CN109078585A - A kind of Chemical Manufacture hydrogenation reaction efficiency optimization method - Google Patents
A kind of Chemical Manufacture hydrogenation reaction efficiency optimization method Download PDFInfo
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- CN109078585A CN109078585A CN201811115967.9A CN201811115967A CN109078585A CN 109078585 A CN109078585 A CN 109078585A CN 201811115967 A CN201811115967 A CN 201811115967A CN 109078585 A CN109078585 A CN 109078585A
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- hydrogenation reaction
- optimization method
- reaction efficiency
- chemical manufacture
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- 238000000034 method Methods 0.000 title claims abstract description 34
- 238000005984 hydrogenation reaction Methods 0.000 title claims abstract description 25
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 22
- 239000000126 substance Substances 0.000 title claims abstract description 19
- 238000005457 optimization Methods 0.000 title claims abstract description 17
- 238000006243 chemical reaction Methods 0.000 claims abstract description 13
- 238000003756 stirring Methods 0.000 claims description 60
- 230000007246 mechanism Effects 0.000 claims description 55
- 239000007788 liquid Substances 0.000 claims description 39
- 238000007599 discharging Methods 0.000 claims description 9
- 230000009471 action Effects 0.000 claims description 8
- 230000000694 effects Effects 0.000 claims description 6
- 238000009826 distribution Methods 0.000 claims description 4
- 238000009434 installation Methods 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 2
- 238000005096 rolling process Methods 0.000 claims description 2
- 230000008450 motivation Effects 0.000 claims 1
- 238000012824 chemical production Methods 0.000 abstract description 2
- 239000007791 liquid phase Substances 0.000 description 8
- 230000009514 concussion Effects 0.000 description 4
- 239000007789 gas Substances 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 238000010586 diagram Methods 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 229910000831 Steel Inorganic materials 0.000 description 2
- 238000013019 agitation Methods 0.000 description 2
- 238000005238 degreasing Methods 0.000 description 2
- 230000005611 electricity Effects 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 239000012071 phase Substances 0.000 description 2
- 239000010959 steel Substances 0.000 description 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 230000005587 bubbling Effects 0.000 description 1
- 229910002091 carbon monoxide Inorganic materials 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000004517 catalytic hydrocracking Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000000295 fuel oil Substances 0.000 description 1
- BGOFCVIGEYGEOF-UJPOAAIJSA-N helicin Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1OC1=CC=CC=C1C=O BGOFCVIGEYGEOF-UJPOAAIJSA-N 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 238000004445 quantitative analysis Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/08—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles
- B01J8/10—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles moved by stirrers or by rotary drums or rotary receptacles or endless belts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The present invention relates to chemical production technical fields, specifically a kind of Chemical Manufacture hydrogenation reaction efficiency optimization method, method includes the following steps: S1, reaction solution is added in hydrogenator, then free-standing oscillator is put into hydrogenator, and free-standing oscillator suspends or swims in reaction solution；Then S2 starts hydrogenator and free-standing oscillator, is reacted.This method cooperates the hydrogenator work of inventor's design by the free-standing oscillator of setting, realizes and reaction solution is sufficiently stirred, the efficiency of the reaction greatly speeded up.
Description
Technical field
The present invention relates to chemical production technical field, specifically a kind of Chemical Manufacture hydrogenation reaction efficiency optimization side
Method.
Background technique
Hydrogenator is a very important equipment in Organic Chemistry Laboratory and actual production process, not only can be with
Container as hydrogenation reaction, and can also be used for liquids and gases and need well-mixed occasion.Hydrogenator is usually used in
The heavies hydrogenator for being most difficult to utilize in petroleum industry there is into extensive purposes in terms of chemical pharmacy, can be used as production
The infrastructure device that product exploitation, organic chemical and pharmaceuticals are studied, it may also be used for catalyst in quantitative analysis industrial process
Activity.Common hydrogenator is roughly divided into two classes: one kind is for high boiling liquid or solid；The liquid-phase hydrogenatin of raw material
Journey, such as the hydrocracking of oil hydrogenation, heavy oil product.Liquid-phase hydrogenatin often carries out under elevated pressure, process can be it is intermittent,
It is also possible to continuous.Interval liquid-phase hydrogenatin is frequently with autoclave pressure or bubbling reactor with agitating device.Continuous Liquid Phase adds
The tubular reactor that trickle bed reactor or gas, liquid, solid three-phase continuously flow in the same direction can be used in hydrogen.Another kind of reactor is used for gas
Mutually continuous hydrogenation process, such as benzene normal pressure gas phase hydrogenation preparing cyclohexane, carbon monoxide high pressure vapor synthesizing methanol by hydrogenating, reactor
Type can be shell and tube or tower.
However traditional liquid phase hydrogenation reactor is in use, in agitation, liquid can rotate with agitating paddle, but
It is that the intracorporal liquid up-flow effect of kettle is bad, the liquid of autoclave body bottom and the liquid mixed effect on autoclave body top are not ideal enough, liquid
Body mixing is enough uneven, the time needed for also adding stirring production, reduces production efficiency；Liquid stirs for a long time inside the shell
After mixing, understands and attached a large amount of liquid on wall inside the shell, influence the circulation of liquid, be unfavorable for the stirring of agitating paddle.
Summary of the invention
For the problems of the prior art, the present invention provides a kind of Chemical Manufacture hydrogenation reaction efficiency optimization method,
This method cooperates the hydrogenator work of inventor's design by the free-standing oscillator of setting, realizes to reaction solution
It is sufficiently stirred, the efficiency of the reaction greatly speeded up.
The technical solution adopted by the present invention to solve the technical problems is: a kind of Chemical Manufacture hydrogenation reaction efficiency optimization
Method, method includes the following steps:
Reaction solution is added in hydrogenator, then free-standing oscillator is put into hydrogenator by S1, and independent
Formula oscillator suspends or swims in reaction solution；
Then S2 starts hydrogenator and free-standing oscillator, is reacted；
The free-standing oscillator can realize the concussion of itself, and concatenated concussion electricity built in free-standing oscillator is mechanical, electrical
The contour structures of pond and switch, the sealed processing in the outer surface of free-standing oscillator, free-standing oscillator can be spherical, hemisphere
Shape, ellipse, square or rectangle；
In the settable overhanging elastic component in the outer surface of free-standing oscillator, elastic component for avoid free-standing oscillator with
The collision of hydrogenator inner wall, the steel bar that elastic component can be 1-2 millimeters for flexible degreasing batten or wooden stick, diameter
Or spring；
Magnet can also be set in the outer surface of free-standing oscillator, the inner surface of hydrogenator is set to the magnet
The opposite magnet of magnetic pole, to avoid the collision between free-standing oscillator and hydrogenator；
This method use hydrogenator include shell, driving mechanism, supporting mechanism, discharging mechanism, rabbling mechanism and
The inner cavity installation of feeding mechanism, the shell is provided with the driving mechanism of power, and runs through the top of the shell, described
The rabbling mechanism for stirring liquid is fixedly connected in driving mechanism；Side on the top of the shell, which is equipped with, to be used for
Inject the feeding mechanism of liquid；The bottom of the shell set there are two be used for output liquid the discharging mechanism；It is described
Shell is fixedly installed with the supporting mechanism on the lateral surface close to bottom.
Specifically, the shell is two hemispheric cylindric stereo hollow structures in bottom.
Specifically, the driving mechanism includes shaft, driving motor, linkage bearing and spring bearing, the top of the shell
Portion is equipped with the driving motor, and the columned shaft connects the driving motor, and through the top of the shell with
The spring bearing rotation connection being mounted on the outer casing bottom inner sidewall；Top of the shaft in the shell inner cavity
Fixing sleeve is connected to the linkage bearing of semicircle pie in portion, and described stir is fixedly connected on the linkage bearing and the shaft
Mix mechanism.
Specifically, the supporting mechanism includes support foot lever and action roller, outer side of shell face bottom is fixedly mounted
The support foot lever for the cube for having radial vertical cross-section L-shaped, the bottom of the support foot lever are equipped with the activity rolling
Wheel.
Specifically, the discharging mechanism includes discharge port and switch valve, the bottom of the shell is fixedly installed with cylindric
The discharge port of through-hole is fixedly installed with the switch valve on the side of the discharge port.
Specifically, the rabbling mechanism includes propeller, linkage stirring rod and stirring convex block, the shaft is described
The spiral propeller is fixedly connected on the part of interior of shell；The linkage bearing bottom end of half round pie
Two sides be fixedly installed with the L-shaped linkage stirring rod respectively, be fixedly connected with conflict on two linkage stirring rods
The outer casing inner wall and the stirring convex block hemispherical, and the other end of the linkage stirring rod is fixedly connected on described turn
The bottom of axis.
