CN109156793A - A kind of flavor dressing agent and preparation method thereof - Google Patents

A kind of flavor dressing agent and preparation method thereof Download PDF

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Publication number
CN109156793A
CN109156793A CN201810924224.XA CN201810924224A CN109156793A CN 109156793 A CN109156793 A CN 109156793A CN 201810924224 A CN201810924224 A CN 201810924224A CN 109156793 A CN109156793 A CN 109156793A
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CN
China
Prior art keywords
dressing agent
flavor
flavor dressing
food
acid content
Prior art date
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Pending
Application number
CN201810924224.XA
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Chinese (zh)
Inventor
崔春
相欢
刘鹏展
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South China University of Technology SCUT
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South China University of Technology SCUT
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Publication date
Application filed by South China University of Technology SCUT filed Critical South China University of Technology SCUT
Priority to CN201810924224.XA priority Critical patent/CN109156793A/en
Publication of CN109156793A publication Critical patent/CN109156793A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/20Synthetic spices, flavouring agents or condiments
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

Abstract

The invention discloses a kind of flavor dressing agents and preparation method thereof.Preparation method includes mixing cane molasses with the ethyl acetate of 0.1-30 times of weight, 10-50 DEG C of extraction 0.5-10h, separating acetic acid ethyl ester phase, and distillation removal ethyl acetate obtains (paste) flavor dressing agent.Coffee acid content is 0.1-10.0%(wt% in flavor dressing agent), gallic acid content 0.1-2.0%(wt%), ferulaic acid content 0.1-10.0%(wt%) and, chlorogenic acid content 0.1-5.0%(wt%).Flavor dressing agent disclosed by the invention can obviously cover the peculiar smell of food under the concentration of 0.01mg/kg-0.1mg/kg, increase the sweet taste, savoury and delicate flavour of food.

Description

A kind of flavor dressing agent and preparation method thereof
Technical field
The present invention relates to flavour of food products chemical fields, and in particular to a kind of flavor dressing agent and preparation method thereof.
Background technique
Flavor is the important organoleptic attribute of food, directly affects its quality and acceptance level.But Partial Food is because of itself Compositing characteristic or carried out fortification, cause it to have a poor flavour.For example, containing a large amount of unsaturated fats in fish products Acid, deterioration easy to oxidize cause fishy smell heavier;Food bitter taste rich in arginine or hydrophobic peptide is heavier.In this case, It the use of flavor dressing agent is preferably to select.
Common flavor dressing agent specifically includes that ethylmaltol, vanillic aldehyde and maltol etc. in food industry.Ethyl wheat Different cotton flavours of candy is presented in bud phenol in higher concentrations, is in burnt odor gas after being heated, the product dissolubility is larger, can be lower At a temperature of distil, this property make it have flavouring characteristic, can be widely used for ice cream, beverage, meat products, candy, biscuit In equal food, product fragrance can be significantly improved.But the food additives such as ethylmaltol are only capable of improving the smell of food, to not Good flavour is without improvement result.In addition, ethylmaltol is chemical synthesis, application is by biggish limitation.MC food in 2010 Scientific and technological Co., Ltd. discloses the flavor improving agent for containing 3 Methylbutanoic acid as effective component.MC food science and technology strain formula in 2015 Commercial firm discloses the flavor improving agent for containing D- amino acid or its salt as effective component, and flavor obtains improveing without destroying taste The manufacturing method and flavor improvement method (201510580835.3) of the diet product of balance.Ajincomoto Co., Inc's public affairs in 2010 The method for assigning food aroma and/or flavor is opened, including imparting fragrance and/or wind containing any one in following component The composition of taste: (i) capric acid, (ii) octanoic acid, (iii) pyruvic alcohol, furfural, methyltetrahydrofuran ketone, 2- acetyl group -5- methyl furan It is more than any one muttered, by the combined amount of (i) capric acid as A parts by weight, the combined amount of (ii) octanoic acid as B parts by weight, (iii) total combined amount of pyruvic alcohol, furfural, methyltetrahydrofuran ketone, 2- acetyl group -5- methylfuran is as C parts by weight, When being scaled A+B+C=100, mixing is made to meet 0≤A≤60,0≤B≤100,0≤C≤100,3A+B≤180.
The present invention is directed to overcome the above-mentioned prior art, a kind of side that flavor dressing agent is prepared using molasses is provided Method.
Summary of the invention
The purpose of the present invention is to solve above-mentioned deficiencies present in currently available technology, provide a kind of flavor dressing agent And preparation method thereof.
The purpose of the present invention is realized at least through one of following technical solution.
A kind of preparation method of flavor dressing agent, cane molasses is mixed with the ethyl acetate of 0.1-30 times of weight, 10- 50 DEG C of extraction 0.5-10h, separating acetic acid ethyl ester phase, distillation removal ethyl acetate obtain flavor dressing agent.
The present invention also provides a kind of flavor dressing agents, and wherein coffee acid content is 0.1-10.0%(wt%), gallic acid contains Amount is 0.1-2.0%(wt%), ferulaic acid content 0.1-10.0%(wt%), chlorogenic acid content 0.1-5.0%(wt%).
It advanced optimizes, the flavor dressing agent further includes one or more of Quercetin, catechin.
Concentration of the flavor dressing agent provided by the invention in food can be covered when being 0.01mg/kg-0.1mg/kg The peculiar smell and bitter taste of lid food increase the sweet taste, savoury and delicate flavour of food.
Compared with the prior art, the invention has the following advantages and beneficial effects:
The present invention prepares flavor dressing agent for the first time using Sugar cane molasses as raw material, by high efficiency extraction and beneficiation technologies.System of the present invention Standby flavor dressing agent can obviously cover the peculiar smell of food under the concentration of 0.01mg/kg-0.1mg/kg, increase the sweet tea of food Taste, savoury and delicate flavour.
In addition, the present invention has, simple process, equipment investment is few, extraction conditions are mild, additive amount is small, Improving flavor is obvious The advantages that, there is preferable industrial prospect.
Specific embodiment
Specific implementation of the invention is described further with reference to embodiments, but implementation and protection of the invention is unlimited In this, if it is noted that the following process or parameter for having not special detailed description, is that those skilled in the art can refer to now Have technology understand or realize.
Embodiment 1
Cane molasses are mixed with the ethyl acetate of 30 times of weight, 50 DEG C of extraction 10h, separating acetic acid ethyl ester phase, distillation removal second Acetoacetic ester obtains paste flavor dressing agent 1.Contain gallic acid mass percent 0.13%, chlorogenic acid in flavor dressing agent 1 Mass percent 0.6%, caffeic acid mass percent 2.13%, ferulic acid mass percent 2.55%.By paste flavor dressing agent 1 Number chicken soup solution, fish soup solution, 0.3% monosodium glutamate+0.5% salt solution (quality percentage are respectively added to the concentration of 0.01mg/kg Than), 0.5%(mass percent) arginine solution in, carry out sensory evaluation.Sensory evaluation is tested by 5 35-45 years old thoughts Official evaluates male and the 5 women composition of experience, evaluates respectively the delicate flavour of solution, savoury, fishy smell, bitter taste, and with mark Quasi- solution is compareed.It the results are shown in Table 1.
Table 1
Solution type Sensory evaluation
Chicken soup Delicate flavour increases, savoury increases
Fish soup Fishy smell weakens, delicate flavour increases
+ 0.5% salt solution of 0.3% monosodium glutamate Savoury increases
0.5% arginine solution Bitter taste obviously weakens
Seen from table 1, after flavor dressing agent 1 for adding 0.01mg/kg, the delicate flavour and savoury of chicken soup increase, the fishy smell of fish soup Weaken, and delicate flavour increases;For+0.5% salt solution of 0.3% monosodium glutamate, thickness after flavor dressing agent 1 of 0.01mg/kg is added Taste increases;Flavor dressing agent 1 of addition 0.01mg/kg can also be substantially reduced bitter taste.
Embodiment 2
Cane molasses are mixed with the ethyl acetate of 0.1 times of weight, 10 DEG C of extraction 0.5h, separating acetic acid ethyl ester phase, distillation removal Ethyl acetate obtains paste flavor dressing agent 2.Contain gallic acid mass percent 0.17%, green original in flavor dressing agent 2 Sour mass percent 0.45%, caffeic acid mass percent 1.86%, ferulic acid mass percent 2.78%, the flavor dressing agent Effect can obviously cover the peculiar smell of food referring to table 1 under the concentration of 0.01mg/kg-0.1mg/kg, increase food sweet taste, Savoury and delicate flavour.
Embodiment 3
Cane molasses are mixed with the ethyl acetate of 20 times of weight, 10 DEG C of extraction 0.5h, separating acetic acid ethyl ester phase, distillation removal second Acetoacetic ester obtains paste flavor dressing agent 3.Contain gallic acid mass percent 0.17%, chlorogenic acid in flavor dressing agent 2 Mass percent 0.45%, caffeic acid mass percent 1.86%, ferulic acid mass percent 2.78%, Quercetin mass percent 0.52% and catechin mass percent 0.21%.
Paste flavor dressing agent 3 concentration with 0.1mg/kg is respectively added to chicken soup solution, fish soup solution, 0.3% taste Smart+0.5% salt solution, 0.5% arginine solution in, carry out sensory evaluation.Sensory evaluation is tested by 5 35-45 years old thoughts Official evaluates male and the 5 women composition of experience, evaluates respectively the delicate flavour of solution, savoury, fishy smell, bitter taste, and with mark Quasi- solution is compareed.It the results are shown in Table 2.
Table, 2
Solution type Sensory evaluation
Chicken soup Delicate flavour obviously increases, savoury obviously increases
Fish soup Fishy smell weakens, delicate flavour obviously increases
+ 0.5% salt solution of 0.3% monosodium glutamate Savoury obviously increases
0.5% arginine solution Bitter taste obviously weakens, almost without bitter taste
As can be seen from Table 2, the delicate flavour and savoury of chicken soup obviously increase, the raw meat of fish soup after flavor dressing agent 3 of addition 0.1mg/kg Taste weakens, and delicate flavour obviously increases;To 0.3% monosodium glutamate+0.5%(mass percent) for salt solution, add 0.1mg/kg's Savoury obviously increases after flavor dressing agent 1;Flavor dressing agent 1 of addition 0.01mg/kg can also be substantially reduced bitter taste, molten Liquid, almost without bitter taste.

