CN1091464A - Cold-drawing antirust lubricating agent - Google Patents
Cold-drawing antirust lubricating agent Download PDFInfo
- Publication number
- CN1091464A CN1091464A CN 93103940 CN93103940A CN1091464A CN 1091464 A CN1091464 A CN 1091464A CN 93103940 CN93103940 CN 93103940 CN 93103940 A CN93103940 A CN 93103940A CN 1091464 A CN1091464 A CN 1091464A
- Authority
- CN
- China
- Prior art keywords
- water
- cold
- lubricating agent
- rosin
- reactor
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Metal Extraction Processes (AREA)
- Lubricants (AREA)
Abstract
The invention discloses the cold-drawing antirust lubricating agent that a kind of cold-drawn industry is used, it is main raw material, is processed into a kind of solid with specific method with animal grease, sodium hydroxide, rosin, water glass and water.The present invention must be placed the pond close with water-soluble during use, the steel that will desire drawing again immerse in the pond, after steel go out the pond, at the composite lubricating film of steel surface absorption layer of transparent.It has advantages such as the technology of use is simple, adsorptive power is strong, and adhesion amount is big, and the caking amount is little, and is pollution-free and antirust.
Description
The present invention relates to the lubricant that a kind of cold-drawn industry is used, particularly a kind of cold-drawing antirust lubricating agent that in the steel cold-drawn course of processing, can play the lubricating and antirust effect.
At present, the lubricant of cold-drawn industry use roughly divides two big classes: dry lube and wet lubricant.Dry lube roughly has calcium soap, soda soap, barium soap, aluminium soap or two or more compound soaps at home, and water-soluble dry lube, resin lubrication agent, tack lubricant are abroad arranged.Wet lubricant has oil soluble lubricating agent and soluble oil.Because of wet lubricant working conditions and narrow range, though have not tool table of many deficiencies in cold-drawn industry.So, based on dry lube, with regard to the weak point of its present situation indicate following some:
1, dry lubes such as domestic calcium soap, soda soap all need be beforehand with the coating processing, and lubricant then must be placed in the diaphragm capsule and be lubricated.Can not directly utilize coating to advance to draw lubricious drawing to the higher ferrous metal of carbon content.
2, the adhesion amount of Steel Wire Surface has only 1.72 grams～2.84 grams for every square metre.Adhesion amount is too little, and the lubricating and antirust performance is all undesirable.
3, the caking amount in the diaphragm capsule have up to 60%, No. 1, minimum Tianjin is also 22%.Not only influence is lubricated for caking in the diaphragm capsule, also can wipe coating off.
4, limy lubricant is after the high temperature drawing, and dust severe contamination air influences worker's physical and mental health.
5, operating procedure complexity, if calcium soap or soda soap improper use, normal " being mould ", the coking phenomenon of taking place.
6, undesirable as selecting calcium soap, soda soap for use, what emit blue or green cigarette phenomenon, polluted air through regular meeting.
7, adsorptive power is poor, refers to the preceding coating of drawing here and handles, and through dilatory, the steel of carrying are easy to coating shedding.
8, be convenient to quality control, steel can be covered the scar and the inhomogeneous situation of pickling of steel surface after coating, finally influence the drawing quality.
Purpose of the present invention be exactly to provide a kind of must not add lubricant just directly drawing have stronger sticking power and lubricity preferably, do not produce pollution, cold-drawing antirust lubricating agent that can be antirust.
The present invention realizes like this; Selecting animal grease, sodium hydroxide, rosin, water glass and water for use is raw material, and through the proportioning combination and by the certain method processing and manufacturing, the cooling back becomes solid shape.
The percentage ratio sum of each component prescription equals 100% in the cold-drawing antirust lubricating agent, wherein: animal grease 55%～65%, sodium hydroxide 5%～7%, rosin 3%～5%, water glass 5%～7%, all the other are water, (proportional quantity of water and above each composition percentage ratio sum are 100%).
The machining manufacture of cold-drawing antirust lubricating agent is undertaken by following program: at first get 3/4 water being inserted in the reactor of proportional quantity of water in the cold-drawing antirust lubricating agent, add rosin thereupon, making reactor be warming up to rosin again can consoluet temperature.
Meanwhile, get 1/3 of water proportional quantity in the cold-drawing antirust lubricating agent in another container, water and water glass are stirred, the water temperature of this moment requires in 25 ℃～30 ℃ scopes.
Animal grease is added in the reactor again and mix with rosin solution, and be heated to 100 ℃～105 ℃, add strong mixing thereupon and control Heating temperature at 105 ℃～110 ℃, the time length is 30 minutes.Afterwards, add in advance and the water-soluble water glass that closes, stir.
