Organic acid can be the composition of citric acid, lauric acid, acetic acid.Optimization citric acid, neutralized reaction product is in pH6.0-
8.0 all have hard water resistance effect；
(4) stop stirring, stand defoaming；Temperature is down to 40-45 DEG C, filling.
Above-mentioned preparation process amelioration purpose is to realize under alkaline condition and promotes sucrose and fat at a temperature of being suitable for
The ester exchange reaction of acid esters.The critical issue needed to pay attention to: alkaline condition is suitable for, to reduce the saponification of vegetable fat and reinforce ester
Exchange reaction；Temperature condition is suitable for accelerating ester exchange reaction and avoiding sucrose coking, avoids the excessive steaming of aromatic essential oil
Hair.The ester exchange reaction of last stage sucrose and vegetable fat needs soap base to keep high alkalinity condition (pH10 or more)；Stage afterwards
Acid adding terminates reaction, needs pH7.0 or more, to avoid the precipitation of fatty excessive acid, without foaming properties；It is preferred that pH7.5-8.5.
Microemulsion be usually Thermodynamically stable and has < dispersion of the partial size of 50nm, it can be stood by simply mixing
Formed.They are the oily phase containing water phase, emulsifier and assistant for emulsifying agent.The emulsifier surface activator composition different with HLB
To be preferred, usually non-ionic or both sexes table is living；Assistant for emulsifying agent, usually the polyalcohol or alkanol of water-insoluble, help
In reducing interfacial tension, to reduce the size of dispersant liquid drop；Oily is usually mutually polarity grease, such as plant fragrance essential oil and plant
Grease can prepare microemulsion, and it is transparent that wherein plant fragrance essential oil, which is easier solubilising,；And nonpolar alkane is then not suitable for
Prepare microemulsion.The representative formula of sucrose ester micro emulsion: 30% Surfhope SE Cosme C 1216,20% glycerol, 50% vegetable fat are formed
One transparent micro emulsion.
Fatty acid salt-polyalcohol-sucrose ester/fatty glyceride system of liquid essential oil soap of the present invention is also one
Stable microemulsion system, water dilution cannot destroy its stability.And under external force, during skin or hair friction
It could be demulsified.Therefore using the cleaning of this micro emulsion, do not need by with the coefficient deposition flocculation process of cation.In skin
When the protection of itself grease of skin, hair is insufficient, is discharged by external force and skin or hair friction, forms discontinuous adipose membrane,
The strong degreasing power that fatty acid salt can not only be alleviated can also significantly improve the hair conditioning of hair wet comb and dry comb.And sucrose ester
As relatively highly polar esters, there is certain emulsifiability can assist in removing when skin and hair grease is thick and heavy for itself
Polarity is weak or nonpolar greasy deposits.Sucrose ester is a kind of function admirable, reproducible liquid crystal emulsifier, is usually used in food
Industry and pharmaceuticals industry: nontoxic food, drug emulsifier；Collaboration improves the inoxidizability of VE；It is right with prebiotic antibacterial action
Bacillus bacteriostasis is significantly and to lactic acid bacteria unrestraint；It is applied in cosmetics usually as advanced creams, the emulsification of shampoo
Agent, the grease that performance is secreted similar to skin.The sucrose ester price of purifying 20-25 member/kilogram, vegetable fat is usually 10-
15 yuan/kg.
The preparation process of sucrose ester includes organic solvent method, micro emulsion method etc..Wherein micro emulsion method mechanism is aliphatic ester and rouge
Fat hydrochlorate, propylene glycol, sucrose aqueous solution, formed have emulsifier and emulsion adjuvant microemulsion system；Micro emulsion attaching space with
And the alkaline condition that fatty acid salt is formed may advantageously facilitate sucrose and aliphatic ester generation ester exchange reaction generation sucrose-fatty
Ester.This preparation process sucrose ester yield is high, and consersion unit is simple, is fatty acid salt, the third two for raw-food material preparation defect
Alcohol is difficult to remove, and influences the purity of product sucrose ester, is unfavorable for its application in food.But this fatty acid salt-is polynary
Alcohol-sucrose ester micro emulsion mixed form is but conducive to soap base and washes shield performance improvement.And the present invention controls sucrose and vegetable oil
The ratio of rouge improves the ratio of reaction product sucrose-fatty monoesters with excessive sucrose；Transparent sucrose ester easy to form is micro-
Cream.
