CN109173998A - A kind of air purifier special purification sterilization material and preparation method thereof - Google Patents
A kind of air purifier special purification sterilization material and preparation method thereof Download PDFInfo
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- CN109173998A CN109173998A CN201811146205.5A CN201811146205A CN109173998A CN 109173998 A CN109173998 A CN 109173998A CN 201811146205 A CN201811146205 A CN 201811146205A CN 109173998 A CN109173998 A CN 109173998A
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- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
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- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01N47/42—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having a double or triple bond to nitrogen, e.g. cyanates, cyanamides containing —N=CX2 groups, e.g. isothiourea
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- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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Abstract
The invention discloses a kind of air purifier special purification sterilization materials and preparation method thereof, the air purifier special purification sterilization material constitutive material includes: that 25~40 parts of active carbon, 8~16 parts of nano silver, 4~10 parts of titanium dioxide, 6~14 parts of carragheen, 10~30 parts of high rare earth, D-araboascorbic acid receive 4~8 parts, 10~20 parts of sodium benzoate and 10~16 parts of streptomysin, and all raw materials calculate by weight；The air purifier special purification sterilization material preparation method is the following steps are included: the preparation of adsorbing base, the preparation of mixture A, the preparation of mixture B and the preparation of purification and sterilization material, described a kind of air purifier special purification sterilization material and preparation method thereof is reasonable, the product of production has good antibacterial and adsorbs the performance of toxic gas, is worth promoting and using in household sphere of life.
Description
Technical field
The present invention relates to household environment-friendlywater field, specifically a kind of air purifier special purification sterilization material and its preparation side
Method.
Background technique
With the development of society, in recent years, the daily production and living of the mankind activity polluted caused by atmosphere it is also more next
It is more serious, lead to greenhouse effects and PM2.5 concentration Continued, compared with thicker Atmospheric particulates, PM2.5 partial size is small,
Area is big, and activity is strong, easily subsidiary poisonous and harmful substances, and residence time in an atmosphere is long, conveying distance is remote, thus to people
The influence of body health and atmosphere quality is bigger.
As people are for the close attention of environmental pollution and the attention of own health, it was recognized that itself breathing is empty
The importance of gas sanitation and hygiene, so in household office life, air purifier using more more and more universal, and then push
The development and growth in air purifier market, the core of air purifier are exactly material for air purification.
The present invention is intended to provide a kind of air purifier special purification sterilization material and preparation method thereof.
Summary of the invention
The purpose of the present invention is to provide a kind of air purifier special purification sterilization materials and preparation method thereof, to solve
The problems mentioned above in the background art.
To achieve the above object, the invention provides the following technical scheme:
A kind of air purifier special purification sterilization material, constitutive material include: 25~40 parts of active carbon, nano silver 8~16
Part, 4~10 parts of titanium dioxide, 6~14 parts of carragheen, 10~30 parts of high rare earth, D-araboascorbic acid receive 4~8 parts, sodium benzoate
10~20 parts and 10~16 parts of streptomysin, all raw materials calculate by weight.
The preparation method of the air purifier special purification sterilization material the following steps are included:
(1) preparation of adsorbing base: the high rare earth in part and active carbon mixing are ground, 140 meshes are crossed after the completion of grinding, so
Carragheen is added in the mixture of the high rare earth and active carbon of completing grinding operation afterwards, keeps its bonding blocking, after the completion of bonding
Operation is dried in drying box, 1~3h is dried at a temperature of 70 DEG C, it is spare that adsorbing base is made after completion drying operation.
(2) preparation of mixture A: nano silver is mixed with 8~10 times of its quality of neutral water, and is stirred using stirring rod
The sufficiently obtained Nano silver solution of mixing, high rare earth remaining in step (1) is received with D-araboascorbic acid and is uniformly mixed, addition is received
In the silver-colored solution of rice, it is placed in reaction vessel and reacts, the reaction condition setting of reaction vessel are as follows: 53~64 DEG C of temperature, reaction vessel
Mixture A is made in sealing, 1.2~1.6h of reaction time after the reaction was completed.
