CN109127165A - It is a kind of for producing the centrifuge of performance characteristics composite polyimide material - Google Patents

It is a kind of for producing the centrifuge of performance characteristics composite polyimide material Download PDF

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Publication number
CN109127165A
CN109127165A CN201811255803.6A CN201811255803A CN109127165A CN 109127165 A CN109127165 A CN 109127165A CN 201811255803 A CN201811255803 A CN 201811255803A CN 109127165 A CN109127165 A CN 109127165A
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China
Prior art keywords
centrifuge
reactor
inner cavity
center
heat
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CN201811255803.6A
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CN109127165B (en
Inventor
丁恒毅
丁兆龙
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Zhenjiang Longcheng Insulation Material Co Ltd
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Zhenjiang Longcheng Insulation Material Co Ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B04CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
    • B04BCENTRIFUGES
    • B04B5/00Other centrifuges
    • B04B5/12Centrifuges in which rotors other than bowls generate centrifugal effects in stationary containers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B04CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
    • B04BCENTRIFUGES
    • B04B15/00Other accessories for centrifuges
    • B04B15/02Other accessories for centrifuges for cooling, heating, or heat insulating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B04CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
    • B04BCENTRIFUGES
    • B04B9/00Drives specially designed for centrifuges; Arrangement or disposition of transmission gearing; Suspending or balancing rotary bowls
    • B04B9/08Arrangement or disposition of transmission gearing ; Couplings; Brakes

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  • Centrifugal Separators (AREA)

Abstract

The present invention relates to centrifuge technique fields, more particularly to a kind of for producing the centrifuge of performance characteristics composite polyimide material, including reactor, the center of top of reactor is equipped with shock mount, the center of top of shock mount is equipped with motor cover, the inner cavity center of motor cover is equipped with centrifuge, the inner cavity center of shock mount is equipped with magnetic coupling, the bottom power output end of centrifuge is connected by shaft with the top copper rotor of magnetic coupling, the inner cavity top center of reactor is equipped with working shaft, the top of working shaft is connected with the bottom p-m rotor of magnetic coupling, the bottom of working shaft is equipped with shaft coupling, the bottom of shaft coupling is equipped with connecting column, the bottom of connecting column is fixedly connected with Electrohydraulic push rod, the bottom end of Electrohydraulic push rod is connected with blender;The present invention can effectively overcome polyimides production traditional present in the prior art not can control operating temperature and the strong defect of shaking force with centrifuge mechanism.