The beneficial effects obtained by the present invention are as follows being: the present invention improves the tune of soap lye using sucrose ester micro emulsion preparation process principle
Rationality avoids damage of the strong basicity soap base product to hair and skin；And provide a kind of liquid shape for being more suitable for quantitative fetching
Formula；Its transparent appearance, the natural origin of formula material and suitable volume production condition are kept simultaneously.
(1) sucrose ester micro emulsion transparent under room temperature is generated by improving production technology, significantly improved to hair and skin
Hair conditioning；
(2) using the content and ratio of suitable fatty acid salt, the generation technique that the later period is moderately acidified is generated in conjunction with sucrose ester and is set
Meter forms liquid transparent and that pH, viscosity are suitable；
(3) sucrose ester production technology and soap preparing process are combined, the production of sucrose ester-fatty acid salt-polyalcohol micro emulsion is made full use of
Product characteristic, the subsequent complicated technology bring product cost for avoiding sucrose ester from purifying increase.
Specific embodiment
Hereinafter, preferred embodiments of the present invention will be described, it should be understood that preferred embodiment described herein is only used
In the description and interpretation present invention, it is not intended to limit the present invention.
Embodiment
Embodiment I-V is prepared according to the proportion of table 1, the preparation method is as follows:
(1) commercial sources of fatty acids and pentanediol mixing are weighed as oily phase by formula rate, is heated to 65-70 DEG C；Other polyalcohols
Addition water phase is made into 30% aqueous slkali and is heated to 65-70 DEG C, and 100-300rpm stirs at low speed stirring water phase, and oil is mutually slowly added to
Water phase, saponification 30min；
(2) sucrose is weighed by formula rate and fragrant plant impregnates oil；Saponification kettle is added, 100-300rpm is stirred at low speed
10-30min, until saponified, polyalcohol, sucrose and fragrant plant impregnate oil uniformly；
(3) stop stirring, temperature is increased to 90 DEG C, keeps the temperature 3-6h, carries out ester exchange reaction；
(4) surplus aqueous carrier is added, adding appropriate citric acid to be neutralized to pH is about that 8.5,50-150rpm stirs 10-30min extremely
Lotion clear homogeneous；
(5) stop stirring, stand defoaming；Temperature is down to 40-45 DEG C, filling.
Table 1: the component of embodiment I-V
Embodiment VI-Ⅹ is prepared according to the proportion of table 2, following steps content is only modified: (1) weighing commercial plant by formula rate
Oil and pentanediol mixing；(4) adding appropriate citric acid to be neutralized to pH is 7.5；The preparation method of other same embodiment I-V.
Table 2: the component of embodiment VI-Ⅹ
Efficacy assessments embodiment of the method:
(1) viscosity measurement: DV-II+ Pro type viscosimeter is used, is operated according to operation instructions；Test result is shown in record sheet 1
With table 2
(2) transparency: using transmitance instrument LS116, calculates light transmittance；Sample transmittance Tx, cuvette light transmittance T0, cuvette
Add sample transmittance T1, Tx=T1/T0 × 100
(3) hair conditioning: using investigation evaluation method on probation.Specific testing program is half a head/half face Blind Test test method；Test specimens
Product are embodiment I-Ⅹ, and control is respectively CK1(3 sample of commercially available no silicone oil type conditioner shampoo) and commercially available soap base mildy wash CK2
(3 samples), chance sample and 2 controls are respectively issued to 30 testers, by subject according to use feel give a mark.
Smoothness when half a head experimental test evaluation index includes hair washing, when drying hair plentiful degree, comprehensive scalp grease balance；Half face is surveyed
Examination evaluation index includes bath property, washes rear salubrious degree (spatter property), washes rear smooth degree (moistness), comprehensive grease balance.Respectively
Item index is using 7 points of systems: it is excellent to be denoted as 6-7 points, 5-6 points are well denoted as, and generally 3-4 divides, and it is dissatisfied to be denoted as 1-2 points, completely
It cannot receive to be denoted as 0 point.