Begin when the temperature in the question response still is increased to 120 ℃, in reactor, to add sodium hydroxide slowly to heating in the reactor, add on one side, stir rapidly on one side.When treating that temperature is elevated to 140 ℃～150 ℃, controlled temperature continues 1.5～2 hours.
Behind the controlled temperature 1.5～2 hours, make the temperature in the reactor be reduced to 80 ℃, can go out still after the solution in the reactor is paste, treat that body of paste continues to cool to below 38 ℃, solid, at this moment can the stripping and slicing packing.
Embodiment 1.Press the lower limit preparation of the prescription of cold-drawing antirust lubricating agent.With animal grease 55%, sodium hydroxide 5%, rosin 3%, water glass 5%, the prescription of water 32% be solid below 38 ℃, but water content is bigger by above-mentioned working method manufacturing, and its hardness is less, still can the stripping and slicing packing.Animal grease, if select butter for use, then be light yellow, if select for use sheep oil or lard to be pale.Use drawing process to be 6.5～3 millimeters of φ, its lubricity is good, and the Steel Wire Surface adhesion amount is 2.68 gram/m
2, steel surface is the transparence crystal.Mould outlet caking amount is 8.2%.No dust pollution in the drawing.Steel Wire Surface smooth finish after the drawing is better, no scar.
Embodiment 2.Press the middle limit preparation of the prescription of cold-drawing antirust lubricating agent.With animal grease 60%, sodium hydroxide 6%, rosin 4%, water glass 6%, the processing and manufacturing as stated above of the prescription of water 24% is solid below 38 ℃, and its hardness is than embodiment 1 height.Animal grease selects butter, and product then is middle yellow, if select sheep oil or lard, then is creamy white.Be example with 6.5～3 millimeters of φ in the drawing process still, its lubricity is better than embodiment 1, and the Steel Wire Surface adhesion amount is 4.95 gram/m
2, the steel surface coating still is a transparent crystals, die orifice caking amount is 9.7%, and no dust pollution, the Steel Wire Surface after the drawing is highly polished, no scar.
Embodiment 3.Press the upper limit preparation of the prescription of cold-drawing antirust lubricating agent.By above-mentioned working method preparation, be solid under 38 ℃ with the prescription of animal grease 65%, sodium hydroxide 7%, rosin 5%, water glass 7%, water 16%, its product hardness is higher than embodiment 2.Animal grease is selected butter for use, and product is middle deep yellow, if select lard or sheep oil, then is creamy white.Be example with 6.5～3 millimeters of drawing process φ still, its lubricity is identical with enforcement 2, and the Steel Wire Surface adhesion amount is 5.4 gram/m
2, the steel surface coating is a hyalosome, die orifice caking amount 10.4%.No dust pollution, the surface smoothness height after the steel drawing.There is not cut.
The present invention can set up good lubricant film, has stronger adhesion property, under high pressure, high temperature drawing condition, can prevent to adhere to; Steel surface before the drawing is coated with the hyalosome that one deck is 0.2～0.4 mm thick, and the one, can make steel and air isolated, prevent that steel from getting rusty between staging life before drawing, the 2nd, be convenient to before drawing, carry out quality inspection; Lubricity is good, and frictional coefficient is little, prolongs the work-ing life of mould relatively; Chemical stability is good, because of the acid that remains in steel surface after water glass and the pickling has neutralizing effect, to drawing wire rod and mould non-corrosiveness; Under hot conditions, do not damage HUMAN HEALTH, free from environmental pollution; Because of its product and water proportioning are at 1.5: 100, so use cost also reduces greatly.
In use of the present invention, must carry out pickling to steel earlier, then, cold-drawing antirust lubricating agent is put into special bath, the ratio of cold-drawing antirust lubricating agent and water is 1.5: 100, heating then to 50 ℃～60 ℃ makes water and cold-drawing antirust lubricating agent fused, to be immersed in this bath by the steel of drawing again, after 2 minutes, steel surface absorption one deck liquid, go out behind the pond promptly to do in 5～8 minutes, steel surface adheres to the transparent film of one deck 0.2～0.4 mm thick.Deposit before the drawing steel are got rusty.
