CN109105723A - A kind of beta carotene lotion and preparation method thereof - Google Patents
A kind of beta carotene lotion and preparation method thereof Download PDFInfo
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- CN109105723A CN109105723A CN201810996513.0A CN201810996513A CN109105723A CN 109105723 A CN109105723 A CN 109105723A CN 201810996513 A CN201810996513 A CN 201810996513A CN 109105723 A CN109105723 A CN 109105723A
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- Prior art keywords
- beta carotene
- lotion
- antioxidant
- preparation
- phase
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- 239000006210 lotion Substances 0.000 title claims abstract description 64
- 235000013734 beta-carotene Nutrition 0.000 title claims abstract description 55
- 239000011648 beta-carotene Substances 0.000 title claims abstract description 55
- OENHQHLEOONYIE-JLTXGRSLSA-N β-Carotene Chemical compound CC=1CCCC(C)(C)C=1\C=C\C(\C)=C\C=C\C(\C)=C\C=C\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C OENHQHLEOONYIE-JLTXGRSLSA-N 0.000 title claims abstract description 55
- OENHQHLEOONYIE-UKMVMLAPSA-N all-trans beta-carotene Natural products CC=1CCCC(C)(C)C=1/C=C/C(/C)=C/C=C/C(/C)=C/C=C/C=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C OENHQHLEOONYIE-UKMVMLAPSA-N 0.000 title claims abstract description 54
- TUPZEYHYWIEDIH-WAIFQNFQSA-N beta-carotene Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CCCC1(C)C)C=CC=C(/C)C=CC2=CCCCC2(C)C TUPZEYHYWIEDIH-WAIFQNFQSA-N 0.000 title claims abstract description 54
- 229960002747 betacarotene Drugs 0.000 title claims abstract description 54
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 239000003963 antioxidant agent Substances 0.000 claims abstract description 22
- 230000003078 antioxidant effect Effects 0.000 claims abstract description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 22
- 235000006708 antioxidants Nutrition 0.000 claims abstract description 21
- 239000011162 core material Substances 0.000 claims abstract description 10
- 239000000463 material Substances 0.000 claims abstract description 10
- 230000001954 sterilising effect Effects 0.000 claims abstract description 6
- 235000015112 vegetable and seed oil Nutrition 0.000 claims abstract description 4
- 239000008158 vegetable oil Substances 0.000 claims abstract description 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical class OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 30
- 239000003921 oil Substances 0.000 claims description 28
- 235000019198 oils Nutrition 0.000 claims description 28
- 239000000839 emulsion Substances 0.000 claims description 27
- 238000003756 stirring Methods 0.000 claims description 19
- 239000013078 crystal Substances 0.000 claims description 12
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical class O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims description 11
- 229930006000 Sucrose Chemical class 0.000 claims description 11
- 150000003904 phospholipids Chemical class 0.000 claims description 11
- 239000005720 sucrose Chemical class 0.000 claims description 11
- BGNXCDMCOKJUMV-UHFFFAOYSA-N Tert-Butylhydroquinone Chemical compound CC(C)(C)C1=CC(O)=CC=C1O BGNXCDMCOKJUMV-UHFFFAOYSA-N 0.000 claims description 10
- 238000005303 weighing Methods 0.000 claims description 10
- 238000000265 homogenisation Methods 0.000 claims description 9
- 238000004321 preservation Methods 0.000 claims description 9
- 235000010378 sodium ascorbate Nutrition 0.000 claims description 8
- 229960005055 sodium ascorbate Drugs 0.000 claims description 8
- PPASLZSBLFJQEF-RKJRWTFHSA-M sodium ascorbate Substances [Na+].OC[C@@H](O)[C@H]1OC(=O)C(O)=C1[O-] PPASLZSBLFJQEF-RKJRWTFHSA-M 0.000 claims description 8
- PPASLZSBLFJQEF-RXSVEWSESA-M sodium-L-ascorbate Chemical group [Na+].OC[C@H](O)[C@H]1OC(=O)C(O)=C1[O-] PPASLZSBLFJQEF-RXSVEWSESA-M 0.000 claims description 8
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims description 6
- 238000004659 sterilization and disinfection Methods 0.000 claims description 5
- 239000004250 tert-Butylhydroquinone Substances 0.000 claims description 5