Table 3: each embodiment tries out efficacy measures
Transparency liquid essential oil soap of the present invention is in hair washing smoothness, moistness aspect and the commercially available production of face cleaning known on probation
Condition is close, and the plentiful degree of washability, hair and the salubrious sense of face, the evaluation of comprehensive grease balance are then higher than corresponding city
Sell product.Illustrate that liquid essential oil soap product of the invention is suitable as hair washing and face cleaning product.
Finally, it should be noted that the foregoing is only a preferred embodiment of the present invention, it is not intended to restrict the invention,
Although the present invention is described in detail referring to the foregoing embodiments, for those skilled in the art, still may be used
To modify the technical solutions described in the foregoing embodiments or equivalent replacement of some of the technical features.
All within the spirits and principles of the present invention, any modification, equivalent replacement, improvement and so on should be included in of the invention
Within protection scope.
Claims (10)
1. a kind of high hair conditioning natural liquid essential oil soap, the vegetable fat containing weight percent 22-28% is saponified, also contains:
(a) sucrose of composition weight percentage 7.0%-20% is accounted for；
(b) the C3-C6 polyalcohol of composition weight percentage 7.0%-14% is accounted for；
(c) fragrant plant for accounting for composition weight percentage 3.0%-6.0% impregnates oil；
(d) the water-soluble carrier of surplus；
The sum of the saponified middle stearate of the vegetable fat and palmitate content < 10%(w/w)；The C3-C6's is more
First alcohol contains 50%(w/w) more than propylene glycol, the fragrant plant impregnates oil for basic vegetable fat and volatile aromatic oil
Mixture contains 95%(w/w) or more fatty glyceride；The sucrose and fragrant plant impregnate the molar ratio > 3 of oil；
Content >=20%(w/w of natural surfactant in the water-soluble carrier).
2. high hair conditioning natural liquid essential oil soap as described in claim 1, which is characterized in that its viscosity is 3,000-8,
000cps。
3. high hair conditioning natural liquid essential oil soap as described in claim 1, which is characterized in that the fragrant plant impregnates oil
Base plants grease be unsaturated fatty acid content > 65%(w/w), and stearic acid content < 10%(w/w) functional plants oil
Rouge.
4. high hair conditioning natural liquid essential oil soap as described in any one of claims 1-3, which is characterized in that the fragrant plant
The base plants grease for impregnating oil is rose hip oil, argan oil, macadimia nut oil, tattoo fruit oil, wheat-germ oil, jade
Any one or more in rice germ oil.
5. high hair conditioning natural liquid essential oil soap as claimed in claim 4, which is characterized in that the fragrant plant impregnates oil
Volatile aromatic oil extracts from cajeputtree, lavender, chamomile, rose, rosemary, Mai Luka, honeysuckle or grape fruit
Any combination.
6. high hair conditioning natural liquid essential oil soap as described in claim 1, which is characterized in that the polyalcohol is with weight
50-80 parts of the propylene glycol of number meter, 20-50 parts and sorbierite 0-30 parts of pentanediol.
7. high hair conditioning natural liquid essential oil soap as described in claim 1, which is characterized in that in the water-soluble carrier
Natural surfactant includes 50-80 parts of alkyl glycosides, and 0-50 parts and saponin 0-50 parts of fatty acyl amino-acid salt.
8. high hair conditioning natural liquid essential oil soap as described in claim 1, which is characterized in that the saponified packet of vegetable fat
50-80 parts of lauric acid soap compound based on parts by weight are included, oleic acid is 20-50 parts saponified, 0-20 parts of palmitic acid soap compound and hard
Saponified 0-8 parts of matter acid；Or coconut oil based on parts by weight is 50-80 parts saponified, olive oleic acid is 20-50 parts saponified, castor
Saponified 20-50 parts of sesame oil acid 0-20 parts saponified with palmitoleic acid.
