CN109078121A - The method that vacuum impulse prepares Processed Product of Rhizoma Gastrodiae - Google Patents
The method that vacuum impulse prepares Processed Product of Rhizoma Gastrodiae Download PDFInfo
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- CN109078121A CN109078121A CN201811016350.1A CN201811016350A CN109078121A CN 109078121 A CN109078121 A CN 109078121A CN 201811016350 A CN201811016350 A CN 201811016350A CN 109078121 A CN109078121 A CN 109078121A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/898—Orchidaceae (Orchid family)
- A61K36/8988—Gastrodia
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/13—Preparation or pretreatment of starting material involving cleaning, e.g. washing or peeling
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/17—Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting
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Abstract
The invention discloses a kind of methods that vacuum impulse prepares Processed Product of Rhizoma Gastrodiae, in particular to a kind of to be impregnated after a certain period of time by being put into after being sliced Rhizoma Gastrodiae in specific salt, it places into baking oven after toasting, it is put into soak, containing by salt in soak, benzyl carbinol, diethanol amine, the components such as water, the effective component in Rhizoma Gastrodiae can be promoted to overflow, it simultaneously can also be in conjunction with the effective component in Rhizoma Gastrodiae, absorb it easily, increase curative effect, after finally passing through freeze-drying again, spray honey liquor, contain specific component in honey liquor, certain protective film is formed after so that honey is entered Rhizoma Gastrodiae tissue, Rhizoma Gastrodiae effective component can be prevented to overflow, increase its stability, therefore it is good to obtain a kind of stability through the invention, dissolution is fast, the Processed Product of Rhizoma Gastrodiae of good absorbing, have in terms of curative effect and significantly improves, preparation method of the present invention is simply controllable simultaneously, it is suitable In industrialization and scale.
Description
Technical field
The present invention relates to a kind of methods that vacuum impulse prepares Processed Product of Rhizoma Gastrodiae, belong to Chinese medicine preparation field.
Background technique
Rhizoma Gastrodiae, Chinese medicine name.This product is the rhizome of orchid Rhizoma Gastrodiae.Winter, the excavation of two season of spring, the winter person's of adopting name winter fiber crops, matter
It measures excellent；The spring person's of adopting name spring fiber crops, quality are good not as good as winter fiber crops.After digging out, the aerial stem of plant and fibrous root are removed, soil is cleaned, is steeped with clear water,
Rough bark is wiped in time, clear water is put into immediately or alum water impregnates, then boiling or steaming are thoroughly, until being degree when center is without white point, taking-up is dried in the air
It is dry, it dries or dries.Major function are as follows: relieve the wind syndrome, arresting convulsion.Control dizziness pupil, cold and headache, extremity numbness, hemiplegia, language
It is not smoothgoing puckery, infantile epilepsy and convulsions.
Rhizoma Gastrodiae general winter, the excavation of two season of spring, the winter person's of adopting name winter fiber crops are superior in quality；The spring person's of adopting name spring fiber crops, quality is not as good as winter fiber crops
It is good.After digging out, the aerial stem of plant and fibrous root are removed, soil is cleaned, is steeped with clear water, wipe rough bark in time, be put into clear water or alum immediately
Water impregnates, then boiling or steaming are thoroughly, until being degree when center is without white point, taking-up dries, dries or dry.
For Rhizoma Gastrodiae as a kind of Chinese medicine, Fast Stripping and absorption can improve the utilization efficiency of Rhizoma Gastrodiae, increase its society
Value, Processed Product of Rhizoma Gastrodiae concocting method domestic at present largely use the concocting method of traditional Chinese medicine, including stock, slice,
Drying and other steps, some can also plus boiling, the Rhizoma Gastrodiae that these traditional preparation methods obtain not only prepared slice quality compared with
Difference is differed greatly between batch in industrialization process, and the dissolution of effective component is slow, and degree of absorption is low, and curative effect is difficult to reach and need
It asks.
Domestic at present a lot of to Processed Product of Rhizoma Gastrodiae research, patent CN 103285247 discloses a kind of preparation of Processed Product of Rhizoma Gastrodiae
Method is mainly characterized by whole process without reaching mould proof by certain fumigation technology using sulfur fumigation
Become effect, but for not making a search in terms of the dissolution of medicine materical crude slice, patent CN 105477382 discloses a kind of system of Processed Product of Rhizoma Gastrodiae
Preparation Method, after mainly being thinly sliced by Rhizoma Gastrodiae, using the micro- of the microwave drying of lower frequency, forced air drying and upper frequency
Wave drying combines, and realizes rapid aging and the drying of Rhizoma Gastrodiae, is not obviously changed yet in effective component dissolution and absorption aspects
It is kind, the present invention by research for many years obtain one kind can Fast Stripping, the Processed Product of Rhizoma Gastrodiae preparation method of good absorbing.
Summary of the invention
To solve the above-mentioned problems of the prior art, the present invention provides a kind of preparation method of Processed Product of Rhizoma Gastrodiae, the present invention
Resulting Processed Product of Rhizoma Gastrodiae preparation method is simple controllably, is suitable for industrialization production, has quickly dissolution and assimilation effect.
In order to realize that foregoing invention, embodiment are as follows:
One, appropriate Rhizoma Gastrodiae is taken, the aerial stem of plant and fibrous root are removed, is sliced after cleaning, with a thickness of 0.6-1.1cm, gastrodia elata slice is put into 10-
After impregnating 3-6 hours under the conditions of ultrasonic vibration in 20% saline solution, gastrodia elata slice surface moisture is dried in taking-up.
Preferably, the Rhizoma Gastrodiae is disease-free, and rhizome is full to be enriched.
Two, gastrodia elata slice is put into baking oven, 31-41 DEG C 6-16 hours dry, and the gastrodia elata slice after drying is put into soak
Middle immersion 3-6 hours takes out, dries surface moisture；Carried out in soaking process it is intermittent vacuumize and vacuum breaker, utilize pressure difference
Variation makes soak enter Rhizoma Gastrodiae histocyte as far as possible.
Preferably, the soak is made of salt, benzyl carbinol, diethanol amine, water, and composition mass ratio is 5:1:1:
93。
Three, the gastrodia elata slice after immersion is put into freeze drier rapidly, vacuum freezedrying.
Preferably, the vacuum freezedrying, which refers to, is put into gastrodia elata slice in freeze drier, and -30 DEG C -- 40 DEG C of freezings
1-3 hours, it is evacuated to 20-50pa with oil pump, then slowly heat up, when heat preservation 2-4 is small when temperature rises to -5 DEG C, finally heated up
To 20 DEG C, 2-4 hours are kept the temperature.
Four, after carrying out by the gastrodia elata slice after drying plus be sweet.
Preferably, described plus honey refers to honey liquor by being coated with or sweet liquid is coated with or is sprayed to by spray appliance
Rhizoma Gastrodiae surface.
Further, the mass ratio of the gastrodia elata slice and sweet liquid is 1:0.2-0.6.
Further, the sweet liquid is made of honey, phosphatide, water, and composition mass ratio is 1:0.2:5.
Present invention is characterized in that
The present invention is soaked by the way that Processed Product of Rhizoma Gastrodiae to be immersed in the salt water of certain concentration, loose Processed Product of Rhizoma Gastrodiae interior tissue in soak
During bubble, there is benzyl carbinol certain bactericidal effect can remove the surface microorganism of gastrodia elata slice, while rapidly enter Rhizoma Gastrodiae group
Inside is knitted, diethanol amine polarity is strong, and degree of ionization is high, promotes benzyl carbinol in conjunction with the effective component Gastrodin of Rhizoma Gastrodiae, improves Rhizoma Gastrodiae
The liposoluble sexuality of element, increases its absorbability.
Also by gastrodia elata slice by the salt water of immersion certain concentration twice, organization internal water passes in and out the present invention repeatedly, makes tissue
Internal water channels increase, and after freeze-drying, moisture is largely lost, and after adding honey, the sugar and phosphatide in honey are fast with moisture
Speed enters tissue, and water stream channel is blocked in condensation, prevents effective component from overflowing, improves the stability of this product.
The beneficial effects of the present invention are:
1. the present invention obtains, a kind of dissolution rate is fast, the Rhizoma Gastrodiae prepared slices of Chinese crude drugs of good absorbing.
2. sulfur fumigation is not added in preparation process of the present invention, safety is good
3. after the present invention is by adding honey to handle, stability is improved, can save for a long time.
Preparation process of the present invention is simple, and controllability is strong, is suitable for industrialization and large-scale production.
Specific embodiment
Main points in order to better understand the present invention are now described in further detail foregoing invention by specific embodiment, but under
Stating embodiment should not be understood as to further limitation of the invention.
Embodiment 1
1, appropriate disease-free, the full substantial Rhizoma Gastrodiae of rhizome is taken, the aerial stem of plant and fibrous root are removed, is sliced after cleaning, thickness 0.9cm,
Gastrodia elata slice is put into 15% saline solution after being impregnated 5 hours under the conditions of ultrasonic vibration, gastrodia elata slice surface moisture is dried in taking-up.
2, Rhizoma Gastrodiae is put into baking oven, 37 DEG C drying 9 hours, the gastrodia elata slice after drying is put into soak impregnate it is 5 small
When, it takes out, dries surface moisture；Carried out in soaking process it is intermittent vacuumize and vacuum breaker, make to impregnate using pressure difference variation
Liquid enters Rhizoma Gastrodiae histocyte as far as possible；The soak is made of salt, benzyl carbinol, diethanol amine, water, forms quality
Than for 5:1:1:93.
3, the Rhizoma Gastrodiae after immersion is put into freeze drier rapidly, freezes 2 hours at -35 DEG C, is evacuated to oil pump
35pa, then slowly heat up, when heat preservation 3 is small when temperature rises to -5 DEG C, 20 DEG C are finally warming up to, keeps the temperature 3 hours.
4, sweet liquid is coated with or is sprayed to Rhizoma Gastrodiae surface by coating or spray appliance by the gastrodia elata slice after drying；Institute
The mass ratio of the Rhizoma Gastrodiae and sweet liquid stated is 1:0.4；The sweet liquid is made of honey, phosphatide, water, and composition mass ratio is 1:
0.2:5。
Embodiment 2
1, appropriate disease-free, the full substantial Rhizoma Gastrodiae of rhizome is taken, the aerial stem of plant and fibrous root are removed, is sliced after cleaning, thickness 0.6cm,
Gastrodia elata slice is put into 10% saline solution after being impregnated 4 hours under the conditions of ultrasonic vibration, gastrodia elata slice surface moisture is dried in taking-up.
2, Rhizoma Gastrodiae is put into baking oven, 32 DEG C drying 6 hours, the gastrodia elata slice after drying is put into soak impregnate it is 4 small
When, it takes out, dries surface moisture；Carried out in soaking process it is intermittent vacuumize and vacuum breaker, make to impregnate using pressure difference variation
Liquid enters Rhizoma Gastrodiae histocyte as far as possible；The soak is made of salt, benzyl carbinol, diethanol amine, water, forms quality
Than for 5:1:1:93.
3, the Rhizoma Gastrodiae after immersion is put into freeze drier rapidly, freezes 1 hour at -30 DEG C, is evacuated to oil pump
20pa, then slowly heat up, when heat preservation 2 is small when temperature rises to -5 DEG C, 20 DEG C are finally warming up to, keeps the temperature 2 hours.
4, sweet liquid is coated with or is sprayed to Rhizoma Gastrodiae surface by coating or spray appliance by the gastrodia elata slice after drying；Institute
The mass ratio of the Rhizoma Gastrodiae and sweet liquid stated is 1:0.2；The sweet liquid is made of honey, phosphatide, water, and composition mass ratio is 1:
0.2:5。
Embodiment 3
1, appropriate disease-free, the full substantial Rhizoma Gastrodiae of rhizome is taken, the aerial stem of plant and fibrous root are removed, is sliced after cleaning, thickness 0.7cm,
Gastrodia elata slice is put into 20% saline solution after being impregnated 5.8 hours under the conditions of ultrasonic vibration, gastrodia elata slice surface water is dried in taking-up
Point.
2, Rhizoma Gastrodiae is put into baking oven, 41 DEG C drying 16 hours, the gastrodia elata slice after drying is put into soak and impregnates 5.8
Hour, it takes out, dries surface moisture；Carried out in soaking process it is intermittent vacuumize and vacuum breaker, make to soak using pressure difference variation
Bubble liquid enters Rhizoma Gastrodiae histocyte as far as possible；The soak is made of salt, benzyl carbinol, diethanol amine, water, forms matter
Amount is than being 5:1:1:93.
3, the Rhizoma Gastrodiae after immersion is put into freeze drier rapidly, freezes 3 hours at -40 DEG C, is evacuated to oil pump
50pa, then slowly heat up, when heat preservation 4 is small when temperature rises to -5 DEG C, 20 DEG C are finally warming up to, keeps the temperature 4 hours.
4, sweet liquid is coated with or is sprayed to Rhizoma Gastrodiae surface by coating or spray appliance by the gastrodia elata slice after drying；Institute
The mass ratio of the Rhizoma Gastrodiae and sweet liquid stated is 1:0.6；The sweet liquid is made of honey, phosphatide, water, and composition mass ratio is 1:
0.2:5。
Comparative example 1
1, appropriate disease-free, the full substantial Rhizoma Gastrodiae of rhizome is taken, the aerial stem of plant and fibrous root are removed, is sliced after cleaning, thickness 0.9cm,
Gastrodia elata slice is put into 15% saline solution after being impregnated 5 hours under the conditions of ultrasonic vibration, gastrodia elata slice surface moisture is dried in taking-up.
2, Rhizoma Gastrodiae is put into baking oven, 37 DEG C drying 9 hours, the gastrodia elata slice after drying is put into soak impregnate it is 5 small
When, it takes out, dries surface moisture；Carried out in soaking process it is intermittent vacuumize and vacuum breaker, make to impregnate using pressure difference variation
Liquid enters Rhizoma Gastrodiae histocyte as far as possible；The soak is made of salt, benzyl carbinol, diethanol amine, water, forms quality
Than for 5:1:1:93.
3, the Rhizoma Gastrodiae after immersion is put into freeze drier rapidly, freezes 2 hours at -35 DEG C, is evacuated to oil pump
35pa, then slowly heat up, when heat preservation 3 is small when temperature rises to -5 DEG C, 20 DEG C are finally warming up to, keeps the temperature 3 hours.
Comparative example 2
1, appropriate disease-free, the full substantial Rhizoma Gastrodiae of rhizome is taken, the aerial stem of plant and fibrous root are removed, is sliced after cleaning, thickness 0.6cm,
Gastrodia elata slice is put into 15% saline solution after being impregnated 4 hours under the conditions of ultrasonic vibration, gastrodia elata slice surface moisture is dried in taking-up.
2, Rhizoma Gastrodiae is put into baking oven, 37 DEG C drying 9 hours, the gastrodia elata slice after drying is impregnated 4 hours into the water, is taken
Out, surface moisture is dried；Carried out in soaking process it is intermittent vacuumize and vacuum breaker, using up soak using pressure difference variation can
It can enter Rhizoma Gastrodiae histocyte.
3, the Rhizoma Gastrodiae after immersion is put into freeze drier rapidly, freezes 2 hours at -35 DEG C, is evacuated to oil pump
35pa, then slowly heat up, when heat preservation 3 is small when temperature rises to -5 DEG C, 20 DEG C are finally warming up to, keeps the temperature 3 hours.
4, sweet liquid is coated with or is sprayed to Rhizoma Gastrodiae surface by coating or spray appliance by the gastrodia elata slice after drying；Institute
The mass ratio of the Rhizoma Gastrodiae and sweet liquid stated is 1:0.4；The sweet liquid is made of honey, phosphatide, water, and composition mass ratio is 1:
0.2:5。
Comparative example 3
1, appropriate disease-free, the full substantial Rhizoma Gastrodiae of rhizome is taken, the aerial stem of plant and fibrous root are removed, is sliced after cleaning, thickness 0.7cm,
Gastrodia elata slice is put into 15% saline solution after being impregnated 3.5 hours under the conditions of ultrasonic vibration, gastrodia elata slice surface water is dried in taking-up
Point.
2, Rhizoma Gastrodiae is put into baking oven, 37 DEG C drying 9 hours, the gastrodia elata slice after drying is impregnated 3.5 hours into the water,
It takes out, dries surface moisture；Carried out in soaking process it is intermittent vacuumize and vacuum breaker, use up soak using pressure difference variation
Possibly into Rhizoma Gastrodiae histocyte.
3, the Rhizoma Gastrodiae after immersion is put into freeze drier rapidly, freezes 2 hours at -35 DEG C, is evacuated to oil pump
35pa, then slowly heat up, when heat preservation 3 is small when temperature rises to -5 DEG C, 20 DEG C are finally warming up to, keeps the temperature 3 hours.
Dissolution rate is investigated
According to the preparation method in embodiment 1-3 and comparative examples 1-3, Processed Product of Rhizoma Gastrodiae is prepared, according to CN 103285247
Two kinds of Processed Product of Rhizoma Gastrodiae are prepared with the optimum embodiment in patent CN 105477382.Distinct methods in above-mentioned 8 are taken to be prepared into
The Processed Product of Rhizoma Gastrodiae 10g arrived, is placed in that material is consistent, in the identical glass of size, and 100ml boiling water is added, respectively 10min,
20min, 30min, 60min, 90min, 120min take 5ml water, according to " Chinese Pharmacopoeia " 2015 editions middle Rhizoma Gastrodiae content detections
Method detects gastrodin content, as a result as follows:
1, according to " Chinese Pharmacopoeia " 2015 editions one middle Rhizoma Gastrodiae detection method of content detection embodiment 1-3, comparative example 1-3 with
And the Processed Product of Rhizoma Gastrodiae obtained according to the preparation method in two patents.
Gastrodin content in 1 Processed Product of Rhizoma Gastrodiae of table
| Embodiment | 1 | 2 | 3 | P- 1 | P- 2 | P- 3 | CN 103285247 | CN 105477382 |
| Content (%) | 0.85 | 0.87 | 0.85 | 0.68 | 0.66 | 0.65 | 0.67 | 0.70 |
Remarks: p- 1 is comparative example 1, and so on.
2, the gastrodin content in the Processed Product of Rhizoma Gastrodiae that different preparation methods obtain is detected, as a result as follows:
Gastrodin content in the Processed Product of Rhizoma Gastrodiae of the different preparation methods of table 2
| Embodiment | 1 | 2 | 3 | P- 1 | P- 2 | P- 3 | CN 103285247 | CN 105477382 |
| 10min(%) | 31.3 | 33.5 | 34.2 | 22.5 | 24.4 | 18.3 | 25.6 | 28.5 |
| 20min(%) | 45.1 | 44.4 | 48.1 | 30.2 | 31.4 | 23.6 | 30.3 | 30.5 |
| 30min(%) | 60.2 | 58.2 | 57.4 | 36.1 | 40.2 | 314 | 41.6 | 39.4 |
| 60min(%) | 82.3 | 83.7 | 84.6 | 44.7 | 43.3 | 44.6 | 53.3 | 51.4 |
| 90min(%) | 89.2 | 88.5 | 89.8 | 52.7 | 54.5 | 50.5 | 61.5 | 65.4 |
| 120min(%) | 90.1 | 93.1 | 94.3 | 57.8 | 60.1 | 54.7 | 70.3 | 73.8 |
It analyzes from the above, the resulting Processed Product of Rhizoma Gastrodiae dissolution rate of the present invention, which has, to be significantly improved, and Gastrodin in Gastrodia eleta Bl.
Content is also higher.
Sedation effect is investigated
Sample treatment: by embodiment 1-3, comparative example 1-3 and the Processed Product of Rhizoma Gastrodiae obtained according to two patent preparation methods
It crushes, crosses 200 meshes, it is spare.
Kunming kind 80 are chosen, mouse weight 20+2g, health degree is similar, is randomly divided into 8 groups, every group 10
Only, half male and half female investigates influence of the Processed Product of Rhizoma Gastrodiae to mouse autonomic activities, and 8h mouse fasting water inlet, is observed after administration before testing
Mouse autonomic activities number is recorded, 1min is reached as sleep index using mouse righting reflex loss in 15min after administration, is observed and recorded
Each group mouse from be administered to fall asleep the time required to and sleep number of elements.Test result is as follows:
| Embodiment | 1 | 2 | 3 | P- 1 | P- 2 | P- 3 | CN 103285247 | CN 105477382 |
| Dosage (g) | 0.2 | 0.2 | 0.2 | 0.2 | 0.2 | 0.2 | 0.2 | 0.2 |
| Sleep number of elements | 8 | 9 | 9 | 4 | 4 | 3 | 5 | 6 |
| Autonomic activities number | 73 | 74 | 75 | 122 | 123 | 131 | 115 | 119 |
| Time for falling asleep (min) | 4.5 | 4.7 | 4.7 | 12.3 | 14.5 | It does not fall asleep | 12.8 | 13.6 |
It analyzes from the above, the tranquilizing soporific significant effect of present invention gained Processed Product of Rhizoma Gastrodiae.
Study on the stability
It respectively by the resulting Processed Product of Rhizoma Gastrodiae of above-mentioned distinct methods, is put into polybag, seals, as being placed in room temperature, respectively 3
The moon, June, September, December, 15 months, 18 months, 24 months detect its content, as a result as follows:
| Embodiment | 1 | 2 | 3 | P- 1 | P- 2 | P- 3 | CN 103285247 | CN 105477382 |
| 0 month (%) | 0.83 | 0.86 | 0.85 | 0.66 | 0.64 | 0.60 | 0.68 | 0.71 |
| March (%) | 0.81 | 0.83 | 0.85 | 0.63 | 0.59 | 0.58 | 0.65 | 0.68 |
| June (%) | 8.3 | 0.83 | 0.87 | 0.50 | 0.54 | 0.52 | 0.60 | 0.65 |
| September (%) | 0.82 | 0.82 | 0.81 | 0.43 | 0.46 | 0.46 | 0.54 | 0.61 |
| December (%) | 0.84 | 0.81 | 0.82 | 0.37 | 0.40 | 0.41 | 0.51 | 0.58 |
| 15 months (%) | 0.78 | 0.78 | 0.79 | 0.33 | 0.36 | 0.37 | 0.50 | 0.57 |
| 18 months (%) | 0.75 | 0.75 | 0.74 | 0.31 | 0.31 | 0.30 | 0.46 | 0.54 |
| 24 months (%) | 0.73 | 0.74 | 0.73 | 0.32 | 0.32 | 0.29 | 0.45 | 0.53 |
From above-mentioned test data analyzer, present invention gained Processed Product of Rhizoma Gastrodiae stability has remarkable result.
Claims (6)
1. a kind of method that vacuum impulse prepares Processed Product of Rhizoma Gastrodiae, it is characterised in that including the following steps:
(1) appropriate Rhizoma Gastrodiae is taken, the aerial stem of plant and fibrous root are removed, is sliced after cleaning, with a thickness of 0.6-1.1cm, gastrodia elata slice is put into 10-
After impregnating 3-6 hours under the conditions of ultrasonic vibration in 20% saline solution, gastrodia elata slice surface moisture is dried in taking-up；
(2) gastrodia elata slice is put into baking oven, 31-41 DEG C 6-16 hours dry, and the gastrodia elata slice after drying is put into soak and is soaked
Bubble 3-6 hours takes out, dries surface moisture；Carried out in soaking process it is intermittent vacuumize and vacuum breaker, changed using pressure difference
Soak is set to enter Rhizoma Gastrodiae histocyte as far as possible；
(3) gastrodia elata slice after immersion is put into freeze drier rapidly, vacuum freezedrying；
(4) gastrodia elata slice after drying is carried out plus honey is handled.
2. the method that vacuum impulse prepares Processed Product of Rhizoma Gastrodiae according to claim 1, it is characterised in that: the soak is by eating
Salt, benzyl carbinol, diethanol amine, water composition, composition mass ratio are 5:1:1:93.
3. the method that vacuum impulse prepares Processed Product of Rhizoma Gastrodiae according to claim 1, it is characterised in that: the freezing vacuum is dry
It is dry refer to gastrodia elata slice is put into freeze drier, -30 DEG C -- 40 DEG C freezing 1-3 hours, be evacuated to 20-50pa with oil pump,
It slowly heats up again, when heat preservation 2-4 is small when temperature rises to -5 DEG C, is finally warming up to 20 DEG C, keeps the temperature 2-4 hours.
4. the method that vacuum impulse prepares Processed Product of Rhizoma Gastrodiae according to claim 1, it is characterised in that: described plus honey refer to by
Sweet liquid is coated with or is sprayed to Rhizoma Gastrodiae surface by coating or spray appliance by honey liquor.
5. the method that vacuum impulse prepares Processed Product of Rhizoma Gastrodiae according to claim 4, it is characterised in that: the Rhizoma Gastrodiae and sweet liquid
Mass ratio be 1:0.2-0.6.
6. the method that vacuum impulse prepares Processed Product of Rhizoma Gastrodiae according to claim 5, it is characterised in that: the sweet liquid is by bee
Honey, phosphatide, water composition, composition mass ratio are 1:0.2:5.
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| CN110151921A (en) * | 2019-06-25 | 2019-08-23 | 中国农业大学 | A kind of Rhizoma Gastrodiae vacuum impulse steams technique and its steams degree quantization method |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110151921A (en) * | 2019-06-25 | 2019-08-23 | 中国农业大学 | A kind of Rhizoma Gastrodiae vacuum impulse steams technique and its steams degree quantization method |
| CN110151921B (en) * | 2019-06-25 | 2021-08-10 | 中国农业大学 | Gastrodia elata vacuum pulsation steaming process and steaming degree quantification method thereof |
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