Specifically, the feeding mechanism includes feed inlet, link block, hinge, feeds lid and feed inlet washer, it is described outer
Side at the top of shell is fixedly connected with the feed inlet in through hole cylindrical, and the top of the feed inlet lateral surface is fixedly mounted
There is the link block, the other end of the link block is fixedly connected with the hinge, and the other end of the hinge is fixedly connected with
The charging lid, the charging lid are rotatablely connected by the hinge and the link block；In the opening of the feed inlet
Equipped with the feed inlet washer.
Specifically, the top of the propeller is in clock wise spirals structure, middle part is in counter-clockwise helical structure, bottom
In clock wise spirals structure.
Specifically, the outer surface of the propeller is equipped with several described propeller protrusions.
Specifically, the stirring convex block on two linkage stirring rods is in the distribution of interlaced formula.
Beneficial effects of the present invention:
(1) hydrogenator that this method uses, the shaft is fixedly connected on the part of the interior of shell is in
The spiral helicine propeller, the top of the propeller are in clock wise spirals structure, and middle part is in counter-clockwise helical
Structure, bottom is in clock wise spirals structure, convenient for passing through interlaced mixing direction, to enable the liquid runs down hand of spiral both
It stirs upwards, and stirring downwards, there is good up-flow effect, so that stirring is more abundant, improve reaction efficiency.
(2) hydrogenator that this method uses is fixedly connected with the conflict shell on two linkage stirring rods
Inner wall and the stirring convex block hemispherical, and the stirring convex block on two linkage stirring rods is in interlaced formula
Distribution, it is described convenient for that will be sticked in while stirring liquid by the stirring convex block inconsistent with the outer casing inner wall
Liquid on outer casing inner wall is timely removed, and enables the liquid in stirring to guarantee good circulation, convenient for stirring.
(3) hydrogenator that this method uses, outer side of shell face bottom are fixedly installed with radial vertical cross-section in L
The bottom of the support foot lever of the cube of shape, the support foot lever is equipped with the action roller, convenient for passing through the work
Dynamic idler wheel shifts this liquid phase hydrogenation reactor at any time, improves the flexibility of device placement.
Detailed description of the invention
Present invention will be further explained below with reference to the attached drawings and examples.
Fig. 1 is the overall structure diagram for the hydrogenator that this method uses；
Fig. 2 is internal structure sectional view shown in FIG. 1；
Fig. 3 is propeller structural schematic diagram shown in FIG. 1；
Fig. 4 is the portion A shown in FIG. 1 enlarged diagram.
In figure: 1, shell, 2, driving mechanism, 21, shaft, 22, driving motor, 23, linkage bearing, 24, spring bearing, 3,
Supporting mechanism, 31, support foot lever, 32, action roller, 4, discharging mechanism, 41, discharge port, 42, switch valve, 5, rabbling mechanism,
51, propeller, 511, auger piece protrusion, 52, linkage stirring rod, 53, stirring convex block, 6, feeding mechanism, 61, charging
Mouthful, 62, link block, 63, hinge, 64, charging lid, 65, feed inlet washer.
Specific embodiment
In order to be easy to understand the technical means, the creative features, the aims and the efficiencies achieved by the present invention, tie below
Specific embodiment is closed, the present invention is further explained.
As Figure 1-Figure 4, a kind of Chemical Manufacture hydrogenation reaction efficiency optimization method of the present invention, this method packet
Include following steps:
Reaction solution is added in hydrogenator, then free-standing oscillator is put into hydrogenator by S1, and independent
Formula oscillator suspends or swims in reaction solution；
Then S2 starts hydrogenator and free-standing oscillator, is reacted；
The free-standing oscillator can realize the concussion of itself, and concatenated concussion electricity built in free-standing oscillator is mechanical, electrical
The contour structures of pond and switch, the sealed processing in the outer surface of free-standing oscillator, free-standing oscillator can be spherical, hemisphere
Shape, ellipse, square or rectangle；
In the settable overhanging elastic component in the outer surface of free-standing oscillator, elastic component for avoid free-standing oscillator with
The collision of hydrogenator inner wall, the steel bar that elastic component can be 1-2 millimeters for flexible degreasing batten or wooden stick, diameter
Or spring；
Magnet can also be set in the outer surface of free-standing oscillator, the inner surface of hydrogenator is set to the magnet
The opposite magnet of magnetic pole, to avoid the collision between free-standing oscillator and hydrogenator；
The hydrogenator that this method uses includes shell 1, driving mechanism 2, supporting mechanism 3, discharging mechanism 4, blender
Structure 5 and feeding mechanism 6, the inner cavity installation of the shell 1 are provided with the driving mechanism 2 of power, and through the shell 1
Top is fixedly connected with the rabbling mechanism 5 for stirring liquid in the driving mechanism 2；On the top of the shell 1
Side is equipped with the feeding mechanism 6 for injecting liquid；The bottom of the shell 1 is used for the described of output liquid there are two setting
Discharging mechanism 4；The shell 1 is fixedly installed with the supporting mechanism 3 on the lateral surface close to bottom.