9. high hair conditioning natural liquid essential oil soap as claimed in claim 5, which is characterized in that the fragrant plant impregnate oil by
Plant vector and base plants grease rich in the volatile aromatic oil are prepared according to the mass volume ratio (g/ml) of 0.1%-2%
It forms.
10. the preparation method of high hair conditioning natural liquid essential oil soap described in claim 1, comprising the following steps:
(1) it after mixing each component in proportion, is stirred at low speed at 65-70 DEG C molten to uniform；
(2) stop stirring, temperature is increased to 85-95 DEG C, keeps the temperature 3.0-6.0h, carries out ester exchange reaction；
(3) water-solubility carrier is added, adding appropriate organic acid to be neutralized to pH is 7.5-8.5, and it is saturating to lotion to stir at low speed 10-30min
It is bright uniform；
(4) stop stirring, stand defoaming；Temperature is down to 40-45 DEG C, filling.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110591843A (en) * | 2019-09-20 | 2019-12-20 | 新疆牧马人生物技术有限公司 | Liquid horse oil soap and preparation method thereof |
| CN110846161A (en) * | 2019-11-28 | 2020-02-28 | 上海绿瑞生物科技有限公司 | Soap-based composition for personal washing care |
| CN113490737A (en) * | 2019-03-01 | 2021-10-08 | 联合利华知识产权控股有限公司 | Soap bars with improved flavor impact and active deposition |
| CN113855593A (en) * | 2021-11-22 | 2021-12-31 | 深圳市科迪生物科技有限公司 | Safe and non-irritant liquid essential oil antibacterial soap and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6357699A (en) * | 1986-08-28 | 1988-03-12 | 株式会社資生堂 | Transparent gel like composition |
| CN1658831A (en) * | 2002-06-07 | 2005-08-24 | 宝洁公司 | Cleansing articles for skin or hair |
| CN106753916A (en) * | 2016-12-09 | 2017-05-31 | 刘彩英 | A kind of pure natural liquid handmade soap and preparation method thereof |
| CN106883959A (en) * | 2017-02-24 | 2017-06-23 | 浙江如美日化有限公司 | A kind of Chinese torreya essential oil soap |
| CN108004064A (en) * | 2016-11-01 | 2018-05-08 | 深圳市科迪生物科技有限公司 | A kind of high transparency craft essential oil soap and preparation method thereof |
-
2018
- 2018-08-01 CN CN201810861403.3A patent/CN109181907A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6357699A (en) * | 1986-08-28 | 1988-03-12 | 株式会社資生堂 | Transparent gel like composition |
| CN1658831A (en) * | 2002-06-07 | 2005-08-24 | 宝洁公司 | Cleansing articles for skin or hair |
| CN108004064A (en) * | 2016-11-01 | 2018-05-08 | 深圳市科迪生物科技有限公司 | A kind of high transparency craft essential oil soap and preparation method thereof |
| CN106753916A (en) * | 2016-12-09 | 2017-05-31 | 刘彩英 | A kind of pure natural liquid handmade soap and preparation method thereof |
| CN106883959A (en) * | 2017-02-24 | 2017-06-23 | 浙江如美日化有限公司 | A kind of Chinese torreya essential oil soap |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113490737A (en) * | 2019-03-01 | 2021-10-08 | 联合利华知识产权控股有限公司 | Soap bars with improved flavor impact and active deposition |
| CN110591843A (en) * | 2019-09-20 | 2019-12-20 | 新疆牧马人生物技术有限公司 | Liquid horse oil soap and preparation method thereof |
| CN110846161A (en) * | 2019-11-28 | 2020-02-28 | 上海绿瑞生物科技有限公司 | Soap-based composition for personal washing care |
| CN110846161B (en) * | 2019-11-28 | 2021-07-13 | 上海绿瑞生物科技有限公司 | Soap-based composition for personal washing care |
| CN113855593A (en) * | 2021-11-22 | 2021-12-31 | 深圳市科迪生物科技有限公司 | Safe and non-irritant liquid essential oil antibacterial soap and preparation method thereof |
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