(3) preparation of mixture B: sodium benzoate and streptomysin are uniformly mixed, toward the mixing of sodium benzoate and streptomysin
Titanium dioxide is added in object, mixture one is made, then mixture one is added in the ethanol solution of 6~8 times of its quality, 45
1.4~1.8h of stir process is sealed under conditions of~60 DEG C, and mixture B is made.
(4) prepared by purification and sterilization material: at 45~60 DEG C after mixture A is mixed with mixture B, ultrasonic power 600
It is ultrasonically treated 30~40min under conditions of~800W, operation is dried after the completion of ultrasonic treatment, in 80~100 DEG C of condition
1.2~1.6h of lower drying is ground into particle using micronizer after the completion of drying, and granularity size requirements were 160 mesh；Make
Adsorbing base aperture is given with drilling machine, then requires to meet to the granularity of adsorbing base filling mixture A and mixture B mixed
Object is closed, is finally compressed using compactor up to purification and sterilization material.
As a further solution of the present invention: micronizer model WFJ-20 used in step (4), discharge grain
Degree is 80-320mesh, and compared with common grinder, discharging-material size is more fine.
As further scheme of the invention: solidifying in the air purifier special purification sterilization material constitutive material
Gu agent is carragheen, compared with other coagulators, carragheen stability is strong, dry powder place for a long time it is not degradable, neutral and
It is also very stable in alkaline solution, it will not be hydrolyzed heating, be suitble to do adsorbing base.
Compared with prior art, the beneficial effects of the present invention are:
A kind of air purifier special purification sterilization material raw material composition is reasonable, nano silver, sodium benzoate and strepto-
Element all has good bactericidal effect；Active carbon has good suction-operated；The air purifier special purification sterilizes material
Expect that the coagulator in constitutive material is carragheen, compared with other coagulators, carragheen stability is strong, and dry powder is placed be not easy for a long time
Degradation, it is also very stable in neutral and alkaline solution, it will not be hydrolyzed heating, be suitble to do adsorbing base.
A kind of air purifier special purification sterilization material preparation method design is reasonable, the micronizer used
Model WFJ-20, discharging-material size 80-320mesh, compared with common grinder, discharging-material size is more fine.
Described a kind of air purifier special purification sterilization material and preparation method thereof is worth pushing away in household environment protection field
Extensively with use.
Detailed description of the invention
Fig. 1 is a kind of preparation method process flow chart of air purifier special purification sterilization material.
Specific embodiment
Technical solution of the present invention is described in more detail With reference to embodiment.
Embodiment 1
A kind of air purifier special purification sterilization material, constitutive material include: 25 parts of active carbon, 8 parts of nano silver, titanium dioxide
4 parts of titanium, 6 parts of carragheen, 10 parts of high rare earth, D-araboascorbic acid receive 4 parts, 10 parts of sodium benzoate and 10 parts of streptomysin, own
Raw material calculates by weight.
The preparation method of the air purifier special purification sterilization material the following steps are included:
(1) preparation of adsorbing base: the high rare earth in part and active carbon mixing are ground, 140 meshes are crossed after the completion of grinding, so
Carragheen is added in the mixture of the high rare earth and active carbon of completing grinding operation afterwards, keeps its bonding blocking, after the completion of bonding
Operation is dried in drying box, 1h is dried at a temperature of 70 DEG C, it is spare that adsorbing base is made after completion drying operation.
(2) preparation of mixture A: nano silver is mixed with 8 times of its quality of neutral water, and is stirred using stirring rod
Sufficiently obtained Nano silver solution, high rare earth remaining in step (1) is received with D-araboascorbic acid and is uniformly mixed, nano silver is added
In solution, it is placed in reaction vessel and reacts, the reaction condition setting of reaction vessel are as follows: 53 DEG C of temperature, reaction vessel sealing, reaction
Mixture A is made in time 1.2h after the reaction was completed.
