CN109064871B - Solidification process simulation experiment device - Google Patents
Solidification process simulation experiment device Download PDFInfo
- Publication number
- CN109064871B CN109064871B CN201811016650.XA CN201811016650A CN109064871B CN 109064871 B CN109064871 B CN 109064871B CN 201811016650 A CN201811016650 A CN 201811016650A CN 109064871 B CN109064871 B CN 109064871B
- Authority
- CN
- China
- Prior art keywords
- water
- water inlet
- pipe
- water outlet
- tank
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Images
Classifications
-
- G—PHYSICS
- G09—EDUCATION; CRYPTOGRAPHY; DISPLAY; ADVERTISING; SEALS
- G09B—EDUCATIONAL OR DEMONSTRATION APPLIANCES; APPLIANCES FOR TEACHING, OR COMMUNICATING WITH, THE BLIND, DEAF OR MUTE; MODELS; PLANETARIA; GLOBES; MAPS; DIAGRAMS
- G09B25/00—Models for purposes not provided for in G09B23/00, e.g. full-sized devices for demonstration purposes
- G09B25/02—Models for purposes not provided for in G09B23/00, e.g. full-sized devices for demonstration purposes of industrial processes; of machinery
Abstract
The invention discloses a solidification process simulation experiment device, and belongs to the field of steel continuous casting. The solidification process simulation experiment device comprises: the device comprises an experiment pool, a metal plate and a water tank, wherein the bottom of the experiment pool is provided with the metal plate; the heat exchange device comprises a heat exchange pool, wherein a water inlet and a water outlet are respectively arranged at two ends of the heat exchange pool; the heat exchange port of the heat exchange pool is provided with an experimental pool in a matching way; the hot water tank and the cold water tank of the water supply unit are respectively connected with a first water inlet pipe, and the first water inlet pipe is connected with the water inlet through a first water pump and a second water inlet pipe; the water inlet ends of a first water outlet pipe and a second water outlet pipe of the drainage unit are respectively connected with the second water outlet pipe, the water outlet ends of the first water outlet pipe and the second water outlet pipe of the drainage unit are respectively connected with the first water inlet pipe, a second water inlet valve is arranged between the two water inlet ends, and a first water inlet valve is arranged between the two water outlet ends; and the observation instrument is arranged above the experimental pond. The invention provides a solidification process simulation experiment device which can simulate the crystallization behavior of molten steel in the solidification process.
Description
Technical Field
The invention relates to the technical field of steel continuous casting, in particular to a solidification process simulation experiment device.
Background
The task of steel production is to obtain a continuous casting billet which is qualified, and the essence of molten steel casting is to complete the transformation of steel from liquid to solid, i.e. the process of steel crystallization, also called steel solidification. The crystallization theory of molten steel is mainly from the thermodynamic point of view, and researches the relationship between crystal nucleation, growth, shape change rule and metal structure and quality. The solidification theory of molten steel is mainly from the point of view of heat transfer, and the relationship between the size of the solidification zone, the solidification time, the solidification characteristics and the quality is studied. At present, the research at home and abroad aiming at the solidification process of the molten steel is mainly the research on the static structure of the molten steel after solidification; for the dynamic research in the molten steel solidification process, because the crystallization behavior in the molten steel is difficult to directly observe under the high-temperature condition, the dynamic research aiming at the molten steel solidification process is difficult to realize under the prior art condition, so a set of experimental equipment specially researching the molten steel solidification process needs to be designed urgently, and the design of the simulation experimental equipment has great significance.
In order to solve the problem of the molten steel solidification simulation device, the applicant has already filed a patent, and the name of the invention is: the molten steel solidifies analogue means, and this patent's application number is: 201810861182X; the application dates of the patents are: 31/7/2018; the molten steel solidification simulation device of the invention comprises: the device comprises an experimental tank, a heat exchange tank, an observer and a water supply unit, wherein a metal plate is arranged at the bottom of the experimental tank, and heating plates are arranged outside the peripheral side wall of the experimental tank; one end of the heat exchange pool is provided with a water inlet, the other end of the heat exchange pool is provided with a water outlet, the experiment pool is arranged on the heat exchange pool, and the metal plate separates the heat exchange pool from the experiment pool; the observation instrument is arranged above the experiment pool; the water supply unit comprises a hot water tank and a cold water tank, a hot water outlet pipe of the hot water tank is connected with a water inlet through a pipeline, a first cold water valve is installed on the hot water outlet pipe, a cold water outlet pipe of the cold water tank is connected with the water inlet through a pipeline, and a first hot water valve is installed on the cold water outlet pipe. Thereby being capable of simulating the crystallization behavior in the process of solidifying the molten steel. However, the application scheme has the following disadvantages: the exchange time of hot water and cold water is longer, which results in poor simulation effect of the experiment. The invention aims to overcome the technical problems, provides an experimental device which can increase the exchange rate of hot water and cold water and improve the experimental simulation effect in the molten steel solidification process, and aims to solve the technical problems in the prior art.
