CN109111214A - A kind of brick base coating material and preparation method thereof - Google Patents
A kind of brick base coating material and preparation method thereof Download PDFInfo
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- CN109111214A CN109111214A CN201811064058.7A CN201811064058A CN109111214A CN 109111214 A CN109111214 A CN 109111214A CN 201811064058 A CN201811064058 A CN 201811064058A CN 109111214 A CN109111214 A CN 109111214A
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/10—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on aluminium oxide
- C04B35/101—Refractories from grain sized mixtures
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/62222—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining ceramic coatings
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3418—Silicon oxide, silicic acids, or oxide forming salts thereof, e.g. silica sol, fused silica, silica fume, cristobalite, quartz or flint
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
- C04B2235/3463—Alumino-silicates other than clay, e.g. mullite
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/349—Clays, e.g. bentonites, smectites such as montmorillonite, vermiculites or kaolines, e.g. illite, talc or sepiolite
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/44—Metal salt constituents or additives chosen for the nature of the anions, e.g. hydrides or acetylacetonate
- C04B2235/447—Phosphates or phosphites, e.g. orthophosphate, hypophosphite
Abstract
The present invention relates to a kind of brick primers and preparation method thereof, the brick primer includes 50~100 parts of sintered bauxite, 0~50 part of cast alumin(i)um alumina, 0~10 part of kaolin, bentonite, at least one of cosmetic soil and porcelain mud, 0~20 part of fire resisting auxiliary material, 5~20 parts of binders and 50~100 parts of water, the brick primer is by by sintered bauxite, cast alumin(i)um alumina and fire resisting dressing, sieving, screen out 200 mesh raw material below, again by the raw material of sieving and kaolin, bentonite, ball mill is added with binder at least one of cosmetic soil and porcelain mud, grinding aid is added, it adds water, the fineness of mixing and ball milling to scheduled slurry is prepared, the brick primer can substantially eliminate ceramic tile bottom sieve frame print, it is greatly improved ceramic tile using effect, and preparation method is simple to operation, control is difficult Spend small, suitable industrialized production.
Description
Technical field
The present invention relates to a kind of preparation fields of coating, more particularly to a kind of brick base coating material and preparation method thereof.
Background technique
When ceramic tile production, for protection ceramic tile and roller stick, need to cover a coating in ceramic tile primary coat.This layer of brick primer category
In a kind of high-temperature refractory, good high temperature resistance is not only needed, it is also necessary in the entire firing from low temperature to high temperature
There is certain adhesiveness in the process, so brick primer has relatively high requirement to adhesion property.
Existing brick primer uses aluminium oxide, magnesia or composite refractory preparation substantially, to improve brick priming coat material
The adhesiveness of material in use, it is general to be handled using, slurrying levigate to brick base coating material, and superfine powder in brick priming coat
Presence, be the generation one of the main reasons for causing ceramic tile bottom sieve frame to print, and bottom sieve frame print is major defect in ceramic tile use process
One of, the use of ceramic tile is seriously affected, prevention and elimination ceramic tile bottom sieve frame print are entire ceramic industry problems to be solved.
Summary of the invention
Based on this, it is necessary to leading to the problem of bottom sieve frame print in ceramic tile production process, provide a kind of brick base coating material
And preparation method thereof.
A kind of brick primer, slurry include each raw material component of following parts by weight:
The slurry includes each raw material component of following parts by weight in one of the embodiments:
In one of the embodiments, the fineness of the slurry be 100 mesh screen residues less than 0.1% and 200 mesh screen residue be greater than
90%.
The fire resisting auxiliary material is at least one of emergy, mullite and quartz in one of the embodiments,.
The binder is at least one in aluminium dihydrogen phosphate, phosphoric acid and phosphoric acid hydrogen two aluminium in one of the embodiments,
Kind.
A kind of preparation method of brick primer, comprising the following steps:
Each raw material is taken by following parts by weight:
Again by sintered bauxite, cast alumin(i)um alumina and fire resisting auxiliary material, sieving screens out 200 mesh raw material below;
By the sintered bauxite, cast alumin(i)um alumina and fire resisting auxiliary material of sieving and the kaolin, bentonite, cosmetic soil and
At least one of porcelain mud, binder, grinding aid and water mixing and ball milling to scheduled slurry fineness.
The fineness of the scheduled slurry is 100 mesh screen residues less than 0.1% and 200 meshes in one of the embodiments,
It is remaining to be greater than 90%.
The fire resisting auxiliary material is at least one of emergy, mullite and quartz in one of the embodiments,.
The binder is at least one in aluminium dihydrogen phosphate, phosphoric acid and phosphoric acid hydrogen two aluminium in one of the embodiments,
Kind.
The grinding aid is at least one in sodium tripolyphosphate and sodium carboxymethylcellulose pyce in one of the embodiments,
Kind.