(3) preparation of mixture B: sodium benzoate and streptomysin are uniformly mixed, toward the mixing of sodium benzoate and streptomysin
Titanium dioxide is added in object, mixture one is made, then mixture one is added in the ethanol solution of 6 times of its quality, at 45 DEG C
Under the conditions of sealing stir process 1.4h be made mixture B.
(4) prepared by purification and sterilization material: at 45 DEG C after mixture A is mixed with mixture B, ultrasonic power is the item of 600W
It is ultrasonically treated 30min under part, operation is dried after the completion of ultrasonic treatment, dry 1.2h, dry to complete under conditions of 80 DEG C
It is ground into particle using micronizer afterwards, granularity size requirements were 160 mesh；Adsorbing base aperture is given using drilling machine,
Then the mixture met is required to the granularity of adsorbing base filling mixture A and mixture B, is finally compressed using compactor
Up to purification and sterilization material.
Micronizer model WFJ-20, discharging-material size 80-320mesh used in step (4).
Embodiment 2
A kind of air purifier special purification sterilization material, constitutive material include: 40 parts of active carbon, 16 parts of nano silver, dioxy
Change 10 parts of titanium, 14 parts of carragheen, 30 parts of high rare earth, D-araboascorbic acid receive 8 parts, 20 parts of sodium benzoate and 16 parts of streptomysin,
All raw materials calculate by weight.
The preparation method of the air purifier special purification sterilization material the following steps are included:
(1) preparation of adsorbing base: the high rare earth in part and active carbon mixing are ground, 140 meshes are crossed after the completion of grinding, so
Carragheen is added in the mixture of the high rare earth and active carbon of completing grinding operation afterwards, keeps its bonding blocking, after the completion of bonding
Operation is dried in drying box, 3h is dried at a temperature of 70 DEG C, it is spare that adsorbing base is made after completion drying operation.
(2) preparation of mixture A: nano silver is mixed with 10 times of its quality of neutral water, and is stirred and mixed using stirring rod
Sufficiently obtained Nano silver solution is closed, high rare earth remaining in step (1) is received with D-araboascorbic acid and is uniformly mixed, nanometer is added
In silver-colored solution, it is placed in reaction vessel and reacts, the reaction condition setting of reaction vessel are as follows: 64 DEG C of temperature, reaction vessel sealing, instead
Mixture A is made in 1.6h between seasonable after the reaction was completed.
(3) preparation of mixture B: sodium benzoate and streptomysin are uniformly mixed, toward the mixing of sodium benzoate and streptomysin
Titanium dioxide is added in object, mixture one is made, then mixture one is added in the ethanol solution of 8 times of its quality, at 60 DEG C
Under the conditions of sealing stir process 1.8h be made mixture B.
(4) prepared by purification and sterilization material: at 60 DEG C after mixture A is mixed with mixture B, ultrasonic power is the item of 800W
It is ultrasonically treated 40min under part, operation is dried after the completion of ultrasonic treatment, dry 1.6h, dry to complete under conditions of 100 DEG C
It is ground into particle using micronizer afterwards, granularity size requirements were 160 mesh；Adsorbing base aperture is given using drilling machine,
Then the mixture met is required to the granularity of adsorbing base filling mixture A and mixture B, is finally compressed using compactor
Up to purification and sterilization material.
Micronizer model WFJ-20, discharging-material size 80-320mesh used in step (4).
Embodiment 3
A kind of air purifier special purification sterilization material, constitutive material include: 30 parts of active carbon, 12 parts of nano silver, dioxy
Change 7 parts of titanium, 10 parts of carragheen, 20 parts of high rare earth, D-araboascorbic acid receive 6 parts, 15 parts of sodium benzoate and 13 parts of streptomysin, institute
There is raw material to calculate by weight.
The preparation method of the air purifier special purification sterilization material the following steps are included:
(1) preparation of adsorbing base: the high rare earth in part and active carbon mixing are ground, 140 meshes are crossed after the completion of grinding, so
Carragheen is added in the mixture of the high rare earth and active carbon of completing grinding operation afterwards, keeps its bonding blocking, after the completion of bonding
Operation is dried in drying box, 2h is dried at a temperature of 70 DEG C, it is spare that adsorbing base is made after completion drying operation.
(2) preparation of mixture A: nano silver is mixed with 9 times of its quality of neutral water, and is stirred using stirring rod
Sufficiently obtained Nano silver solution, high rare earth remaining in step (1) is received with D-araboascorbic acid and is uniformly mixed, nano silver is added
In solution, it is placed in reaction vessel and reacts, the reaction condition setting of reaction vessel are as follows: 59 DEG C of temperature, reaction vessel sealing, reaction
Mixture A is made in time 1.4h after the reaction was completed.
(3) preparation of mixture B: sodium benzoate and streptomysin are uniformly mixed, toward the mixing of sodium benzoate and streptomysin
Titanium dioxide is added in object, mixture one is made, then mixture one is added in the ethanol solution of 7 times of its quality, at 50 DEG C
Under the conditions of sealing stir process 1.6h be made mixture B.
(4) prepared by purification and sterilization material: at 50 DEG C after mixture A is mixed with mixture B, ultrasonic power is the item of 700W
It is ultrasonically treated 35min under part, operation is dried after the completion of ultrasonic treatment, dry 1.4h, dry to complete under conditions of 90 DEG C
It is ground into particle using micronizer afterwards, granularity size requirements were 160 mesh；Adsorbing base aperture is given using drilling machine,
Then the mixture met is required to the granularity of adsorbing base filling mixture A and mixture B, is finally compressed using compactor
Up to purification and sterilization material.
Micronizer model WFJ-20, discharging-material size 80-320mesh used in step (4).
Embodiment 4
A kind of air purifier special purification sterilization material, constitutive material include: 28 parts of active carbon, 10 parts of nano silver, dioxy
Change 5 parts of titanium, 8 parts of carragheen, 15 parts of high rare earth, D-araboascorbic acid receive 5 parts, 12 parts of sodium benzoate and 12 parts of streptomysin, institute
There is raw material to calculate by weight.
The preparation method of the air purifier special purification sterilization material the following steps are included:
(1) preparation of adsorbing base: the high rare earth in part and active carbon mixing are ground, 140 meshes are crossed after the completion of grinding, so
Carragheen is added in the mixture of the high rare earth and active carbon of completing grinding operation afterwards, keeps its bonding blocking, after the completion of bonding
Operation is dried in drying box, 1h is dried at a temperature of 70 DEG C, it is spare that adsorbing base is made after completion drying operation.
(2) preparation of mixture A: nano silver is mixed with 8 times of its quality of neutral water, and is stirred using stirring rod
Sufficiently obtained Nano silver solution, high rare earth remaining in step (1) is received with D-araboascorbic acid and is uniformly mixed, nano silver is added
In solution, it is placed in reaction vessel and reacts, the reaction condition setting of reaction vessel are as follows: 56 DEG C of temperature, reaction vessel sealing, reaction
Mixture A is made in time 1.3h after the reaction was completed.
(3) preparation of mixture B: sodium benzoate and streptomysin are uniformly mixed, toward the mixing of sodium benzoate and streptomysin
Titanium dioxide is added in object, mixture one is made, then mixture one is added in the ethanol solution of 6 times of its quality, at 46 DEG C
Under the conditions of sealing stir process 1.5h be made mixture B.
