CN109179578A - A kind of processing method of coal mine water and/or coal washing waste water - Google Patents
A kind of processing method of coal mine water and/or coal washing waste water Download PDFInfo
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- CN109179578A CN109179578A CN201811146522.7A CN201811146522A CN109179578A CN 109179578 A CN109179578 A CN 109179578A CN 201811146522 A CN201811146522 A CN 201811146522A CN 109179578 A CN109179578 A CN 109179578A
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/44—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/44—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis
- C02F1/441—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis by reverse osmosis
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L5/00—Solid fuels
- C10L5/40—Solid fuels essentially based on materials of non-mineral origin
- C10L5/46—Solid fuels essentially based on materials of non-mineral origin on sewage, house, or town refuse
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2209/00—Controlling or monitoring parameters in water treatment
- C02F2209/11—Turbidity
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2301/00—General aspects of water treatment
- C02F2301/04—Flow arrangements
- C02F2301/046—Recirculation with an external loop
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2303/00—Specific treatment goals
- C02F2303/14—Maintenance of water treatment installations
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/30—Fuel from waste, e.g. synthetic alcohol or diesel
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
Abstract
The invention discloses the processing method of a kind of coal mine water and/or coal washing waste water, include the following steps: that coal mine water and/or coal washing waste water are sent into conditioning tank by (1), regulating water quality water obtains raw water;(2) raw water is sent into flat ceramic membrane cisterna, is purified with flat ceramic membrane module, to completely remove tiny particles content therein, drops the turbidity of low-yield water;The method of operation of the flat ceramic membrane module is suction, stops with backwashing period alternately;(3) bed mud of above-mentioned flat ceramic membrane cisterna is fabricated to the coal washing mud cake that can be mixed with coal wind fuel, forms fuel again, realizes that recycling sludge utilizes;The production water of above-mentioned flat ceramic membrane module is subjected to advanced treating or as water direct reuse in industry.Processing method of the invention can not only remove large particle, and can effectively remove tiny particles content, be not necessarily to dosing, gained bed mud can reuse be used as fuel, gained producing water water quality stabilization, meet reuse standard.
Description
Technical field
The invention belongs to mine wastewater processing technology fields, and in particular to a kind of coal mine water and/or coal washing waste water
Processing method.
Background technique
Coal mine water, gangue, coal mine gas are the typical three wastes of coal mining industry.Coal mine water, which refers to, to be adopted
During coal, all water for penetrating into down-hole mining space also have the spy having a large capacity and a wide range containing the surface water penetrated on a small quantity sometimes
Point.It is counted according to Coal Industry Society (CIS), it is contemplated that arrive the year two thousand twenty, coal in China exploitation total amount is up to 4,000,000,000 tons, generates mine water 60
Billion cubic meter.Coal mine water mainly contains suspended matter, inorganic salts, heavy metal etc., will be to surrounding body, soil if direct emission
Earth, people and animals cause damages.Therefore, coal purification of mine drainage and water resources comprehensive utilization become the new emphasis of industry.
Coal washing waste water include wet type coal washing generate waste water, the black water of coal preparation plant, coal-burning power plant ground flushing waste water
Deng being all the mixture of water and fine breeze, be mainly characterized by turbidity height, particulate size is thin, and solid particles surface mostly band is negative
Charge, the repulsion between homophilic charge make these particles keep dispersity in water, are influenced by gravity and Brownian movement;Due to
Interaction (such as adsorb, dissolve, chemical combination) in black water between solid particle interface, keeps the property of coal washing waste water quite multiple
It is miscellaneous, not only with the property of suspension, also with the property of colloid.Coal washing waste water is difficult nature clarification due to the above reasons, and
And supernatant is still the black liquor with suspended matters such as a large amount of coal slimes to this kind of waste water after precipitation, wherein processed containing coal separation
The harmful substances such as various additives and heavy metal in journey.The below standard discharge of a large amount of coal washing waste water, causes water pollution, river
Silt up, coal slime loss, also results in great water resource waste.There is no strictly distinguish above-mentioned coal mine water for most of coal mines
And/or coal washing waste water, but mix and handled into sewage treatment plant.
The conventional processes of coal mine water and/or coal washing waste water are " coagulating sedimentation+filtering " at present, using coagulant
(aluminium polychloride etc.) and high polymer coagulant (polyacrylamide etc.) and coal slime particle or coal slime colloid contact action neutralize coal
Low-surface-energy drops in the electrical property on mud surface, so that coal slime particle coagulation precipitates.The technique can remove a part of big coal particles,
Suspended matter, but there are still many drawbacks: coagulant, flocculant usage are big, and medicament is costly;Medicament has equipment certain
Corrosivity, once and flocculant excessive addition, subsequent advanced treating will be caused to seriously affect;Tiny particles content is removed
Effect is undesirable, is easy to cause Flushing nozzle fouling blockage;Effluent quality fluctuation is big, can not meet discharge and reuse standard etc..