Claims (4)

1. a kind of preparation method of flavor dressing agent, it is characterised in that: by the ethyl acetate of cane molasses and 0.1-30 times of weight Mixing, 10-50 DEG C of extraction 0.5-10h, separating acetic acid ethyl ester phase, distillation removal ethyl acetate obtain flavor dressing agent.
2. a kind of flavor dressing agent made from the preparation method as described in claim 1, it is characterised in that wherein coffee acid content is 0.1-10.0%(wt%), gallic acid content 0.1-2.0%(wt%), ferulaic acid content 0.1-10.0%(wt%), chlorogenic acid Content is 0.1-5.0%(wt%).
3. flavor dressing agent according to claim 2, it is characterised in that further include one of Quercetin, catechin with On.
4. flavor dressing agent according to claim 1, it is characterized in that the concentration in food is 0.01mg/kg-0.1mg/ The peculiar smell and bitter taste that food can be covered when kg increase the sweet taste, savoury and delicate flavour of food.
CN201810924224.XA 2018-08-14 2018-08-14 A kind of flavor dressing agent and preparation method thereof Pending CN109156793A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
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Application Number Priority Date Filing Date Title
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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1516553A (en) * 2001-06-13 2004-07-28 ����µ��ɷ����޹�˾ Taste modifiers comprising chlorogenic acid
CN1748582A (en) * 2004-09-17 2006-03-22 太阳化学株式会社 Flavour improving composition, food and beverage and medicine and method for improving food and beverage and medicine flavour
CN103561585A (en) * 2011-02-08 2014-02-05 视界科技有限公司 Sugar extracts
CN103622134A (en) * 2013-11-13 2014-03-12 华南理工大学 Method of preparing antioxidant and antibacterial food preservative by using molasses as raw material
CN104323268A (en) * 2006-09-19 2015-02-04 视界科技有限公司 Extracts derived from sugar cane and a process for their manufacture
MX2013013972A (en) * 2013-11-28 2015-05-28 Héctor Alejandro Álvarez De La Cadena Sillas Process for obtaining a sugar cane flavoring agent from concentrates of sugar cane or intermediate syrups and molasses derived from the extraction of sugar in sugar mills, as a high performance sweetening additive and resulting product.

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1516553A (en) * 2001-06-13 2004-07-28 ����µ��ɷ����޹�˾ Taste modifiers comprising chlorogenic acid
CN1748582A (en) * 2004-09-17 2006-03-22 太阳化学株式会社 Flavour improving composition, food and beverage and medicine and method for improving food and beverage and medicine flavour
CN104323268A (en) * 2006-09-19 2015-02-04 视界科技有限公司 Extracts derived from sugar cane and a process for their manufacture
CN103561585A (en) * 2011-02-08 2014-02-05 视界科技有限公司 Sugar extracts
CN103622134A (en) * 2013-11-13 2014-03-12 华南理工大学 Method of preparing antioxidant and antibacterial food preservative by using molasses as raw material
MX2013013972A (en) * 2013-11-28 2015-05-28 Héctor Alejandro Álvarez De La Cadena Sillas Process for obtaining a sugar cane flavoring agent from concentrates of sugar cane or intermediate syrups and molasses derived from the extraction of sugar in sugar mills, as a high performance sweetening additive and resulting product.

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