Specifically, the shell 1 is two hemispheric cylindric stereo hollow structures in bottom, in use, for reality
The existing shell 1 can store a certain amount of liquid.
Specifically, the driving mechanism 2 includes shaft 21, driving motor 22, link bearing 23 and spring bearing 24, it is described
The top of shell 1 is equipped with the driving motor 22, and the columned shaft 21 connects the driving motor 22, and runs through institute
The top for stating shell 1 and the spring bearing 24 being mounted on the 1 bottom inside wall of shell are rotatablely connected；The shaft 21
Fixing sleeve is connected to the linkage bearing 23 of semicircle pie, 23 He of linkage bearing on the top in 1 inner cavity of shell
The rabbling mechanism 5 is fixedly connected in the shaft 21, in use, the rotation in order to realize rabbling mechanism 5.
Specifically, the supporting mechanism 3 includes support foot lever 31 and action roller 32, the 1 lateral surface bottom of shell is solid
Dingan County is equipped with the support foot lever 31 of the L-shaped cube of radial vertical cross-section, and the bottom of the support foot lever 31 is equipped with
The action roller 32, in use, the placement and transfer of this liquid phase hydrogenation reactor for convenience.
Specifically, the discharging mechanism 4 includes discharge port 41 and switch valve 42, the bottom of the shell 1 is fixedly installed with
The discharge port 41 of cylindric through-hole is fixedly installed with the switch valve 42 on the side of the discharge port 41, in use, being
The liquid is facilitated to flow out inside the shell 1.
Specifically, the rabbling mechanism 5 includes propeller 51, link stirring rod 52 and stirring convex block 53, described turn
Axis 21 is fixedly connected with the spiral propeller 51 on the part inside the shell 1；The institute of half round pie
The two sides for stating linkage 23 bottom end of bearing are fixedly installed with the L-shaped linkage stirring rod 52, two linkage stirrings respectively
It is fixedly connected on bar 52 and contradicts 1 inner wall of shell and the stirring convex block 53 hemispherical, and the linkage stirring rod
52 other end is fixedly connected on the bottom of the shaft 21, in use, in order to realization device to the stirring action of liquid.
Specifically, the feeding mechanism 6 includes feed inlet 61, link block 62, hinge 63, charging lid 64 and feed inlet pad
Circle 65, the side at 1 top of shell are fixedly connected with the feed inlet 61 in through hole cylindrical, 61 outside of feed inlet
The link block 62 is fixedly installed at the top of face, the other end of the link block 62 is fixedly connected with the hinge 63, described
The other end of hinge 63 is fixedly connected with the charging lid 64, and the charging lid 64 passes through the hinge 63 and the connection
Block 62 is rotatablely connected；The opening of the feed inlet 61 is equipped with the feed inlet washer 65, in use, liquid enters for convenience
Inside the shell 1.
Specifically, the top of the propeller 51 is in clock wise spirals structure, middle part is in counter-clockwise helical structure, bottom
Portion be in clock wise spirals structure, in use, in order to allow liquid can stirring when above and below convection current so that stirring it is more uniform.
Specifically, the outer surface of the propeller 51 is equipped with several described propeller protrusions 511, use
When, in order to increase the contact area of the propeller 51 and liquid, so that stirring is more abundant.
Specifically, the stirring convex block 53 on two linkage stirring rods 52 is in the distribution of interlaced formula, use
When, in order to guarantee that the stirring convex block 53 can remove the liquid of adhesion on 1 inner sidewall of shell in time, also save simultaneously
Material.