(4) prepared by purification and sterilization material: at 47 DEG C after mixture A is mixed with mixture B, ultrasonic power is the item of 650W
It is ultrasonically treated 31min under part, operation is dried after the completion of ultrasonic treatment, dry 1.3h, dry to complete under conditions of 85 DEG C
It is ground into particle using micronizer afterwards, granularity size requirements were 160 mesh；Adsorbing base aperture is given using drilling machine,
Then the mixture met is required to the granularity of adsorbing base filling mixture A and mixture B, is finally compressed using compactor
Up to purification and sterilization material.
Micronizer model WFJ-20, discharging-material size 80-320mesh used in step (4).
Embodiment 5
A kind of air purifier special purification sterilization material, constitutive material include: 35 parts of active carbon, 15 parts of nano silver, dioxy
Change 8 parts of titanium, 13 parts of carragheen, 25 parts of high rare earth, D-araboascorbic acid receive 7 parts, 18 parts of sodium benzoate and 15 parts of streptomysin, institute
There is raw material to calculate by weight.
The preparation method of the air purifier special purification sterilization material the following steps are included:
(1) preparation of adsorbing base: the high rare earth in part and active carbon mixing are ground, 140 meshes are crossed after the completion of grinding, so
Carragheen is added in the mixture of the high rare earth and active carbon of completing grinding operation afterwards, keeps its bonding blocking, after the completion of bonding
Operation is dried in drying box, 3h is dried at a temperature of 70 DEG C, it is spare that adsorbing base is made after completion drying operation.
(2) preparation of mixture A: nano silver is mixed with 10 times of its quality of neutral water, and is stirred and mixed using stirring rod
Sufficiently obtained Nano silver solution is closed, high rare earth remaining in step (1) is received with D-araboascorbic acid and is uniformly mixed, nanometer is added
In silver-colored solution, it is placed in reaction vessel and reacts, the reaction condition setting of reaction vessel are as follows: temperature 60 C, reaction vessel sealing, instead
Mixture A is made in 1.5h between seasonable after the reaction was completed.
(3) preparation of mixture B: sodium benzoate and streptomysin are uniformly mixed, toward the mixing of sodium benzoate and streptomysin
Titanium dioxide is added in object, mixture one is made, then mixture one is added in the ethanol solution of 8 times of its quality, at 56 DEG C
Under the conditions of sealing stir process 1.7h be made mixture B.
(4) prepared by purification and sterilization material: at 58 DEG C after mixture A is mixed with mixture B, ultrasonic power is the item of 750W
Operation is dried after the completion in 39min at ultrasound, ultrasonic treatment under part, dry 1.5h under conditions of 95 DEG C, after the completion of dry
It is ground into particle using micronizer, granularity size requirements were 160 mesh；Adsorbing base aperture is given using drilling machine, so
The mixture met is required to the granularity of adsorbing base filling mixture A and mixture B afterwards, is finally using compactor compression
Obtain purification and sterilization material.
Micronizer model WFJ-20, discharging-material size 80-320mesh used in step (4).
Experiment effect detection is carried out to the product of five embodiment production, experimental result is as shown in table 1:
Table 1
It is drawn a conclusion by table 1 are as follows:
Formaldehyde removal rate sorts from large to small in five embodiments are as follows: 4 > embodiment of embodiment 3 > embodiment, 5 > embodiment, 2 >
Embodiment 1.
Ammonia removal rate sorts from large to small in five embodiments are as follows: 3 > embodiment of embodiment, 5 > embodiment, 4 > is implemented
2 > embodiment 1 of example.
Five embodiment mould antibiotic rates sort from large to small are as follows: 3 > embodiment of embodiment, 5 > embodiment, 4 > embodiment 2
> embodiment 1.
Five embodiment bacillus antibiotic rates sort from large to small are as follows: 3 > embodiment of embodiment, 5 > embodiment, 4 > is real
Apply 2 > embodiment 1 of example.
So to sum up, the product effect that embodiment 3 makes is the most excellent.