Description

It is a kind of for producing the centrifuge of performance characteristics composite polyimide material
Technical field
The present invention relates to centrifuge technique fields, and in particular to one kind is for producing performance characteristics polyimides composite wood The centrifuge of material.
Background technique
Polyimides can be applied in many occasions as one of optimal high-molecular organic material of current comprehensive performance It arrives, and has a vast market foreground.Polyimides synthetic method is mainly by molten in polarity by dianhydride and diamines at present Agent, such as DMF, DMAC first carry out low-temperature polycondensation in NMP or THE/ methanol mixed solvent, obtain soluble polyamic acid, film forming or It is heated to 300 DEG C or so dehydration cyclization after spinning and is changed into polyimides;Acetic anhydride and tertiary amine can also be added into polyamic acid Class catalyst carries out chemical dehydration cyclisation, obtains polyimide solution and powder, has related to the step being separated by solid-liquid separation among these Suddenly.
It is main at present to be separated by solid-liquid separation by the way of centrifugation, the polyimide solution of synthesis and powder are separated Come, isolated effect determines the purity and performance of the polyimides of synthesis.But also there are many problems, polyimide solution is tool There is viscosity, when carrying out centrifugal solid-liquid separation, it may appear that the phenomenon that separation is not deposited, and polyimides is very stringent to temperature requirement, If default reaction temperature is not achieved in temperature, the polyimides performance of synthesis also will receive influence.
Therefore, there is an urgent need to a kind of Multifunctional centrifuges, can control the height of temperature, reduce shaking force, and be centrifuged effect Fruit is prominent.
Summary of the invention
(1) the technical issues of solving
For disadvantages mentioned above present in the prior art, it is multiple for producing performance characteristics polyimides that the present invention provides one kind The centrifuge of condensation material can effectively overcome polyimides production centrifuge mechanism traditional present in the prior art cannot Control operating temperature and the strong defect of shaking force.
(2) technical solution
In order to achieve the above object, the present invention is achieved by the following technical programs:
It is a kind of for producing the centrifuge of performance characteristics composite polyimide material, including reactor, the top of the reactor Portion center is equipped with shock mount, and the center of top of the shock mount is equipped with motor cover, and the inner cavity center of the motor cover is equipped with centrifugation Machine, the inner cavity center of the shock mount are equipped with magnetic coupling, and the bottom power output end of the centrifuge passes through shaft and magnetic The top copper rotor of mechanical couple is connected, and the inner cavity top center of the reactor is equipped with working shaft, the top of the working shaft It is connected with the bottom p-m rotor of magnetic coupling, the bottom of the working shaft is equipped with shaft coupling, and the bottom of the shaft coupling is set There is connecting column, the bottom of the connecting column is fixedly connected with Electrohydraulic push rod, and the bottom end of the Electrohydraulic push rod is connected with blender, institute The left and right sides central symmetry for stating reactor is equipped with cooling mechanism, and the intracavity bottom of the reactor is equipped in convex shape structure Heating element, the bottom of the reactor are equipped with U-shaped seat, and the bottom of the U-shaped seat is connected with shockproof bottom plate, the U-shaped seat and The inner cavity center of shockproof bottom plate is embedded with heater, is electrically connected between the heating element and heater.
Preferably, the cooling mechanism includes heat-conducting plate, thermal trough, thermal insulation board, two groups of Miniature retractable bars, connecting plate, dissipates Hot plate, heat conductive rod, two groups of attachment bases.
Preferably, the heat-conducting plate is set to the inner wall center of reactor, side wall of the thermal insulation board through reactor And fit with the side wall of heat-conducting plate, the thermal trough uniform intervals through thermal insulation board inner cavity and extend to the side of heat-conducting plate Wall, the attachment base two sides symmetrical above and below up and down for being set to thermal insulation board, and the left side wall center of two sides attachment base connects up and down It is connected to Miniature retractable bar, the end of upper and lower two sides Miniature retractable bar is connected with connecting plate, and the heat sink is set to connecting plate Left-side center, the right side of the connecting plate, which is uniformly run through, is connected with heat conductive rod, and the heat conductive rod, which runs through, is sticked in the interior of thermal trough Chamber.
Preferably, the Miniature retractable bar is electrically connected with controller, and the output end and heater of the controller are electrical Connection, the input terminal of the controller are electrically connected with temperature-sensing probe, and the temperature-sensing probe is set to the inner cavity top of reactor.
Preferably, the output end of the controller is wirelessly connected with Digiplex by wireless receiver.
Preferably, the inner cavity of the heat conductive rod is inoculated with conduction oil.
The present invention have also been devised it is a kind of for producing the application of the centrifuge of performance characteristics composite polyimide material, from Magnetic coupling 5 is arranged in the bottom power output end of scheming 4, by magnetic coupling 5 by the shaft and working shaft on centrifuge 4 6 is attracted, and magnetic coupling 5 is set to the inner cavity of shock mount 2, so that centrifuge 4 reduces vibration force in the process of work Influence, improve service efficiency simultaneously prolong the service life, the left and right sides inner wall center of reactor 1 pass through heat-conducting plate 110 will Temperature is transferred to outside reactor 1, and thermal insulation board 112 completely cuts off temperature, avoids the heat-conducting plate 110 during heater 13 works will Temperature is transferred to outside, so that heating process slows down and by temperature Centralized between thermal insulation board 112 and heat-conducting plate 110, thermal insulation board 112 inner cavity is equipped at intervals with thermal trough 111, and thermal trough 111 is connected with heat-conducting plate 110, and will by adjusting Miniature retractable bar 113 The insertion of heat conductive rod 116 111 inner cavity of thermal trough progress is thermally conductive, and the side of heat sink 115 is connected with the end of heat conductive rod 116, and leads The inner cavity of hot pin 116 is inoculated with conduction oil, and convenient for heat is quickly transferred to outside, temperature-sensing probe, control are equipped with inside reactor 1 Device finds out temperature information by temperature-sensing probe, and controls controller to heater 13 or Miniature retractable bar by Digiplex 113 are adjusted, to cool down or to heat up.
(3) beneficial effect
Compared with prior art, provided by the present invention a kind of for producing the centrifugation of performance characteristics composite polyimide material Machine designs a kind of Novel centrifuge in such a way that multiple functions combine, and has abandoned current traditional polyimides production and has used Centrifuge mechanism not can control operating temperature and the strong situation of shaking force, the present invention are set in the bottom power output end of centrifuge Set magnetic coupling, by magnetic coupling by centrifuge shaft and working shaft it is attracted, and magnetic coupling is set to The inner cavity of shock mount, so that centrifuge reduces the influence of vibration force in the process of work, in the left and right sides inner wall of reactor Temperature is transferred to outside reactor by heat-conducting plate by centre, and thermal insulation board completely cuts off temperature, is avoided during heater works Temperature is transferred to outside by heat-conducting plate, so that heating process slows down, the inner cavity of thermal insulation board is equipped at intervals with thermal trough, thermal trough with lead Hot plate be connected, and by adjust Miniature retractable bar by heat conductive rod be inserted into thermal trough inner cavity carry out it is thermally conductive, the side of heat sink with lead The end of hot pin is connected, and convenient for heat is quickly transferred to outside, inside reactor is equipped with temperature-sensing probe, and controller passes through temperature-sensitive Temperature information is found out, and controller is controlled by Digiplex, heater or Miniature retractable bar is adjusted, so as to Cooling or heating.
Detailed description of the invention
In order to more clearly explain the embodiment of the invention or the technical proposal in the existing technology, to embodiment or will show below There is attached drawing needed in technical description to be briefly described.It should be evident that the accompanying drawings in the following description is only this Some embodiments of invention for those of ordinary skill in the art without creative efforts, can be with It obtains other drawings based on these drawings.
Fig. 1 is schematic structural view of the invention;
Fig. 2 is Fig. 1 cooling mechanism structural schematic diagram;
In figure:
1, reactor;2, shock mount;3, motor cover;4, centrifuge;5, magnetic coupling;6, working shaft;7, connecting column;8, shaft coupling Device;9, Electrohydraulic push rod;10, blender;11, cooling mechanism;12, heating element;13, heater;14, U-shaped seat;15, shockproof bottom Plate;110, heat-conducting plate;111, thermal trough;112, thermal insulation board;113, Miniature retractable bar;114, connecting plate;115, heat sink;116, Heat conductive rod;117, attachment base.
Specific embodiment
In order to make the object, technical scheme and advantages of the embodiment of the invention clearer, below in conjunction with the embodiment of the present invention In attached drawing, technical scheme in the embodiment of the invention is clearly and completely described.Obviously, described embodiment is A part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, those of ordinary skill in the art Every other embodiment obtained without creative efforts, shall fall within the protection scope of the present invention.
It is a kind of for producing the centrifuge of performance characteristics composite polyimide material, as shown in Figs. 1-2, including reactor 1, the center of top of reactor 1 is equipped with shock mount 2, and the center of top of shock mount 2 is equipped with motor cover 3, the inner cavity center of motor cover 3 Equipped with centrifuge 4, the inner cavity center of shock mount 2 is equipped with magnetic coupling 5, and the bottom power output end of centrifuge 4 passes through shaft It is connected with the top copper rotor of magnetic coupling 5, the inner cavity top center of reactor 1 is equipped with working shaft 6, the top of working shaft 6 It is connected with the bottom p-m rotor of magnetic coupling 5, the bottom of working shaft 6 is equipped with shaft coupling 8, and the bottom of shaft coupling 8, which is equipped with, to be connected Column 7 is connect, the bottom of connecting column 7 is fixedly connected with Electrohydraulic push rod 9, and the bottom end of Electrohydraulic push rod 9 is connected with blender 10, reactor 1 Left and right sides central symmetry be equipped with cooling mechanism 11, the intracavity bottom of reactor 1 is equipped with the heating element in convex shape structure 12, the bottom of reactor 1 is equipped with U-shaped seat 14, and the bottom of U-shaped seat 14 is connected with shockproof bottom plate 15, U-shaped seat 14 and shockproof bottom plate 15 Inner cavity center be embedded with heater 13, be electrically connected between heating element 12 and heater 13;
Cooling mechanism 11 include heat-conducting plate 110, thermal trough 111,112, two groups of Miniature retractable bars 113 of thermal insulation board, connecting plate 114, 116, two groups of heat sink 115, heat conductive rod attachment bases 117;
Heat-conducting plate 110 is set to the inner wall center of reactor 1, side wall and and heat-conducting plate of the thermal insulation board 112 through reactor 1 110 side wall fits, 111 uniform intervals of thermal trough through thermal insulation board 112 inner cavity and extend to the side of heat-conducting plate 110 Wall, the two sides symmetrical above and below up and down for being set to thermal insulation board 112 of attachment base 117, and the left side wall center of two sides attachment base 117 up and down It is respectively connected with Miniature retractable bar 113, the end of upper and lower two sides Miniature retractable bar 113 is connected with connecting plate 114, and heat sink 115 is set It is placed in the left-side center of connecting plate 114, the right side of connecting plate 114, which is uniformly run through, is connected with heat conductive rod 116, and heat conductive rod 116 runs through It is sticked in the inner cavity of thermal trough 111;
Miniature retractable bar 113 is electrically connected with controller, and the output end and heater 13 of controller are electrically connected, controller it is defeated Enter end and be electrically connected with temperature-sensing probe, temperature-sensing probe is set to the inner cavity top of reactor 1;
The output end of controller is wirelessly connected with Digiplex by wireless receiver;
The inner cavity of heat conductive rod 116 is inoculated with conduction oil.
The course of work of the invention: magnetic coupling 5 is arranged in the bottom power output end of centrifuge 4, passes through magnetic coupling Device 5 by centrifuge 4 shaft and working shaft 6 it is attracted, and magnetic coupling 5 is set to the inner cavity of shock mount 2, so that centrifugation Machine 4 reduces the influence of vibration force in the process of work, improves service efficiency and prolongs the service life, the left and right two of reactor 1 Side inner wall center passes through heat-conducting plate 110 and temperature is transferred to outside reactor 1, and thermal insulation board 112 completely cuts off temperature, avoids heating Temperature is transferred to outside by heat-conducting plate 110 during device 13 works, so that heating process slows down and by temperature Centralized heat-insulated Between plate 112 and heat-conducting plate 110, the inner cavity of thermal insulation board 112 is equipped at intervals with thermal trough 111, thermal trough 111 and 110 phase of heat-conducting plate Even, and by adjusting Miniature retractable bar 113 heat conductive rod 116 is inserted into 111 inner cavity of thermal trough thermally conductive, the side of heat sink 115 of progress Face is connected with the end of heat conductive rod 116, and the inner cavity of heat conductive rod 116 is inoculated with conduction oil, convenient for heat is quickly transferred to outside, Temperature-sensing probe is equipped with inside reactor 1, controller finds out temperature information by temperature-sensing probe, and controls and control by Digiplex Heater 13 or Miniature retractable bar 113 is adjusted in device processed, to cool down or to heat up.
A kind of centrifuge for producing performance characteristics composite polyimide material provided by the present invention is using a variety of The mode that function combines designs a kind of Novel centrifuge, has abandoned current traditional polyimides production centrifuge mechanism Operating temperature and the strong situation of shaking force are not can control, magnetic coupling is arranged in the bottom power output end of centrifuge in the present invention Device, by magnetic coupling by centrifuge shaft and working shaft it is attracted, and magnetic coupling is set to the interior of shock mount Chamber, so that centrifuge reduces the influence of vibration force in the process of work, the left and right sides inner wall center of reactor, which passes through, is led Temperature is transferred to outside reactor by hot plate, thermal insulation board completely cut off temperature, avoid heater work during heat-conducting plate will be warm Degree is transferred to outside, so that heating process slows down, the inner cavity of thermal insulation board is equipped at intervals with thermal trough, and thermal trough is connected with heat-conducting plate, And heat conductive rod is inserted into thermal trough inner cavity progress thermally conductive, the side of heat sink and the end of heat conductive rod by adjusting Miniature retractable bar It is connected, convenient for heat is quickly transferred to outside, inside reactor is equipped with temperature-sensing probe, and controller finds out temperature by temperature-sensing probe Information is spent, and controller is controlled by Digiplex, heater or Miniature retractable bar is adjusted, to cool down or to heat up.
The above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations;Although with reference to the foregoing embodiments Invention is explained in detail, those skilled in the art should understand that: it still can be to aforementioned each implementation Technical solution documented by example is modified or equivalent replacement of some of the technical features;And these modification or Replacement, can't be such that the essence of corresponding technical solution departs from the spirit and scope of the technical scheme of various embodiments of the present invention.

Claims (6)

1. a kind of for producing the centrifuge of performance characteristics composite polyimide material, it is characterised in that: including reactor (1), the center of top of the reactor (1) is equipped with shock mount (2), and the center of top of the shock mount (2) is equipped with motor cover (3), the inner cavity center of the motor cover (3) is equipped with centrifuge (4), and the inner cavity center of the shock mount (2) is equipped with magnetic coupling The bottom power output end of device (5), the centrifuge (4) is connected by shaft with the top copper rotor of magnetic coupling (5), institute The inner cavity top center for stating reactor (1) is equipped with working shaft (6), the top of the working shaft (6) and the bottom of magnetic coupling (5) Portion's p-m rotor is connected, and the bottom of the working shaft (6) is equipped with shaft coupling (8), and the bottom of the shaft coupling (8) is equipped with connecting column (7), the bottom of the connecting column (7) is fixedly connected with Electrohydraulic push rod (9), and the bottom end of the Electrohydraulic push rod (9) is connected with stirring The left and right sides central symmetry of device (10), the reactor (1) is equipped with cooling mechanism (11), the interior bottom of chamber of the reactor (1) Portion is equipped with the heating element (12) in convex shape structure, and the bottom of the reactor (1) is equipped with U-shaped seat (14), the U-shaped seat (14) bottom is connected with shockproof bottom plate (15), and the inner cavity center of the U-shaped seat (14) and shockproof bottom plate (15) is embedded with heater (13), it is electrically connected between the heating element (12) and heater (13).
2. it is according to claim 1 a kind of for producing the centrifuge of performance characteristics composite polyimide material, it is special Sign is: the cooling mechanism (11) includes heat-conducting plate (110), thermal trough (111), thermal insulation board (112), two groups of Miniature retractable bars (113), connecting plate (114), heat sink (115), heat conductive rod (116), two groups of attachment bases (117).
3. it is according to claim 2 a kind of for producing the centrifuge of performance characteristics composite polyimide material, it is special Sign is: the heat-conducting plate (110) is set to the inner wall center of reactor (1), and the thermal insulation board (112) is through reactor (1) side wall simultaneously fits with the side wall of heat-conducting plate (110), and thermal trough (111) uniform intervals are through thermal insulation board (112) Inner cavity and extend to the side walls of heat-conducting plate (110), the attachment base (117) is symmetrical above and below to be set to the upper of thermal insulation board (112) Lower two sides, and the left side wall center of two sides attachment base (117) is respectively connected with Miniature retractable bar (113) up and down, upper and lower two sides are miniature The end of telescopic rod (113) is connected with connecting plate (114), and the heat sink (115) is set in the left side of connecting plate (114) Centre, the right side of the connecting plate (114), which is uniformly run through, to be connected with heat conductive rod (116), and the heat conductive rod (116), which runs through to be sticked in, leads The inner cavity of heat channel (111).
4. it is according to claim 3 a kind of for producing the centrifuge of performance characteristics composite polyimide material, it is special Sign is: the Miniature retractable bar (113) is electrically connected with controller, and the output end of the controller and heater (13) are electrically Connection, the input terminal of the controller are electrically connected with temperature-sensing probe, and the temperature-sensing probe is set to the inner cavity top of reactor (1) Portion.
5. it is according to claim 4 a kind of for producing the centrifuge of performance characteristics composite polyimide material, it is special Sign is: the output end of the controller is wirelessly connected with Digiplex by wireless receiver.
6. it is according to claim 2 a kind of for producing the centrifuge of performance characteristics composite polyimide material, it is special Sign is: the inner cavity of the heat conductive rod (116) is inoculated with conduction oil.
CN201811255803.6A 2018-10-26 2018-10-26 Centrifugal machine for producing polyimide composite material with high performance characteristics Active CN109127165B (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110806626A (en) * 2019-11-20 2020-02-18 杭州昱华科技有限公司 Core direct-melting type optical cable cross-connecting box

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GB566477A (en) * 1943-09-03 1945-01-01 Western States Machine Co Improvements in or relating to suspended centrifugal machines
GB1262961A (en) * 1968-02-26 1972-02-09 Physik Chem Forschungs Inst Pr Apparatus for the separating of flowable mixtures of components of different weights under the influence of centrifugal force
US20090206186A1 (en) * 2004-01-16 2009-08-20 Michael Joseph Morrison Processing Apparatus and Methods
CN204974220U (en) * 2015-09-21 2016-01-20 广东能标检测技术服务有限公司 Desk -top high -speed centrifuge
CN205253377U (en) * 2015-12-24 2016-05-25 太仓市微贯机电有限公司 Novel miniature centrifugal separator
CN206199496U (en) * 2016-11-07 2017-05-31 南阳师范学院 A kind of efficient centrifugal machine
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WO2017141394A1 (en) * 2016-02-18 2017-08-24 エイブル株式会社 Reaction device capable of performing centrifugation
CN206549848U (en) * 2017-01-20 2017-10-13 镇江亿清复合材料有限公司 A kind of centrifuge for being used to produce high-performance special composite polyimide material
CN209093623U (en) * 2018-10-26 2019-07-12 镇江龙成绝缘材料有限公司 It is a kind of for producing the centrifuge of performance characteristics composite polyimide material

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GB566477A (en) * 1943-09-03 1945-01-01 Western States Machine Co Improvements in or relating to suspended centrifugal machines
GB1262961A (en) * 1968-02-26 1972-02-09 Physik Chem Forschungs Inst Pr Apparatus for the separating of flowable mixtures of components of different weights under the influence of centrifugal force
US20090206186A1 (en) * 2004-01-16 2009-08-20 Michael Joseph Morrison Processing Apparatus and Methods
US20170189916A1 (en) * 2014-05-23 2017-07-06 Andreas Hettich Gmbh & Co. Kg Centrifuge
CN204974220U (en) * 2015-09-21 2016-01-20 广东能标检测技术服务有限公司 Desk -top high -speed centrifuge
CN205253377U (en) * 2015-12-24 2016-05-25 太仓市微贯机电有限公司 Novel miniature centrifugal separator
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110806626A (en) * 2019-11-20 2020-02-18 杭州昱华科技有限公司 Core direct-melting type optical cable cross-connecting box

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