When in use, firstly, this liquid phase hydrogenation reactor is transferred to suitable place by the action roller 32, then
The charging lid 64 is moved manually, the charging lid 64 is opened, and liquid to be reacted will be needed to pass through the feed inlet 61
It pours into the inner cavity of the shell 1, then the charging lid 64 is shut, the driving motor 22 is connected to power supply, the drive
The dynamic rotation of motor 22 drives the shaft 21 to rotate, and drives the linkage bearing 23 to rotate therewith, the linkage bearing 23 rotates
The linkage stirring rod 52 is driven to rotate, then the propeller 51 and stirring convex block 53 rotate with it, and stir liquid
It mixes；In whipping process, due to being in clock wise spirals structure at the top of the propeller 51, middle part is in counter-clockwise helical structure,
Bottom is in clock wise spirals structure, so that the liquid at top, middle part and bottom generates convection current interaction, is mixed mutually, so that
The liquid of stirring is more uniform；It is stirred since the stirring convex block 53 is hemispherical and contradicts the inner sidewall of the shell 1
Cheng Zhong, while the stirring convex block 53 is to liquid agitation, also can by stick in the adherency on 1 inner wall of shell liquid and
When removing, enable stirring when liquid guarantee good circulation, convenient for stirring；After the completion of stirring, by the switch
Valve 42 is opened, and the liquid for stirring completion then passes through the discharge port 41 and the shell 1 is discharged, and is finally completed the entire work of device
Process.
The basic principles, main features and advantages of the invention have been shown and described above.The technical staff of the industry should
Understand, the present invention is not limited to the above embodiments, and the description in above embodiment and specification only illustrates the present invention
Principle, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these variation and
Improvement is both fallen in the scope of protection of present invention.The claimed scope of the invention is by appended claims and its equivalent
Object defines.
Claims (10)
1. a kind of Chemical Manufacture hydrogenation reaction efficiency optimization method, which is characterized in that method includes the following steps:
Reaction solution is added in hydrogenator, then free-standing oscillator is put into hydrogenator by S1, and stand alone type vibration
Device is swung to suspend or swim in reaction solution；
Then S2 starts hydrogenator and free-standing oscillator, is reacted；
The hydrogenator that this method uses includes shell (1), driving mechanism (2), supporting mechanism (3), discharging mechanism (4), stirs
Mechanism (5) and feeding mechanism (6) are mixed, the inner cavity installation of the shell (1) is provided with the driving mechanism (2) of power, and passes through
The top of the shell (1) is worn, the rabbling mechanism (5) for stirring liquid is fixedly connected on the driving mechanism (2)；
Side on the top of the shell (1) is equipped with the feeding mechanism (6) for injecting liquid；The bottom of the shell (1)
If there are two the discharging mechanisms (4) for being used for output liquid；The shell (1) is fixedly mounted on the lateral surface close to bottom
There are the supporting mechanism (3).
2. a kind of Chemical Manufacture hydrogenation reaction efficiency optimization method according to claim 1, it is characterised in that: described outer
Shell (1) is two hemispheric cylindric stereo hollow structures in bottom.
3. a kind of Chemical Manufacture hydrogenation reaction efficiency optimization method according to claim 2, it is characterised in that: the drive
Motivation structure (2) includes shaft (21), driving motor (22), linkage bearing (23) and spring bearing (24), the top of the shell (1)
Portion is equipped with the driving motor (22), and the columned shaft (21) connects the driving motor (22), and through described
The top of shell (1) is rotatablely connected with the spring bearing (24) being mounted on the shell (1) bottom inside wall；Described turn
Axis (21) fixing sleeve on the top in the shell (1) inner cavity is connected to the linkage bearing (23) of semicircle pie, described
The rabbling mechanism (5) are fixedly connected in dynamic bearing (23) and the shaft (21).
4. a kind of Chemical Manufacture hydrogenation reaction efficiency optimization method according to claim 3, it is characterised in that: the branch
Support mechanism (3) includes support foot lever (31) and action roller (32), and shell (1) the lateral surface bottom is fixedly installed with radial hang down
The support foot lever (31) of the L-shaped cube in straightforward face, the bottom of support foot lever (31) are equipped with the activity rolling
It takes turns (32).
5. a kind of Chemical Manufacture hydrogenation reaction efficiency optimization method according to claim 4, it is characterised in that: it is described go out
Expect that mechanism (4) include discharge port (41) and switch valve (42), the bottom of the shell (1) is fixedly installed with the institute of cylindric through-hole
It states discharge port (41), is fixedly installed with the switch valve (42) on the side of the discharge port (41).
6. a kind of Chemical Manufacture hydrogenation reaction efficiency optimization method according to claim 5, it is characterised in that: described to stir
Mixing mechanism (5) includes propeller (51), linkage stirring rod (52) and stirring convex block (53), and the shaft (21) is described outer
Shell (1) is fixedly connected with the spiral propeller (51) on internal part；The universal driving shaft of half round pie
The two sides for holding (23) bottom end are fixedly installed with the L-shaped linkage stirring rod (52), two linkage stirring rods respectively
(52) it is fixedly connected on and contradicts shell (1) inner wall and the stirring convex block (53) hemispherical, and the linkage is stirred
The other end for mixing bar (52) is fixedly connected on the bottom of the shaft (21).
7. a kind of Chemical Manufacture hydrogenation reaction efficiency optimization method according to claim 5, it is characterised in that: it is described into
Material mechanism (6) includes feed inlet (61), link block (62), hinge (63), feeds lid (64) and feed inlet washer (65), described
Side at the top of shell (1) is fixedly connected with the feed inlet (61) in through hole cylindrical, feed inlet (61) lateral surface
Top be fixedly installed with the link block (62), the other end of the link block (62) is fixedly connected with the hinge (63),
The other end of the hinge (63) is fixedly connected with the charging lid (64), and the charging lid (64) passes through the hinge
(63) it is rotatablely connected with the link block (62)；The opening of the feed inlet (61) is equipped with the feed inlet washer (65).
8. a kind of Chemical Manufacture hydrogenation reaction efficiency optimization method according to claim 6, it is characterised in that: the spiral shell
The top for revolving agitating paddle (51) is in clock wise spirals structure, and middle part is in counter-clockwise helical structure, and bottom is in clock wise spirals structure.
9. a kind of Chemical Manufacture hydrogenation reaction efficiency optimization method according to claim 6, it is characterised in that: the spiral shell
The outer surface for revolving agitating paddle (51) is equipped with several described propeller protrusions (511).
10. a kind of Chemical Manufacture hydrogenation reaction efficiency optimization method according to claim 6, it is characterised in that: two
The stirring convex block (53) on linkage stirring rod (52) is in the distribution of interlaced formula.
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| CN201811115967.9A CN109078585A (en) | 2018-09-25 | 2018-09-25 | A kind of Chemical Manufacture hydrogenation reaction efficiency optimization method |
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| CN201811115967.9A CN109078585A (en) | 2018-09-25 | 2018-09-25 | A kind of Chemical Manufacture hydrogenation reaction efficiency optimization method |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114160077A (en) * | 2021-12-03 | 2022-03-11 | 山东成泰新材料有限公司 | Hydrogenation reaction method for producing isododecane |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH06343846A (en) * | 1993-06-07 | 1994-12-20 | Yoshimitsu Inai | Agitator |
| CN201644020U (en) * | 2010-02-05 | 2010-11-24 | 温州市天瑞制药机械有限公司 | Contrarotating homogeneous sol mixing tank |
| CN207342615U (en) * | 2017-09-12 | 2018-05-11 | 湖州光博生物科技有限公司 | A kind of agitating device for Cosmetic Manufacture |
| CN108217880A (en) * | 2018-02-02 | 2018-06-29 | 曾国琼 | A kind of sewage disposal flocculation plant based on unordered stirring technique |
-
2018
- 2018-09-25 CN CN201811115967.9A patent/CN109078585A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH06343846A (en) * | 1993-06-07 | 1994-12-20 | Yoshimitsu Inai | Agitator |
| CN201644020U (en) * | 2010-02-05 | 2010-11-24 | 温州市天瑞制药机械有限公司 | Contrarotating homogeneous sol mixing tank |
| CN207342615U (en) * | 2017-09-12 | 2018-05-11 | 湖州光博生物科技有限公司 | A kind of agitating device for Cosmetic Manufacture |
| CN108217880A (en) * | 2018-02-02 | 2018-06-29 | 曾国琼 | A kind of sewage disposal flocculation plant based on unordered stirring technique |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114160077A (en) * | 2021-12-03 | 2022-03-11 | 山东成泰新材料有限公司 | Hydrogenation reaction method for producing isododecane |
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Application publication date: 20181225 |