Better embodiment of the invention is explained in detail above, but the present invention is not limited to above-mentioned embodiment party
Formula within the knowledge of one of ordinary skill in the art can also be without departing from the purpose of the present invention
Various changes can be made.
Claims (6)
1. a kind of air purifier special purification sterilization material, it is characterised in that constitutive material are as follows: active carbon 25~40 part, nanometer
8~16 parts of silver, 4~10 parts of titanium dioxide, 6~14 parts of carragheen, 10~30 parts of high rare earth, D-araboascorbic acid receive 4~8 parts,
10~20 parts of sodium benzoate and 10~16 parts of streptomysin, all raw materials calculate by weight.
2. a kind of air purifier special purification sterilization material according to claim 1, it is characterised in that constitutive material are as follows:
30~35 parts of active carbon, 10~14 parts of nano silver, 6~8 parts of titanium dioxide, 8~12 parts of carragheen, 12~28 parts of high rare earth, D-
Arabo-ascorbic acid receives 6~8 parts, 12~18 parts of sodium benzoate and 12~14 parts of streptomysin, and all raw materials calculate by weight.
3. a kind of air purifier special purification sterilization material according to claim 1, it is characterised in that constitutive material are as follows:
30 parts of active carbon, 10 parts of nano silver, 6 parts of titanium dioxide, 8 parts of carragheen, 12 parts of high rare earth, D-araboascorbic acid receive 6 parts, benzene first
12 parts of sour sodium and 12 parts of streptomysin, all raw materials calculate by weight.
4. a kind of preparation method of the air purifier special purification sterilization material as described in claim 1-3 is any, feature exist
In: it comprises the steps of:
1) preparation of adsorbing base: the high rare earth in part and active carbon mixing are ground, 140 meshes are crossed after the completion of grinding, so
Carragheen is added in the mixture of the high rare earth and active carbon of completing grinding operation afterwards, keeps its bonding blocking, after the completion of bonding
Operation is dried in drying box, 1~3h is dried at a temperature of 70 DEG C, it is spare that adsorbing base is made after completion drying operation.
2) preparation of mixture A: nano silver is mixed with 8~10 times of its quality of neutral water, and is stirred using stirring rod
Sufficiently obtained Nano silver solution, high rare earth remaining in step (1) is received with D-araboascorbic acid and is uniformly mixed, nano silver is added
In solution, it is placed in reaction vessel and reacts, the reaction condition setting of reaction vessel are as follows: 53~64 DEG C of temperature, reaction vessel sealing,
Mixture A is made in 1.2~1.6h of reaction time after the reaction was completed.
3) preparation of mixture B: sodium benzoate and streptomysin are uniformly mixed, and are added into the mixture of sodium benzoate and streptomysin
Enter titanium dioxide and mixture one is made, then mixture one is added in the ethanol solution of 6~8 times of its quality, at 45~60 DEG C
Under conditions of sealing 1.4~1.8h of stir process be made mixture B.
4) prepared by purification and sterilization material: at 45~60 DEG C after mixture A is mixed with mixture B, ultrasonic power is 600~800W
Under conditions of be ultrasonically treated 30~40min, operation is dried after the completion of ultrasonic treatment, it is dry under conditions of 80~100 DEG C
1.2~1.6h is ground into particle using micronizer after the completion of drying, and granularity size requirements were 160 mesh；Use drilling
Machine gives adsorbing base aperture, then requires the mixture met to the granularity of adsorbing base filling mixture A and mixture B,
Finally compressed using compactor up to purification and sterilization material.
5. a kind of preparation method of air purifier special purification sterilization material according to claim 4, it is characterised in that:
Micronizer model WFJ-20, discharging-material size 80-320mesh used in step (4).
6. a kind of air purifier using the air purifier special purification sterilization material as described in claim 1-5 is any,
It is characterized in that including: gentle breeze fan, air filter, water tank, intelligent monitor system, anion generator and high-tension circuit.
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