CN109085236A - Utilize the method for air bubble content in ultrasound examination resin and curing agent de-aeration - Google Patents
Utilize the method for air bubble content in ultrasound examination resin and curing agent de-aeration Download PDFInfo
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- CN109085236A CN109085236A CN201810964639.XA CN201810964639A CN109085236A CN 109085236 A CN109085236 A CN 109085236A CN 201810964639 A CN201810964639 A CN 201810964639A CN 109085236 A CN109085236 A CN 109085236A
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- 229920005989 resin Polymers 0.000 title claims abstract description 98
- 239000011347 resin Substances 0.000 title claims abstract description 98
- 238000002604 ultrasonography Methods 0.000 title claims abstract description 42
- 238000000034 method Methods 0.000 title claims abstract description 41
- 238000005273 aeration Methods 0.000 title claims abstract description 37
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 95
- 238000001514 detection method Methods 0.000 claims abstract description 35
- 230000005611 electricity Effects 0.000 claims abstract description 22
- 230000007547 defect Effects 0.000 claims abstract description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 13
- 230000003068 static effect Effects 0.000 claims abstract description 11
- 238000004581 coalescence Methods 0.000 claims abstract description 7
- 239000000523 sample Substances 0.000 claims description 40
- 238000004458 analytical method Methods 0.000 claims description 24
- 238000013480 data collection Methods 0.000 claims description 17
- 230000008569 process Effects 0.000 claims description 13
- 230000000712 assembly Effects 0.000 claims description 12
- 238000000429 assembly Methods 0.000 claims description 12
- 239000003822 epoxy resin Substances 0.000 claims description 11
- 229920000647 polyepoxide Polymers 0.000 claims description 11
- 238000005259 measurement Methods 0.000 claims description 7
- 238000005086 pumping Methods 0.000 claims description 6
- 238000010586 diagram Methods 0.000 claims description 5
- 238000003672 processing method Methods 0.000 claims description 4
- 238000003860 storage Methods 0.000 claims description 4
- 238000012360 testing method Methods 0.000 claims description 4
- 230000003321 amplification Effects 0.000 claims description 3
- 230000007423 decrease Effects 0.000 claims description 3
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 claims description 3
- 238000003199 nucleic acid amplification method Methods 0.000 claims description 3
- 238000007711 solidification Methods 0.000 claims description 3
- 230000008023 solidification Effects 0.000 claims description 3
- 230000007717 exclusion Effects 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 description 9
- 239000007788 liquid Substances 0.000 description 7
- 239000003292 glue Substances 0.000 description 5
- 238000009826 distribution Methods 0.000 description 3
- 230000005540 biological transmission Effects 0.000 description 2
- 238000007689 inspection Methods 0.000 description 2
- 238000009434 installation Methods 0.000 description 2
- 238000012423 maintenance Methods 0.000 description 2
- 239000011159 matrix material Substances 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 230000008439 repair process Effects 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000005266 casting Methods 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000007405 data analysis Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- -1 divides three root Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 230000000644 propagated effect Effects 0.000 description 1
- 238000004445 quantitative analysis Methods 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 238000004513 sizing Methods 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N29/00—Investigating or analysing materials by the use of ultrasonic, sonic or infrasonic waves; Visualisation of the interior of objects by transmitting ultrasonic or sonic waves through the object
- G01N29/02—Analysing fluids
- G01N29/032—Analysing fluids by measuring attenuation of acoustic waves
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2291/00—Indexing codes associated with group G01N29/00
- G01N2291/02—Indexing codes associated with the analysed material
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- G01N2291/02433—Gases in liquids, e.g. bubbles, foams
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Abstract
The invention discloses a kind of methods using air bubble content in ultrasound examination resin and curing agent de-aeration, first with the air bubble content of ultrasonic unit detection pure water under static state, and according to the energy value one that ultrasonic unit in the detection captures, energy reference value is determined;Then the air bubble content in ultrasonic unit detection resin and/or curing agent de-aeration is utilized, the energy value two that ultrasonic unit in the detection captures is compared with energy reference value, after energy value two is higher than energy reference value and predetermined hold-time, then determine that the air bubble content in resin and/or curing agent reaches standard.The air bubble content trend of energy rapid qualitative of the present invention reflected in resin and/or curing agent de-aeration in solution, it effectively avoids that wind electricity blade is caused to whiten to form the defect of various grades due to bubble coalescence, exclusion is not normally functioning since these defects may cause blower, even results in the hidden danger that wind electricity blade is scrapped.