Disclosure of Invention
1. Technical problem to be solved by the invention
The invention aims to overcome the defect that the simulation effect of the experiment is poor due to the fact that the exchange time of hot water and cold water in a molten steel solidification simulation experiment is long in the prior art, and provides a solidification process simulation experiment device which can improve the simulation effect of the molten steel solidification experiment.
2. Technical scheme
In order to achieve the purpose, the technical scheme provided by the invention is as follows:
the invention relates to a solidification process simulation experiment device, which comprises: the device comprises an experiment pool, a metal plate and a water tank, wherein the bottom of the experiment pool is provided with the metal plate; the heat exchange device comprises a heat exchange pool, wherein a water inlet and a water outlet are respectively arranged at two ends of the heat exchange pool; an experiment pool is arranged on a heat exchange port of the heat exchange pool in a matching way, and the metal plate separates the heat exchange pool from the experiment pool; the water supply unit comprises a hot water tank and a cold water tank, outlets of the hot water tank and the cold water tank are respectively connected with a first water inlet pipe, the first water inlet pipe is connected with a second water inlet pipe through a first water pump, and the end part of the second water inlet pipe is connected with a water inlet; the drainage unit comprises a first water outlet pipe provided with a first water outlet valve and a second water outlet pipe provided with a second water outlet valve; the water inlet end of the first water outlet pipe and the water inlet end of the second water outlet pipe are respectively connected with the second water outlet pipe, and a second water inlet valve is arranged between the two water inlet ends; the water outlet end of the first water outlet pipe and the water outlet end of the second water outlet pipe are respectively connected with the first water inlet pipe, and a first water inlet valve is arranged between the two water outlet ends; and the observation instrument is arranged above the experimental pond.
As a further improvement of the present invention, the water inlet end of the second water outlet pipe is closer to the water outlet end of the first water pump than the water inlet end of the first water outlet pipe; the water outlet end of the first water outlet pipe is closer to the water inlet end of the first water pump than the water outlet end of the second water outlet pipe.
As a further improvement of the invention, the bottom of the side wall of the experiment pool is provided with a heat insulation part, the heat insulation part is provided with a mounting groove, and a metal plate is embedded and mounted in the mounting groove.
As a further improvement of the invention, the hot water tank is connected with the first water inlet pipe through a hot water outlet pipe; and/or the cold water tank is connected with the first water inlet pipe through a cold water outlet pipe; the first water inlet pipe is connected with the inlet end of the first water pump; the outlet end of the first water pump is connected with the water inlet through a second water inlet pipe.
As a further improvement of the invention, the water outlet is connected with a first hot water pipe through a pipeline, the first hot water pipe is positioned at the upper part of the hot water tank, and a first hot water valve is arranged on the first hot water pipe; and/or the water outlet is connected with a cold water inlet pipe through a pipeline, the cold water inlet pipe is positioned at the upper part of the cold water tank, and a cold water inlet valve is arranged on the cold water inlet pipe.
As a further improvement of the invention, the water outlet is arranged at the top of the heat exchange pool, and a water outlet valve is arranged on the water outlet.
As a further improvement of the invention, the lower part of the first water inlet pipe is provided with a drainage box, the drainage box is connected with the bottom of the first water inlet pipe through a drainage pipe, and the drainage pipe is provided with a drainage valve.
As a further improvement of the invention, the metal plate is horizontally arranged at the bottom of the experiment pool, and the horizontal height of the metal plate is lower than that of the top wall of the heat exchange pool.
As a further improvement of the invention, the bottom of the heat insulation component is provided with a slide rail which is positioned at the lower part of the metal plate, and the bubble brush is arranged on the slide rail in a sliding way; the top of the bubble brush is in contact with the lower portion of the metal plate.
As a further improvement of the invention, a refrigerator is arranged in the cold water tank, and the refrigerator is arranged corresponding to the cold water inlet pipe.
3. Advantageous effects
Compared with the prior art, the technical scheme provided by the invention has the following beneficial effects:
(1) according to the solidification process simulation experiment device, when water is discharged from the heat exchange tank, the first water outlet valve and the second water outlet valve are opened, and the first water inlet valve and the second water inlet valve are closed; under the effect of first water pump, can take water out in the heat transfer pond fast to can accelerate the change speed of hot water, cold water, and then can improve the simulation effect of experiment, improve the accuracy of experiment simulation.
