CN109112624A - It is a kind of for producing the polycrystalline furnace of solar level high-efficiency polycrystalline silicon wafer - Google Patents

It is a kind of for producing the polycrystalline furnace of solar level high-efficiency polycrystalline silicon wafer Download PDF

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Publication number
CN109112624A
CN109112624A CN201710488874.XA CN201710488874A CN109112624A CN 109112624 A CN109112624 A CN 109112624A CN 201710488874 A CN201710488874 A CN 201710488874A CN 109112624 A CN109112624 A CN 109112624A
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CN
China
Prior art keywords
furnace body
outer cylinder
furnace
cooling water
flange
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Pending
Application number
CN201710488874.XA
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Chinese (zh)
Inventor
余刚
丁一
王剑
姚玖洪
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ZHENJIANG RENDE NEW ENERGY TECHNOLOGY Co Ltd
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ZHENJIANG RENDE NEW ENERGY TECHNOLOGY Co Ltd
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Priority to CN201710488874.XA priority Critical patent/CN109112624A/en
Publication of CN109112624A publication Critical patent/CN109112624A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B28/00Production of homogeneous polycrystalline material with defined structure
    • C30B28/12Production of homogeneous polycrystalline material with defined structure directly from the gas state
    • C30B28/14Production of homogeneous polycrystalline material with defined structure directly from the gas state by chemical reaction of reactive gases
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/02Elements
    • C30B29/06Silicon

Abstract

The present invention provides a kind of for producing the polycrystalline furnace of solar level high-efficiency polycrystalline silicon wafer, including furnace body inner cylinder, furnace body outer cylinder, and the helical form deflector in the interlayer cavity being set between the furnace body inner cylinder and furnace body outer cylinder;Furnace body outer cylinder bottom is provided with the first cooling water inlet, can import cooling water in the interlayer cavity between furnace body inner cylinder and furnace body outer cylinder, and flow along helical form deflector spiral;It is provided with the first cooling water outlet at the top of the furnace body outer cylinder, the cooling water in the interlayer cavity between furnace body inner cylinder and furnace body outer cylinder can be exported.The pressure (hydraulic) water water conservancy diversion of in-furnace temperature and furnace body can be maintained cooling and the local water cooling of double glass viewing mirror.

Description

It is a kind of for producing the polycrystalline furnace of solar level high-efficiency polycrystalline silicon wafer
Technical field
The present invention relates to the polycrystalline furnaces of production solar level high-efficiency polycrystalline silicon wafer.
Background technique
Currently, the production technology for preparing silicon for solar cell ingot mainly includes that pulling single crystal silicon and polysilicon are drawn.It is more Crystal silicon ingot casting technology due to can directly founding go out to be suitable for the square silicon ingot of large-scale production, manufacturing process it is relatively easy, from forming For the main stream approach of silicon for solar cell ingot preparation.Polycrystalline silicon ingot casting technology is usually applied in polycrystalline furnace.
Reduction furnace is the core equipment and decision systems production capacity energy consumption, environmental protection index for producing polysilicon, and reliably, The key factor of safety.Trichlorosilane restores in polycrystalline furnace generates polycrystalline silicon rod, while also generating silicon tetrachloride, chlorination Hydrogen, hydrogen etc..Untreated silicon tetrachloride is a kind of liquid for having extremely strong corrosivity, being difficult to save.By by silicon tetrachloride Continuous hydrogenation generates the recycling such as trichlorosilane, hydrogen chloride and uses in hydrogenation furnace, can recycle benefit with rectifying by repeatedly recycling With most silicon, reduces cost, reduces pollution.In addition to a small number of producers, most domestic does not all build up tail gas hydrogenation recycling system System, causes China's production of polysilicon cost to remain high, and seriously polluted.
It is hydrogenating and is restoring in process, electric energy heating electrode is needed to maintain 1000 DEG C or more the conditions of high temperature in furnace, thus it is more The safe handling and service life of the cooling direct relation reacting furnace of crystalline substance reaction furnace body.
Summary of the invention
In view of the problems of the existing technology, the present invention provides a kind of for producing the more of solar level high-efficiency polycrystalline silicon wafer Brilliant furnace can maintain the pressure (hydraulic) water water conservancy diversion of in-furnace temperature and furnace body cooling and the local water cooling of double glass viewing mirror.
The technical scheme is that a kind of for producing the polycrystalline furnace of solar level high-efficiency polycrystalline silicon wafer, including furnace body Helical form deflector in inner cylinder, furnace body outer cylinder, and the interlayer cavity that is set between the furnace body inner cylinder and furnace body outer cylinder;Institute It states furnace body outer cylinder bottom and is provided with the first cooling water inlet, cooling water can be imported to the folder between furnace body inner cylinder and furnace body outer cylinder In layer cavity, and flowed along helical form deflector spiral;The first cooling water outlet, energy are provided at the top of the furnace body outer cylinder Enough cooling waters by the interlayer cavity between furnace body inner cylinder and furnace body outer cylinder export.
Further, bottom of furnace body is provided with flange in the bottom.
Further, water-cooling double glass viewing mirror is provided on furnace body.
Further, the water-cooling double glass viewing mirror includes passing through spaced glass outer and inner glass, institute It states and passes through casing off between glass outer and inner glass;Second flange, the second flange one are cased on the outside of described sleeve pipe Side is provided with third cooling water inlet, and the opposite other side is provided with third cooling water outlet.
Further, the two sides of the second flange axial direction are respectively arranged with first flange and third flange, and described first Flange, second flange and third flange are fixedly connected by screw bolt and nut.
Further, the inner glass is provided with the double glass viewing mirror inner cylinder that can pass through furnace body towards furnace body side With double glass viewing mirror outer cylinder;Double glass viewing mirror outer cylinder side is provided with the second cooling water inlet, can be by cooling water It imports in the interlayer cavity between double glass viewing mirror inner cylinder and double glass viewing mirror outer cylinder;The double glass viewing mirror outer cylinder phase Pair the other side be provided with the second cooling water outlet, can will be between double glass viewing mirror inner cylinder and double glass viewing mirror outer cylinder Cooling water export in interlayer cavity.
The beneficial effects of the present invention are: inside, in outer cylinder sealing cavity be arranged helical form deflector, pressurize cooling water in sky It is intracavitary to be flowed along deflector direction, inner cylinder, the external visor of furnace body are cooled down, guarantee its work at reliable temperature Make.Water-cooling double glass viewing mirror is set on outer cylinder, it can be with the growing state of silicon rod in inspection section body by visor.It can maintain furnace Interior temperature, and guarantee the local water cooling of pressure (hydraulic) water the water conservancy diversion cooling and double glass viewing mirror of furnace body.
Detailed description of the invention
Fig. 1 is overall structure diagram of the invention;
Fig. 2 is the structure chart of water-cooling double glass viewing mirror.
In figure: 1 is the first cooling water outlet, and 2 be furnace body inner cylinder, and 3 be furnace body outer cylinder, and 4 be deflector, and 5 be water cooled double-layered Glass mirror, 6 be the first cooling water inlet, and 7 be flange in the bottom, and 8 be the second cooling water inlet, and 9 be third cooling water inlet, 10 It is bolt for nut, 11,12 be glass outer, and 13 be inner glass, and 14 be first flange, and 15 be second flange, and 16 be third Cooling water outlet, 17 be third flange, and 18 be the second cooling water outlet, and 19 be double glass viewing mirror inner cylinder, and 20 be double glazing Visor outer cylinder.
Specific embodiment
Following further describes the present invention with reference to the drawings.
As shown in Figure 1, a kind of for producing the polycrystalline furnace of solar level high-efficiency polycrystalline silicon wafer, including furnace body inner cylinder 2, furnace body Helical form deflector 4 in outer cylinder 3, and the interlayer cavity that is set between furnace body inner cylinder 2 and furnace body outer cylinder 3.Bottom of furnace body is set It is equipped with flange in the bottom 7.3 bottom of furnace body outer cylinder is provided with the first cooling water inlet 6, cooling water can be imported 2 He of furnace body inner cylinder In interlayer cavity between furnace body outer cylinder 3, and flowed along 4 spiral of helical form deflector.Is provided at the top of furnace body outer cylinder 3 One cooling water outlet 1 can export the cooling water in the interlayer cavity between furnace body inner cylinder 2 and furnace body outer cylinder 3.
As shown in Fig. 2, being provided with water-cooling double glass viewing mirror 5 on furnace body.Water-cooling double glass viewing mirror 5 includes passing through interval The glass outer 12 and inner glass 13 of setting, pass through casing off between glass outer 12 and inner glass 13.Outside of sleeve It is cased with second flange 15,15 side of second flange is provided with third cooling water inlet 9, and it is cooling that the opposite other side is provided with third Water out 16.
Inner glass 13 is provided with the double glass viewing mirror inner cylinder 19 and the double-deck glass that can pass through furnace body towards furnace body side Glass visor outer cylinder 20.20 side of double glass viewing mirror outer cylinder is provided with the second cooling water inlet 8, can import cooling water double-deck In interlayer cavity between glass mirror inner cylinder 19 and double glass viewing mirror outer cylinder 20.Opposite another of double glass viewing mirror outer cylinder 20 Side is provided with the second cooling water outlet 18, can will be between double glass viewing mirror inner cylinder 19 and double glass viewing mirror outer cylinder 20 Cooling water export in interlayer cavity.
As preferred embodiment, the axial two sides of second flange 15 are respectively arranged with first flange 14 and third flange 17, first flange 14, second flange 15 and third flange 17 are fixedly connected by bolt 11 with nut 10.
The present invention can maintain the pressure (hydraulic) water water conservancy diversion of in-furnace temperature and furnace body cooling and the office of double glass viewing mirror Portion's water cooling.
The above is only a preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art For member, various improvements and modifications may be made without departing from the principle of the present invention, these improvements and modifications are also answered It is considered as protection scope of the present invention.