- 235000019281 tert-butylhydroquinone Nutrition 0.000 claims description 5
- 239000004322 Butylated hydroxytoluene Substances 0.000 claims description 4
- 235000010354 butylated hydroxytoluene Nutrition 0.000 claims description 4
- 229930003427 Vitamin E Natural products 0.000 claims description 3
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 claims description 3
- 239000002994 raw material Substances 0.000 claims description 3
- 235000019165 vitamin E Nutrition 0.000 claims description 3
- 229940046009 vitamin E Drugs 0.000 claims description 3
- 239000011709 vitamin E Substances 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 2
- 235000002864 food coloring agent Nutrition 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- GDSOZVZXVXTJMI-SNAWJCMRSA-N (e)-1-methylbut-1-ene-1,2,4-tricarboxylic acid Chemical compound OC(=O)C(/C)=C(C(O)=O)\CCC(O)=O GDSOZVZXVXTJMI-SNAWJCMRSA-N 0.000 claims 1
- 241000220259 Raphanus Species 0.000 claims 1
- 235000006140 Raphanus sativus var sativus Nutrition 0.000 claims 1
- IPCSVZSSVZVIGE-UHFFFAOYSA-M hexadecanoate Chemical compound CCCCCCCCCCCCCCCC([O-])=O IPCSVZSSVZVIGE-UHFFFAOYSA-M 0.000 claims 1
- 238000010008 shearing Methods 0.000 abstract description 7
- 235000013361 beverage Nutrition 0.000 abstract description 3
- 239000003086 colorant Substances 0.000 abstract description 3
- 229920002472 Starch Polymers 0.000 abstract description 2
- 239000002253 acid Substances 0.000 abstract description 2
- 238000010438 heat treatment Methods 0.000 abstract description 2
- 239000008107 starch Substances 0.000 abstract description 2
- 235000019698 starch Nutrition 0.000 abstract description 2
- 230000000052 comparative effect Effects 0.000 description 17
- 238000000034 method Methods 0.000 description 12
- 239000002245 particle Substances 0.000 description 10
- 238000000386 microscopy Methods 0.000 description 6
- 235000019486 Sunflower oil Nutrition 0.000 description 5
- 239000002600 sunflower oil Substances 0.000 description 5
- 235000013305 food Nutrition 0.000 description 4
- 235000019483 Peanut oil Nutrition 0.000 description 3
- 238000004090 dissolution Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000011156 evaluation Methods 0.000 description 3
- 230000005251 gamma ray Effects 0.000 description 3
- 238000003475 lamination Methods 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
- 238000012986 modification Methods 0.000 description 3
- 239000000312 peanut oil Substances 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- 241000213006 Angelica dahurica Species 0.000 description 2
- RRHGJUQNOFWUDK-UHFFFAOYSA-N Isoprene Chemical compound CC(=C)C=C RRHGJUQNOFWUDK-UHFFFAOYSA-N 0.000 description 2
- 235000021466 carotenoid Nutrition 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000005286 illumination Methods 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 150000003254 radicals Chemical class 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 235000012424 soybean oil Nutrition 0.000 description 2
- 239000003549 soybean oil Substances 0.000 description 2
- FPIPGXGPPPQFEQ-UHFFFAOYSA-N 13-cis retinol Natural products OCC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-UHFFFAOYSA-N 0.000 description 1
- 208000000412 Avitaminosis Diseases 0.000 description 1
- NLZUEZXRPGMBCV-UHFFFAOYSA-N Butylhydroxytoluene Chemical compound CC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 NLZUEZXRPGMBCV-UHFFFAOYSA-N 0.000 description 1
- -1 Carotenoids compound Chemical class 0.000 description 1
- 206010021135 Hypovitaminosis Diseases 0.000 description 1
- QAQJMLQRFWZOBN-LAUBAEHRSA-N L-ascorbyl-6-palmitate Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](O)[C@H]1OC(=O)C(O)=C1O QAQJMLQRFWZOBN-LAUBAEHRSA-N 0.000 description 1
- 239000011786 L-ascorbyl-6-palmitate Substances 0.000 description 1
- GUBGYTABKSRVRQ-QKKXKWKRSA-N Lactose Natural products OC[C@H]1O[C@@H](O[C@H]2[C@H](O)[C@@H](O)C(O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@H]1O GUBGYTABKSRVRQ-QKKXKWKRSA-N 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 244000170916 Paeonia officinalis Species 0.000 description 1