(2) According to the solidification process simulation experiment device, before the experiment solution is added, the peripheral side walls of the experiment pool are heated and insulated through the heating plates, the metal plate at the bottom of the experiment pool is heated and insulated through hot water in the hot water tank, so that the temperature of the peripheral side walls of the experiment pool and the temperature of the metal plate are not lower than that of the experiment solution, the experiment solution is prevented from being crystallized and separated immediately when being added into the experiment pool, the crystallization behavior in the solidification process of the molten steel can be simulated, and the observation effect in the crystallization process of the experiment solution is improved; overcomes the defect that the crystallization behavior of the molten steel is difficult to be directly observed under the high-temperature condition.
(3) According to the solidification process simulation experiment device, the heat insulation part arranged at the bottom of the side wall of the experiment pool prevents the metal plate from being in direct contact with the heating plate, so that the metal plate is not influenced by the temperature of the heating plate in the cooling process; the metal sheet sets up for the level, and the visualizer of being convenient for is observed the crystallization product on the metal sheet, avoids bringing observation error because of producing the slope between visualizer and the metal sheet, influences the accuracy of experiment.
(4) According to the solidification process simulation experiment device, the servo motor arranged on the bubble brush drives the bubble brush to slide back and forth along the length direction of the sliding rail; the top of bubble brush contacts with the lower part of metal sheet, and the bubble brush can erase the adnexed bubble in metal sheet bottom at reciprocating motion's in-process for bubble and metal sheet bottom separation have improved the heat transfer effect between water in the heat transfer pond and the metal sheet, and then have reduced the error of experiment.
(5) According to the solidification process simulation experiment device, the horizontal height of the metal plate is lower than that of the top wall of the heat exchange pool, so that bubbles erased by the bubble brush are gathered on the inner walls of the two ends of the top wall of the heat exchange pool, the bubbles cannot be attached to the lower part of the metal plate, and the heating effect or the cooling effect of water flow on the metal plate is further improved; the hot plate has the interval with the heat exchange pond roof for the hot plate can not heat the heat exchange pond roof, thereby has avoided the temperature of the water in the heat exchange pond to receive the influence.
Drawings
In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the drawings needed to be used in the embodiments will be briefly described below, it should be understood that the following drawings only illustrate some embodiments of the present invention and therefore should not be considered as limiting the scope, and for those skilled in the art, other related drawings can be obtained according to the drawings without inventive efforts.
FIG. 1 is a schematic view of the overall structure of a solidification process simulation experiment apparatus according to the present invention;
FIG. 2 is a schematic structural diagram of a heat exchange tank of the present invention;
FIG. 3 is a schematic structural view of the bottom of the experimental tank of the present invention;
FIG. 4 is a schematic structural view of the experimental tank without a metal plate at the bottom.
The reference numerals in the schematic drawings illustrate:
100. an experimental pond; 110. a metal plate; 120. a heat insulating member; 130. heating plates; 140. a bubble brush; 150. a servo motor;
200. a heat exchange pool; 201. a water inlet; 202. a water outlet; 203. the top wall of the heat exchange pool; 204. a heat exchange port; 210. a hot water tank; 220. a cold water tank; 221. storing the refrigerator; 230. a drainage box;
300. a first water pump; 310. a second water pump;
400. a hot water outlet pipe; 410. a cold water outlet pipe; 420. a first water inlet pipe; 430. a second water inlet pipe; 440. a first hot water pipe; 441. a second hot water pipe; 450. a cold water inlet pipe; 460. a first water outlet pipe; 470. a second water outlet pipe; 480. a drainage tube; 490. a breather pipe;
500. a hot water outlet valve; 510. a cold water outlet valve; 520. a first water inlet valve; 530. a second water inlet valve; 540. a first hot water valve; 541. a second hot water valve; 550. a cold water inlet valve; 560. a first water outlet valve; 570. a second water outlet valve; 580. a drainage valve; 590. a water outlet valve; 591. a vent valve;
600. an observation instrument; 610. a guide rail.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are some embodiments of the present invention, but not all embodiments; moreover, the embodiments are not relatively independent, and can be combined with each other according to needs, so that a better effect is achieved. Thus, the following detailed description of the embodiments of the present invention, presented in the figures, is not intended to limit the scope of the invention, as claimed, but is merely representative of selected embodiments of the invention. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
For a further understanding of the invention, reference should be made to the following detailed description taken in conjunction with the accompanying drawings and examples.
