CN109060481B - Cluster pre-tightening device and method for ceramic fiber bundle sample irradiation test - Google Patents

Cluster pre-tightening device and method for ceramic fiber bundle sample irradiation test Download PDF

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Publication number
CN109060481B
CN109060481B CN201811069316.0A CN201811069316A CN109060481B CN 109060481 B CN109060481 B CN 109060481B CN 201811069316 A CN201811069316 A CN 201811069316A CN 109060481 B CN109060481 B CN 109060481B
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fiber bundle
irradiation
fixing screw
metal annular
ceramic fiber
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CN109060481A (en
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席航
刘晓松
李国云
孙凯
赵文斌
黄娟
李福荣
刘洋
张海生
雷阳
吴亚贞
聂良兵
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Nuclear Power Institute of China
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Nuclear Power Institute of China
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/286Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q involving mechanical work, e.g. chopping, disintegrating, compacting, homogenising
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/44Sample treatment involving radiation, e.g. heat

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  • Life Sciences & Earth Sciences (AREA)
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  • General Health & Medical Sciences (AREA)
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  • Investigating Strength Of Materials By Application Of Mechanical Stress (AREA)

Abstract

The invention discloses a cluster pre-tightening device and method for a ceramic fiber bundle sample irradiation test, which comprises the following steps: the device comprises an irradiation outer tank, an irradiation inner tank and 2 metal annular wiring supports; the 2 metal annular wiring supports are respectively fixed at two ends of the irradiation inner tank, and the axes of the irradiation outer tank, the irradiation inner tank and the metal annular wiring supports are superposed; a plurality of wire columns and a plurality of groups of fiber bundle pressing and fixing screw holes are uniformly distributed on each metal annular wiring support, and 2 metal annular wiring supports are symmetrical about the central line of the irradiation inner tank; the inner end and the outer end of the lead column are both convex, the arc of the outer edge of the outer convex end of the lead column is consistent with the arc radian of the inner surface of the irradiation outer tank, and the fiber pressing and fixing screw hole is matched with the screw and the gasket to press and fix the ceramic fiber bundles wound on the screw, so that the bundling and pre-tightening of the ceramic fiber bundles are realized, and the fibers in the ceramic fiber bundles are compact and uniform in stress state.

Description

Cluster pre-tightening device and method for ceramic fiber bundle sample irradiation test
Technical Field
The invention relates to the field of irradiation tests, in particular to a bundling pre-tightening device and method for a ceramic fiber bundle sample irradiation test.
Background
Compared with the traditional zirconium alloy cladding material, the ceramic fuel cladding material has better high-temperature oxidation resistance and strength, and therefore, the ceramic fuel cladding material is one of important candidate materials of accident-resistant fuel cladding materials. In the process of developing the cladding material for the reactor, in-reactor irradiation performance verification is required, and mechanical property changes such as material strength are measured. At present, the ceramic fuel cladding result form at home and abroad mainly takes a ceramic fiber bundle reinforced ceramic matrix as a main form, so that the irradiation tensile property data of the ceramic fiber bundle also becomes one of important reference indexes in the research and development process of the ceramic cladding material. Ceramic fiber bundles generally have tens to hundreds of dispersed fibers in different compositions, and the state is relatively loose, and each fiber in the fiber bundles is required to be uniformly stressed during a tensile test, so that the loose state is avoided. At present, the conventional method before irradiation is to perform pre-tightening bundling treatment on a fiber bundle through a metal frame before the fiber is subjected to a tensile test, and then perform curing treatment on the fiber in a pre-tightening bundling state through resin glue solution. Because the irradiation test temperature of the ceramic fiber bundle is far higher than the melting temperature of the resin, the ceramic fiber bundle must be pre-tightened and bundled in the irradiation test process of the ceramic fiber bundle. Because the irradiation space of the irradiation device is limited, the ceramic fiber bundle must meet the effective quantity of mechanical samples after subsequent irradiation and the preparation requirement of pre-tightening bundling, and the stacking irradiation form of the ceramic fiber bundle material becomes a technical problem. At present, no report is found in the research of stacking forms of ceramic fiber bundle materials at home and abroad, and the scientific problem needs to be solved by means of a scientific and reasonable bundling pre-tightening device to finish bundling pre-tightening of the ceramic fiber bundle materials in a limited narrow space.
Disclosure of Invention
The invention provides a bundling and pre-tightening device and method for an irradiation test of a ceramic fiber bundle sample, which solve the bundling and pre-tightening problem of the irradiation test of a ceramic fiber bundle material, realize bundling and pre-tightening of the ceramic fiber bundle and achieve the technical effects of making fibers in the ceramic fiber bundle more compact and uniform in stress state.
In order to achieve the above object, the present application provides a ceramic fiber bundle sample irradiation test bundling pre-tightening device, which comprises:
the device comprises an irradiation outer tank, an irradiation inner tank and 2 metal annular wiring supports; the 2 metal annular wiring supports are respectively fixed at two ends of the irradiation inner tank, and the axes of the irradiation outer tank, the irradiation inner tank and the metal annular wiring supports are superposed; a plurality of wire columns and a plurality of groups of fiber bundle pressing and fixing screw holes are uniformly distributed on each metal annular wiring support, 2 metal annular wiring supports are symmetrical about the central line of the irradiation inner tank, the number of each group of fiber bundle pressing and fixing screw holes is 2, and a connecting line of the 2 fiber bundle pressing and fixing screw holes in each group penetrates through the circle center of the metal annular wiring support; the inner end and the outer end of the lead column are both convex, the arc of the outer edge of the outer convex end of the lead column is consistent with the arc radian of the inner surface of the irradiation outer tank, and the fiber pressing and fixing screw hole is matched with the screw and the gasket to press and fix the ceramic fiber bundle wound on the screw.
The application is realized by the following technical scheme:
the utility model provides a ceramic fiber bundle irradiation test pretension device tied in a bundle, includes the irradiation inner tank, the irradiation inner tank about the terminal surface meet with coaxial metal annular wiring support, metal annular wiring support on the protruding metallic channel groove of taking both ends (being the wire column) and the fibre bundle of symmetry evenly distributed compress tightly fixed screw (fixed screw can be a plurality of, but must be symmetrical evenly distributed, guarantee that its packing force is even), protruding metallic channel mainly to ceramic fiber bundle pretension winding tied in a bundle. The outer edge arc of the convex wire groove distributed by the metal annular wiring support is consistent with the arc radian of the inner surface of the irradiation tank, and the outer edge of the convex wire groove distributed by the metal annular wiring support is well matched with the inside of the irradiation tank in the assembling process through size design, so that the assembly is facilitated. And the pressing and fixing screw holes distributed on the metal annular wiring support are matched with the screws and the gaskets to press and fix the ceramic fiber bundles wound on the screws. After one end of the ceramic fiber bundle is pressed and fixed on the metal annular wiring support, the ceramic fiber bundle is wound back and forth along the pre-tightening wire grooves which are raised at the upper end and the lower end of the irradiation inner tank to perform bundling pre-tightening, and the ceramic fiber bundle is pressed through the position of the compression screw of the metal annular wiring support.
The hollow part of the irradiation inner tank can be used for avoiding the waste of irradiation space and putting other irradiation samples, the upper end surface and the lower end surface of the hollow part are welded with the metal annular wiring bracket, and ceramic fiber bundles are arranged in the annular gap part of the irradiation inner tank and the outer irradiation tank on the same axis.
The annular cloth bunch frame is provided with fixing screw holes, fixing screws and gaskets which are matched to play a role in compressing and fixing the wound ceramic fiber bunch, the protruding wire grooves of the metal annular wiring support play a role in bunching and supporting and guiding the wound ceramic fiber bunch, and the outward arc parts of the dumbbell-shaped wire grooves are in contact with the inner wall of the irradiation outer tank to play a role in guiding and supporting the whole bunching pre-tightening device.
In another aspect, the present application provides a method for pre-tightening a ceramic fiber bundle sample, based on a pre-tightening device, the method including:
selecting a fiber bundle pressing and fixing screw hole on one of 2 metal annular wiring, connecting a gasket and a fixing screw on the fiber bundle pressing and fixing screw hole in a matching manner, forming a wire slot between the end face of the fiber bundle pressing and fixing screw hole and the end face of the gasket, which faces the fiber bundle pressing and fixing screw hole, winding the ceramic fiber bundle in the wire slot, pressing the ceramic fiber bundle by screwing the fixing screw, bundling and pre-tightening the ceramic fiber bundle by a corresponding wire column on the other metal annular wiring bracket, then returning the ceramic fiber bundle to the first metal annular wiring for winding on the wire column or pressing on the fiber bundle pressing and fixing screw hole, changing to another metal annular wiring bracket for winding on the wire column or pressing on the fiber bundle pressing and fixing screw hole after winding on the wire column on one metal annular wiring bracket or pressing on the fiber bundle pressing and fixing screw hole, and each metal annular wiring support is provided with a winding or pressing device which sequentially winds or presses in a clockwise or anticlockwise direction, the process is circulated until the last fiber bundle pressing and fixing screw hole presses, and the ceramic fiber bundles are placed into the irradiation outer tank after the metal annular wiring supports at the two ends complete winding and pre-tightening.
One or more technical solutions provided by the present application have at least the following technical effects or advantages:
according to the ceramic fiber sample irradiation test bundling pre-tightening device, the screw and the gasket on the wiring support are used for compressing and fixing the wound ceramic fibers, bundling pre-tightening is conducted on the ceramic fiber bundles through winding in the protruding wire groove, and therefore fibers in the ceramic fiber bundles are compact and uniform in stress state.
A ceramic fiber sample irradiation test pretension device tied in a bundle in this application, the distribution of the tow irradiation sample that makes through structural design only occupies the clearance space of irradiation inner tank and outer irradiation jar, and other types of samples can still be deposited to irradiation inner tank inner space, obtain optimizing from the space utilization. Meanwhile, the inner and outer irradiation tanks play a certain role in protecting the ceramic fibers in the irradiation process.
A ceramic fiber sample irradiation test pretension device tied in a bundle in this application for ceramic fiber bundle keeps even atress and state tied in a bundle among the irradiation process, after the irradiation test was accomplished, can take out the direct gumming solidification of going on of pretension device from the irradiation jar, stretch the sample preparation after the follow-up irradiation of being convenient for.
Drawings
The accompanying drawings, which are included to provide a further understanding of the embodiments of the invention and are incorporated in and constitute a part of this application, illustrate embodiments of the invention and together with the description serve to explain the principles of the invention;
FIG. 1 is a schematic cross-sectional view of a metal ring wiring mount of the present application;
FIG. 2 is a schematic structural view of a metal ring wiring support according to the present application;
FIG. 3 is a schematic structural diagram of a cluster pre-tightening device for a ceramic fiber sample irradiation test in the application;
FIG. 4 is a partially enlarged schematic view of a cluster pre-tightening device for a ceramic fiber sample irradiation test in the application;
reference numerals and corresponding part names:
1-metal annular wiring support, 2-raised wire groove, 3-fixing screw hole, 4-metal gasket, 5-fixing screw, 6-irradiation inner tank, 7-irradiation outer tank and 8-ceramic fiber bundle.
Detailed Description
In order that the above objects, features and advantages of the present invention can be more clearly understood, a more particular description of the invention will be rendered by reference to the appended drawings. It should be noted that the embodiments and features of the embodiments of the present application may be combined with each other without conflicting with each other.
In the following description, numerous specific details are set forth in order to provide a thorough understanding of the present invention, however, the present invention may be practiced in other ways than those specifically described and thus the scope of the present invention is not limited by the specific embodiments disclosed below.
Referring to fig. 1-4, a cluster pre-tightening device for a ceramic fiber sample irradiation test comprises a metal ring wiring support 1, an irradiation inner tank 6 and fixing screws 5, and is characterized in that the cluster pre-tightening device is composed of two metal ring wiring supports 1 and the irradiation inner tank 6 which are identical in structure, fixing screw holes 3 are formed in two ends of each metal ring wiring support along a symmetrical axis (the fixing force of the fixing screw holes is uniformly distributed, so that the fixing screw holes are not suggested to be on the same central line), in the assembling process, the axes corresponding to the fixing screw holes 3 of the two metal ring wiring supports 1 are vertically intersected (the purpose of vertical intersection is that each 1/4 circular arcs are provided with one fixing screw hole, so that the uniform compression force of a fiber bundle can be realized), and dumbbell-shaped wire grooves 2 are symmetrically and uniformly distributed in two ends of each fixing screw hole 3. The wire position of 2 wire casings in dumbbell shape wire casing has certain chamfer, and 2 peripheral radians in protruding wire casing are unanimous and on the round axle with the inner wall radian of outer irradiation jar, guarantee through size design that can realize good cooperation in the protruding wire casing outward flange that the metal ring shape wiring support distributes and the irradiation jar in the assembling process, the equipment of being convenient for. The dumbbell guide slots 2 can be designed in different sizes to accommodate the ceramic fiber bundles 8. Select the fixed screw 3 of one end at metal ring shape wiring support 1, gasket 4, set screw 6 cooperation is connected on fixed screw 3, ceramic fiber bundle 8 twines towards the wire inslot that fixed screw terminal surface formed through fixed screw terminal surface and gasket 3, it compresses tightly ceramic fiber bundle 8 to move set screw 5 through twisting, let ceramic fiber bundle 8 in proper order again according to the order nearby go up corresponding dumbbell shape metallic channel 2 on the metal ring shape wiring support 1 of the other end and cluster and pretension ceramic fiber, the dumbbell shape metallic channel 2 that jar 6 both ends metal ring shape wiring support 1 corresponds in the irradiation twines back and forth, it compresses tightly to carry out similar winding again through first fixed screw 3 at last. After the ceramic fiber bundle 8 is wound and pre-tightened on the metal annular wiring supports 1 at the two ends, the whole pre-tightening step of the ceramic fiber bundle 8 is completed, and then the whole device is placed into the irradiation outer tank 7.
The application has the main technical characteristics that: the loose ceramic fiber bundle sample for the irradiation test is subjected to sectional bundling and pre-tightening through the dumbbell-shaped wire guide groove and the fixing screw, so that the situation that the irradiated ceramic fiber bundle is loose is avoided, the preparation of a tensile sample of the ceramic fiber bundle in a hot chamber is facilitated, the organization mode of the ceramic fiber bundle sample only occupies the gap between the irradiation inner tank and the irradiation appearance, and the irradiation test space is saved.
While preferred embodiments of the present invention have been described, additional variations and modifications in those embodiments may occur to those skilled in the art once they learn of the basic inventive concepts. Therefore, it is intended that the appended claims be interpreted as including preferred embodiments and all such alterations and modifications as fall within the scope of the invention.
It will be apparent to those skilled in the art that various changes and modifications may be made in the present invention without departing from the spirit and scope of the invention. Thus, if such modifications and variations of the present invention fall within the scope of the claims of the present invention and their equivalents, the present invention is also intended to include such modifications and variations.

Claims (5)

1. A ceramic fiber bundle sample irradiation test bundling pre-tightening device is characterized by comprising:
the device comprises an irradiation outer tank, an irradiation inner tank and 2 metal annular wiring supports; the 2 metal annular wiring supports are respectively fixed at two ends of the irradiation inner tank, and the axes of the irradiation outer tank, the irradiation inner tank and the metal annular wiring supports are superposed; a plurality of wire columns and a plurality of groups of fiber bundle pressing and fixing screw holes are uniformly distributed on each metal annular wiring support, 2 metal annular wiring supports are symmetrical about the central line of the irradiation inner tank, the number of each group of fiber bundle pressing and fixing screw holes is 2, and a connecting line of the 2 fiber bundle pressing and fixing screw holes in each group penetrates through the circle center of the metal annular wiring support; the inner end and the outer end of the lead column are both convex, the arc of the outer edge of the outer convex end of the lead column is consistent with the arc radian of the inner surface of the irradiation outer tank, and the fiber pressing and fixing screw hole is matched with the screw and the gasket to press and fix the ceramic fiber bundle wound on the screw.
2. The ceramic fiber bundle sample irradiation test bundling pretension device according to claim 1, characterized in that the annular gap portion of the irradiation inner tank and the irradiation outer tank is used for arranging ceramic fiber bundles.
3. The ceramic fiber bundle sample irradiation test bundling preloading device of claim 1, characterized in that the arc part of the outer convex end of the lead column is in contact with the inner wall of the irradiation outer tank.
4. The ceramic fiber bundle sample irradiation test bundling and pre-tightening device according to claim 1, wherein 2 groups of fiber bundle pressing and fixing screw holes are uniformly distributed on each metal annular wiring support, and 4 fiber bundle pressing and fixing screw holes are uniformly distributed on the metal annular wiring support.
5. A method of pre-tensioning a sample of ceramic fibre tow based on a pre-tensioning device according to any one of claims 1 to 4, the method comprising:
selecting a fiber bundle pressing and fixing screw hole on one of 2 metal annular wiring supports, connecting a gasket and a fixing screw on the fiber bundle pressing and fixing screw hole in a matching manner, forming a wire slot between the end face of the fiber bundle pressing and fixing screw hole and the end face of the gasket, which faces the fiber bundle pressing and fixing screw hole, winding a ceramic fiber bundle in the wire slot, pressing the ceramic fiber bundle by screwing the fixing screw, bundling and pre-tightening the ceramic fiber bundle by a corresponding wire column on the other metal annular wiring support, returning the ceramic fiber bundle to the first metal annular wiring support to wind on the wire column or press on the fiber bundle pressing and fixing screw hole, changing to another metal annular wiring support to wind on the wire column or press on the fiber bundle pressing and fixing screw hole after winding on the wire column on one metal annular wiring support or pressing on the fiber bundle pressing and fixing screw hole, and each metal annular wiring support is provided with a winding or pressing device which sequentially winds or presses in a clockwise or anticlockwise direction, the process is circulated until the last fiber bundle pressing and fixing screw hole presses, and the ceramic fiber bundles are placed into the irradiation outer tank after the metal annular wiring supports at the two ends complete winding and pre-tightening.
CN201811069316.0A 2018-09-13 2018-09-13 Cluster pre-tightening device and method for ceramic fiber bundle sample irradiation test Active CN109060481B (en)

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CN109855934A (en) * 2019-02-27 2019-06-07 北京市理化分析测试中心 A kind of carbon fiber boundling sample and preparation method thereof
CN109900534B (en) * 2019-02-27 2023-09-01 北京市理化分析测试中心 Carbon fiber bundling sample preparation device and carbon fiber bundling preparation method
CN113334271B (en) * 2021-05-25 2022-08-09 中国科学院上海硅酸盐研究所 Frock clamp is used in preparation of single bundle of fiber reinforcement ceramic matrix composite

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KR20000013054A (en) * 1998-08-04 2000-03-06 강병호 Optical cluster cable divergence apparatus for high-core and diverging method using thereof
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