ZL201611025222.4 discloses a kind of method of coal-contained wastewater processing, passes through one preliminary sedimentation tank of design and a tubular type
Microfiltration membrane system removes granule foreign tiny in waste water.But tube microfiltration membrane 1.5~4.0bar of system running pressure, according to
Alleviate fouling membrane by high surface velocity, simultaneously, tube microfiltration membrane system is easily contaminated for operation energy consumption height, and cleaning frequency is high.And it manages
The filter membrane system that declines can only remove tiny particles content, not can be removed various additives, coloration and heavy metal etc., and producing water water quality is low,
It is unable to satisfy high-quality water demand.
Summary of the invention
It is an object of the invention to overcome prior art defect, a kind of processing method of coal washing waste water is provided.
Technical scheme is as follows:
The processing method of a kind of coal mine water and/or coal washing waste water, it is characterised in that include the following steps:
(1) coal mine water and/or coal washing waste water are sent into conditioning tank, regulating water quality water obtains raw water;
(2) raw water is sent into flat ceramic membrane cisterna, is purified with flat ceramic membrane module, it is therein thin to completely remove
The turbidity of low-yield water drops in small particle;The method of operation of the flat ceramic membrane module is suction, stops and backwashing period sexual intercourse
For progress, every suction 8-9min stops 1-2min, every 30min-60min, carries out primary backwash to restore the initial of membrane flux
Value, while the lasting progress of aeration or intermittence carry out;The diaphragm precision of flat ceramic membrane module is 0.1-0.2 μm, and suction is born
Pressure is -5~-30KPa, membrane flux 100-500LMH;
(3) bed mud of above-mentioned flat ceramic membrane cisterna is fabricated to the coal washing mud cake that can be mixed with coal wind fuel, is formed again
Fuel realizes that recycling sludge utilizes;The production water of above-mentioned flat ceramic membrane module is subjected to advanced treating or as water in industry
Direct reuse (coal washery moisturizing, the dirt that goes out, coal yard spray, plant area's greening).
In a preferred embodiment of the invention, the material of the ceramic membrane is aluminium oxide, cordierite, carbonization
At least one of silicon and kaolin.
In a preferred embodiment of the invention, the time of the backwash is 30-60s, pressure 2bar, flux
For 200-1000LMH.
In a preferred embodiment of the invention, the gas-water ratio 10~20: 1 of the aeration, blower pressure 0.25-
0.35bar。
It is further preferred that the step (1) are as follows: coal mine water and/or coal washing waste water are sent into conditioning tank, adjust water
It is re-fed into preliminary sedimentation tank after matter water, by the substance of bulky grain by precipitating removal, raw water is obtained, the bed mud of preliminary sedimentation tank is made
The coal washing mud cake of Cheng Keyu coal wind fuel mixing, forms fuel again, realizes that recycling sludge utilizes.
Still more preferably, the hydraulic detention time in the preliminary sedimentation tank is 0.5-2h.
In a preferred embodiment of the invention, further include step (4): the production water of flat ceramic membrane module is sent into
The further impurity and purification of reverse osmosis membrane system, to remove various additives, coloration, heavy metal and organic pollution.
It is further preferred that the membrane flux of the reverse osmosis membrane is 15-18LMH, pressure 6-20bar, rate of recovery 60-
80%, reverse osmosis membrane dialyzate enters water producing tank, and concentrate is back to the flat ceramic membrane cisterna.
The beneficial effects of the present invention are:
1, processing method of the invention can not only remove large particle, and can effectively remove tiny particles content, be not necessarily to dosing,
The influence that elimination secondary pollution and medicament handle successive depths, gained bed mud concentrate SS content is higher, is easy to happen itself
Precipitating, sludge is more closely knit, more easy to handle, can reuse be used as fuel, realize recycling sludge utilization, gained producing water water quality is steady
It is fixed, meet reuse standard.
2, ceramic membrane of the invention is completely removed tiny particles content, and production water turbidity is low, and swabbing pressure is often below
80KPa, operating cost are low.Through calculating, 1.0 ten thousand ton/days for the treatment of capacities, the operating cost of ceramic membrane is only tubular ceramic membrane
1/4。
3, flat ceramic membrane module of the invention is directly dipped to membrane cisterna, compared with the tubular type micro-filtration of external, accounts for
Ground area is small, and contamination capacity is bigger, and cleaning frequency is low, and the contaminated rear cleaning of film is easier to restore.