Claims (6)

1. a kind of for producing the polycrystalline furnace of solar level high-efficiency polycrystalline silicon wafer, it is characterised in that: including furnace body inner cylinder (2), furnace Helical form deflector in external cylinder (3), and the interlayer cavity that is set between the furnace body inner cylinder (2) and furnace body outer cylinder (3) (4);Furnace body outer cylinder (3) bottom is provided with the first cooling water inlet (6), can by cooling water import furnace body inner cylinder (2) and In interlayer cavity between furnace body outer cylinder (3), and flowed along helical form deflector (4) spiral;Furnace body outer cylinder (3) top Portion is provided with the first cooling water outlet (1), can will be cold in the interlayer cavity between furnace body inner cylinder (2) and furnace body outer cylinder (3) But water exports.
2. according to claim 1 a kind of for producing the polycrystalline furnace of solar level high-efficiency polycrystalline silicon wafer, it is characterised in that: Bottom of furnace body is provided with flange in the bottom (7).
3. according to claim 1 a kind of for producing the polycrystalline furnace of solar level high-efficiency polycrystalline silicon wafer, it is characterised in that: Water-cooling double glass viewing mirror (5) are provided on furnace body.
4. according to claim 3 a kind of for producing the polycrystalline furnace of solar level high-efficiency polycrystalline silicon wafer, it is characterised in that: The water-cooling double glass viewing mirror (5) includes passing through spaced glass outer (12) and inner glass (13), the outer layer Pass through casing off between glass (12) and inner glass (13);It is cased with second flange (15) on the outside of described sleeve pipe, described second Flange (15) side is provided with third cooling water inlet (9), and the opposite other side is provided with third cooling water outlet (16).
5. according to claim 4 a kind of for producing the polycrystalline furnace of solar level high-efficiency polycrystalline silicon wafer, it is characterised in that: The two sides of second flange (15) axial direction are respectively arranged with first flange (14) and third flange (17), the first flange (14), second flange (15) is fixedly connected by bolt (11) with nut (10) with third flange (17).
6. according to claim 4 a kind of for producing the polycrystalline furnace of solar level high-efficiency polycrystalline silicon wafer, it is characterised in that: The inner glass (13) is provided with the double glass viewing mirror inner cylinder (19) and the double-deck glass that can pass through furnace body towards furnace body side Glass visor outer cylinder (20);Double glass viewing mirror outer cylinder (20) side is provided with the second cooling water inlet (8), can be by cooling Water imports in the interlayer cavity between double glass viewing mirror inner cylinder (19) and double glass viewing mirror outer cylinder (20);The double glazing The opposite other side of visor outer cylinder (20) is provided with the second cooling water outlet (18), can by double glass viewing mirror inner cylinder (19) and Cooling water export in interlayer cavity between double glass viewing mirror outer cylinder (20).
CN201710488874.XA 2017-06-23 2017-06-23 It is a kind of for producing the polycrystalline furnace of solar level high-efficiency polycrystalline silicon wafer Pending CN109112624A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110983440A (en) * 2019-12-25 2020-04-10 南京晶升能源设备有限公司 Hydraulic power rotational flow cooling induction heating vacuum furnace body
CN112281212A (en) * 2020-11-10 2021-01-29 无锡双雄通用机械有限公司 Polycrystalline silicon growth furnace

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2003146641A (en) * 2001-11-20 2003-05-21 Sumitomo Titanium Corp Reaction furnace for manufacturing high-purity silicon and method of manufacturing high-purity silicon
CN201180088Y (en) * 2008-03-12 2009-01-14 江苏双良锅炉有限公司 Novel polysilicon reduction furnace for fast-open type, water cooling structure
CN201180089Y (en) * 2008-03-12 2009-01-14 江苏双良锅炉有限公司 Water cooling double-layer glass viewing mirror of novel polysilicon reduction furnace
CN102424387A (en) * 2011-09-06 2012-04-25 江苏中圣高科技产业有限公司 Uniform temperature type polysilicon reducing furnace

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2003146641A (en) * 2001-11-20 2003-05-21 Sumitomo Titanium Corp Reaction furnace for manufacturing high-purity silicon and method of manufacturing high-purity silicon
CN201180088Y (en) * 2008-03-12 2009-01-14 江苏双良锅炉有限公司 Novel polysilicon reduction furnace for fast-open type, water cooling structure
CN201180089Y (en) * 2008-03-12 2009-01-14 江苏双良锅炉有限公司 Water cooling double-layer glass viewing mirror of novel polysilicon reduction furnace
CN102424387A (en) * 2011-09-06 2012-04-25 江苏中圣高科技产业有限公司 Uniform temperature type polysilicon reducing furnace

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110983440A (en) * 2019-12-25 2020-04-10 南京晶升能源设备有限公司 Hydraulic power rotational flow cooling induction heating vacuum furnace body
CN112281212A (en) * 2020-11-10 2021-01-29 无锡双雄通用机械有限公司 Polycrystalline silicon growth furnace

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Application publication date: 20190101