Example 1
Referring to fig. 1 and 2, the solidification process simulation experiment apparatus of the present embodiment includes an experiment tank 100, a heat exchange tank 200, an observer 600, a water supply unit, and a drainage unit, wherein a heat insulation member 120 is disposed at the bottom of a side wall of the experiment tank 100, a mounting groove is disposed on the heat insulation member 120, a metal plate 110 is embedded in the mounting groove, and the metal plate 110 may be a copper plate, an aluminum plate, or a silver plate; the copper plate adopted in the embodiment can ensure the heat-conducting property of the metal plate 110 on one hand, and has corrosion resistance and certain mechanical strength on the other hand, and the experiment cost is greatly reduced. In this embodiment, the heating plates 130 are installed outside the peripheral side walls of the experimental tank 100, and the heat insulating member 120 prevents the metal plate 110 from directly contacting the heating plates 130, so that the metal plate 110 is not affected by the temperature of the heating plates 130 during the cooling process; the metal plate 110 is horizontally arranged, so that the observation instrument 600 can observe the crystallized product on the metal plate 110 conveniently, and the observation effect is prevented from being influenced by the inclination between the observation instrument 600 and the metal plate 110; the heating plate 130 is used for heating and insulating the peripheral side walls of the experiment pool 100, so that the experiment solution in the experiment pool 100 is prevented from being cooled and separated out on the inner sides of the peripheral side walls, the experiment error is reduced, and the number of crystals separated out of the experiment solution on the metal plate 110 is ensured, so that enough crystal samples can be separated out on the metal plate 110 to facilitate observation, and the simulation effect of the experiment is improved; the heating temperature of the heating plate 130 of the embodiment is 90 ± 2 ℃, and the heating plate 130 is provided with a temperature detector for detecting the temperature of the heating plate 130; the heating plate 130 is not in contact with the top wall 203 of the heat exchange tank, so that when cold water is introduced into the heat exchange tank 200, the temperature of the cold water is not affected by the temperature of the heating plate 130, and further the metal plate 110 can be cooled at low temperature.
The heat exchange tank 200 is connected with the experiment tank 100, and is specifically explained as follows: the experiment pool 100 is arranged on the heat exchange port 204 of the heat exchange pool 200 in a matching way, and the heat exchange pool 200 and the experiment pool 100 are separated by the metal plate 110; one end of the heat exchange pool 200 is provided with a water inlet 201, the other end of the heat exchange pool 200 is provided with a water outlet 202, the water outlet 202 is arranged at the top of the heat exchange pool 200, so that bubbles in the heat exchange pool 200 can flow out from the water outlet 202 along with water flow, and the heating effect or the cooling effect of the water flow on the metal plate 110 can be improved. And a water outlet valve 590 is arranged on the water outlet 202; the top of the heat exchange pool 200 close to the water outlet 202 is connected with a vent pipe 490, the vent pipe 490 is provided with a vent valve 591, when the water in the heat exchange pool 200 needs to be drained, the vent valve 591 on the vent pipe 490 is opened, so that the situation that the external pressure is higher than the internal pressure of the device in the water draining process is avoided, the water in the device is difficult to drain, and the water in the heat exchange pool 200 can be smoothly drained.
The water supply unit is connected with the heat exchange pool 200, the water supply unit comprises a hot water tank 210 and a cold water tank 220, the hot water tank 210 is connected with a hot water outlet pipe 400, the hot water outlet pipe 400 is connected with a water inlet 201 through a pipeline, and a hot water outlet valve 500 is arranged on the hot water outlet pipe 400; the hot water tank 210 is provided with a heater for heating hot water in the hot water tank 210 so that the temperature of the water in the hot water tank 210 is maintained at 90 ± 2 ℃; the cold water tank 220 is connected with a cold water outlet pipe 410, the cold water outlet pipe 410 is connected with the water inlet 201 through a pipeline, and a cold water outlet valve 510 is arranged on the cold water outlet pipe 410; the cold water tank 220 is internally provided with the ice storage tank 221, ice cubes are contained in the ice storage tank 221, and the ice cubes can cool water in the cold water tank 220, so that the water in the cold water tank 220 is kept in a low-temperature state, wherein the temperature of the water in the cold water tank 220 is 0-4 ℃, and the cooling effect on the metal plate 110 can be further improved.
Wherein, a first water pump 300 is arranged on the pipeline between the hot water outlet pipe 400 and the water inlet 201, and/or a first water pump 300 is arranged on the pipeline between the cold water outlet pipe 410 and the water inlet 201; in this embodiment, the first water pump 300 is also disposed on the pipeline between the cold water outlet pipe 410 and the water inlet 201. The specific description is as follows:
the hot water outlet pipe 400 and the cold water outlet pipe 410 are respectively connected with a first water inlet pipe 420, a drainage box 230 is arranged at the lower part of the first water inlet pipe 420, the drainage box 230 is connected with the bottom of the first water inlet pipe 420 through a drainage pipe 480, a drainage valve 580 is arranged on the drainage pipe 480, and the horizontal height of the drainage box 230 is lower than the height of all the pipelines mentioned above; when the residual water in the first inlet pipe 420 needs to be discharged, the drainage valve 580 is opened to communicate the first inlet pipe 420 with the drainage pipe 480, and the residual water in the first inlet pipe 420 can be rapidly discharged into the drainage box 230, so that the water in the pipeline can be replaced. The first water inlet pipe 420 is connected to the water inlet end of the first water pump 300, and the water outlet end of the first water pump 300 is connected to the water inlet 201 through the second water inlet pipe 430.