Description
Technical field
It is especially a kind of de- using ultrasound examination resin and curing agent the present invention relates to wind electricity blade manufacturing technology field
The method of air bubble content during bubble.
Background technique
Wind electricity blade is shell structure made of a kind of composite material, divides three root, shell, web parts in structure,
For wind-power electricity generation.To obtain more powerful, more regular wind field environment, the installation of blower is gone to via land away from seashore
The increasingly remoter sea of line, this transformation propose increasingly higher demands to the safety of wind electricity blade, reliability.And wind-powered electricity generation leaf
In the scale manufacturing process of piece, occur that wind electricity blade is caused to whiten to form the defect of various grades due to bubble coalescence often,
Though these defects repair in factory, its hidden danger buried may cause blower and be not normally functioning, and even result in wind-powered electricity generation
Thus blade rejection brings huge maintenance cost or other economic losses to blade factory, main engine plants.
The reason of being analyzed through field investigation, leading to bubble coalescence in wind electricity blade production process first is that due to wind electricity blade
Main raw material(s) epoxy resin and its curing agent itself or its mixed process in there is or generate bubble, though produced on-site process
In deaeration processing can be carried out to one-component and mixed resin, and artificial judgment whether there is bubble, but mixed tree
Microbubble naked eyes in rouge are difficult to.It is still at present to be in for the detection of matrix resin air bubble content in wind electricity blade industry
Blank stage has a kind of method using ultrasound examination bubble, this method is not by connecting through inspection information in medical industry
Ultrasonic wave is captured continuously, determines to whether there is bubble in transfusion system, but there are bubbles in raw material system known to us
In the case of, what this method cannot be qualitative or quantitative judges the content of bubble, therefore is badly in need of a kind of simple, reliable method, realizes
The content of bubble in resin after mixing quickly is detected at the scene.
In the prior art, application No. is the applications for a patent for invention of CN201810083400.1 to disclose a kind of ultrasonic bubble
Detection method and system, including obtaining bubble velocity and largest air bubbles volume threshold in test object;When determining bubble detection
Detection node interval time;In each detection node, ultrasonic detecting equipment emits ultrasonic wave to test object, and receives detection
Object reflection or the ultrasonic wave of transmission analyze received ultrasonic wave to judge whether the detection node detects bubble;Statistics connects
The number of the continuous detection cycle for detecting bubble appearance, and bubble is calculated according to detection node interval time and bubble velocity
Bulking value.Bubble class in a kind of quantitative analysis slab is disclosed application No. is the application for a patent for invention of CN201310020345.9 to lack
The method for falling into distribution.Its main thought is to carry out slice sampling to casting blank section, then by X-ray diffractometer to each thin slice
Internal bubble class defect is imaged, and size, quantity and the distribution of different bubble class defects in sliced piece specimen are obtained;Pass through again
Summarize and finally obtains bubble class defect in slab, size, the overall distribution of quantity rule with the size of defect, position in statistical picture
Rule.The above prior art is not for how to realize at the scene after quickly detection mixing in resin in wind electricity blade manufacturing process
The content of bubble.
Summary of the invention
The present invention provides a kind of method using air bubble content in ultrasound examination resin and curing agent de-aeration, energy
The content of bubble in solution after field quick detection resin and curing agent mixing is realized in wind electricity blade manufacturing process.
The technical scheme is that a kind of utilize air bubble content in ultrasound examination resin and curing agent de-aeration
Method, first with the air bubble content of ultrasonic unit detection pure water under static state, and with ultrasonic unit in the detection
According to the energy value one of capture, energy reference value is determined;Then using ultrasonic unit detection resin and/or curing agent de-
The energy value two that ultrasonic unit in the detection captures is compared by the air bubble content during bubble with energy reference value, from
And whether the air bubble content to determine in resin and/or curing agent reaches standard, when energy value two is higher than energy reference value and holds
After the continuous predetermined time, then determine that the air bubble content in resin and/or curing agent reaches standard.
The method using air bubble content in ultrasound examination resin and curing agent de-aeration, including walk as follows
It is rapid:
Step 1: obtaining energy reference value: getting out ultrasonic wave detecting system, ultrasonic wave detecting system include ultrasonic unit and
Control analysis module;The air bubble content of pure water under static state is detected, obtains energy reference value, and energy a reference value is stored up
In the presence of in control analysis module;
Step 2: the air bubble content of detection resin and/or curing agent specifically includes as follows step by step:
S1: probe placement: probe is placed in resin and/or curing agent, it is ensured that two probe spacing are stable in detection process and visit
Head does not shake;
S2: ultrasound examination: resin and/or curing agent start deaeration, de-aeration include I-stage andStage, I-stage are tree
Air bubble content in rouge and/or curing agent gradually decreases the stage,Stage is in resin under current pumping state and/or curing agent
Air bubble content reach the minimum stage;Meanwhile ultrasonic unit is opened, start to detect resin and/or curing agent in deaeration
Air bubble content in journey;
S3: collect data: collect the data that ultrasonic unit detects by data collection module: ultrasonic wave passes through in I-stage
Resin and/or curing agent decaying after energy variation data andWhat ultrasonic unit can capture in the stage reaches acme
Energy datum;
S4: obtain ultrasound examination energy diagram: the data being collected into are sent to control analysis module by data collection module, control
Analysis module is analyzed and processed the data received, and real-time synchronization is drawn in resin and/or curing agent de-aeration and surpassed
Sonic detection energy curve figure, and shown by display module real-time synchronization;
S5: ultrasound examination energy curve figure in observation resin and/or curing agent de-aeration, whenUltrasonic unit in stage
After the energy value for reaching acme that can be captured is located at a certain numberical range and predetermined hold-time, stops resin and/or consolidate
Agent deaeration, is simultaneously stopped ultrasound examination;
Step 3: it compares to determine:
It willThe energy value that stage ultrasound device is captured is compared with energy reference value, determines resin and/or curing agent
Whether can be used for producing, whenWhen the energy value that stage ultrasound device is captured is higher than energy reference value, the resin and/or solid
Agent can be used for producing.
In step 1, when detecting the air bubble content of pure water under static state, making probe apart is preset distance,
Under the preset distance, the ceiling capacity that ultrasonic unit can capture is 300000(mV*ms)/S, determine that energy reference value is
300000(mV*ms)/S.
Probe is installed using tooling;Two of ultrasonic unit, which pop one's head in, is separately fixed at the two sides of a tooling, and two
A probe is oppositely arranged.
The tooling includes being mounted on hold resin and/or slide assemblies on curing agent device, be mounted on slide assemblies
On probe mounting base and the fixing piece that is arranged in probe mounting base, probe mounting base can move, and move along slide assemblies
It can be fixed on slide assemblies by fixing piece after moving required position.
It is detected using ultrasonic wave detecting system, the ultrasonic wave detecting system includes ultrasonic unit, data collection
Module, display module, memory module, control analysis module and the tooling for installing probe;The ultrasonic unit connection number
According to collection module, ultrasonic unit, data collection module, display module, memory module are all connected with control analysis module;Ultrasonic wave
Device ultrasonic wave for transmitting and receiving;Data collection module is for collecting the data that ultrasonic unit receives, and by data
Pass to control analysis module;Control analysis module is for being analyzed and processed the data received, drafting energy curve figure,
It obtains testing result, and sends memory module storage for all data, send display module in real time for energy curve graph and show
Show;Memory module is for storing all data, including energy reference value, energy value two and energy curve figure;Display module is used for
It real-time display energy curve figure and is convenient for operating.
Ultrasonic unit is ultrasonic measurement instrument, and ultrasonic measurement instrument includes supersonic generator, ultrasonic wave transducer
Device and amplification filter.
A kind of resin and curing agent mixed liquor deaeration processing method utilize ultrasound examination resin and solidification including above-mentioned
The method of air bubble content in agent de-aeration;By using ultrasonic unit to detect resin and curing agent mixing in the deaeration process
Air bubble content in liquid, so that the air bubble content variation of the reacting resin of rapid qualitative and curing agent mixed liquor in the deaeration process becomes
The energy value in acme that gesture and ultrasonic unit are captured, and so that energy value is reached available by using predetermined air-extractor
In the standard of production, avoid causing wind electricity blade to whiten to form defect due to bubble coalescence.
De-aeration include I-stage andStage, I-stage are that the air bubble content in resin and curing agent mixed liquor gradually drops
Low order section,Stage is that the air bubble content under current pumping state in resin and curing agent mixed liquor reaches the minimum stage;It is described
Resin is epoxy resin.
Beneficial effects of the present invention: the present invention detects resin using ultrasonic unit in wind electricity blade manufacturing for the first time
And its air bubble content in curing agent, the bubble of energy rapid qualitative reflected in resin and/or curing agent de-aeration in solution
Content trend is the detection method for having very much application value.It effectively avoids that wind electricity blade is caused to whiten to be formed respectively due to bubble coalescence
The defect of kind grade, exclusion are not normally functioning since these defects may cause blower, even result in what wind electricity blade was scrapped
Thus hidden danger is greatly reduced to blade factory, the huge maintenance cost of main engine plants' bring or other economic losses.This method letter
It is single, reliable, the matrix resin class material of wind electricity blade suitable for wind electricity blade industry.
Detailed description of the invention
Fig. 1 is ultrasound examination energy curve figure in normal capacity resin and curing agent mixed liquor de-aeration;Fig. 2 is
Ultrasonic unit schematic diagram.
Specific embodiment
Embodiment one:
Fig. 1 to Fig. 2 is please referred to, a method of it is first using air bubble content in ultrasound examination resin and curing agent de-aeration
First, the air bubble content by detection pure water under static state, obtains energy reference value.Ultrasonic unit is connected, is adopted
After being fixed probe with tooling, probe is placed in pure water.Pay attention to not thering is particle, impurity or other pollutants in water.It opens
Ultrasonic unit and its data acquisition relevant device and software are opened, is kept for tooling static a period of time, then adjust tooling position, then
Keep the static acquisition standard energy figure of tooling.Stable data can be obtained when probe is fixed on a certain position, but adjust probe position
Energy value has larger fluctuation when setting.The reason is that the detection method location sensitive, the reason of belonging to the detection method itself.Make to visit
Head is at a distance of being required preset distance appropriate, and under the preset distance, the ceiling capacity that ultrasonic unit can capture is about
300000(mV*ms)/S.It is carried when multinomial in Fig. 1 is original system machine forming curves, is that waveform is more with certain
Item formula is converted to curve representated by multinomial in Fig. 1.
It is then detected that the air bubble content of resin and/or curing agent solution.It is specific include again it is following step by step:
1, ultrasonic unit is connected;
2, probe placement.Two probes of ultrasonic unit are fixed in tooling, and ensure that two probes are opposite.By ultrasonic wave
The probe of device is placed in epoxy resin and its curing agent mixed liquor, it is ensured that spacing of popping one's head in detection process is stable and does not shake.
This kind of laying method should be noted that protection probe is not contaminated.
3, the energy diagram of epoxy resin and its curing agent is obtained.The probe being fixed in tooling is put into need in solution
Notice that protection probe is not contaminated.Open ultrasonic unit and its data acquisition relevant device and software.Open ultrasonic unit
And its data acquire relevant device and software, detect air bubble content in epoxy resin and its curing agent.
4, data collection and analysis.Ultrasound examination after certain brand epoxy resin and its curing agent mixing in de-aeration
Curve (ultrasound examination energy curve figure in normal capacity resin and curing agent mixed liquor de-aeration), as shown in Figure 1.In I
Air bubble content is lower and lower in stage de-aeration, and the energy that ultrasonic wave passes through glue decaying is fewer and fewer, thus energy curve
It is higher and higher;Work as arrivalStage, ultrasonic energy curve reach acme can tend towards stability (i.e. near the value of peak it is a certain compared with
Fluctuated between narrow numberical range), illustrate the content of bubble in glue (epoxy resin and curing agent mixed liquor) to reach current pumping
Minimum under gaseity.Checked the stabilization sub stage by energy curve (Stage) whether the energy that is captured be higher than 300000
(mV*ms/S), determine whether mixed liquor (epoxy resin and curing agent mixed liquor) can be used for producing.When ultrasonic unit is captured
Energy be higher than 300000 (mV*ms/S), the epoxy resin and its curing agent mixed liquor can be used for producing.Standard is such as not achieved,
Replaceable air-extractor as needed increases pumping strength, continues to carry out deaeration processing to resin and curing agent mixed liquor, directly
Until reaching standard.
This programme principle is described as follows.Ultrasonic unit (ultrasonic measurement instrument), please refers to Fig. 2.
Ultrasonic wave is propagated in uniform dielectric by rectilinear direction, but reaches interface or when encountering different medium also like light wave one
Sample generate reflection with reflect and submit to the similar reflection of geometric optics, the law of refraction, according to ultrasonic wave in gas, liquid, solid
Absorption and decaying in body is different, is emitted using transmission beam method come detecting ultrasonic wave and whether receive between energy converter has gas to deposit
So that air bubble content detection device be made.
Air bubble content in glue is detected, is equal to the ultrasonic examination of continuous media, the bubble in glue can be regarded as
The internal flaw of liquid, when zero defect in liquid, ultrasonic wave passes through the energy attenuation very little of liquid, and energy converter receives super
Acoustic wave energy is stronger;When there is bubble, ultrasonic wave major part energy is actually taken up by gas, the energy that at this moment ultrasonic transducer receives
Measure very little.
Ultrasonic equipment emits and receives ultrasonic wave, is characterized in glue by receiving the energy size that energy converter receives
Air bubble content.Resin bubble is more, and the loss that energy penetrates resin is more, and final received energy is with regard to smaller, on software
The energy value of display is lower.
Ultrasonic wave in pure water can be stablized the energy of capture as energy base by basic bubble-free under stationary state in pure water
It is available then to determine that the air bubble content in resin has reached when the energy for stablizing capture in resin is higher than energy reference value for quasi- value
In the standard of production.
This programme can be used for measuring other liquid air bubble contents.Tooling up-sizing or diminution ruler in this programme
It is very little.
Embodiment two:
A method of using air bubble content in ultrasound examination resin and curing agent de-aeration, include the following steps:
Step 1: obtaining energy reference value: getting out ultrasonic wave detecting system, ultrasonic wave detecting system include ultrasonic unit and
Control analysis module;The air bubble content of pure water under static state is detected, obtains energy reference value, and energy a reference value is stored up
In the presence of in control analysis module;Make probe at a distance of for preset distance, under the preset distance, maximum that ultrasonic unit can capture
Energy is 300000(mV*ms)/S, determine that energy reference value is 300000(mV*ms)/S.
Step 2: the air bubble content of detection resin and/or curing agent solution in the deaeration process obtains ultrasonic unit energy
The energy value two enough captured;
S1: probe probe placement: is installed using tooling;Two probes of ultrasonic unit are separately fixed in two toolings,
And two probes are oppositely arranged;Tooling includes being mounted on to hold resin and/or the slide assemblies on curing agent solution device, installation
Probe mounting base on slide assemblies can be moved with the fixing piece popped one's head in mounting base, probe mounting base is arranged in along slide assemblies
It is dynamic, and can be fixed on slide assemblies by fixing piece after being moved to required position;
S2: ultrasound examination: resin and/or curing agent solution start deaeration, de-aeration include I-stage andStage, I-stage
The stage is gradually decreased for the air bubble content in resin and/or curing agent solution,Stage be current pumping state under resin and/or
Air bubble content in curing agent solution reaches the minimum stage;Meanwhile ultrasonic unit is opened, start to detect resin and/or is consolidated
Air bubble content in agent solution de-aeration;
S3: collect data: collect the data that ultrasonic unit detects by data collection module: ultrasonic wave passes through in I-stage
Resin and/or curing agent solution decaying after energy variation data andWhat ultrasonic unit can capture in the stage reaches peak
The energy datum of phase;
S4: obtain the ultrasound examination energy diagram of resin and/or curing agent solution: data collection module sends out the data being collected into
Give control analysis module, control analysis module is analyzed and processed the data received, and real-time synchronization draw resin and/
Or ultrasound examination energy curve figure in curing agent solution de-aeration, and shown by display module real-time synchronization;
S5: ultrasound examination energy curve figure in observation resin and/or curing agent solution de-aeration, whenUltrasonic wave in stage
After the energy value (energy value two) that device can capture reach acme is located at a certain numberical range and predetermined hold-time, stop
Only resin and/or curing agent solution deaeration, are simultaneously stopped ultrasound examination;
Step 3: it compares to determine:
It willThe energy value that stage ultrasound device is captured is compared with energy reference value, determines resin and/or curing agent
Whether solution, which can be used for, produces, whenThe energy value that stage ultrasound device is captured be higher than energy reference value when, the resin and/
Or curing agent can be used for producing.It is judged by observing energy curve figure in real time.
Detected using ultrasonic wave detecting system, ultrasonic wave detecting system include ultrasonic unit, data collection module,
Display module, memory module, control analysis module and the tooling for installing probe;The ultrasonic unit connects data collection
Module, ultrasonic unit, data collection module, display module, memory module are all connected with control analysis module;Ultrasonic unit is used
In transmitting and receive ultrasonic wave;Data collection module is passed data to for collecting the data that ultrasonic unit receives
Control analysis module;Control analysis module draws energy curve figure, obtains inspection for being analyzed and processed to the data received
Survey as a result, and by all data be sent to memory module storage, send display module in real time for energy curve graph and show;Storage
Module is for storing all data, including energy reference value, energy value two and energy curve figure;Display module is used for real-time display
It energy curve figure and is convenient for operating.Ultrasonic unit is ultrasonic measurement instrument, and ultrasonic measurement instrument includes ultrasonic wave
Generator, ultrasonic transducer and amplification filter.
A kind of resin and curing agent mixed liquor deaeration processing method utilize ultrasound examination resin and solidification including above-mentioned
The method of air bubble content in agent de-aeration;By using ultrasonic unit to detect resin and curing agent mixing in the deaeration process
Air bubble content in liquid, so that the air bubble content variation of the reacting resin of rapid qualitative and curing agent mixed liquor in the deaeration process becomes
The energy value in acme that gesture and ultrasonic unit are captured, and so that energy value is reached available by using predetermined air-extractor
In the standard of production, avoid causing wind electricity blade to whiten to form defect due to bubble coalescence.Resin is epoxy resin.
Above two embodiments do not collide or do not repeat place, can mutually share or general.
The foregoing is only a preferred embodiment of the present invention, is not intended to restrict the invention, for the skill of this field
For art personnel, the invention may be variously modified and varied.All within the spirits and principles of the present invention, made any to repair
Change, equivalent replacement, improvement etc., is all included in the scope of protection of the present invention.
Claims (9)
1. a kind of method using air bubble content in ultrasound examination resin and curing agent de-aeration, characterized in that first with
Ultrasonic unit detects the air bubble content of pure water under static state, and the energy value captured with ultrasonic unit in the detection
According to one, energy reference value is determined;Then the gas using ultrasonic unit detection resin and/or curing agent in the deaeration process
Content is steeped, the energy value two that ultrasonic unit in the detection captures is compared with energy reference value, thus to determine resin
And/or whether the air bubble content in curing agent reaches standard, after energy value two is higher than energy reference value and predetermined hold-time,
Then determine that the air bubble content in resin and/or curing agent reaches standard.
2. the method according to claim 1 using air bubble content in ultrasound examination resin and curing agent de-aeration,
It is characterized in that including the following steps:
Step 1: obtaining energy reference value: getting out ultrasonic wave detecting system, ultrasonic wave detecting system include ultrasonic unit and
Control analysis module;The air bubble content of pure water under static state is detected, obtains energy reference value, and energy a reference value is stored up
In the presence of in control analysis module;
Step 2: the air bubble content of detection resin and/or curing agent specifically includes as follows step by step:
S1: probe placement: probe is placed in resin and/or curing agent, it is ensured that two probe spacing are stable in detection process and visit
Head does not shake;
S2: ultrasound examination: resin and/or curing agent start deaeration, de-aeration include I-stage andStage, I-stage are tree
Air bubble content in rouge and/or curing agent gradually decreases the stage,Stage is in resin under current pumping state and/or curing agent
Air bubble content reach the minimum stage;Meanwhile ultrasonic unit is opened, start to detect resin and/or curing agent in deaeration
Air bubble content in journey;
S3: collect data: collect the data that ultrasonic unit detects by data collection module: ultrasonic wave passes through in I-stage
Resin and/or curing agent decaying after energy variation data andWhat ultrasonic unit can capture in the stage reaches acme
Energy datum;
S4: obtain ultrasound examination energy diagram: the data being collected into are sent to control analysis module by data collection module, control
Analysis module is analyzed and processed the data received, and real-time synchronization is drawn in resin and/or curing agent de-aeration and surpassed
Sonic detection energy curve figure, and shown by display module real-time synchronization;
S5: ultrasound examination energy curve figure in observation resin and/or curing agent de-aeration, whenUltrasonic unit in stage
After the energy value for reaching acme that can be captured is located at a certain numberical range and predetermined hold-time, stops resin and/or consolidate
Agent deaeration, is simultaneously stopped ultrasound examination;
Step 3: it compares to determine:
It willThe energy value that stage ultrasound device is captured is compared with energy reference value, determines resin and/or curing agent is
It is no to can be used for producing, whenWhen the energy value that stage ultrasound device is captured is higher than energy reference value, the resin and/or solidification
Agent can be used for producing.
