CN109100176A - A kind of sampling system - Google Patents

A kind of sampling system Download PDF

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Publication number
CN109100176A
CN109100176A CN201810951051.0A CN201810951051A CN109100176A CN 109100176 A CN109100176 A CN 109100176A CN 201810951051 A CN201810951051 A CN 201810951051A CN 109100176 A CN109100176 A CN 109100176A
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CN
China
Prior art keywords
pipeline
sampling
steel cylinder
medium
solenoid valve
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810951051.0A
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Chinese (zh)
Inventor
杨伟
张鹏程
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jiangsu Xintai Chemical Equipment Co Ltd
Original Assignee
Jiangsu Xintai Chemical Equipment Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by Jiangsu Xintai Chemical Equipment Co Ltd filed Critical Jiangsu Xintai Chemical Equipment Co Ltd
Priority to CN201810951051.0A priority Critical patent/CN109100176A/en
Publication of CN109100176A publication Critical patent/CN109100176A/en
Pending legal-status Critical Current

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/10Devices for withdrawing samples in the liquid or fluent state

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  • Life Sciences & Earth Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

The present invention relates to a kind of sampling systems, including medium pipeline, medium blowdown pipeline, blow-down pipe, nitrogen purging device, pressure-detecting device and sampling steel cylinder, the medium of the medium pipeline flows to the end media outlet pipeline N2 by the end medium entrance pipeline N1, one end of the sampling steel cylinder is connected with medium entrance pipeline and medium blowdown pipeline, the other end is connected with media outlet pipeline and blow-down pipe, wherein the nitrogen purging device is connected in parallel on one end of sampling steel cylinder by pipeline and medium entrance pipeline;It is described to be equipped with pressure-detecting device towards the pipeline of media outlet pipeline and blow-down pipe.This sampling of the invention is automatically performed by system substantially, effectively prevents the harm of maloperation bring, while improving sampling efficiency.Purging, blowdown, cooling are concentrated, live pipeline arrangement is reduced, maintains easily, while being convenient for environmental protection.

Description

A kind of sampling system
Technical field
The present invention relates to a kind of sampling systems, belong to sampling technique field.
Background technique
Sampling analysis is the important means of technique and the control of product in petrochemical iy produced.Traditional direct sampling method is by purging A large amount of nocuousness material direct emissions, not only pollute environment, but also endanger worker health.Sealing sampler will purge object by parallel pipeline The shortcomings that expecting in circulating involuting system, overcoming direct sampling.Recently as the strong of technological progress and Environmental Safety health idea Change, sealing sampler in petroleum chemical enterprise using increasing.But in the actual operation process, sealing sampler still has one Fixed problem.
(1) closed sampler utensil weight, volume are larger: since to be generally steel etc. highly dense for the sampler of existing enclosed sampling Material production is spent, the container wall for being for pressure resistance in addition is thicker, the vial for causing the volume and weight of utensil all more traditional Or airbag greatly increases.The opposite reduction of the sampling utensil quantity that sample collector is once carried by, especially climbing device When, heavy sampling utensil increases the homework burden of sample collector.
(2) sealing sampler itself designs existing defects: sealing sampler having itself design have the defects that it is certain, Such as in order to which closed weld sampling box rear cover is tied, cause the maintenance of inconvenient rear valve, pressure gauge, connector.Some operations Technique is cumbersome, and worker samples every time requires to turn five or six valves, is easy to happen order mistake.
(3) complicated with circuits arrangement: the sealing sampler requirement having has the functions such as purging, blowdown, cooling, heat tracing, needs Corresponding pipeline is configured, causes pipeline construction is complicated to repeat, is unfavorable for maintenance and management.
Summary of the invention
It is an object of the invention to: in view of the drawbacks of the prior art, a kind of sampling system is proposed, to solve above-mentioned technology Problem.
The technical scheme adopted by the invention is that: a kind of sampling system, including medium pipeline, medium blowdown pipeline, emptying The medium of pipeline, nitrogen purging device, pressure-detecting device and sampling steel cylinder, the medium pipeline passes through medium entrance pipeline The end N1 flows to the end media outlet pipeline N2, and one end of the sampling steel cylinder is connected with medium entrance pipeline and medium sewage pipe Line, the other end are connected with media outlet pipeline and blow-down pipe, wherein the nitrogen purging device by pipeline and medium into Mouth pipeline is connected in parallel on one end of sampling steel cylinder;It is described to be equipped with pressure detecting towards the pipeline of media outlet pipeline and blow-down pipe Device.
In the present invention: the both ends of the sampling steel cylinder are respectively equipped with sampling steel cylinder needle-valve Z7 and sampling steel cylinder needle-valve Z8.
In the present invention: the medium entrance pipeline is equipped with solenoid valve Z1, is connected with the pipeline of nitrogen purging device It is equipped with solenoid valve Z2, and is connected after two pipelines parallel connections with sampling steel cylinder input end, the pipeline and sampling steel cylinder after parallel connection Between be equipped with sampling steel cylinder shut-off valve Z9.
In the present invention: the media outlet pipeline is equipped with solenoid valve Z4, and blow-down pipe is equipped with solenoid valve Z5, and It is connected after two pipelines are in parallel with sampling steel cylinder outlet end, is cut between the pipeline and sampling steel cylinder after parallel connection equipped with sampling steel cylinder Only valve Z10.
In the present invention: the medium blowdown pipeline is equipped with solenoid valve Z6, and medium blowdown pipeline and medium blowdown General pipeline is connected.
In the present invention: connecting pipeline is equipped between the inlet end and an outlet end of the sampling steel cylinder, on the connecting pipeline Equipped with solenoid valve Z3.
In the present invention: the medium entrance pipeline and the outlet being connected with after the pipeline parallel connection of nitrogen purging device are set There is cooler, the cooler is connected with cooling water pipeline and cooling water return pipe line, wherein the cooling water supplies Water pipeline is equipped with solenoid valve Z11, and cooling water return pipe line is equipped with solenoid valve Z12.
In the present invention: the cooler is connected by cooling water blowdown pipeline with cooling water blowdown general pipeline, wherein institute The cooling water blowdown pipeline stated is equipped with solenoid valve Z13.
In the present invention: the pipeline that the cooler is connected with sampling steel cylinder is equipped with temperature-detecting device.
After adopting the above technical scheme, concentration is blown the invention has the benefit that the configuration of the present invention is simple, design are reasonable It sweeps, blowdown, cooling, heat tracing, reduces live pipeline arrangement, maintain easily, while being convenient for environmental protection, cluster sampling, reduction is adopted The amount of labour of sample personnel, improves efficiency, realize automatic sampling, have excellent leakproofness, sampling precision, reliability, stability, The performances such as anti-interference ability reduce manual operation or maloperation bring are answered to endanger, improve safety.
Detailed description of the invention
Fig. 1 is schematic structural view of the invention;
Fig. 2 is another schematic diagram of the invention.
In figure: 1. medium entrance pipelines;2. media outlet pipeline;3. medium blowdown pipeline;4. blow-down pipe;5. nitrogen is blown Sweeping device;6. pressure-detecting device;7. sampling steel cylinder;8. cooler;9. temperature-detecting device;
Z1-Z6, Z11-Z13 are solenoid valve, Z9-Z10 is sampling steel cylinder shut-off valve;Z7-Z8 is sampling steel cylinder needle-valve.
Specific embodiment
The present invention will be further explained below with reference to the accompanying drawings.
By Fig. 1-2 as it can be seen that a kind of sampling system, including medium pipeline, medium blowdown pipeline 3, blow-down pipe 4, nitrogen are blown The medium of sweeping device 5, pressure-detecting device 6 and sampling steel cylinder 7, the medium pipeline is flowed by the end medium entrance pipeline 1N1 To the end media outlet pipeline 2N2, one end of the sampling steel cylinder 7 is connected with medium entrance pipeline 1 and medium blowdown pipeline 3, The other end is connected with media outlet pipeline 2 and blow-down pipe 4, wherein the nitrogen purging device 5 by pipeline and medium into Mouth pipeline 1 is connected in parallel on one end of sampling steel cylinder 7;It is described to be equipped with pressure towards the pipeline of media outlet pipeline 2 and blow-down pipe 4 Detection device 6.
In the present invention: the both ends of the sampling steel cylinder 7 are respectively equipped with sampling steel cylinder needle-valve Z7 and sampling steel cylinder needle-valve Z8. The medium entrance pipeline 1 is equipped with solenoid valve Z1, and the pipeline for being connected with nitrogen purging device 5 is equipped with solenoid valve Z2, and It is connected after two pipelines are in parallel with 7 input end of sampling steel cylinder, sampling steel cylinder is equipped between the pipeline and sampling steel cylinder 7 after parallel connection Shut-off valve Z9.The media outlet pipeline 2 is equipped with solenoid valve Z4, and blow-down pipe 4 is equipped with solenoid valve Z5, and this two pipes It is connected after line is in parallel with 7 outlet end of sampling steel cylinder, sampling steel cylinder shut-off valve is equipped between the pipeline and sampling steel cylinder 7 after parallel connection Z10.The medium blowdown pipeline 3 is equipped with solenoid valve Z6, and medium blowdown pipeline 3 is connected with medium blowdown general pipeline.It is described Connecting pipeline is equipped between the inlet end and an outlet end of sampling steel cylinder 7, which is equipped with solenoid valve Z3.The medium Outlet after inlet line 1 and the pipeline for being connected with nitrogen purging device 5 are in parallel is equipped with cooler 8, and the cooler 8 connects There are cooling water pipeline and cooling water return pipe line, wherein the cooling water pipeline is equipped with solenoid valve Z11, it is cooling Water return piping is equipped with solenoid valve Z12.The cooler 8 passes through cooling water blowdown pipeline and cooling water blowdown general pipeline phase Even, wherein the cooling water blowdown pipeline is equipped with solenoid valve Z13.The pipeline that the cooler 8 is connected with sampling steel cylinder 7 It is equipped with temperature-detecting device 9.
When it is implemented, as shown in Figure 1, solenoid valve Z9, Z10 be sampling steel cylinder shut-off valve, sampling steel cylinder 7 is put into before sampling After automatically open, sample complete sampling steel cylinder 7 remove before be automatically closed.
Before sampling, solenoid valve Z2, Z5, Z6, Z9 and sampling steel cylinder needle-valve Z7, Z8 are opened, starting nitrogen purging device 5 carries out Residual gas is drained into torch by blow-down pipe 4 by nitrogen purging, and residual liquid drains into medium row by medium blowdown pipeline 3 Dirty general pipeline, until after the completion of nitrogen purging, closing solenoid valve Z2, Z5, Z6, Z9 and sampling steel cylinder needle-valve Z7, Z8 to 2~3min.
Solenoid valve Z1, Z3, Z4 are opened, medium flows to the end media outlet pipeline 2N2 by the end medium entrance pipeline 1N1.According to The pressure medium data that pressure-detecting device 6 is fed back judge that pressure is stablized, and prompt can carry out in next step;Solenoid valve Z3 is closed, is beaten Open electromagnetic valve Z9 and sampling steel cylinder needle-valve Z7, Z8 are sampled.The pressure medium parameter fed back according to pressure-detecting device 6 is steady It is fixed, that is, it is considered as medium sampling in sampling steel cylinder and completes, closes solenoid valve Z1, Z4 and steel cylinder Z7, Z8.Solenoid valve Z6 is opened, it will be residual Liquid discharge, removes sampling steel cylinder 7, and metal hose is connected to (quick coupling not will cause Jie with self-sealing with quick coupling Matter leakage), solenoid valve Z6 is closed, solenoid valve Z1, Z3, Z4 are opened.
When double sampling, metal hose is separated with quick coupling (quick coupling have self-sealing, not will cause medium Leakage), load onto sampling steel cylinder device 7, it is ensured that sampling steel cylinder needle-valve Z7, Z8 are closed, and are repeated the above steps.
As shown in Fig. 2, when sample temperature be greater than 60 DEG C when, first system run cooling arrangement, be then turned on sample into Pipeline out carries out cooling treatment to sample.Note: 1. solenoid valve Z9, Z10 is sampling steel cylinder shut-off valve, and sampling steel is put into before sampling It automatically opened after bottle 7, sample and complete to be automatically closed before sampling steel cylinder 7 is removed.
2. opening solenoid valve Z13 when sampler is out of service or is replaced, emptied by cooling water blowdown pipeline cold But coolant liquid in device.
Before sampling, open solenoid valve Z2, Z4, Z9, Z10 and sampling steel cylinder needle-valve Z7, Z8, starting nitrogen purging device 5 into Residual gas is drained into torch by blow-down pipe 4 by row nitrogen purging, and residual liquid drains into medium by medium blowdown pipeline 3 Blowdown general pipeline, until to 2~3min, after the completion of nitrogen purging, close solenoid valve Z2, Z4, Z9, Z10 and sampling steel cylinder needle-valve Z7, Z8。
Before sampling for the first time, solenoid valve Z11, Z12 are opened, cooling water, cooling water are injected by the cooling water end of cooler 8 It flows out, is recycled from cooling water backwater end, judge whether cooler 8 runs well according to flow switch feedback, run well Solenoid valve Z1, Z5, Z3 are opened afterwards.
Solenoid valve Z1, Z3, Z5 are opened, medium flows to 2 end N2 of media outlet pipeline by 1 end N1 of medium entrance pipeline.Root The medium temperature and pressure data fed back according to temperature-detecting device 9 and pressure-detecting device 6 judge temperature within the allowable range, press Power is stablized, and prompt can carry out in next step;Solenoid valve Z5 is closed, solenoid valve Z9 is opened and steel cylinder needle-valve Z7, Z8 is sampled.According to The media data that temperature and pressure force checking device 6 is fed back judges that pressure is stablized, that is, is considered as medium sampling in sampling steel cylinder and completes, close Solenoid valve Z1, Z3, Z9 and sampling steel cylinder needle-valve Z7, Z8.Solenoid valve Z6 is opened, raffinate is discharged, sampling steel cylinder 7 is removed, it will be golden Belong to hose and be connected to (quick coupling has self-sealing, not will cause medium leakage) with quick coupling, closes solenoid valve Z6, open Solenoid valve Z1, Z5, Z3.
When double sampling, metal hose is separated with quick coupling (quick coupling have self-sealing, not will cause medium Leakage), load onto sampling steel cylinder, it is ensured that steel cylinder needle-valve Z7, Z8 are closed.It repeats the above steps.
Above specific embodiments of the present invention have been described, but the present invention is not limited to above description.For this For the technical staff in field, the equal modification and substitution of any pair of the technical program are all within the scope of the invention.Cause This, made equal transformation and modification, all should be contained within the scope of the invention without departing from the spirit and scope of the invention.

Claims (9)

1. a kind of sampling system, it is characterised in that: blown including medium pipeline, medium blowdown pipeline (3), blow-down pipe (4), nitrogen The medium of sweeping device (5), pressure-detecting device (6) and sampling steel cylinder (7), the medium pipeline passes through medium entrance pipeline (1) end N1 flows to media outlet pipeline (2) end N2, one end of the sampling steel cylinder (7) be connected with medium entrance pipeline (1) and Medium blowdown pipeline (3), the other end are connected with media outlet pipeline (2) and blow-down pipe (4), wherein the nitrogen purges dress Set one end that (5) are connected in parallel on sampling steel cylinder (7) by pipeline and medium entrance pipeline (1);It is described to lead to media outlet pipeline (2) Pressure-detecting device (6) are equipped with the pipeline of blow-down pipe (4).
2. a kind of sampling system according to claim 1, it is characterised in that: the both ends of the sampling steel cylinder (7) are set respectively There are sampling steel cylinder needle-valve Z7 and sampling steel cylinder needle-valve Z8.
3. a kind of sampling system according to claim 1, it is characterised in that: the medium entrance pipeline (1) is equipped with Solenoid valve Z1, the pipeline for being connected with nitrogen purging device (5) are equipped with solenoid valve Z2, and two pipelines it is in parallel after with sampling steel Bottle (7) input end is connected, and sampling steel cylinder shut-off valve Z9 is equipped between the pipeline and sampling steel cylinder (7) after parallel connection.
4. a kind of sampling system according to claim 3, it is characterised in that: the media outlet pipeline (2) is equipped with electricity Magnet valve Z4, blow-down pipe (4) is equipped with solenoid valve Z5, and is connected after two pipelines parallel connections with sampling steel cylinder (7) outlet end, Sampling steel cylinder shut-off valve Z10 is equipped between pipeline and sampling steel cylinder (7) after parallel connection.
5. a kind of sampling system according to claim 1, it is characterised in that: the medium blowdown pipeline (3) is equipped with Solenoid valve Z6, and medium blowdown pipeline (3) is connected with medium blowdown general pipeline.
6. a kind of sampling system according to claim 4, it is characterised in that: the input end of the sampling steel cylinder (7) and go out Connecting pipeline is equipped between mouth end, which is equipped with solenoid valve Z3.
7. a kind of sampling system according to claim 6, it is characterised in that: the medium entrance pipeline (1) and connection Outlet after having the pipeline parallel connection of nitrogen purging device (5) is equipped with cooler (8), and the cooler (8) is connected with cooling water Water supply line and cooling water return pipe line, wherein the cooling water pipeline is equipped with solenoid valve Z11, cooling water return pipe Line is equipped with solenoid valve Z12.
8. a kind of sampling system according to claim 7, it is characterised in that: the cooler (8) passes through cooling water drainage Dirty pipeline is connected with cooling water blowdown general pipeline, wherein the cooling water blowdown pipeline is equipped with solenoid valve Z13.
9. a kind of sampling system according to claim 7, it is characterised in that: the cooler (8) and sampling steel cylinder (7) Connected pipeline is equipped with temperature-detecting device (9).
CN201810951051.0A 2018-08-21 2018-08-21 A kind of sampling system Pending CN109100176A (en)

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Application Number Priority Date Filing Date Title
CN201810951051.0A CN109100176A (en) 2018-08-21 2018-08-21 A kind of sampling system

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Application Number Priority Date Filing Date Title
CN201810951051.0A CN109100176A (en) 2018-08-21 2018-08-21 A kind of sampling system

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CN109100176A true CN109100176A (en) 2018-12-28

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113702103A (en) * 2021-09-10 2021-11-26 江苏信泰化工装备有限公司 Integrated sampling system

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN203405345U (en) * 2012-11-30 2014-01-22 内蒙古神舟硅业有限责任公司 Chlorosilane liquid sampling device
CN205620167U (en) * 2016-05-09 2016-10-05 启东市恒盛仪表设备有限公司 Airtight sample thief
CN106908285A (en) * 2017-04-06 2017-06-30 洛阳中硅高科技有限公司 On-line period device
CN206862711U (en) * 2017-05-27 2018-01-09 爱文思控制系统工程(上海)有限公司 One kind sampling and sample pretreatment system

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN203405345U (en) * 2012-11-30 2014-01-22 内蒙古神舟硅业有限责任公司 Chlorosilane liquid sampling device
CN205620167U (en) * 2016-05-09 2016-10-05 启东市恒盛仪表设备有限公司 Airtight sample thief
CN106908285A (en) * 2017-04-06 2017-06-30 洛阳中硅高科技有限公司 On-line period device
CN206862711U (en) * 2017-05-27 2018-01-09 爱文思控制系统工程(上海)有限公司 One kind sampling and sample pretreatment system

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113702103A (en) * 2021-09-10 2021-11-26 江苏信泰化工装备有限公司 Integrated sampling system

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Application publication date: 20181228