4, the system operation energy consumption of processing method of the invention is low, and cleaning frequency is low.
5, reverse osmosis membrane of the invention can effectively remove various additives, coloration, heavy metal and organic pollution etc., improve
Producing water water quality can guarantee that high-quality produces water regardless of influent quality.
Detailed description of the invention
Fig. 1 is the process flow diagram of the embodiment of the present invention 1 and 2.
Specific embodiment
Technical solution of the present invention is further explained and described below by way of specific embodiment combination attached drawing.
Embodiment 1:
It is tested using Taiyuan, Shanxi coal mine water and/or coal washing waste water mixing water as raw water, influent quality has wave
It is dynamic, SS 1000-2500mg/L, COD 1-10mg/L, NH3- N value 2-6m/L, petroleum-type 2-3mgg/L, Fe 10-20mg/L, Mn
5-10mg/L, pH 7-7.5.
As shown in Figure 1, this Process operating parameters is as follows: raw water is directly entered flat ceramic membrane cisterna, plate after conditioning tank
Ceramic diaphragm material is silicon carbide, and aperture is 0.1 μm, and membrane module area is 25m2, every operation 9min, stops 1min, and suction is negative
Pressure is -10~-20KPa, membrane flux 400-500LMH.Every 60min is once backwashed, backwashing time 30s, and pressure is
2bar, backwash flux 1000LMH, after backwash, membrane flux can restore to 500LMH.Aeration is intermittent to carry out, film group
It is aerated and stops when part is aspirated, aeration carries out when membrane module stops suction, gas-water ratio 10: 1, blower pressure 0.3bar.
After the processing of flat ceramic membrane cisterna, assay plate ceramic membrane producing water water quality parameter, SS < 1mg/L, COD 1-
5mg/L, NH3- N value 2-6m/L, petroleum-type 0mg/L, Fe 3-5mg/L, Mn 2-5mg/L, pH 7-7.5.Ceramic membrane produces water
As water direct reuse in industry (coal washery moisturizing, the dirt that goes out, coal yard spray, plant area's greening).The bottom of above-mentioned flat ceramic membrane cisterna
When mud bed mud water content is excessively high, it can be dehydrated with folded spiral shell machine, make water content 70-85%, be further fabricated to bed mud
The coal washing mud cake that can be mixed with coal wind fuel forms fuel again, realizes that recycling sludge utilizes.
Embodiment 2:
It is tested using Zhengzhou, henan coal mine coal washing waste water as raw water, influent quality has fluctuation, SS 6000-
10000mg/L, COD 100-200mg/L, petroleum-type 5-8mg/L, pH 5.0-7.3.
As shown in Figure 1, this Process operating parameters is as follows: raw water is after conditioning tank, and into preliminary sedimentation tank, the water conservancy residence time is
1h。
Preliminary sedimentation tank supernatant enters flat ceramic membrane cisterna, and flat ceramic film sheet matter is aluminium oxide, and aperture is 0.2 μm, film
Component area is 50m2, every operation 8.5min stops 1.5min, and suction is -10~-30KPa, membrane flux 100-
350LMH.Every 30min is once backwashed, backwashing time 60s, pressure 2bar, backwash flux 700LMH, recoil
After washing, membrane flux can restore to 350LMH.Aeration is lasting to carry out, gas-water ratio 20: 1, blower pressure 0.3bar.
After the processing of flat ceramic membrane cisterna, assay plate ceramic membrane producing water water quality parameter, SS < 1mg/L, COD 50-
100mg/L, petroleum-type 0mg/L, pH 5.0-7.3, turbidity 0.1-0.5NTU.Ceramic membrane dialyzate can be used as in industry
Water reuse (coal washery moisturizing, the dirt that goes out, coal yard spray, plant area's greening).
Ceramic membrane produces water using the further impurity and purification of reverse osmosis membrane system.RO membrane flux: 15-18LMH, pressure
Power: 15bar, the rate of recovery: 70%.RO film dialyzate enters water producing tank, and concentrate is back to flat ceramic membrane cisterna.It is saturating to measure RO film
Analyse liquid water quality parameter, COD 5-10mg/L, petroleum-type 0mg/L, pH 5.0-7.3, turbidity 0NTU.RO film dialyzate meets high
Quality water demand (bathing, prepares medicament at cooling water), a part of water is as the backwash of flat ceramic membrane module and RO film and clear
Scouring water.When the bed mud bed mud water content in above-mentioned preliminary sedimentation tank and ceramic membrane pond is excessively high, it can be dehydrated with folded spiral shell machine, make to contain
Water is 70-85%, and bed mud is further fabricated to the coal washing mud cake that can be mixed with coal wind fuel, forms fuel again, real
Existing recycling sludge utilizes.
