CN109170911A - A kind of ferric pyrophosphate production method made an addition in food containing vitamins - Google Patents
A kind of ferric pyrophosphate production method made an addition in food containing vitamins Download PDFInfo
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- CN109170911A CN109170911A CN201811440486.5A CN201811440486A CN109170911A CN 109170911 A CN109170911 A CN 109170911A CN 201811440486 A CN201811440486 A CN 201811440486A CN 109170911 A CN109170911 A CN 109170911A
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- Prior art keywords
- ferric pyrophosphate
- containing vitamins
- addition
- food containing
- production method
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Links
- 235000007144 ferric diphosphate Nutrition 0.000 title claims abstract description 44
- 239000011706 ferric diphosphate Substances 0.000 title claims abstract description 44
- CADNYOZXMIKYPR-UHFFFAOYSA-B ferric pyrophosphate Chemical compound [Fe+3].[Fe+3].[Fe+3].[Fe+3].[O-]P([O-])(=O)OP([O-])([O-])=O.[O-]P([O-])(=O)OP([O-])([O-])=O.[O-]P([O-])(=O)OP([O-])([O-])=O CADNYOZXMIKYPR-UHFFFAOYSA-B 0.000 title claims abstract description 44
- 229940036404 ferric pyrophosphate Drugs 0.000 title claims abstract description 44
- 229940088594 vitamin Drugs 0.000 title claims abstract description 24
- 229930003231 vitamin Natural products 0.000 title claims abstract description 24
- 239000011782 vitamin Substances 0.000 title claims abstract description 24
- 235000013343 vitamin Nutrition 0.000 title claims abstract description 24
- 235000013305 food Nutrition 0.000 title claims abstract description 21
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 15
- 239000000843 powder Substances 0.000 claims abstract description 18
- 239000002994 raw material Substances 0.000 claims abstract description 12
- 239000004227 calcium gluconate Substances 0.000 claims abstract description 9
- 229960004494 calcium gluconate Drugs 0.000 claims abstract description 9
- 235000013927 calcium gluconate Nutrition 0.000 claims abstract description 9
- NEEHYRZPVYRGPP-UHFFFAOYSA-L calcium;2,3,4,5,6-pentahydroxyhexanoate Chemical compound [Ca+2].OCC(O)C(O)C(O)C(O)C([O-])=O.OCC(O)C(O)C(O)C(O)C([O-])=O NEEHYRZPVYRGPP-UHFFFAOYSA-L 0.000 claims abstract description 9
- 239000000725 suspension Substances 0.000 claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 8
- 235000013826 starch sodium octenyl succinate Nutrition 0.000 claims abstract description 6
- 239000001334 starch sodium octenyl succinate Substances 0.000 claims abstract description 6
- 238000001694 spray drying Methods 0.000 claims description 10
- -1 polyacrylic resinIII Substances 0.000 claims description 5
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 3
- 239000003595 mist Substances 0.000 claims description 3
- 229910052708 sodium Inorganic materials 0.000 claims description 3
- 238000001035 drying Methods 0.000 claims description 2
- 229940005574 sodium gluconate Drugs 0.000 claims description 2
- 239000013049 sediment Substances 0.000 claims 1
- 239000000176 sodium gluconate Substances 0.000 claims 1
- 235000012207 sodium gluconate Nutrition 0.000 claims 1
- 239000000463 material Substances 0.000 abstract description 7
- 239000000047 product Substances 0.000 abstract description 7
- 239000002244 precipitate Substances 0.000 abstract description 6
- 239000002417 nutraceutical Substances 0.000 abstract description 5
- 235000021436 nutraceutical agent Nutrition 0.000 abstract description 5
- 150000003722 vitamin derivatives Chemical class 0.000 abstract description 5
- 238000012545 processing Methods 0.000 abstract description 4
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 11
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 6
- 229910052742 iron Inorganic materials 0.000 description 5
- 229920002472 Starch Polymers 0.000 description 4
- 239000008107 starch Substances 0.000 description 4
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 description 3
- 229930003268 Vitamin C Natural products 0.000 description 3
- XPPKVPWEQAFLFU-UHFFFAOYSA-N diphosphoric acid Chemical compound OP(O)(=O)OP(O)(O)=O XPPKVPWEQAFLFU-UHFFFAOYSA-N 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 229940005657 pyrophosphoric acid Drugs 0.000 description 3
- 235000019154 vitamin C Nutrition 0.000 description 3
- 239000011718 vitamin C Substances 0.000 description 3
- 235000013373 food additive Nutrition 0.000 description 2
- 239000002778 food additive Substances 0.000 description 2
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 description 2
- 239000006210 lotion Substances 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 230000035764 nutrition Effects 0.000 description 2
- 125000004365 octenyl group Chemical group C(=CCCCCCC)* 0.000 description 2
- 238000012856 packing Methods 0.000 description 2
- 239000008213 purified water Substances 0.000 description 2
- 230000003014 reinforcing effect Effects 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 235000019698 starch Nutrition 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 239000004925 Acrylic resin Substances 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 235000009754 Vitis X bourquina Nutrition 0.000 description 1