The drainage unit of the present embodiment includes a first outlet pipe 460 and a second outlet pipe 470; the water inlet end of the first water outlet pipe 460 is connected with the second water inlet pipe 430, the water outlet end of the first water outlet pipe 460 is connected with the first water inlet pipe 420, and the first water outlet pipe 460 is provided with a first water outlet valve 560; the water inlet end of the second water outlet pipe 470 is connected with the second water inlet pipe 430; the water outlet end of the second water outlet pipe 470 is connected with the first water inlet pipe 420, and the second water outlet pipe 470 is provided with a second water outlet valve 570; a second water inlet valve 530 is arranged between the water inlet end of the first water outlet pipe 460 and the water inlet end of the second water outlet pipe 470, and the water inlet end of the second water outlet pipe 470 is closer to the water outlet end of the first water pump 300 than the water inlet end of the first water outlet pipe 460; a first water inlet valve 520 is arranged between the water outlet end of the first water outlet pipe 460 and the water outlet end of the second water outlet pipe 470, and the water outlet end of the first water outlet pipe 460 is closer to the water inlet end of the first water pump 300 than the water outlet end of the second water outlet pipe 470. When water is discharged from the heat exchange tank 200, the first water outlet valve 560 and the second water outlet valve 570 are opened, and the first water inlet valve 520 and the second water inlet valve 530 are closed; under the effect of first water pump 300, can take water out from heat exchange tank 200 fast to can accelerate the change speed of hot water, cold water, and then can improve the simulation effect of experiment, improve the accuracy of experiment simulation.
In this embodiment, the observation instrument 600 is installed above the experimental tank 100, and the observation instrument 600 is slidably installed on the guide rail 610, so that an experimenter can conveniently and directly observe the crystallization process of the experimental solution on the metal plate 110; by sliding the observation instrument 600 on the guide rail 610, the observation position of the observation instrument 600 can be changed, and the crystallization process of the experimental solution on the metal plate 110 can be conveniently and comprehensively observed.
In the method for simulating the solidification process of molten steel of the embodiment, hot water in the hot water tank 210 enters the heat exchange tank 200 through a pipeline, and the hot water in the heat exchange tank 200 heats the metal plate 110; the heating plate 130 heats and preserves the temperature of the peripheral side wall of the experimental pond 100; the experimental solution is poured into the experimental tank 100, then after the hot water in the heat exchange tank 200 is discharged, the cold water in the cold water tank 220 enters the heat exchange tank 200 through a pipeline, the cold water in the heat exchange tank 200 cools the metal plate 110, the experimental solution is crystallized and separated out on the surface of the metal plate 110, and the crystallization process is observed by using the observer 600. The method comprises the following specific steps:
the method comprises the following steps: heating and heat preservation
Heating plates 130 arranged outside the peripheral side walls of the experimental tank 100 are electrically heated, so that the temperature of the peripheral side walls of the experimental tank 100 is not lower than that of the experimental solution; in this embodiment, all the valves are initially closed, the hot water outlet valve 500, the first water inlet valve 520, the second water inlet valve 530 and the first water pump 300 are opened, and the vent valve 591 is opened; hot water in the hot water tank 210 flows into the heat exchange tank 200 from the water inlet 201 under the pumping action of the first water pump 300, when hot water overflows from the vent pipe 490, the heat exchange tank 200 is filled with hot water, at the moment, the water outlet valve 590 is opened, so that the hot water in the heat exchange tank 200 flows out from the water outlet 202, and meanwhile, the vent valve 591 is closed, so that the metal plate 110 is continuously heated in the process of flowing in and out of the heat exchange tank 200;
step two: adding the test solution
After heating for a period of time and when the temperature of the metal plate 110 is not lower than the temperature of the experimental solution, pouring the experimental solution into the experimental tank 100, wherein the experimental solution is NH4Aqueous Cl solution or Na2S2O3Aqueous solution, the experimental solution used in this example was NH4Saturated aqueous solution of Cl, the temperature of the added experimental solution is 80 +/-2 ℃; the experiment tank 100 is subjected to preheating treatment, so that the experiment solution can be prevented from being immediately crystallized when being poured into the experiment tank 100;
step three: discharging hot water
Firstly, closing the hot water outlet valve 500, the first water inlet valve 520 and the second water inlet valve 530, opening the vent valve 591 to communicate the heat exchange pool 200 with the outside, and opening the first water outlet valve 560 and the second water outlet valve 570; at this time, the drainage valve 580 is also opened, so that the first inlet pipe 420 is communicated with the drainage box 230; under the action of the first water pump 300, hot water in the heat exchange pool 200 flows out from the water inlet 201, enters the water inlet end of the first water pump 300 through the first water outlet pipe 460, flows out from the water outlet end of the first water pump 300 again, flows into the first water inlet pipe 420 through the second water outlet pipe 470, and is discharged into the drainage box 230 through the drainage pipe 480, so that the hot water in the pipeline and the heat exchange pool 200 is drained completely;