Each bed mud in above-described embodiment is thick sludge, and the sludge in this stage is pumped into height with sludge feed pump
It presses in sludge filter press, machinery is carried out to sludge and is pressed dry, form moisture content in 35% or so coal washing mud cake, there is combustion abundant
Value, can mix with coal wind fuel, form fuel again, realize that recycling sludge utilizes.
The foregoing is only a preferred embodiment of the present invention, the range that the present invention that therefore, it cannot be limited according to is implemented, i.e.,
Equivalent changes and modifications made in accordance with the scope of the invention and the contents of the specification should still be within the scope of the present invention.
Claims (8)
1. the processing method of a kind of coal mine water and/or coal washing waste water, characterized by the following steps:
(1) coal mine water and/or coal washing waste water are sent into conditioning tank, regulating water quality water obtains raw water;
(2) raw water is sent into flat ceramic membrane cisterna, is purified with flat ceramic membrane module, to completely remove tiny therein
The turbidity of low-yield water, drops in grain object;The method of operation of the flat ceramic membrane module be suction, stop with backwashing period alternately into
Row, every suction 8-9min stop 1-2min, every 30min-60min, carry out primary backwash to restore the initial value of membrane flux,
It is aerated lasting progress simultaneously or intermittence carries out;The diaphragm precision of flat ceramic membrane module is 0.1-0.2 μm, the negative pressure of suction
For -5~-30KPa, membrane flux 100-500LMH;
(3) bed mud of above-mentioned flat ceramic membrane cisterna is fabricated to the coal washing mud cake that can be mixed with coal wind fuel, forms fuel again,
Realize that recycling sludge utilizes;The production water of above-mentioned flat ceramic membrane module is subjected to advanced treating or is directly returned as water in industry
With.
2. processing method as described in claim 1, it is characterised in that: the material of the ceramic membrane is aluminium oxide, violet blueness
At least one of stone, silicon carbide and kaolin.
3. processing method as described in claim 1, it is characterised in that: the time of the backwash is 30-60s, and pressure is
2bar, flux 200-1000LMH.
4. processing method as described in claim 1, it is characterised in that: the gas-water ratio 10~20: 1 of the aeration, blower pressure
0.25-0.35bar。
5. the processing method as described in any claim in Claims 1-4, it is characterised in that: the step (1) are as follows: will
Coal mine water and/or coal washing waste water are sent into conditioning tank, preliminary sedimentation tank are re-fed into after regulating water quality water, by the substance of bulky grain
It is removed by precipitating, obtains raw water, the bed mud of preliminary sedimentation tank is fabricated to the coal washing mud cake that can be mixed with coal wind fuel, is formed again
Fuel realizes that recycling sludge utilizes.
6. processing method as claimed in claim 5, it is characterised in that: the hydraulic detention time in the preliminary sedimentation tank is 0.5-
2h。
7. processing method as described in claim 1, it is characterised in that: further include step (4): by the production of flat ceramic membrane module
Water is sent into the further impurity and purification of reverse osmosis membrane system, to remove various additives, coloration, heavy metal and organic pollution.
8. processing method as claimed in claim 7, it is characterised in that: the membrane flux of the reverse osmosis membrane is 15-18LMH, pressure
Power is 6-20bar, rate of recovery 60-80%, and reverse osmosis membrane dialyzate enters water producing tank, and concentrate is back to the flat ceramic
Membrane cisterna.
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111392921A (en) * | 2020-05-18 | 2020-07-10 | 范誉委 | Comprehensive treatment process for coal washing wastewater and mine wastewater |
CN111392922A (en) * | 2020-05-18 | 2020-07-10 | 范誉委 | Coal washing wastewater and mine wastewater comprehensive treatment system |
CN112194334A (en) * | 2020-09-25 | 2021-01-08 | 南京工业大学 | Method for dehydrating materialized sludge |
CN112794496A (en) * | 2020-12-25 | 2021-05-14 | 国家能源投资集团有限责任公司 | Method and system for removing suspended matters and recycling coal slime from mine water |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111392921A (en) * | 2020-05-18 | 2020-07-10 | 范誉委 | Comprehensive treatment process for coal washing wastewater and mine wastewater |
CN111392922A (en) * | 2020-05-18 | 2020-07-10 | 范誉委 | Coal washing wastewater and mine wastewater comprehensive treatment system |
CN112194334A (en) * | 2020-09-25 | 2021-01-08 | 南京工业大学 | Method for dehydrating materialized sludge |
CN112794496A (en) * | 2020-12-25 | 2021-05-14 | 国家能源投资集团有限责任公司 | Method and system for removing suspended matters and recycling coal slime from mine water |
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Application publication date: 20190111 |