Compared with traditional technology, the invention has the following advantages: above-mentioned brick bottom material uses cast alumin(i)um alumina and wrought aluminium
Alumina is raw material, not only increased the paintability of brick primer but also increase eliminate brick face bottom sieve frame print effect, and emergy and
Kaolin is preferable refractory material, and emergy and kaolinic use make brick primer fire resisting effect prepared by the present invention more
It is good, ball milling is carried out to raw material in the preparation method of above-mentioned brick primer, and set slurry fineness requirement to be achieved, gram
It has taken and has occurred the problem of superfine powder in the slurry, what the brick primer coating brick bottom obtained by adopting the above technical scheme was fired
Ceramic tile, brick face has no that bottom sieve frame prints after tested.
Specific embodiment
It to facilitate the understanding of the present invention, below will be to invention is more fully described.But the present invention can be to be permitted
Mostly different form is realized, however it is not limited to embodiment described herein.On the contrary, purpose of providing these embodiments is makes
It is more thorough and comprehensive to the understanding of the disclosure.
Unless otherwise defined, all technical and scientific terms used herein and belong to technical field of the invention
The normally understood meaning of technical staff is identical.Term as used herein in the specification of the present invention is intended merely to description tool
The purpose of the embodiment of body, it is not intended that in the limitation present invention.
A kind of brick primer, slurry include each raw material component of following parts by weight:
Preferably, a kind of brick primer includes each raw material component of following parts by weight:
The effect for eliminating bottom sieve frame print can be increased in brick primer using sintered bauxite, and the use of cast alumin(i)um alumina makes brick bottom
Coating coats better effect during use, and sintered bauxite and cast alumin(i)um alumina make brick bottom material have both elimination
The effect of bottom sieve frame print and coating.
A kind of preparation method of brick primer, comprising the following steps:
Step S1: each raw material component is weighed.
Each raw material is taken by following parts by weight:
The fire resisting auxiliary material can be at least one of emergy, mullite and quartz;
The binder is at least one of aluminium dihydrogen phosphate, phosphoric acid and phosphoric acid hydrogen two aluminium.
Step S2: raw material sieving.
Again by sintered bauxite, cast alumin(i)um alumina and fire resisting auxiliary material, sieving screens out 200 mesh raw material below.
Step S3: ball milling slurry to certain fineness.
At least one of the raw material being sieved in step S2 and kaolin, bentonite, cosmetic soil and porcelain mud, binder are mixed
It closes, 0.1~0.8% part of grinding aid sodium tripolyphosphate is added or sodium carboxymethylcellulose pyce is 0.3~1.2% part or two kinds and grinds
Milling aid is used cooperatively, and is added water, be milled to fineness be 100 mesh screen residues less than 0.1% and 200 mesh screen residue be greater than 90% when stop
Only ball milling.
Finally, the consistency of water adjusting slurry can be added according to actual needs.
The following examples and comparative example will use following test mode:
Above-mentioned slurry is coated on ceramic tile ontology bottom, paint thickness is 0.05mm~1.0mm, is burnt with ceramic tile ontology
At;
Two blocks of ceramic tiles are taken, are stacked together, place counterweight on the ceramic tile of upper layer, so that lower layer's ceramic tile pressure is 1.765
± 0.1kPa is piled up 7 days under conditions of temperature is 25 ± 1 DEG C and humidity is 80 ± 5%, and observation brick face bottom sieve frame prints situation.
Below in conjunction with specific embodiment, the present invention is described in further detail.
Embodiment 1:
Sintered bauxite 100kg, kaolin 8kg, aluminium dihydrogen phosphate 15kg, water 80kg are weighed in parts by weight;
Sintered bauxite is sieved, screens out 200 mesh raw material below, and by sintered bauxite and kaolin, aluminium dihydrogen phosphate with
And water mixing and sodium tripolyphosphate 0.4kg ball milling, make fineness reach 100 mesh screen residues less than 0.1% and 200 mesh screen residue be greater than
Stop ball milling when 90%.
Above-mentioned slurry is coated on ceramic tile ontology bottom, paint thickness 0.1mm is burnt into ceramic tile ontology;
Two blocks of ceramic tiles are taken, are stacked together, place counterweight on the ceramic tile of upper layer, so that lower layer's ceramic tile pressure is 1.765
± 0.1kPa is piled up 7 days under conditions of temperature is 25 ± 1 DEG C and humidity is 80 ± 5%, and observation brick face bottom sieve frame prints situation.
It visually observes, brick face has no that bottom sieve frame prints.
Embodiment 2:
Sintered bauxite 70kg, cast alumin(i)um alumina 30kg, kaolin 3kg, emergy 5kg, biphosphate are weighed in parts by weight
Aluminium 5kg and water 100kg;
Sintered bauxite, cast alumin(i)um alumina and emergy are sieved, 200 mesh raw material below is screened out;
The raw material of sieving is mixed with kaolin aluminium dihydrogen phosphate and water again, and grinding aid sodium tripolyphosphate 0.4kg is added,
Sodium carboxymethylcellulose pyce 0.8Kg carry out ball milling, when the fineness of slurry reach 100 mesh screen residues less than 0.1% and 200 mesh screen residue be greater than
Stop ball milling when 90%;
Above-mentioned slurry is coated on ceramic tile ontology bottom, paint thickness 0.1mm is burnt into ceramic tile ontology;
Two blocks of ceramic tiles are taken, are stacked together, place counterweight on the ceramic tile of upper layer, so that lower layer's ceramic tile pressure is 1.765
± 0.1kPa is piled up 7 days under conditions of temperature is 25 ± 1 DEG C and humidity is 80 ± 5%, and observation brick face bottom sieve frame prints situation.
It visually observes, brick face has no that bottom sieve frame prints.
Embodiment 3:
Sintered bauxite 80kg, cast alumin(i)um alumina 20kg, porcelain mud 3kg, mullite 5kg, aluminium dihydrogen phosphate are weighed in parts by weight
8kg and water 90kg;
Sintered bauxite, cast alumin(i)um alumina and mullite are sieved, 200 mesh raw material below is screened out;
The raw material of sieving is mixed with porcelain mud aluminium dihydrogen phosphate and water again, and grinding aid sodium tripolyphosphate 0.4kg, first is added
Base sodium cellulosate 0.8Kg carry out ball milling, when the fineness of slurry reach 100 mesh screen residues less than 0.1% and 200 mesh screen residue be greater than 90%
When stop ball milling;
Above-mentioned slurry is coated on ceramic tile ontology bottom, paint thickness 0.1mm is burnt into ceramic tile ontology;
Two blocks of ceramic tiles are taken, are stacked together, place counterweight on the ceramic tile of upper layer, so that lower layer's ceramic tile pressure is 1.765
± 0.1kPa is piled up 7 days under conditions of temperature is 25 ± 1 DEG C and humidity is 80 ± 5%, and observation brick face bottom sieve frame prints situation.
It visually observes, brick face has no that bottom sieve frame prints.
Comparative example 1:
Sintered bauxite 70kg, cast alumin(i)um alumina 30kg, kaolin 3kg, emergy 5kg, biphosphate are weighed in parts by weight
Aluminium 5kg and water 100kg;
Each raw material is not sieved direct mixing, grinding aid sodium tripolyphosphate 0.4kg, sodium carboxymethylcellulose pyce 0.8Kg is added
Carry out ball milling, when the fineness of slurry reach 200 mesh screen residues less than 0.1% and 300 mesh screen residue be greater than 90% when stop ball milling;
Above-mentioned slurry is coated on ceramic tile ontology bottom, paint thickness 0.1mm is burnt into ceramic tile ontology;
Two blocks of ceramic tiles are taken, are stacked together, place counterweight on the ceramic tile of upper layer, so that lower layer's ceramic tile pressure is 1.765
± 0.1kPa, after piling up 7 days under conditions of temperature is 25 ± 1 DEG C and humidity is 80 ± 5%, observation brick face bottom sieve frame prints situation.
It visually observes, the visible obvious bottom sieve frame print in brick face.
Comparative example 2:
Sintered bauxite 30kg, cast alumin(i)um alumina 70kg, kaolin 3kg, emergy 5kg, biphosphate are weighed in parts by weight
Aluminium 5kg and water 100kg;
Sintered bauxite, cast alumin(i)um alumina and emergy are sieved, 200 mesh raw material below is screened out;
The raw material of sieving is mixed with kaolin aluminium dihydrogen phosphate and water again, and grinding aid sodium tripolyphosphate 0.4kg is added
Carry out ball milling, when the fineness of slurry reach 100 mesh screen residues less than 0.1% and 200 mesh screen residue be greater than 90% when stop ball milling;
Above-mentioned slurry is coated on ceramic tile ontology bottom, paint thickness 0.1mm is burnt into ceramic tile ontology;
Two blocks of ceramic tiles are taken, are stacked together, place counterweight on the ceramic tile of upper layer, so that lower layer's ceramic tile pressure is 1.765
± 0.1kPa is piled up 7 days under conditions of temperature is 25 ± 1 DEG C and humidity is 80 ± 5%, and observation brick face bottom sieve frame prints situation.
It visually observes, the visible apparent bottom sieve frame print in brick face.
Comparative example 3:
Magnesia 100kg, kaolin 8kg, emergy 5kg and water 100kg are weighed in parts by weight;
Raw material is not sieved processing, and grinding aid sodium tripolyphosphate 0.4kg is added, and sodium carboxymethylcellulose pyce 0.8Kg adds water 90kg,
It carries out levigate to 200 mesh screen residue < 10%, slurry is made;
Above-mentioned slurry is coated on ceramic tile ontology bottom, paint thickness 0.1mm is burnt into ceramic tile ontology;
Two blocks of ceramic tiles are taken, are stacked together, place counterweight on the ceramic tile of upper layer, so that lower layer's ceramic tile pressure is 1.765
± 0.1kPa is piled up 7 days under conditions of temperature is 25 ± 1 DEG C and humidity is 80 ± 5%, and observation brick face bottom sieve frame prints situation.
It visually observes, the visible apparent bottom sieve frame print in brick face.
The fineness of slurry is printed on influence to ceramic tile bottom sieve frame is eliminated it can be seen from embodiment 2 and comparative example 1, works as slurry
The fineness of material be fineness reach 100 mesh screen residues less than 0.1% and 200 mesh screen residue be greater than 90% when just there is not bottom sieve frame print, when
The fineness of slurry be 200 mesh screen residues less than 0.1% and 300 mesh screen residue be greater than 90% when ceramic tile bottom sieve frame print it is obvious, by 2 He of embodiment
The weight fraction ratio that comparative example 2 can be seen that sintered bauxite and cast alumin(i)um alumina also has an impact to ceramic tile bottom sieve frame print is eliminated, when
When the parts by weight of sintered bauxite are greater than cast alumin(i)um alumina, ceramic tile is printed without bottom sieve frame, when the parts by weight of sintered bauxite are less than cast alumin(i)um alum
When native, ceramic tile has bottom sieve frame print, it can be seen that the parts by weight of sintered bauxite otherwise be less than cast alumin(i)um alumina just have elimination ceramic tile bottom
The effect of lattice print by comparative example 3 it can be seen that using magnesia in traditional technology, and carries out levigate, slurrying processing to raw material,
Ceramic tile bottom sieve frame print is obvious, and the present invention has very big shadow to the effect for eliminating bottom sieve frame print to the selection of raw material and the control of fineness
It rings.
The embodiments described above only express several embodiments of the present invention, and the description thereof is more specific and detailed, but simultaneously
It cannot therefore be construed as limiting the scope of the patent.It should be pointed out that coming for those of ordinary skill in the art
It says, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to protection of the invention
Range.Therefore, the scope of protection of the patent of the invention shall be subject to the appended claims.
Claims (10)
1. a kind of brick primer, which is characterized in that its slurry includes each raw material component of following parts by weight:
2. brick primer according to claim 1, which is characterized in that the slurry includes each raw material of following parts by weight
Component:
3. brick primer according to claim 1 or 2, which is characterized in that the fineness of the slurry is that 100 mesh screen residues are less than
0.1% and 200 mesh screen residue be greater than 90%.
4. brick primer according to claim 1 or 2, which is characterized in that the fire resisting auxiliary material be emergy, mullite and
At least one of quartz.
5. brick primer according to claim 1 or 2, which is characterized in that the binder be aluminium dihydrogen phosphate, phosphoric acid and
At least one of phosphoric acid hydrogen two aluminium.
6. a kind of preparation method of brick primer described in Claims 1 to 5 any one, comprising the following steps:
Each raw material is taken by following parts by weight:
By sintered bauxite, cast alumin(i)um alumina and fire resisting auxiliary material, sieving screens out 200 mesh raw material below;
By the sintered bauxite, cast alumin(i)um alumina and fire resisting auxiliary material of sieving and the kaolin, bentonite, cosmetic soil and porcelain mud
At least one of, the fineness of binder, grinding aid and water mixing and ball milling to scheduled slurry.
7. the preparation method of brick primer according to claim 6, which is characterized in that the fineness of the scheduled slurry is
100 mesh screen residues less than 0.1% and 200 mesh screen residue be greater than 90%.
8. the preparation method of brick primer according to claim 6, which is characterized in that the fire resisting auxiliary material be emergy,
At least one of mullite and quartz.
9. the preparation method of brick primer according to claim 6, which is characterized in that the binder is biphosphate
At least one of aluminium, phosphoric acid and phosphoric acid hydrogen two aluminium.
10. the preparation method of brick primer according to claim 6, which is characterized in that the grinding aid is trimerization phosphorus
At least one of sour sodium and sodium carboxymethylcellulose pyce.
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN114213134A (en) * | 2021-12-23 | 2022-03-22 | 新明珠集团股份有限公司 | Brick bottom slurry and preparation method and application thereof |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN114213134A (en) * | 2021-12-23 | 2022-03-22 | 新明珠集团股份有限公司 | Brick bottom slurry and preparation method and application thereof |
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