step four: simulating the solidification process of molten steel
Closing the flow-guiding valve 580, the first outlet valve 560 and the second outlet valve 570, and opening the cold water outlet valve 510, the first inlet valve 520 and the second inlet valve 530; the first water pump 300 pumps cold water in the cold water tank 220 into the heat exchange pool 200, when cold water overflows from the vent pipe 490, the heat exchange pool 200 is filled with cold water, the water outlet valve 590 is opened to enable the cold water in the heat exchange pool 200 to flow out from the water outlet 202, the vent valve 591 is closed, and the cold water continuously cools the metal plate 110 in the process of flowing in and out of the heat exchange pool 200, so that the temperature of the metal plate 110 is rapidly reduced, and an experimental solution is crystallized and precipitated on the surface of the metal plate 110;
the method for observing the simulated precipitated crystal by adopting the device comprises the following steps: the experimental solution is crystallized and precipitated on the surface of the metal plate 110 by using the above-mentioned steps, and the crystallization and precipitation process of the experimental solution is vertically observed by using the observer 600.
According to the invention, before the experimental solution is added, the metal plate 110 is heated and insulated by hot water in the hot water tank 210, and the peripheral side walls of the experimental tank 100 are heated and insulated by the heating plate 130, so that the temperature of the metal plate 110 and the temperature of the peripheral side walls of the experimental tank 100 are not lower than the temperature of the experimental solution, and the experimental solution is prevented from being crystallized and separated immediately when being added into the experimental tank 100, so that an experimenter can effectively observe the crystallization and separation process of the experimental solution, and the simulation effect of the experiment is improved.
Example 2
As shown in fig. 3 and 4, the basic content of this embodiment is the same as that of embodiment 1, except that: the first water pump 300 generates bubbles during pumping water, and the bubbles are attached to the lower portion of the metal plate 110. The bottom of the experimental tank 100 is provided with a slide rail, the slide rail is positioned at the lower part of the metal plate 110, the bubble brush 140 is slidably mounted on the slide rail, the bubble brush 140 is provided with a servo motor 150, and the servo motor 150 is used for driving the bubble brush 140 to slide back and forth along the length direction of the slide rail; the top of the bubble brush 140 contacts with the lower part of the metal plate 110, and the bubble brush 140 can wipe off bubbles attached to the bottom of the metal plate 110 in the reciprocating process, so that the attached bubbles are separated from the bottom of the metal plate 110, and the separated bubbles are discharged from the water outlet 202 under the driving of hot water or cold water, thereby improving the heating effect or the cooling effect of water flow on the metal plate 110.
The level of metal sheet 110 is less than the level of heat exchange pond roof 203, and the difference in height of metal sheet 110 and heat exchange pond roof 203 is 3 ~ 10cm, and this embodiment is 5 cm. So that the bubbles wiped by the bubble brush 140 are gathered on the inner walls of the two ends of the top wall 203 of the heat exchange tank and can be discharged from the water outlet 202; the bubbles are not attached to the lower portion of the metal plate 110, thereby improving the heating effect or the cooling effect of the water flow to the metal plate 110.
Example 3
The basic contents of this embodiment are the same as embodiment 1, except that: the bottom of the heat exchange tank 200 is connected with the hot water tank 210 through a second hot water pipe 441, and a second hot water valve 541 is arranged on the second hot water pipe 441, so that hot water can flow back to the hot water tank 210 along the second hot water pipe 441, thereby promoting the discharge of hot water and saving hot water resources; the second hot water pipe 441 is provided with a second hot water valve 541 so that the second hot water pipe 441 can be controlled to flow only hot water.
The water outlet 202 is connected with the water inlet end of the second water pump 310 through a pipeline, the water outlet end of the second water pump 310 is connected with the first hot water pipe 440, and the first hot water pipe 440 is positioned at the upper part of the hot water tank 210, so that the water outlet 202 is indirectly connected with the hot water tank 210, hot water used in the preheating process can flow back into the hot water tank 210 through the pipeline, the hot water is recycled, and hot water resources are greatly saved; the first hot water pipe 440 is provided with a first hot water valve 540 for controlling a hot water recovery process. The water outlet end of the second water pump 310 is connected with a cold water inlet pipe 450, the cold water inlet pipe 450 is positioned at the upper part of the cold water tank 220, and cold water used in the cooling crystallization process can be circulated into the cold water tank 220 through a pipeline, so that the cold water is recycled; the cold water inlet pipe 450 is disposed corresponding to the ice storage tank 221, and thus the recovered cold water can be cooled again, so that the water in the cold water tank 220 is kept at a low temperature; and a cold water inlet valve 550 is provided on the cold water inlet pipe 450 for controlling the recovery process of the cold water.
Example 4
The basic contents of this embodiment are the same as embodiment 1, except that: when the crystallization process of the experimental solution is observed, a certain dyeing reagent is added to form a sharp contrast with the crystal, so that the crystallization process can be observed more clearly; potassium permanganate or CuCl can be adopted in the experimental process2The solution acts as a staining reagent. The experimental solution used in this example was NH4Saturated aqueous solution of Cl, and CuCl as staining reagent2Solution of due to NH4Cl-H2Transparency of O solution and NH4Translucency of Cl crystals, CuCl2The solution is light blue and can be mixed with translucent NH4The Cl crystals form a sharp contrast, and experimenters can observe more conveniently; and CuCl2The chlorine ion in the solution can promote NH4And Cl is separated out, so that more crystals can be separated out from the experimental solution, and the simulation effect of the experiment is improved.
The present invention and its embodiments have been described above schematically, without limitation, and what is shown in the drawings is only one of the embodiments of the present invention, and the actual structure is not limited thereto. Therefore, if the person skilled in the art receives the teaching, without departing from the spirit of the invention, the person skilled in the art shall not inventively design the similar structural modes and embodiments to the technical solution, but shall fall within the scope of the invention.
Claims (8)
1. A solidification process simulation experiment device is characterized by comprising:
an experimental tank (100), wherein a metal plate (110) is arranged at the bottom of the experimental tank (100); a heat insulation part (120) is arranged at the bottom of the side wall of the experiment pool (100), a mounting groove is arranged on the heat insulation part (120), and a metal plate (110) is embedded and mounted in the mounting groove; the bottom of the heat insulation component (120) is provided with a slide rail which is positioned at the lower part of the metal plate (110), and the bubble brush (140) is installed on the slide rail in a sliding way; the top of the bubble brush (140) is in contact with the lower part of the metal plate (110);
the heat exchange device comprises a heat exchange pool (200), wherein a water inlet (201) and a water outlet (202) are respectively arranged at two ends of the heat exchange pool (200); the experimental tank (100) is arranged on the heat exchange port (204) of the heat exchange tank (200) in a matching way, and the metal plate (110) separates the heat exchange tank (200) from the experimental tank (100);
the water supply unit comprises a hot water tank (210) and a cold water tank (220), outlets of the hot water tank (210) and the cold water tank (220) are respectively connected with a first water inlet pipe (420), the first water inlet pipe (420) is connected with a second water inlet pipe (430) through a first water pump (300), and the end part of the second water inlet pipe (430) is connected with a water inlet (201);
a drainage unit comprising a first outlet pipe (460) provided with a first outlet valve (560) and a second outlet pipe (470) provided with a second outlet valve (570); the water inlet end of the first water outlet pipe (460) and the water inlet end of the second water outlet pipe (470) are respectively connected with the second water outlet pipe (470), and a second water inlet valve (530) is arranged between the two water inlet ends; the water outlet end of the first water outlet pipe (460) and the water outlet end of the second water outlet pipe (470) are respectively connected with the first water inlet pipe (420), and a first water inlet valve (520) is arranged between the two water outlet ends;
and the observation instrument (600) is arranged above the experiment pool (100).
2. The solidification process simulation experiment device of claim 1, wherein: the water inlet end of the second water outlet pipe (470) is closer to the water outlet end of the first water pump (300) than the water inlet end of the first water outlet pipe (460); the water outlet end of the first water outlet pipe (460) is closer to the water inlet end of the first water pump (300) than the water outlet end of the second water outlet pipe (470).
3. The solidification process simulation experiment device of claim 1, wherein:
the hot water tank (210) is connected with the first water inlet pipe (420) through a hot water outlet pipe (400); and/or the cold water tank (220) is connected with the first water inlet pipe (420) through a cold water outlet pipe (410);
the first water inlet pipe (420) is connected with the inlet end of the first water pump (300); the outlet end of the first water pump (300) is connected with the water inlet (201) through a second water inlet pipe (430).
4. The solidification process simulation experiment device of claim 1, wherein:
the water outlet (202) is connected with a first hot water pipe (440) through a pipeline, the first hot water pipe (440) is positioned at the upper part of the hot water tank (210), and a first hot water valve (540) is arranged on the first hot water pipe (440); and/or
The water outlet (202) is connected with a cold water inlet pipe (450) through a pipeline, the cold water inlet pipe (450) is positioned at the upper part of the cold water tank (220), and a cold water inlet valve (550) is arranged on the cold water inlet pipe (450).
5. The solidification process simulation experiment device of claim 1, wherein: the water outlet (202) is arranged at the top of the heat exchange pool (200), and a water outlet valve (590) is arranged on the water outlet (202).
6. The solidification process simulation experiment device of claim 1, wherein: the lower part of the first water inlet pipe (420) is provided with a drainage box (230), the drainage box (230) is connected with the bottom of the first water inlet pipe (420) through a drainage pipe (480), and the drainage pipe (480) is provided with a drainage valve (580).
7. The solidification process simulation experiment device of claim 1, wherein: the metal plate (110) is horizontally arranged at the bottom of the experimental tank (100), and the horizontal height of the metal plate (110) is lower than that of the top wall (203) of the heat exchange tank.
8. A coagulation process simulation experiment device according to any one of claims 1 to 7, wherein: a cold water storage tank (221) is arranged in the cold water tank (220), and the cold water storage tank (221) is arranged corresponding to the cold water inlet pipe (450).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811016650.XA CN109064871B (en) | 2018-08-31 | 2018-08-31 | Solidification process simulation experiment device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811016650.XA CN109064871B (en) | 2018-08-31 | 2018-08-31 | Solidification process simulation experiment device |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109064871A CN109064871A (en) | 2018-12-21 |
| CN109064871B true CN109064871B (en) | 2021-02-12 |
Family
ID=64758980
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811016650.XA Active CN109064871B (en) | 2018-08-31 | 2018-08-31 | Solidification process simulation experiment device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109064871B (en) |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2011253060A (en) * | 2010-06-02 | 2011-12-15 | Nihon Univ | Manufacturing apparatus for three-dimensional viscoelastic structure and manufacturing method therefor |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2003054533A1 (en) * | 2001-12-13 | 2003-07-03 | Sokolowski Jerzy H | Method and apparatus for universal metallurgical simulation and analysis |
-
2018
- 2018-08-31 CN CN201811016650.XA patent/CN109064871B/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2011253060A (en) * | 2010-06-02 | 2011-12-15 | Nihon Univ | Manufacturing apparatus for three-dimensional viscoelastic structure and manufacturing method therefor |
Also Published As
| Publication number | Publication date |
|---|---|
| CN109064871A (en) | 2018-12-21 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105092578B (en) | Moisture transition process follow-up mechanism and its experimental method in a kind of frozen soil | |
| CN109064871B (en) | Solidification process simulation experiment device | |
| CN101722291A (en) | Method and device for simulating horizontal growth process of solidification structure | |
| CN103586427A (en) | Method and device for preparing magnesium alloy liquid-state/semisolid-state melt through chilling and mechanical stirring | |
| CN109087570B (en) | Solidification process simulation experiment method | |
| CN108961972B (en) | Molten steel solidification simulator | |
| CN108982578B (en) | Method for simulating molten steel solidification process | |
| CN109036083B (en) | Device based on cold state experiment simulation solidification process | |
| CN208985532U (en) | A kind of device using Cold simulating test simulation solidification of molten steel process | |
| CN208721596U (en) | It is a kind of for studying the experimental provision of process of setting | |
| CN208985533U (en) | A kind of multi-pipeline device for simulating solidification of molten steel process | |
| CN109142426B (en) | Method for simulating crystallization rain phenomenon in molten steel solidification process | |
| CN108922367B (en) | Cold experimental device for solidification process | |
| CN108682277A (en) | A kind of experimental provision of simulation molten steel crystallisation by cooling | |
| RU84515U1 (en) | THERMOELECTRIC MODULE FOR HEATING AND / OR COOLING-FREEZING LIQUID OR SOLID PRODUCTS | |
| CN109164130B (en) | Cold state experimental method for solidification process | |
| CN106525893A (en) | Pavement semi-rigid base material freeze thawing test machine | |
| CN202562869U (en) | Visualization device for accurately measuring multi-phase thermal conductivity coefficients at low temperature | |
| CN208903550U (en) | A kind of experimental provision of mock inspection molten steel crystallization | |
| CN209015560U (en) | A kind of experimental system of solidification of molten steel process crystallization rain phenomenon | |
| RU2404132C2 (en) | Water purification method | |
| RU2472601C2 (en) | Method of simulating melt hydrodynamics in casting mould | |
| CN108961973A (en) | A kind of experimental system convenient for observing solidification of molten steel process crystallization rain phenomenon | |
| Himes et al. | Zone freezing demineralizing saline waters | |
| CN211451483U (en) | Ice mould, ice maker |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |