CN109174213A - Multifunctional operating box for mercurous device safety operation and mercury solution environmental protection recycling - Google Patents
Multifunctional operating box for mercurous device safety operation and mercury solution environmental protection recycling Download PDFInfo
- Publication number
- CN109174213A CN109174213A CN201811190508.7A CN201811190508A CN109174213A CN 109174213 A CN109174213 A CN 109174213A CN 201811190508 A CN201811190508 A CN 201811190508A CN 109174213 A CN109174213 A CN 109174213A
- Authority
- CN
- China
- Prior art keywords
- mercury
- mercurous
- environmental protection
- treatment trough
- safety operation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 title claims abstract description 69
- 229910052753 mercury Inorganic materials 0.000 title claims abstract description 69
- 238000004064 recycling Methods 0.000 title claims abstract description 22
- 230000007613 environmental effect Effects 0.000 title claims abstract description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 28
- 238000004140 cleaning Methods 0.000 claims abstract description 20
- 239000011347 resin Substances 0.000 claims abstract description 8
- 229920005989 resin Polymers 0.000 claims abstract description 8
- 239000000243 solution Substances 0.000 claims description 28
- 238000010521 absorption reaction Methods 0.000 claims description 4
- 239000008367 deionised water Substances 0.000 claims description 4
- 229910021641 deionized water Inorganic materials 0.000 claims description 4
- 239000011521 glass Substances 0.000 claims description 4
- 239000000463 material Substances 0.000 claims description 4
- 238000012545 processing Methods 0.000 claims description 4
- 239000007864 aqueous solution Substances 0.000 claims description 3
- 239000003599 detergent Substances 0.000 claims description 3
- 238000010348 incorporation Methods 0.000 claims description 2
- 238000009434 installation Methods 0.000 claims description 2
- 238000000034 method Methods 0.000 description 8
- 239000003921 oil Substances 0.000 description 5
- 239000000523 sample Substances 0.000 description 4
- 238000013461 design Methods 0.000 description 2
- 238000007654 immersion Methods 0.000 description 2
- 238000002347 injection Methods 0.000 description 2
- 239000007924 injection Substances 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 208000008763 Mercury poisoning Diseases 0.000 description 1
- 206010027439 Metal poisoning Diseases 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 1
- 239000005864 Sulphur Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000005266 casting Methods 0.000 description 1
- 230000006837 decompression Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 210000002249 digestive system Anatomy 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 239000010720 hydraulic oil Substances 0.000 description 1
- 238000001727 in vivo Methods 0.000 description 1
- 239000006101 laboratory sample Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000010408 sweeping Methods 0.000 description 1
- 238000009423 ventilation Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01L—CHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
- B01L1/00—Enclosures; Chambers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01L—CHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
- B01L1/00—Enclosures; Chambers
- B01L1/50—Enclosures; Chambers for storing hazardous materials in the laboratory, e.g. cupboards, waste containers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B3/00—Cleaning by methods involving the use or presence of liquid or steam
- B08B3/02—Cleaning by the force of jets or sprays
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B3/00—Cleaning by methods involving the use or presence of liquid or steam
- B08B3/04—Cleaning involving contact with liquid
- B08B3/10—Cleaning involving contact with liquid with additional treatment of the liquid or of the object being cleaned, e.g. by heat, by electricity or by vibration
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01L—CHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
- B01L2200/00—Solutions for specific problems relating to chemical or physical laboratory apparatus
- B01L2200/06—Fluid handling related problems
- B01L2200/0631—Purification arrangements, e.g. solid phase extraction [SPE]
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01L—CHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
- B01L2200/00—Solutions for specific problems relating to chemical or physical laboratory apparatus
- B01L2200/14—Process control and prevention of errors
- B01L2200/141—Preventing contamination, tampering
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01L—CHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
- B01L2200/00—Solutions for specific problems relating to chemical or physical laboratory apparatus
- B01L2200/16—Reagents, handling or storing thereof
Abstract
Multifunctional operating box for mercurous device safety operation and mercury solution environmental protection recycling, including three workspaces, three workspaces are divided into disassembly area, hot water cleaning area and depth cleaning area, three workspaces are respectively arranged with treatment trough, it is interconnected between each treatment trough, connectivity part is provided with outlet pipe, outlet pipe is located at the position apart from groove top end one third slot body, three treatment troughs from left to right arrange from high to low, the water of depth cleaning area discharge is connected to mercury by pipeline and adsorbs in resin box, the present invention has easily operated, device suitable for mercurous device safety operation and environmental protection recycling, the characteristics of realizing mercury solution safety operation and recycling.
Description
Technical field
The present invention relates to safety and environmental protection equipment manufacturing technology fields, in particular to are used for mercurous device safety operation and mercury solution
The Multifunctional operating box of environmental protection recycling.
Background technique
Since mercurous device is still widely used in the fields such as chemical industry, metallurgical casting and medical treatment, and mercury is accidentally
It will form very subtle little particle after being spread across ground, be attached to wall, clothing, on ground, if without processing following several
It is always existed in the even time of decades in year.The currently used method for dropping mercury that handles is to spread one layer again on removing the mercury fallen
Sulphur powder makes mercuric sulphide, to reduce its volatilization.But adopt this method very big, that is, be not easily recycled
It using mercury, and handles not clean thorough enough, still has part mercury that can evaporate into air.Mercury can not only be breathed by skin
Organ or digestive system enter in vivo, are detrimental to health, the mercury vapour of high concentration can also make one to be poisoned through the air,
And this is the major way for causing human body mercury poisoning.Even if being mounted with ventilation device of good performance, mercuryvapour is discharged to the outside
Still outside air can be polluted, against the environmentally protective theory in laboratory.For the safe handling of specification mercury, national duty
Industry safety and health, environmental protection department all establish the rule and standard for being suitable for contacting practitioner's health and safety of mercury.
Still it is suitable for the safety operation of laboratory mercury without a set of safe and reliable method and apparatus at present.International well-known pressure
Merck & Co., Inc of the U.S. of Gong Yi manufacturer is also without the operation of matched mercury solution, recyclable device.Therefore, development is a set of safely, conveniently to tear open
Mercury injection apparatus dilatometer is washed, mercury solution volatilization is thoroughly avoided, drops, and effectively recycling the device of mercury solution is a significantly work
Make.
Summary of the invention
In order to overcome the above-mentioned deficiencies of the prior art, the purpose of the present invention is to provide for mercurous device safety operation with
The Multifunctional operating box of mercury solution environmental protection recycling has easily operated dress suitable for mercurous device safety operation and environmental protection recycling
The characteristics of setting, realizing mercury solution safety operation and recycling.
To achieve the goals above, the technical solution adopted by the present invention is that:
It is described for the Multifunctional operating box of mercurous device safety operation and mercury solution environmental protection recycling, including three workspaces
Three workspaces be followed successively by disassembly area, hot water cleaning area and depth cleaning area, three workspaces are respectively arranged with treatment trough, phase
It is interconnected between adjacent treatment trough, connectivity part is provided with outlet pipe 15, and outlet pipe 15 is located at apart from groove top end one third slot body
Position, disassembly area, hot water cleaning area and depth cleaning area treatment trough from left to right arrange from high to low, the depth is clear
The water for washing area's discharge is connected to mercury by pipeline and adsorbs in resin box 11.
The 15 ° of settings of inclination upwards of the outlet pipe 15 of each treatment trough.
15 side of outlet pipe is equipped with stabilier 7.
The treatment trough uses transparent organic glass material, and the top for the treatment of trough is the pros of 400 × 400 × 400mm
Body, lower part are designed as cone-shaped collection area, and all seamed edges in the treatment trough all do fillet processing.
The cone-shaped collection area bottom sets valve 13, mercury collection vessel 14 is placed below slot, each treatment trough left side is all
Equipped with oil discharge outlet 3, height is flushed with 15 position of outlet pipe on right side；The greasy dirt that the oil discharge outlet 3 is discharged, which collects, flows into mercury suction
Attached resin box 11, mercury absorption 11 bottom of resin box are provided with greasy dirt collection vessel 12.
The collection vessel 12 of the mercury solution collection vessel 14 and greasy dirt is placed on lifting platform 19.
Control valve 20 is equipped on the outlet pipe 15 and oil discharge outlet 3.
Each treatment trough is provided with support arm 4, fixture 1 and spanner 5, and support arm 4 is for fixing mercurous device 6, fixture 1
It can be used for the installation and removal of device with spanner 5；It is equipped with plastic septum 10 among the treatment trough, is used for placement operation tool 5
With vessel 8.
The row's of placement mercury beaker 8 and mercurous sample beaker 9 in disassembly area treatment trough.
Aqueous solution equipped with incorporation detergent in the treatment trough of the hot water cleaning area, rinse bath top elute head equipped with hot water
17。
Pure water or deionized water, preferably deionized water are housed in the treatment trough of the depth cleaning area, matched above rinse bath
There is pure water to elute head 18.
Beneficial effects of the present invention:
(1) it is designed using immersion water-stop, avoids mercury in operating process to be exposed to the volatilization in air completely, and operate
The mercury that process is dropped directly recycles in water-stop, avoids security risk；
(2) it is designed using with the support arm of sink one, is effectively reduced and is beaten due to caused by the be stained with hydraulic oil of device outer wall
The sliding and accident that fractures (dilatometer in such as mercury injection apparatus).Even if fractureing accident, a large amount of mercury solutions of outflow can also be in watertight
It is all directly recycled in envelope, avoids waste and environmental pollution.