- 235000012333 Vitis X labruscana Nutrition 0.000 description 1
- 240000006365 Vitis vinifera Species 0.000 description 1
- 235000014787 Vitis vinifera Nutrition 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 229960005069 calcium Drugs 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- NEEHYRZPVYRGPP-IYEMJOQQSA-L calcium gluconate Chemical compound [Ca+2].OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O.OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O NEEHYRZPVYRGPP-IYEMJOQQSA-L 0.000 description 1
- 239000013065 commercial product Substances 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 235000021004 dietary regimen Nutrition 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 235000004280 healthy diet Nutrition 0.000 description 1
- 210000000987 immune system Anatomy 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 235000008935 nutritious Nutrition 0.000 description 1
- 230000001766 physiological effect Effects 0.000 description 1
- 238000006479 redox reaction Methods 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/16—Inorganic salts, minerals or trace elements
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Inorganic Chemistry (AREA)
- Mycology (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention discloses a kind of ferric pyrophosphate production methods made an addition in food containing vitamins, and commercially available ferric pyrophosphate raw material is pulverized；Then plus water and polyacrylic resinⅢ, starch Sodium Octenyl Succinate and calcium gluconate are configured to suspension in proportion, adjust pH to 6.0 ~ 8.0；The suspension of preparation is subjected to high speed shear, homogeneous, is then spray-dried, obtains ferric pyrophosphate finished product powder.The advantage of the invention is that using glucide as wall material, embedding treatment is carried out to common ferric pyrophosphate raw material using microencapsulation technology, treated, and ferric pyrophosphate free-running property is good, processing performance is improved, it is used in nutraceutical containing vitamins as chalybeate is strengthened, it can avoid reacting with vitamin, will not generate black precipitate during reconstituting, it is in good taste and drink more healthy.
Description
Technical field
The present invention relates to food addition molysite, more particularly, to a kind of pyrophosphoric acid made an addition in food containing vitamins
Iron production method.
Background technique
Iron is one of the essential trace elements of the human body, though its content in human body is low, but constitutes the blood red egg of human body
White main component, and it is closely bound up with the immune system of human body, the physiological activity of human body is played a crucial role, institute
Ferro element cannot be lacked in human body.And supplement ferro element, except through diet regimen outside, some reinforcings can also be taken
The nutraceutical of ferro element.
The advantages that ferric pyrophosphate is applied widely and highly-safe using its mostly adds in food as reinforcing chalybeate, as
When to strengthen ferro element addition in nutraceutical containing vitamins (such as reconstituted food), variable valency metal Fe can occur with vitamin
Redox reaction generates black precipitate, not only influences the appearance of food, will also result in adverse effect to healthy diet；And it is general
The free-running property of logical ferric pyrophosphate is poor (powdered Electrostatic Absorption generates phenomenon of uniting), and influences processing performance.Therefore it needs to mention
Molysite (ferric pyrophosphate) production method that ferric pyrophosphate mobility can be improved for one kind, and do not reacted with vitamin.
Summary of the invention
The purpose of the present invention is to provide a kind of ferric pyrophosphate production methods made an addition in food containing vitamins, use
The ferric pyrophosphate that this method is produced not only increases free-running property, is added to when being reconstituted in nutraceutical as raw material, no
Black precipitate can be generated.
To achieve the above object, the present invention can take following technical proposals:
The ferric pyrophosphate production method of the present invention made an addition in food containing vitamins includes the following steps:
The first step pulverizes commercially available ferric pyrophosphate raw material；Plus water and polyacrylic resinⅢ, octenyl amber then
Amber acid-starch sodium and calcium gluconate are configured to suspension in proportion, adjust pH to 6.0 ~ 8.0；
Second step, by the first step prepare suspension carry out high speed shear, homogeneous, be then spray-dried, obtain ferric pyrophosphate at
Product powder.
The ferric pyrophosphate micro mist, polyacrylic resinⅢ, starch Sodium Octenyl Succinate and calcium gluconate quality
Per distribution ratio is 30 ~ 80%:5 ~ 25%:10 ~ 60%:2 ~ 10%.
When the spray drying, inlet air temperature is 170 ~ 190 DEG C, and leaving air temp is 85 ~ 95 DEG C.
Powder after being spray-dried in the second step will carry out 60 ~ 120 meshes point.
Powder drying weightlessness≤8% after being spray-dried in second step.
In use, being added to it in food containing vitamins in proportion, mixed processing according to a conventional method.
The advantage of the invention is that using glucide as wall material, using microencapsulation technology to common ferric pyrophosphate raw material into
Row embedding treatment, treated, and ferric pyrophosphate free-running property is good, and processing performance is improved, and is used to contain vitamin as chalybeate is strengthened
In nutritious food, it can avoid reacting with vitamin, will not generate black precipitate during reconstituting, it is in good taste and drink more
For health.
Embedding raw material used of the invention is commercial product, and at low cost, production method is simple.In raw materials used, pyrophosphoric acid
Iron micro mist is ferro element nutrition fortifier, and polyacrylic resinⅢ, starch Sodium Octenyl Succinate are wall material and octenyl succinic
The also simultaneous emulsification of acid-starch sodium, calcium gluconate is Water-solubility Material, and a small amount of calcium gluconate is compounding nutrition fortifier
Middle calcium constituent；Ferric pyrophosphate disperses in water after being pulverized to 1500 mesh or so, is conducive to subsequent spray；Polyacrylic resin
III, starch Sodium Octenyl Succinate is wall material, not stratified after clipped, homogeneous, guarantees that product quality is uniform and facilitates industrialization
Large-scale production.
Detailed description of the invention
Fig. 1 is the effect contrast figure after product of the present invention is reconstituted with conventional ferric pyrophosphate.
Specific embodiment
More detailed explanation is done to the present invention below by specific embodiment, in order to the reason of those skilled in the art
Solution.In the raw materials used in the present invention, ferric pyrophosphate is Zhengzhou Ruipu Bioengineering Co., Ltd.'s production, and polyacrylic resinⅢ is purchased from
Anhui Shanhe Medicinal Subsidiary Material Co., Ltd., starch Sodium Octenyl Succinate is purchased from the rich Food Co., Ltd in Deqing three, grape
Calciofon is Zhengzhou Ruipu Bioengineering Co., Ltd.'s production.
Embodiment 1 prepares the ferric pyrophosphate powder made an addition in food containing vitamins
Commercially available ferric pyrophosphate raw material is pulverized first, it is stand-by to be allowed to be formed 10 μm or so of ultra micro powder；
The ferric pyrophosphate powder that investment 100Kg is pulverized in 1000Kg purified water, 20Kg polyacrylic resinⅢ, 70Kg are pungent
Starch alkenyl succinate sodium, 10Kg calcium gluconate are stirred into suspension, then using 2 tons preparing tank revolving speed 20 ~
High speed shear, homogeneous (continuing 55 ~ 60 minutes) are carried out under the conditions of 25 revs/min, and finally lotion is sent into spray drying tower and is carried out
Spray drying, keeps 180 DEG C of inlet air temperature of spray drying tower, 90 DEG C of leaving air temp, the powder after spray drying is through 80 meshes
After point, packing storage is weighed.
As food additive in use, being added by the 10% of total weight of material, it is evenly mixed in and is sought containing vitamins
It supports in food.Boiled water reconstitutes when edible.
Embodiment 2 prepares the ferric pyrophosphate powder made an addition in food containing vitamins
Equally first commercially available ferric pyrophosphate raw material is pulverized, it is stand-by to be allowed to be formed 10 μm or so of ultra micro powder；
The ferric pyrophosphate powder that investment 150Kg is pulverized in 1000Kg purified water, 25Kg polyacrylic resinⅢ, 70Kg are pungent
Starch alkenyl succinate sodium, 5Kg calcium gluconate are stirred into suspension, then using 2 tons preparing tank revolving speed 20 ~
High speed shear, homogeneous (continuing 55 ~ 60 minutes) are carried out under the conditions of 25 revs/min, and finally lotion is sent into spray drying tower and is carried out
Spray drying, keeps 170 DEG C of inlet air temperature of spray drying tower, 85 DEG C of leaving air temp, the powder after spray drying is through 100 meshes
After point, packing storage is weighed.
As food additive in use, being added by the 10% of total weight of material, it is evenly mixed in and is sought containing vitamins
It supports in food.Boiled water reconstitutes when edible.
The performance comparison of embodiment 3 ferric pyrophosphate produced by the invention and commercially available ferric pyrophosphate
The ferric pyrophosphate finished product powder that common commercially available ferric pyrophosphate is produced with the embodiment of the present invention 1 is pressed with vitamin C respectively
Same ratio carries out reconstituting experiment after being mixed.As a result as shown in Figure 1.
Left figure is the solution after the vitamin C containing conventional ferric pyrophosphate reconstitutes in Fig. 1, can clearly show that generation is anti-in figure
The black precipitate that should be generated afterwards；Right figure is the solution after the vitamin C containing embedding ferric pyrophosphate (product of the present invention) reconstitutes, can be with
Find out that solution is limpid, does not generate black precipitate.
Using ferric pyrophosphate produced by the invention as ferro element addition is strengthened in nutraceutical containing vitamins, weigh etc.
10 parts of pulvis of amount measure the iron content in solution after reconstituting, show essentially identical；Prove pyrophosphoric acid flowing molten iron produced by the invention
Dynamic property is good and the mixing of other raw materials it is highly uniform.
The ferric pyrophosphate finished product powder that embodiment 2 produces is done into same test, effect is the same as embodiment 1.
Claims (5)
1. a kind of ferric pyrophosphate production method made an addition in food containing vitamins, it is characterised in that: include the following steps:
The first step pulverizes ferric pyrophosphate raw material；Then plus water and polyacrylic resinⅢ, ocentyl succinic form sediment
Powder sodium and calcium gluconate are configured to suspension in proportion, adjust pH to 6.0 ~ 8.0；
Second step, by the first step prepare suspension carry out high speed shear, homogeneous, be then spray-dried, obtain ferric pyrophosphate at
Product powder.
2. the ferric pyrophosphate production method according to claim 1 made an addition in food containing vitamins, it is characterised in that:
The ferric pyrophosphate micro mist, polyacrylic resinⅢ, starch Sodium Octenyl Succinate and calcium gluconate percent mass proportioning
For 30 ~ 80%:5 ~ 25%:10 ~ 60%:2 ~ 10%.
3. the ferric pyrophosphate production method according to claim 1 made an addition in food containing vitamins, it is characterised in that:
When the spray drying, inlet air temperature is 170 ~ 190 DEG C, and leaving air temp is 85 ~ 95 DEG C.
4. the ferric pyrophosphate production method according to claim 1 made an addition in food containing vitamins, it is characterised in that:
Powder after being spray-dried in the second step carries out 60 ~ 120 meshes point.
5. the ferric pyrophosphate production method according to claim 1 made an addition in food containing vitamins, it is characterised in that:
Powder drying weightlessness≤8% after being spray-dried in second step.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811440486.5A CN109170911A (en) | 2018-11-29 | 2018-11-29 | A kind of ferric pyrophosphate production method made an addition in food containing vitamins |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811440486.5A CN109170911A (en) | 2018-11-29 | 2018-11-29 | A kind of ferric pyrophosphate production method made an addition in food containing vitamins |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109170911A true CN109170911A (en) | 2019-01-11 |
Family
ID=64938426
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
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| CN201811440486.5A Withdrawn CN109170911A (en) | 2018-11-29 | 2018-11-29 | A kind of ferric pyrophosphate production method made an addition in food containing vitamins |
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| Country | Link |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110236201A (en) * | 2019-06-04 | 2019-09-17 | 宁波希诺亚海洋生物科技有限公司 | Preparation method applied to the ferric pyrophosphate in infant food |
| CN112205625A (en) * | 2020-10-28 | 2021-01-12 | 江苏瑞丰医药有限公司 | Ferric pyrophosphate and production method thereof |
| CN112205624A (en) * | 2020-10-28 | 2021-01-12 | 江苏瑞丰医药有限公司 | Ferric pyrophosphate |
| CN113966844A (en) * | 2021-10-26 | 2022-01-25 | 河南瑞贝佳生物科技有限公司 | Ferric pyrophosphate microcapsule powder applied to Vc-containing series products and preparation method thereof |
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| CN103504026A (en) * | 2012-06-25 | 2014-01-15 | 浙江康恩贝健康产品有限公司 | Dry-method preparation process of infant formula milk powder |
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| CN107518235A (en) * | 2017-08-22 | 2017-12-29 | 郑州瑞普生物工程有限公司 | A kind of suspension ferric pyrophosphate production method |
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| CN1422553A (en) * | 2001-12-06 | 2003-06-11 | 上海黄金搭档生物科技有限公司 | Vitamin, mineral substance nutrient composition for women |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN113966844A (en) * | 2021-10-26 | 2022-01-25 | 河南瑞贝佳生物科技有限公司 | Ferric pyrophosphate microcapsule powder applied to Vc-containing series products and preparation method thereof |
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