- 235000006484 Paeonia officinalis Nutrition 0.000 description 1
- 235000019482 Palm oil Nutrition 0.000 description 1
- 235000019484 Rapeseed oil Nutrition 0.000 description 1
- FPIPGXGPPPQFEQ-BOOMUCAASA-N Vitamin A Natural products OC/C=C(/C)\C=C\C=C(\C)/C=C/C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-BOOMUCAASA-N 0.000 description 1
- 240000008042 Zea mays Species 0.000 description 1
- 235000016383 Zea mays subsp huehuetenangensis Nutrition 0.000 description 1
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical compound OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 description 1
- 239000002246 antineoplastic agent Substances 0.000 description 1
- 229940041181 antineoplastic drug Drugs 0.000 description 1
- 235000010385 ascorbyl palmitate Nutrition 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 239000010495 camellia oil Substances 0.000 description 1
- 150000001747 carotenoids Chemical class 0.000 description 1
- 239000000490 cosmetic additive Substances 0.000 description 1
- 230000032798 delamination Effects 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 201000008220 erythropoietic protoporphyria Diseases 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 238000006317 isomerization reaction Methods 0.000 description 1
- 239000008101 lactose Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 235000009973 maize Nutrition 0.000 description 1
- 239000003094 microcapsule Substances 0.000 description 1
- 229930014626 natural product Natural products 0.000 description 1
- 235000008935 nutritious Nutrition 0.000 description 1
- 230000008520 organization Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 239000002540 palm oil Substances 0.000 description 1
- 230000035479 physiological effects, processes and functions Effects 0.000 description 1
- 238000005498 polishing Methods 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 235000019155 vitamin A Nutrition 0.000 description 1
- 239000011719 vitamin A Substances 0.000 description 1
- 229940045997 vitamin a Drugs 0.000 description 1
- 208000030401 vitamin deficiency disease Diseases 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/40—Colouring or decolouring of foods
- A23L5/42—Addition of dyes or pigments, e.g. in combination with optical brighteners
- A23L5/43—Addition of dyes or pigments, e.g. in combination with optical brighteners using naturally occurring organic dyes or pigments, their artificial duplicates or their derivatives
- A23L5/44—Addition of dyes or pigments, e.g. in combination with optical brighteners using naturally occurring organic dyes or pigments, their artificial duplicates or their derivatives using carotenoids or xanthophylls
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P10/00—Shaping or working of foodstuffs characterised by the products
- A23P10/30—Encapsulation of particles, e.g. foodstuff additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Cosmetics (AREA)
Abstract
The present invention relates to a kind of beta carotene lotion and preparation method thereof, the lotion includes each component of following mass percentage: wall material 30-45%；Core material 10-15%；Antioxidant 1-2%；Pure water 38-59%；The core material includes beta carotene and vegetable oil；In the lotion, the mass percentage of beta carotene is 1-5%.It is of the invention the preparation method comprises the following steps: first that wall material and its antioxidant is soluble in water, then core material and its antioxidant are dissolved by heating, then the two is mixed, shearing, homogeneous, the obtained lotion of sterilizing.Present invention is mainly applied to the colorants of cake, jam product, beverage etc..Wall material of the invention avoids the acid labile of protide and the peculiar smell of converted starch, is more widely applied its finished product.Prepared beta carotene lotion has sheltered the peculiar smell of beta carotene itself, improves the stability of beta carotene, extends the application field and market acceptance of product.
Description
Technical field
The invention belongs to food skilled worker's technical field, more particularly, to a kind of beta carotene lotion and preparation method thereof,
Mainly as the colorant of cake, jam product, beverage etc..
Background technique
Carotenoid is the general name of a kind of natural products, and up to the present, the mankind have found more than 600 in nature
Carotenoids compound.Wherein, precursor of the beta carotene as vitamin A is FAO (Food and Agriculture Organization of the United Nation) and world health
The A nutritious food hardening agent for organizing the food additives joint specialist committee to assert.There are 52 countries and ground in the world
Area's approval uses the product.
Beta carotene is to belong to four patch hydrocarbons, containing there are two β -one root of Dahurian angelica ring and 4 isoprene sides in molecule
Chain, entire molecule are that symmetrically, i.e. for two β -one root of Dahurian angelica rings at both ends, be broken can produce two VA molecules in its center, in molecule
Have and be conjugated each other between multiple double bonds and double bond, its molecular formula is C40H60, molecular weight 536.88, fusing point is 180 DEG C or so,
In the glossiness oblique parallelepiped of peony to kermesinus, there are slight foreign odor or peculiar smell, weak solution is in orange-yellow to orange, concentration
Band is red when increase.Beta carotene is more stable under the conditions of weak base, but meets oxygen, in unstable when light and heat.Just because of it
Unsaturated structure, make it that there is stronger antioxidant activity and remove ability of free radical, thus living with certain physiology
Property.But also just because of multiple double bonds are contained in its molecule, make its unstable chemcial property, easily in illumination and heating
Oxidation deterioration and isomerization reaction occurs.So direct illumination should be avoided, heat and contacted with air.Currently, beta carotene master
It is used for the toner of food, additive, provitamin A and cosmetic additive, in addition, beta carotene is also controlled as drug
Treat erythrohepatic protoporphyria, vitamin-deficiency and the anticancer drug for inhibiting tumour to be formed.
Microencapsulation technology is using filmogen by solid, and liquid or gas wrapping wherein, form microcapsules, to protect
Shield core material is not influenced by external environment conditions such as temperature, PH, light, free radicals, to improve the stability and shelf life of core material, control
Make a kind of embedding techniques of its release.In microencapsulation processes, the step of most critical is the emulsification of core material.And current β-Hu Luo
In terms of the development & production of Bu Su preparation, mainly using polishing, high temperature high pressure process method, the physical chemistry means such as solvent method,
And gained finished product is that each associated production application field is sold to solid powder state mostly, these methods are effective in beta carotene
The bioavailability of ingredient, there are certain drawback in terms of the inoxidizability and flavor of finished product, and current market, consumer is to product
Effective absorptivity and smell, mouthfeel etc. have higher demand, in order to meet the market demand, product fill vacancy,
Spy invents this patent.
Summary of the invention
In view of the drawbacks of the prior art, the object of the present invention is to provide a kind of beta carotene lotions and preparation method thereof.
The purpose of the present invention is what is be achieved through the following technical solutions:
The present invention provides a kind of beta carotene lotion, each raw material component including following mass percentage:
The core material includes beta carotene and vegetable oil；In the lotion, the mass percentage of beta carotene is
1.2-6%.
Preferably, the wall material includes modified phospholipid, glycerol and sucrose.
Preferably, in the wall material, the mass ratio of modified phospholipid, glycerol and sucrose is 1-6:0.7-2:1.
Preferably, the antioxidant includes water phase antioxidant and oily phase antioxidant；The water phase antioxidant is
Sodium ascorbate, it is described oil phase antioxidant include vitamin E, ascorbyl palmitate, TBHQ, BHT one of which or
Any two kinds of mixture.
Preferably, in the antioxidant, the mass ratio of the water phase antioxidant and oily phase antioxidant is 1:0.33-
3。
Preferably, the vegetable oil include soybean oil, sunflower oil, peanut oil, palm oil, rapeseed oil, maize germ oil,
At least one of Rice oil, camellia oil.
The present invention also provides a kind of preparation methods of beta carotene lotion, comprising the following steps:
A, prepared by Emulsion Phase: weighing wall material, water phase antioxidant is dissolved in pure water, is stirred, and heat preservation obtains Emulsion Phase；
B, prepared by oil phase: weighing core material and oily phase antioxidant, stirs, keep the temperature, up to oily phase after no crystal；
C, the oil for preparing step B is mutually poured slowly into the Emulsion Phase of step A preparation, stirs 2-3min, shears 2-afterwards
5min obtains lotion；
D, lotion homogeneous 1-3 times for preparing step C, homogenization pressure 20-40Mpa of second level, level-one 3-5Mpa；
E, by the lotion after step D homogeneous after irradiation or ultra high temperature short time sterilization, obtain beta carotene lotion at
Product.
Preferably, in step A, the temperature for being dissolved in pure water is 65-70 DEG C, and holding temperature is 65-70 DEG C, the time is
25-40min；
In step B, the heat preservation degree is 140-160 DEG C, time 5-20min.
Preferably, in step C, the speed of agitator is 20-100r/min, stirs 2-3min；The shear rate is
6000-10000r/min, time 2-5min.
Preferably, in step D, the homogenization pressure is 20-40Mpa of second level, level-one 3-5Mpa.
Preferably, the density of the beta carotene lotion finished product of the preparation is 1.1-1.25g/cm3。
The present invention also provides a kind of application of beta carotene lotion in food color.
Compared with prior art, the present invention have it is following the utility model has the advantages that
1) wall material invented avoids the acid labile of protide and the peculiar smell of converted starch, makes the application of its finished product more
Extensively.
2) the beta carotene lotion prepared by the present invention has sheltered the peculiar smell of beta carotene itself, improves β-carrot
The stability of element, extends the application field and market acceptance of product.
3) raw material involved in the present invention and process flow are relatively simple, suitable for modern chemical industry production.
4) present invention is lotion, is more easier compared with pulvis soluble in water, facilitates the application of downstream client.
Specific embodiment
The present invention is described in detail combined with specific embodiments below.Following embodiment will be helpful to the technology of this field
Personnel further understand the present invention, but the invention is not limited in any way.It should be pointed out that the ordinary skill of this field
For personnel, without departing from the inventive concept of the premise, various modifications and improvements can be made.These belong to the present invention
Protection scope.
Embodiment 1
1) prepared by Emulsion Phase: weighing modified phospholipid 10kg, glycerol 10kg, sucrose 10kg, sodium ascorbate 0.75kg is dissolved in
65 DEG C, in the pure water of 59kg, stirring keeps the temperature 25min.
2) oil is mutually prepared: beta carotene 1.2kg, soybean oil 8.8kg are weighed, vitamin E 0.25kg is heated to 140 DEG C,
20min is kept the temperature, later microscopy, is carried out in next step after no crystal.
3) by step 2 prepare oil be mutually poured slowly into Emulsion Phase prepared by step 1, stirring 2min, after cut with cutter
2min is cut, oil is made mutually to be well-dispersed in Emulsion Phase.
4) lotion is with homogenizer homogeneous 1 time after shearing, homogenization pressure second level 20Mpa, level-one 3Mpa.
5) lotion after homogeneous obtains the lotion finished product that content beta-carotene is 1% after gamma-ray irradiation.
Embodiment 2
1) prepared by Emulsion Phase: weighing modified phospholipid 30kg, glycerol 10kg, sucrose 5kg, sodium ascorbate 0.5kg is dissolved in 70
DEG C, in the pure water of 38kg, stirring keeps the temperature 40min.
2) oil is mutually prepared: being weighed beta carotene 6kg, sunflower oil 9kg, TBHQ 1.5kg, is heated to 160 DEG C, heat preservation
5min, later microscopy carry out in next step after no crystal.
3) by step 2 prepare oil be mutually poured slowly into Emulsion Phase prepared by step 1, stirring 3min, after cut with cutter
5min is cut, oil is made mutually to be well-dispersed in Emulsion Phase.
4) lotion is with homogenizer homogeneous 3 times after shearing, homogenization pressure second level 40Mpa, level-one 5Mpa.
5) for the lotion after homogeneous after 127 DEG C, ultra high temperature short time sterilization in 8 seconds, obtaining content beta-carotene is 5%
Lotion finished product.
Embodiment 3
1) prepared by Emulsion Phase: weighing modified phospholipid 20kg, glycerol 7kg, sucrose 10kg, sodium ascorbate 0.75kg is dissolved in 68
DEG C, in the pure water of 48.5kg, stirring keeps the temperature 32min.
2) oil is mutually prepared: being weighed beta carotene 3.2kg, peanut oil 9.8kg, BHT 0.75kg, is heated to 150 DEG C, heat preservation
10min, later microscopy carry out in next step after no crystal.
3) by step 2 prepare oil be mutually poured slowly into Emulsion Phase prepared by step 1, stirring 3min, after cut with cutter
4min is cut, oil is made mutually to be well-dispersed in Emulsion Phase.
4) lotion is with homogenizer homogeneous 2 times after shearing, homogenization pressure second level 30Mpa, level-one 4Mpa.
5) lotion after homogeneous obtains the lotion finished product that content beta-carotene is 3% after gamma-ray irradiation sterilizes.
Embodiment 4
1) prepared by Emulsion Phase: weighing modified phospholipid 25kg, glycerol 2kg, sucrose 10kg, sodium ascorbate 1.0kg is dissolved in 68
℃、In the pure water of 48.67kg, stirring keeps the temperature 32min.
2) oil is mutually prepared: being weighed beta carotene 3.2kg, peanut oil 9.8kg, BHT 0.33kg, is heated to 150 DEG C, heat preservation
10min, later microscopy carry out in next step after no crystal.
3) by step 2 prepare oil be mutually poured slowly into Emulsion Phase prepared by step 1, stirring 3min, after cut with cutter
4min is cut, oil is made mutually to be well-dispersed in Emulsion Phase.
4) lotion is with homogenizer homogeneous 2 times after shearing, homogenization pressure second level 30Mpa, level-one 4Mpa.
5) lotion after homogeneous obtains the lotion finished product that content beta-carotene is 3% after gamma-ray irradiation sterilizes.
Embodiment 5
1) prepared by Emulsion Phase: weighing modified phospholipid 25kg, glycerol 15kg, sucrose 5kg, sodium ascorbate 0.5kg is dissolved in 70
DEG C, in the pure water of 38kg, stirring keeps the temperature 40min.
2) oil is mutually prepared: being weighed beta carotene 6kg, sunflower oil 9kg, TBHQ 1.5kg, is heated to 160 DEG C, heat preservation
5min, later microscopy carry out in next step after no crystal.
3) by step 2 prepare oil be mutually poured slowly into Emulsion Phase prepared by step 1, stirring 3min, after cut with cutter
5min is cut, oil is made mutually to be well-dispersed in Emulsion Phase.
4) lotion is with homogenizer homogeneous 3 times after shearing, homogenization pressure second level 40Mpa, level-one 5Mpa.
5) for the lotion after homogeneous after 127 DEG C, ultra high temperature short time sterilization in 8 seconds, obtaining content beta-carotene is 5%
Lotion finished product.
Embodiment 6
1) prepared by Emulsion Phase: weighing modified phospholipid 30kg, glycerol 5kg, sucrose 10kg, sodium ascorbate 0.5kg is dissolved in 70
DEG C, in the pure water of 38kg, stirring keeps the temperature 40min.
2) oil is mutually prepared: being weighed beta carotene 6kg, sunflower oil 9kg, TBHQ 1.5kg, is heated to 160 DEG C, heat preservation
5min, later microscopy carry out in next step after no crystal.
3) by step 2 prepare oil be mutually poured slowly into Emulsion Phase prepared by step 1, stirring 3min, after cut with cutter
5min is cut, oil is made mutually to be well-dispersed in Emulsion Phase.
4) lotion is with homogenizer homogeneous 3 times after shearing, homogenization pressure second level 40Mpa, level-one 5Mpa.
5) for the lotion after homogeneous after 127 DEG C, ultra high temperature short time sterilization in 8 seconds, obtaining content beta-carotene is 5%
Lotion finished product.
Comparative example 1
The method of this comparative example and embodiment 1 is essentially identical, the difference is that only: in step 1), this comparative example is used
Phosphatide replaces modified phospholipid.
Comparative example 2
The method of this comparative example and embodiment 1 is essentially identical, the difference is that only: in step 1), this comparative example is used
Lactose replaces sucrose.
Comparative example 3
The method of this comparative example and embodiment 2 is essentially identical, the difference is that only: in step 1), the β-of this comparative example
Carrotene is 8kg, sunflower oil 7kg.
Performance evaluation:
Beta carotene lotion finished product obtained by each embodiment and comparative example is tested for the property respectively, evaluation index
It include: beta carotene dissolution of crystals situation, embedding effect, stability of emulsion, lotion density etc..Evaluation method is successively are as follows: micro-
Mirror amplifies 100 times of observations, microscope amplifies 1000 times of observations, 50 DEG C of water-bath 2 hours observation delaminations, weighs 50mL lotion
Quality converts.
As a result as follows:
| Dissolution of crystals | Embed effect | Stability of emulsion | Lotion density (g/cm3) | |
| Embodiment 1 | It is completely dissolved | Particle is small, uniform | It is not layered | 1.1 |
| Embodiment 2 | It is completely dissolved | Particle is small, uniform | It is not layered | 1.25 |
| Embodiment 3 | It is completely dissolved | Particle is small, uniform | It is not layered | 1.18 |
| Embodiment 4 | It is completely dissolved | Particle is small, uniform | It is not layered | 1.08 |
| Embodiment 5 | It is completely dissolved | Particle is big, uneven | Layering | / |
| Embodiment 6 | It is completely dissolved | Particle is small, uniform | It is not layered | 1.28 |
| Comparative example 1 | It is completely dissolved | It is all larger oil droplet | Layering | / |
| Comparative example 2 | It is completely dissolved | Particle is small, uniform | It is not layered | 1.05 |
| Comparative example 3 | It is undissolved | Particle is small, uneven | Layering | / |
Remarks: the lotion of layering can not accurately measure the density of lotion due to oily mutually with the separation of water phase
As can be known from the results of Table 1, its crystal of the beta carotene lotion of embodiment 1-3 preparation is completely dissolved, the particle of embedding
It is small, uniform, good emulsion stability, and lotion density is in 1.1-1.25g/cm3In the range of, which answer it as colorant
Used time is particularly applied in beverage, not will cause the lamination of color.And the lotion density of embodiment 4,6 and comparative example 2 point
It Wei not 1.08g/cm3、1.28g/cm3And 1.05g/cm3, caused unevenly in application, color made lamination occur.
And there is lamination in embodiment 5, comparative example 1 and 3, and the embedded particles of comparative example 1 are larger oil droplet, embedding effect is poor,
And the dissolution of crystals of comparative example 3 is poor.
The above description of the embodiments is intended to facilitate ordinary skill in the art to understand and use the invention.
Person skilled in the art obviously easily can make various modifications to these embodiments, and described herein general
Principle is applied in other embodiments without having to go through creative labor.Therefore, the present invention is not limited to the above embodiments, ability
Field technique personnel announcement according to the present invention, improvement and modification made without departing from the scope of the present invention all should be of the invention
Within protection scope.
Claims (11)
1. a kind of beta carotene lotion, which is characterized in that each raw material component including following mass percentage:
The core material includes beta carotene and vegetable oil；In the lotion, the mass percentage of beta carotene is 1.2-
6%.
2. beta carotene lotion according to claim 1, which is characterized in that the wall material include modified phospholipid, glycerol and
Sucrose.
3. beta carotene lotion according to claim 2, which is characterized in that in the wall material, modified phospholipid, glycerol and
The mass ratio of sucrose is 1-6:0.7-2:1.
4. beta carotene lotion according to claim 1, which is characterized in that the antioxidant includes that water phase is anti-oxidant
Agent and oily phase antioxidant；The water phase antioxidant is sodium ascorbate, and the oil phase antioxidant includes vitamin E, resists
Bad hematic acid palmitate, the one of which of TBHQ, BHT or any two kinds of mixture.
5. beta carotene lotion according to claim 4, which is characterized in that in the antioxidant, the water phase antioxygen
The mass ratio of agent and oily phase antioxidant is 1:0.33-3.
6. a kind of preparation method of beta carotene lotion according to claim 1-5, which is characterized in that including
Following steps:
A, prepared by Emulsion Phase: weighing wall material, water phase antioxidant is dissolved in pure water, is stirred, and heat preservation obtains Emulsion Phase；
B, prepared by oil phase: weighing core material and oily phase antioxidant, stirs, keep the temperature, up to oily phase after no crystal；
C, the oil for preparing step B is mutually poured slowly into the Emulsion Phase of step A preparation, stirs 2-3min, shears 2-5min afterwards,
Obtain lotion；
D, lotion homogeneous 1-3 times for preparing step C, homogenization pressure 20-40Mpa of second level, level-one 3-5Mpa；
E, by the lotion after step D homogeneous after irradiation or ultra high temperature short time sterilization, beta carotene lotion finished product is obtained.
7. the preparation method of beta carotene lotion according to claim 6, which is characterized in that described to be dissolved in step A
The temperature of pure water is 65-70 DEG C, and holding temperature is 65-70 DEG C, time 25-40min；
In step B, the heat preservation degree is 140-160 DEG C, time 5-20min.
8. the preparation method of beta carotene lotion according to claim 6, which is characterized in that in step C, the stirring
Revolving speed is 20-100r/min, stirs 2-3min；The shear rate is 6000-10000r/min, time 2-5min.
9. the preparation method of beta carotene lotion according to claim 6, which is characterized in that in step D, the homogeneous
Pressure is 20-40Mpa of second level, level-one 3-5Mpa.
10. the preparation method of beta carotene lotion according to claim 6, which is characterized in that β-Hu of the preparation
The density of radish element lotion finished product is 1.1-1.25g/cm3。
11. a kind of application of beta carotene lotion according to claim 1-5 in food color.
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| CN113265175B (en) * | 2021-05-13 | 2022-07-05 | 广州市纳趣尔食品有限责任公司 | Edible natural ink product and preparation method thereof |
| CN114304453A (en) * | 2021-12-15 | 2022-04-12 | 河北东康乳业有限公司 | Low-GI diglyceride microencapsulated protein-free emulsion beverage and preparation method thereof |
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