(3) ad hoc greasy dirt outlet can be such that the greasy dirt sticked directly recycles with the mercury drop wherein swept along, avoid oil completely
Secondary pollution that is dirty and sweeping along mercury to drip.
(4) stabilier and Overruning water out design, it is therefore prevented that upper layer greasy dirt enters drainage pipeline, while can make in water
The mercury drop spread of escaping has the sufficient sedimentation time in gentle water flow, and mercury drop is avoided to flow out with waste water.
(5) outlet pipe uses upward 15 ° of inclined designs, avoids the deposition of Residual Mercury in outlet conduit, makes wherein mercury drop
It can directly backflow to slot bottom.
(6) it dismantles slot and sink all uses organic glass material, observation is easy to operate, at low cost.
Detailed description of the invention
Fig. 1 is the structural diagram of the present invention.
Specific embodiment
The present invention is described in further detail below in conjunction with the accompanying drawings.
As shown in Figure 1: 1, realize that disassembly, cleaning and depth to mercurous device are cleaned by three workspaces；2, pass through
The conical region for handling trench bottom realizes the recycling of mercury；3, the mode operated by using immersion water-stop, it is entirely avoided
Mercury is directly exposed to the volatilization of air；4, suction of the resin box stiffening device to mercury is adsorbed by the way that mercury is arranged in water outlet and oil outlet
It is attached；5, by the way that 15 ° of water outlets and stabilier are arranged in the treatment trough of three connections, guarantee mercury solution filling in currently processed slot
Fractional precipitation；4, treatment trough uses material based on transparent organic glass, observes convenient for operator.
Working principle of the present invention:
Dilatometer is fixed on support arm 4 in the treatment trough in disassembly area by operator first, using tool by sealing ring
It is unscrewed with metal cover, can avoid fractureing due to sample cell caused by skidding.After the metal cover of dilatometer is opened, pressure reduces,
Inflow is placed in row's mercury beaker 8 immediately below it by most of mercury solution in pipe, this part mercury solution can directly recycle use.But
Not all mercury being pressed into can be discharged in decompression process, and a small amount of mercury still can remain or get deeply stuck in the sample, this portion
Divide mercury solution that will be introduced into mercurous sample beaker 9 together with laboratory sample, to further clean and recycle.After being dissembled
Dilatometer will be moved in the treatment trough of hot water cleaning area, and the aqueous solution that detergent has been impregnated in the treatment trough in the area is filled,
Head 17 is eluted equipped with hot water above rinse bath, for the greasy dirt and Residual Mercury of each component of dilatometer after clean-drain.Then will
Dilatometer is transferred to depth cleaning area, elutes head 18 equipped with pure water above area's treatment trough, dilatometer is further cleaned dry
After net, it can directly take away and do drying and processing, in case next time uses.In cleaning process, the mercury solution that is accidentally spilled into each sink
It can deposit to bottom of gullet, when running up to a certain amount of, the control valve 20 of openable trench bottom is recycled.The receipts of mercury solution and greasy dirt
Collection container is placed on a lifting platform, to guarantee that safety picks and places.
Claims (10)
1. the Multifunctional operating box for mercurous device safety operation and mercury solution environmental protection recycling, which is characterized in that including three works
Make area, three workspaces are followed successively by disassembly area, hot water cleaning area and depth cleaning area, three workspaces and are respectively arranged with
Treatment trough is interconnected between adjacent treatment trough, and connectivity part is provided with outlet pipe (15), and outlet pipe (15) is located at apart from groove top end
The treatment trough of the position of one third slot body, disassembly area, hot water cleaning area and depth cleaning area from left to right arranges from high to low,
The water of the depth cleaning area discharge is connected in mercury absorption resin box (11) by pipeline.
2. the Multifunctional operating box according to claim 1 for mercurous device safety operation and mercury solution environmental protection recycling,
It is characterized in that, the 15 ° of settings of inclination upwards of the outlet pipe (15) of each treatment trough.
3. the Multifunctional operating box according to claim 1 for mercurous device safety operation and mercury solution environmental protection recycling,
It is characterized in that, outlet pipe (15) side is equipped with stabilier (7).
4. the Multifunctional operating box according to claim 1 for mercurous device safety operation and mercury solution environmental protection recycling,
It is characterized in that, the treatment trough uses transparent organic glass material, and the top for the treatment of trough is the pros of 400 × 400 × 400mm
Body, lower part are designed as cone-shaped collection area, and all seamed edges in the treatment trough all do fillet processing.
5. the Multifunctional operating box according to claim 4 for mercurous device safety operation and mercury solution environmental protection recycling,
It is characterized in that, the cone-shaped collection area bottom is set valve (13), places mercury collection vessel (14) below slot, and each treatment trough is left
Side is designed with oil discharge outlet (3), and height is flushed with outlet pipe (15) position on right side；The greasy dirt of oil discharge outlet (3) discharge converges
Collection flows into mercury absorption resin box (11), and mercury absorption resin box (11) bottom is provided with greasy dirt collection vessel (12)；
The collection vessel (12) of the mercury solution collection vessel (14) and greasy dirt is placed on lifting platform (19).
6. the Multifunctional operating box according to claim 5 for mercurous device safety operation and mercury solution environmental protection recycling,
It is characterized in that, is equipped with control valve (20) on the outlet pipe (15) and oil discharge outlet (3).
7. the Multifunctional operating box according to claim 1 for mercurous device safety operation and mercury solution environmental protection recycling,
It is characterized in that, each treatment trough is provided with support arm (4), fixture (1) and spanner (5), and support arm (4) is for fixing mercurous device
Part (6), fixture (1) and spanner (5) can be used for the installation and removal of device；Plastic septum (10) are equipped among the treatment trough,
For placement operation tool (5) and vessel (8).
8. the Multifunctional operating box according to claim 1 for mercurous device safety operation and mercury solution environmental protection recycling,
It is characterized in that, the row of placement mercury beaker (8) and mercurous sample beaker (9) in disassembly area treatment trough.
9. the Multifunctional operating box according to claim 1 for mercurous device safety operation and mercury solution environmental protection recycling,
It is characterized in that, the aqueous solution equipped with incorporation detergent in the treatment trough of the hot water cleaning area, is eluted above rinse bath equipped with hot water
Head (17).
10. the Multifunctional operating box according to claim 1 for mercurous device safety operation and mercury solution environmental protection recycling,
It is characterized in that, pure water or deionized water, preferably deionized water is housed in the treatment trough of the depth cleaning area, matched above rinse bath
There is pure water to elute head (18).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811190508.7A CN109174213A (en) | 2018-10-12 | 2018-10-12 | Multifunctional operating box for mercurous device safety operation and mercury solution environmental protection recycling |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811190508.7A CN109174213A (en) | 2018-10-12 | 2018-10-12 | Multifunctional operating box for mercurous device safety operation and mercury solution environmental protection recycling |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109174213A true CN109174213A (en) | 2019-01-11 |
Family
ID=64948262
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811190508.7A Pending CN109174213A (en) | 2018-10-12 | 2018-10-12 | Multifunctional operating box for mercurous device safety operation and mercury solution environmental protection recycling |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109174213A (en) |
Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20110024364A1 (en) * | 2009-07-31 | 2011-02-03 | Kuo-Yuan Chang | Filtration separation method for waste resin containing highly radioactive uranium powder and device thereof |
| CN102350377A (en) * | 2011-09-08 | 2012-02-15 | 杭州泰林生物技术设备有限公司 | Negative-pressure barrier system |
| CN202888112U (en) * | 2012-09-18 | 2013-04-17 | 广东巨洋集团有限公司 | Recovery installation for fluorescent lamp containing mercury with washing unit |
| CN206276401U (en) * | 2016-12-08 | 2017-06-27 | 四川国际旅行卫生保健中心 | A kind of multifunctional bio safety cabinet |
| CN107020168A (en) * | 2017-04-11 | 2017-08-08 | 中国科学院武汉岩土力学研究所 | It is a kind of dedicated for placing the workbench containing mercury instrument |
| CN206716667U (en) * | 2017-04-11 | 2017-12-08 | 李剑 | A kind of chemical examination operation device for poisonous sample |
| CN207441649U (en) * | 2017-10-27 | 2018-06-01 | 湖北凯昌光电科技有限公司 | A kind of mercury retracting device of mercurous mercury lamp |
| CN108097345A (en) * | 2017-12-28 | 2018-06-01 | 赣州市亿研机械设计研究院有限公司 | A kind of chemistry teaching experimental bench |
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| CN209438620U (en) * | 2018-10-12 | 2019-09-27 | 清华大学 | Multifunctional operating box for mercurous device safety operation and mercury solution environmental protection recycling |
-
2018
- 2018-10-12 CN CN201811190508.7A patent/CN109174213A/en active Pending
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|---|---|---|---|---|
| US20110024364A1 (en) * | 2009-07-31 | 2011-02-03 | Kuo-Yuan Chang | Filtration separation method for waste resin containing highly radioactive uranium powder and device thereof |
| CN102350377A (en) * | 2011-09-08 | 2012-02-15 | 杭州泰林生物技术设备有限公司 | Negative-pressure barrier system |
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