3. the method according to claim 2 using air bubble content in ultrasound examination resin and curing agent de-aeration,
It is characterized in that, when detecting the air bubble content of pure water under static state, making probe apart is pre- spacing in step 1
From under the preset distance, the ceiling capacity that ultrasonic unit can capture is 300000(mV*ms)/S, determine energy reference value
For 300000(mV*ms)/S.
4. the side according to claim 2 or 3 using air bubble content in ultrasound examination resin and curing agent de-aeration
Method, characterized in that probe is installed using tooling;Two of ultrasonic unit, which pop one's head in, is separately fixed at the two sides of a tooling,
And two probes are oppositely arranged.
5. the method according to claim 4 using air bubble content in ultrasound examination resin and curing agent de-aeration,
It is characterized in that the tooling includes being mounted on hold resin and/or slide assemblies on curing agent device, be mounted on slide assemblies
On probe mounting base and the fixing piece that is arranged in probe mounting base, probe mounting base can move, and move along slide assemblies
It can be fixed on slide assemblies by fixing piece after moving required position.
6. the method according to claim 2 using air bubble content in ultrasound examination resin and curing agent de-aeration,
It is characterized in that being detected using ultrasonic wave detecting system, the ultrasonic wave detecting system includes ultrasonic unit, data collection
Module, display module, memory module, control analysis module and the tooling for installing probe;The ultrasonic unit connection number
According to collection module, ultrasonic unit, data collection module, display module, memory module are all connected with control analysis module;Ultrasonic wave
Device ultrasonic wave for transmitting and receiving;Data collection module is for collecting the data that ultrasonic unit receives, and by data
Pass to control analysis module;Control analysis module is for being analyzed and processed the data received, drafting energy curve figure,
It obtains testing result, and sends memory module storage for all data, send display module in real time for energy curve graph and show
Show;Memory module is for storing all data, including energy reference value, energy value two and energy curve figure;Display module is used for
It real-time display energy curve figure and is convenient for operating.
7. the method according to claim 1 using air bubble content in ultrasound examination resin and curing agent de-aeration,
It is characterized in that ultrasonic unit is ultrasonic measurement instrument, ultrasonic measurement instrument includes supersonic generator, ultrasonic wave transducer
Device and amplification filter.
8. a kind of resin and curing agent mixed liquor deaeration processing method, characterized in that utilize ultrasound including described in claim 1
The method that wave detects air bubble content in resin and curing agent de-aeration;By using ultrasonic unit to detect in the deaeration process
Air bubble content in resin and curing agent mixed liquor, so that the reacting resin of rapid qualitative and curing agent mixed liquor are in the deaeration process
Air bubble content variation tendency and the energy value in acme that is captured of ultrasonic unit, and by using predetermined air-extractor
So that energy value is reached the standard that can be used for producing, avoids causing wind electricity blade to whiten to form defect due to bubble coalescence.
9. resin according to claim 8 and curing agent mixed liquor deaeration processing method, characterized in that de-aeration includes
I-stage andStage, I-stage are that the air bubble content in resin and curing agent mixed liquor gradually decreases the stage,Stage is current takes out
Air bubble content under gaseity in resin and curing agent mixed liquor reaches the minimum stage;The resin is epoxy resin.
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