CN109094861A - A kind of packing method of chunk polysilicon - Google Patents

A kind of packing method of chunk polysilicon Download PDF

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Publication number
CN109094861A
CN109094861A CN201710474790.0A CN201710474790A CN109094861A CN 109094861 A CN109094861 A CN 109094861A CN 201710474790 A CN201710474790 A CN 201710474790A CN 109094861 A CN109094861 A CN 109094861A
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CN
China
Prior art keywords
packaging bag
packing method
polysilicon
independent
bag
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710474790.0A
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Chinese (zh)
Inventor
刘小品
杨宇杰
胡旭
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Xinte Energy Co Ltd
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Xinte Energy Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Xinte Energy Co Ltd filed Critical Xinte Energy Co Ltd
Priority to CN201710474790.0A priority Critical patent/CN109094861A/en
Publication of CN109094861A publication Critical patent/CN109094861A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B65CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
    • B65BMACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
    • B65B31/00Packaging articles or materials under special atmospheric or gaseous conditions; Adding propellants to aerosol containers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B65CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
    • B65BMACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
    • B65B51/00Devices for, or methods of, sealing or securing package folds or closures; Devices for gathering or twisting wrappers, or necks of bags
    • B65B51/10Applying or generating heat or pressure or combinations thereof
    • B65B51/22Applying or generating heat or pressure or combinations thereof by friction or ultrasonic or high-frequency electrical means, i.e. by friction or ultrasonic or induction welding
    • B65B51/225Applying or generating heat or pressure or combinations thereof by friction or ultrasonic or high-frequency electrical means, i.e. by friction or ultrasonic or induction welding by ultrasonic welding
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B65CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
    • B65BMACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
    • B65B2220/00Specific aspects of the packaging operation
    • B65B2220/16Packaging contents into primary and secondary packaging
    • B65B2220/20Packaging contents into primary and secondary packaging the primary packaging being bags, the secondary packaging being further bags, the primary bags being either finished or formed concurrently with the secondary bags

Abstract

The present invention provides a kind of packing method of chunk polysilicon comprising following steps: the polysilicon block that weighing finishes is introduced into the first packaging bag;Remove the air in the first packaging bag;Processing is sealed to the first packaging bag;The first packaging bag that sealing finishes is introduced into the second packaging bag;Inert gas is filled with into the gap between the first packaging bag and the second packaging bag;Processing is sealed to the second packaging bag, to form independent packaging bag.Will not only polysilicon be made to be contaminated during transportation using the packaged polysilicon of packing method of the present invention, but also will not phase mutual friction generation pSi powder.

Description

A kind of packing method of chunk polysilicon
Technical field
The present invention relates to technical field of polysilicon production, and in particular to a kind of packing method of chunk polysilicon.
Background technique
The production technology of polysilicon (polycrystalline silicon) is generally, and utilizes generation by Siemens process Alkyl halide (such as trichlorosilane) is deposited into silicon rod, and then silicon rod is ground into the more of minimum pollution by way of hand breaking Crystal silicon block.Polysilicon block with minimum pollution is the ideal material of semiconductor and solar energy, is transported by polysilicon block The defeated probability that should ensure that polysilicon block is contaminated before into client's hand is minimum.
Polysilicon block is the massive material with the non-free flowing of sharp edges, needs to guarantee that its packaging bag is being packed And will not be damaged in process of container transportation, or only puncture first layer packaging bag (i.e. internal layer packaging bag) in the worst case, And overpack bag (i.e. outer packaging bag) is intact, to guarantee that the polysilicon block of minimum pollution will not be in transport to client's hand In process in pollution level increase.Therefore the packing method of polysilicon block just determines polysilicon block during transportation The size for the probability being contaminated.
At present, it is common to use packaging bag be thickness 0.25mm the high-purity PE polybag of bilayer, wherein first layer polybag Size be 580*300mm, the size of second layer polybag is 590*355mm.Specific packing method is, first by polysilicon block Body is introduced into first layer polybag, and first layer polybag is introduced into second again after carrying out heat seal to first layer polybag In layer polybag, heat seal finally is carried out to second layer polybag;Or polysilicon block is being introduced into first layer plastics Bag before just first layer polybag has been inserted into second layer polybag, then to first layer and second layer polybag successively into Row sealing.
Packaged chunk polysilicon will receive vibration in transport and storage process, jolt, when the polycrystalline of clear-cut margin For silicon bulk when orientation is bad in packaging bag, polysilicon block can isolate packaging bag, Huo Zheduo relative to the mobile of packaging bag Pressure of the crystal silicon block in packaging bag can penetrate packaging bag, so that polysilicon block be made to expose from packaging bag.From packaging bag The polysilicon block cognition of middle exposing is directly polluted by adjacent material, and the environment that the block inside packaging bag also suffers from inflow is empty Gas pollution.
In addition, the chunk polysilicon phase mutual friction always during transportation in packaging bag, and generate unnecessary fine Object (i.e. pSi powder), and downstream client also needs to screen out the fine content in chunk polysilicon before further, processing.
Therefore, it is whether polluted caused by polysilicon during transportation, still during transportation because of polysilicon phase Mutual friction and the pSi powder generated, can all bring unnecessary trouble to downstream client.
Summary of the invention
The technical problem to be solved by the present invention is to provide a kind of bulk for the drawbacks described above in the presence of the prior art The packing method of polysilicon will not both be such that polysilicon is contaminated during transportation using the packaged polysilicon of this method, It again will not phase mutual friction generation pSi powder.
Solving technical solution used by present invention problem is:
The present invention provides a kind of packing method of chunk polysilicon comprising following steps:
The polysilicon block that weighing finishes is introduced into the first packaging bag;
Remove the air in the first packaging bag;
Processing is sealed to the first packaging bag;
The first packaging bag that sealing finishes is introduced into the second packaging bag;
Inert gas is filled with into the gap between the first packaging bag and the second packaging bag;
Processing is sealed to the second packaging bag, to form independent packaging bag.
Optionally, first packaging bag and the second packaging bag are all made of high-purity polyethylene plastic bag.
Optionally, vacuumize process is carried out to the air in the first packaging bag using vacuum suction apparatus, thus removal the Air in one packaging bag.
Optionally, processing is sealed to the first packaging bag and the second packaging bag using heat seal device.
Optionally, the inert gas is high pure nitrogen.
Optionally, the linear dimension range of the polysilicon block is 5-150mm;The weight of each independent packaging bag is 10Kg±5g。
Optionally, the total volume of the first packaging bag after sealing and the polysilicon block that is introduced in the first packaging bag is total The ratio range of volume is 1.1-1.3;The totality of the total volume of the second packaging bag after sealing and the first packaging bag after sealing Long-pending ratio range is 2.0-2.3.
Optionally, the packing method further includes following steps: each independent packaging bag is put into corrugated case.
It is optionally, described that each independent packaging bag is put into the step in corrugated case specifically:
Several corrugated paper plates are put into corrugated case to form honeycomb compartment;
An independent packaging bag is put into each of being separated out in small.
Further, further include following steps:
After piling one layer of packaging bag in corrugated case, corrugation partition is placed in this layer of packaging bag;
Several corrugated paper plates are placed on the corrugation partition to form honeycomb compartment;
It is put into an independent packaging bag each of being separated out in small, to be packed into two layers of packaging in corrugated case Bag.
The utility model has the advantages that
After the packing method of chunk polysilicon of the present invention eliminates the air in the first packaging bag, so that the first packaging Biggish relative movement will not occur between chunk polysilicon in bag, both reduced polysilicon block and pierced through the first packaging bag Probability, and fine content will not be generated because being mutually shifted between polysilicon block;It is filled between the second packaging bag and the first packaging bag After entering inert gas, even if polysilicon block has punctured the first packaging bag, what is directly contacted is also inert gas, therefore Polysilicon will not be made by air pollution, moreover it is possible to make the independent packaging bag to be formed in air bag state, to external mechanical punching Hitting can play a buffer role in.
Detailed description of the invention
Fig. 1 is the flow chart of the packing method of chunk polysilicon provided in an embodiment of the present invention.
Specific embodiment
Technical solution in order to enable those skilled in the art to better understand the present invention, with reference to the accompanying drawings and examples to this Invention is described in further detail.
It is more during pack since interior outer bag assembles completion in advance in existing polysilicon block packaging process Crystal silicon block easily falls the pollution that polysilicon is caused in the interlayer of interior outer bag;Packaged polysilicon is being transported and is being stored in a warehouse It will receive vibration in the process, jolt, when orientation is bad in packaging bag for the polysilicon block of clear-cut margin, polysilicon block The mobile pressure that can cut open packaging bag or polysilicon block in packaging bag relative to packaging bag can penetrate packaging bag, from The polysilicon block cognition exposed in packaging bag is directly polluted by adjacent material, and the block inside packaging bag also suffers from inflow Environmental air pollution.
To solve the above-mentioned problems, the present invention provides a kind of packing method of novel chunk polysilicon, mainly for need Transport for long-distance the enterprise of packaged chunk polysilicon, and reduce polysilicon block in transportational process be contaminated it is general Rate.Its packaging process is not only suitable for full automatic mechanical packaging, is also applied for manual operation.It specially uses the first packaging bag After vacuumizing and sealing, then the first packaging bag is introduced into the second packaging bag, and between the first packaging bag and the second packaging bag It is filled with the packing method of high pure nitrogen, to greatly reduce the probability that polysilicon block is contaminated during transportation.Under Face is described in detail by specific embodiment.
As shown in Figure 1, the embodiment of the present invention provides a kind of packing method of chunk polysilicon comprising following steps S101-S106。
S101. the polysilicon block that weighing finishes is introduced into the first packaging bag.
S102. the air in the first packaging bag is removed.
Wherein, vacuum suction apparatus can be used, vacuumize process is carried out to the air in the first packaging bag, thus removal the Air in one packaging bag.It is of course also possible to use the mode of manual squeezing, using fixture or percussion mechanism, using vacuum chamber Deng the air in the first packaging bag of removal.
In the present embodiment, to directly vacuumize process is carried out with the first packaging bag of polysilicon contact of blocks, so that first The irregular polysilicon block accommodated in packaging bag is closely combined together under the action of outer boundary's atmospheric pressure, sharp in this way Biggish relative movement would not occur between polysilicon block and the first packaging bag, so that reducing polysilicon block pierces through the The probability of one packaging bag.
S103. processing is sealed to the first packaging bag.
Wherein, heat seal device can be used, processing is sealed to the first packaging bag.Supersonic thermal setting specifically can be used Sealing device.
More preferably, the total volume of the first packaging bag after vacuumizing and seal and the polysilicon being introduced in the first packaging bag The ratio range of the total volume of block is 1.1-1.3.
S104. the first packaging bag that sealing finishes is introduced into the second packaging bag.
S105. inert gas is filled with into the gap between the first packaging bag and the second packaging bag.
Wherein, the method for being filled with inert gas can use existing sealing gas flush packaging method.
In the present invention, the inert gas refers to chemically inert gas, specially at normal temperature chemically The inactive gas of matter, such as nitrogen are not to refer exclusively to the rare gas such as He-Ne argon krypton xenon radon.
In the present embodiment, chunk polysilicon will be equipped with and vacuumize and seal the second packet of the first packaging bag loading finished After in pack, it is filled with high pure nitrogen between the first packaging bag and the second packaging bag, even when the polycrystalline in the first packaging bag Silicon bulk has punctured the first packaging bag, and what the polysilicon block exposed from the first packaging bag directly contacted is also high pure nitrogen, So that polysilicon not will receive air pollution.
S106. processing is sealed to the second packaging bag, to form independent packaging bag.The independent packaging bag because It is in air bag state filled with inert gas between first packaging bag and the second packaging bag, external mechanical shock can be played slow Punching effect.
Wherein, heat seal device can be used, processing is sealed to the second packaging bag.Supersonic thermal setting specifically can be used Sealing device.
More preferably, the ratio model of the total volume of the second packaging bag after sealing and the total volume of the first packaging bag after sealing It encloses for 2.0-2.3.
In the present embodiment, first packaging bag and the second packaging bag are all made of high-purity polyethylene (polyethylene, letter Claim PE) polybag, high-purity PE polybag have the advantages that antistatic, thicken puncture-resistant, anti-puncture intensity be 6.685N, metal Impurity content is 150.6ppbw, with a thickness of 25.
Moreover, the linear dimension range of the polysilicon block is 5-150mm;It is independent through each of abovementioned steps formation The weight of packaging bag is 10Kg ± 5g.Environment temperature in packaging process is preferably 18-25 DEG C;Relative air humidity is preferably 30-70%.Packaging process should carry out under the clean environment for crossing air filtering.
In addition, the packing method further includes following steps S107 and S108.
S107. each independent packaging bag is put into corrugated case.
S108. joint sealing.
Wherein, step S107 may include following steps S107A-S107B.
S107A. several corrugated paper plates are put into corrugated case to form honeycomb compartment.Such as formed 3 × 5 every Between.
S107B. an independent packaging bag is put into each of being separated out in small.In this step, it need to make each independent Packaging bag is combined closely with surrounding corrugated paper wall, to prevent packaging bag in the small interior play being separated out.
Further, the S107 may also include the steps of S107C-S107E.
S107C. after piling one layer of packaging bag in corrugated case, corrugation partition is placed in this layer of packaging bag.
S107D. several corrugated paper plates are placed on the corrugation partition to form honeycomb compartment.Such as form 3 × 5 compartments.
S107E. an independent packaging bag is put into each of being separated out in small, to pile one layer of packaging bag again, from And two layers of packaging bag is packed into corrugated case.In this step, also need to make each independent packaging bag with surrounding watt Stupefied paper wall is combined closely.
In conclusion the advantage after the packing method use of chunk polysilicon described in the present embodiment is:
1) the first packaging bag is after taking out certain vacuum, the bulk by the effect of external pressure, in the first packaging bag It is mutually closely combined between polysilicon, fine content will not be generated because being mutually shifted between polysilicon block.
2) the first packaging bag will not occur larger after taking out certain vacuum between the chunk polysilicon in the first packaging bag Relative movement, therefore the case where sharp polysilicon scratches packaging bag, can be reduced, so that reducing polysilicon block pierces through the The probability of one packaging bag.
3) high pure nitrogen is filled between the second packaging bag and the first packaging bag, it is ensured that sharp in the worst case It is high pure nitrogen that polysilicon block, which has punctured directly contact after the first packaging bag, is contaminated in air without exposure.
4) the corrugated paper wall of the independent package bag and packing case that are formed is combined closely, and independent packaging bag is in inflatable balloon-like State can play a buffer role in external mechanical shock.
It is understood that the principle that embodiment of above is intended to be merely illustrative of the present and the exemplary implementation that uses Mode, however the present invention is not limited thereto.For those skilled in the art, essence of the invention is not being departed from In the case where mind and essence, various changes and modifications can be made therein, these variations and modifications are also considered as protection scope of the present invention.

Claims (10)

1. a kind of packing method of chunk polysilicon, which comprises the steps of:
The polysilicon block that weighing finishes is introduced into the first packaging bag;
Remove the air in the first packaging bag;
Processing is sealed to the first packaging bag;
The first packaging bag that sealing finishes is introduced into the second packaging bag;
Inert gas is filled with into the gap between the first packaging bag and the second packaging bag;
Processing is sealed to the second packaging bag, to form independent packaging bag.
2. packing method according to claim 1, which is characterized in that first packaging bag and the second packaging bag are all made of High-purity polyethylene plastic bag.
3. packing method according to claim 1, which is characterized in that using vacuum suction apparatus in the first packaging bag Air carries out vacuumize process, thus the air in the first packaging bag of removal.
4. packing method according to claim 1, which is characterized in that using heat seal device to the first packaging bag and the Two packaging bags are sealed processing.
5. packing method according to claim 1, which is characterized in that the inert gas is high pure nitrogen.
6. packing method according to any one of claims 1-5, which is characterized in that the linear ruler of the polysilicon block Very little range is 5-150mm;The weight of each independent packaging bag is 10Kg ± 5g.
7. packing method according to any one of claims 1-5, which is characterized in that the first packaging bag after sealing it is total The ratio range of volume and the total volume for the polysilicon block being introduced in the first packaging bag is 1.1-1.3;Second after sealing The ratio range of the total volume of packaging bag and the total volume of the first packaging bag after sealing is 2.0-2.3.
8. packing method according to any one of claims 1-5, which is characterized in that the packing method further includes as follows Step: each independent packaging bag is put into corrugated case.
9. packing method according to claim 8, which is characterized in that described that each independent packaging bag is put into corrugated paper Step in case specifically:
Several corrugated paper plates are put into corrugated case to form honeycomb compartment;
An independent packaging bag is put into each of being separated out in small.
10. packing method according to claim 9, which is characterized in that further include following steps:
After piling one layer of packaging bag in corrugated case, corrugation partition is placed in this layer of packaging bag;
Several corrugated paper plates are placed on the corrugation partition to form honeycomb compartment;
It is put into an independent packaging bag each of being separated out in small, to be packed into two layers of packaging bag in corrugated case.
CN201710474790.0A 2017-06-21 2017-06-21 A kind of packing method of chunk polysilicon Pending CN109094861A (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109533451A (en) * 2019-01-10 2019-03-29 Oppo(重庆)智能科技有限公司 Storage method
CN113173285A (en) * 2021-05-24 2021-07-27 上海超硅半导体有限公司 Packaging method of silicon wafer
CN113401412A (en) * 2020-03-17 2021-09-17 新特能源股份有限公司 Packaging system and packaging method of polycrystalline silicon
CN115535346A (en) * 2022-12-01 2022-12-30 江苏鑫华半导体科技股份有限公司 Packaging method of polycrystalline silicon block
CN115610727A (en) * 2022-11-10 2023-01-17 内蒙古大全新能源有限公司 Packaging method for irregular polycrystalline silicon lump material

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CN102633002A (en) * 2011-02-09 2012-08-15 瓦克化学股份公司 Method and device for dosing and packaging polysilicon chunks and dosing and packaging unit
JP5514081B2 (en) * 2010-11-12 2014-06-04 株式会社トクヤマ Method for manufacturing polysilicon package
CN103863586A (en) * 2012-12-14 2014-06-18 瓦克化学股份公司 Packing polycrystalline silicon

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CN101678905A (en) * 2007-06-13 2010-03-24 瓦克化学股份公司 Method and device for packaging polycrystalline bulk silicon
CN101461756A (en) * 2007-12-17 2009-06-24 丽珠集团利民制药厂 Medicine liquid flexible package and method for packing the same
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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109533451A (en) * 2019-01-10 2019-03-29 Oppo(重庆)智能科技有限公司 Storage method
CN113401412A (en) * 2020-03-17 2021-09-17 新特能源股份有限公司 Packaging system and packaging method of polycrystalline silicon
CN113173285A (en) * 2021-05-24 2021-07-27 上海超硅半导体有限公司 Packaging method of silicon wafer
CN115610727A (en) * 2022-11-10 2023-01-17 内蒙古大全新能源有限公司 Packaging method for irregular polycrystalline silicon lump material
CN115535346A (en) * 2022-12-01 2022-12-30 江苏鑫华半导体科技股份有限公司 Packaging method of polycrystalline silicon block
CN115535346B (en) * 2022-12-01 2023-03-14 江苏鑫华半导体科技股份有限公司 Packaging method of polycrystalline silicon block

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