Claims (1)
1, a kind of cold-drawing antirust lubricating agent is to form by animal grease, sodium hydroxide, rosin, water glass and the combination of water proportioning and by the certain method manufacturing, it is characterized in that:
A. the prescription of cold-drawing antirust lubricating agent is:
Animal grease: 55%～65%
Sodium hydroxide: 5%～7%
Rosin: 3%～5%
Water glass: 5%～7%
Water: its proportional quantity and above each composition percentage ratio sum are 100%,
B. the manufacture method of cold-drawing antirust lubricating agent is undertaken by following program:
At first get water in the cold-drawing antirust lubricating agent proportional quantity 3/4, water is inserted in the reactor, add rosin thereupon, making reactor be warming up to rosin again can consoluet temperature,
Simultaneously, in the another one container, water and water glass stirred with 1/3 of the proportional quantity of water in the cold-drawing antirust lubricating agent,
Animal grease is added in the reactor again and mix with rosin solution, and be heated to 100 ℃～105 ℃, add strong mixing, the control Heating temperature is at 105 ℃～110 ℃, after half an hour, adds in advance and water blended water glass, stir,
At last, when the question response temperature in the kettle is increased to 120 ℃, slowly in reactor, add sodium hydroxide, add strong mixing, maintain the temperature in 140 ℃～150 ℃ scopes, 1.5 hour～after 2 hours, begin to cool down, go out still when solution is for paste to reactor, be cooled to normal temperature shape following time, will doubt solid solid stripping and slicing packing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 93103940 CN1031756C (en) | 1993-04-02 | 1993-04-02 | Cold-drawing antirust lubricating agent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 93103940 CN1031756C (en) | 1993-04-02 | 1993-04-02 | Cold-drawing antirust lubricating agent |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1091464A true CN1091464A (en) | 1994-08-31 |
| CN1031756C CN1031756C (en) | 1996-05-08 |
Family
ID=4984916
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 93103940 Expired - Fee Related CN1031756C (en) | 1993-04-02 | 1993-04-02 | Cold-drawing antirust lubricating agent |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1031756C (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1039821C (en) * | 1996-04-11 | 1998-09-16 | 株洲电力机车工厂 | Multipurpose water-base cutting fluid |
| CN1040124C (en) * | 1995-04-21 | 1998-10-07 | 株式会社日立制作所 | Lubricant oil composition and lubricant grease composition |
| CN101935582A (en) * | 2010-09-23 | 2011-01-05 | 王程玉 | Production process of lubricant for cold drawn seamless steel tube |
| CN105779097A (en) * | 2016-04-19 | 2016-07-20 | 常州市蓝勖化工有限公司 | Method for preparing high-temperature-resistant grease |
-
1993
- 1993-04-02 CN CN 93103940 patent/CN1031756C/en not_active Expired - Fee Related
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1040124C (en) * | 1995-04-21 | 1998-10-07 | 株式会社日立制作所 | Lubricant oil composition and lubricant grease composition |
| CN1039821C (en) * | 1996-04-11 | 1998-09-16 | 株洲电力机车工厂 | Multipurpose water-base cutting fluid |
| CN101935582A (en) * | 2010-09-23 | 2011-01-05 | 王程玉 | Production process of lubricant for cold drawn seamless steel tube |
| CN105779097A (en) * | 2016-04-19 | 2016-07-20 | 常州市蓝勖化工有限公司 | Method for preparing high-temperature-resistant grease |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1031756C (en) | 1996-05-08 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CA2258638C (en) | Waterborne lubricant for the cold plastic working of metals | |
| CA1052367A (en) | Lubricant coating compositions for use in metal drawing operations | |
| CN102268320B (en) | Food-grade lubricating grease as well as preparation method and application thereof | |
| CN1077594C (en) | Composite lithium- and calcium-base lubricating grease and its preparation | |
| AU604395B2 (en) | Process for phosphating metal surfaces | |
| JPS6328478B2 (en) | ||
| CN1031756C (en) | Cold-drawing antirust lubricating agent | |
| JPS61291687A (en) | Lubricant for cold forging aluminum | |
| JP4054539B2 (en) | Method for producing metal material for plastic working having inclined two-layer lubricating film | |
| US2074224A (en) | Drawing wire | |
| JPS6156275B2 (en) | ||
| JPS6295396A (en) | Pressing and anticorrosive oil | |
| CN102618377B (en) | Air conditioner copper threaded tube rolling lubricating fluid, preparation method and using method | |
| US2377106A (en) | Lubricant and process for preparing and using same | |
| JPS6019357B2 (en) | Lubricant for cold working of metals | |
| CN1202225C (en) | Lubricant for cold drawing of metal and its preparing process | |
| CA1311462C (en) | Process for lubricating the surface of metal parts, made of copper or of iron- or copper- based alloys, to be cold or warm worked and means of lubrication implemented | |
| JP2002361302A (en) | Method for rolling metal material plate | |
| US2070014A (en) | Solid lubricants and method of manufacturing the same | |
| CN1435472A (en) | Lubricating oil composition for wide steel strip hot continuous mill rolling process | |
| SU1268610A1 (en) | Lubricant for plastic cold working of metals | |
| CN106520282A (en) | Preparation method for low-noise bearing anti-rust oil | |
| CN1039054A (en) | Rust-proof cold-drawing lubricant | |
| JPS62190294A (en) | Pinion for automobile | |
| CN86102438A (en) | A kind of water-base nondrip cutting liquid |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C19 | Lapse of patent right due to non-payment of the annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |