CN109046202A - A kind of reaction kettle structure for silicone oil processing - Google Patents
A kind of reaction kettle structure for silicone oil processing Download PDFInfo
- Publication number
- CN109046202A CN109046202A CN201810912995.7A CN201810912995A CN109046202A CN 109046202 A CN109046202 A CN 109046202A CN 201810912995 A CN201810912995 A CN 201810912995A CN 109046202 A CN109046202 A CN 109046202A
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- CN
- China
- Prior art keywords
- reaction kettle
- reactor tank
- silicone oil
- oil processing
- kettle structure
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
- B01J19/10—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing sonic or ultrasonic vibrations
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00094—Jackets
Abstract
The invention discloses a kind of reaction kettle structures for silicone oil processing, the agitating device for including reaction kettle and being built in the reaction kettle, several ultrasonic transmitters are installed on the inner sidewall of the reaction kettle, several described ultrasonic transmitters are electrically connected with controller, the controller is electrically connected with detection device, the detection device is provided with probe, and described pop one's head in is mounted on the inside of the reaction kettle, so that in silicone oil raw material mixed process, raw molecule moves in solution, so that raw material is more fully mixed, agitating device is stirred simultaneously, not only increase the quality of production, make the rate for improving production simultaneously.
Description
Technical field
The present invention relates to the technical fields of silicone oil processing, and in particular to a kind of reaction kettle structure for silicone oil processing.
Background technique
The reaction kettle of silicone oil is comprehensive reaction vessel, to reaction kettle structure function and configures attachment according to reaction condition
Design.Pre-set reaction step can be completed with higher the degree of automation from charging-reaction-discharging of beginning,
The important parameters such as (stirring, air blast etc.), reactant/product concentration are controlled to the temperature in reaction process, pressure, mechanics to carry out sternly
The regulation of lattice.
Existing reaction kettle is mainly stirred to react by the agitating device in kettle, but mixed effect is bad, and
Reaction rate is slower, so need to design a kind of good mixing effect, and the fast device of reaction rate is used for the processing of silicone oil.
Summary of the invention
The present invention provides a kind of reaction kettle structure for silicone oil processing, to solve showing for above-mentioned background technique proposition
There is the mixed effect of technology bad, and the technical problem that reaction rate is slower.
To solve the problems, such as that above-mentioned background technique proposes the technical solution used are as follows: a kind of reaction for silicone oil processing
The agitating device that kettle structure includes reactor tank and is built in the reactor tank is equipped on the inner sidewall of the reactor tank
Several ultrasonic transmitters, several described ultrasonic transmitters are electrically connected with controller, and the controller is electrically connected
There is detection device, the detection device is provided with probe, and described pop one's head in is mounted on the inside of the reactor tank.
Preferably, described to have ultrasonic transmitter to be set as three groups, one group two, three groups of ultrasonic transmitters are pacified respectively
On upper end, middle part and lower inner side wall loaded on the reactor tank, and every group of two ultrasonic transmitters are symmetrically installed.
Preferably, the tank skin of the reactor tank is equipped with heating interlayer, and the heating interlayer is liquid heating interlayer.
Preferably, the top of the reactor tank is equipped with solid feedstock mouth, liquid feed mouth and water inlet pipe, in the water inlet pipe
Flowmeter and solenoid valve are installed, the flowmeter is electrically connected with modulator, and the modulator is equipped with screen display and regulation button,
And the modulator and solenoid valve are electrically connected.
Preferably, erector is provided at the top of the reaction kettle, the erector is equipped with temperature measuring set, and described
Temperature measuring set runs through the top of reactor tank, and extends to the inner cavity of reactor tank.
Preferably, the temperature measuring set is electrically connected at the controller.
Preferably, the agitating device is connected with driving motor by bearing, and the agitating device is sphere of movements for the elephants type frame.
Preferably, the solid feedstock mouth is " funnel " type, and the solid feedstock mouth is located at the edge of the reactor tank
Side.
Preferably, the bottom of the reactor tank is at " taper ", and the least significant end of " taper " is provided with discharge port.
Compared with prior art, the invention has the benefit that the present invention is sent out by being equipped with ultrasonic wave in reactor tank
Emitter, so that raw material is more fully mixed, is stirred simultaneously so that raw molecule moves in solution in silicone oil raw material mixed process
It mixes device to be stirred, mixing rate can be accelerated;Ultrasonic wave connection there is into controller, while controller is connected with detection device,
Detection mixed effect is carried out by detection device, the intensity of regulation ultrasonic transmitter, present invention behaviour can be carried out by controller
Facilitate, reaction effect is more preferable.
Detailed description of the invention
Fig. 1 is the structural diagram of the present invention;
Fig. 2 is cross-sectional view of the invention.
In figure: 1- reactor tank;2- heating interlayer;3- solid feedstock mouth;4- liquid feed mouth;5- water inlet pipe;6- flowmeter;
7- solenoid valve;8- modulator;801- screen display;802- regulates and controls button;9- bearing;10- driving motor;11- agitating device;12- installation
Device;13- temperature measuring set;14- controller;15- ultrasonic transmitter;16- detection device;17- probe;18- discharge port.
Specific embodiment
To facilitate the understanding of the present invention, the present invention is described more fully below with reference to relevant drawings, attached drawing
In give several embodiments of the invention, but the present invention can be realized by different forms, however it is not limited to text institute
The embodiment of description, opposite, it theses embodiments are provided so that more thorough and comprehensive to present disclosure.
It should be noted that it can directly on the other element when element is referred to as " being fixedly arranged on " another element
There may also be elements placed in the middle, and when an element is considered as " connection " another element, it can be directly to separately
One element may be simultaneously present centering elements, term as used herein "vertical", "horizontal", "left" and "right"
And similar statement is for illustrative purposes only.
Unless otherwise defined, all technical and scientific terms used herein and belong to technical field of the invention
The meaning that technical staff usually connects is identical, and term knowledge as used herein in the specification of the present invention is in order to describe to have
The purpose of the embodiment of body, it is not intended that in the limitation present invention, term " and or " used herein includes one or more phases
Any and all combinations of the listed item of pass.
Embodiment 1 please refers to Fig. 1-2, and a kind of reaction kettle structure for silicone oil processing includes reactor tank 1 and interior
The agitating device 11 in the reactor tank 1 is set, several ultrasonic transmitters are installed on the inner sidewall of the reactor tank 1
15, several described ultrasonic transmitters 15 are electrically connected with controller 14, and the controller 14 is electrically connected with detection device
16, the detection device 16 is provided with probe 17, and the probe 17 is mounted on the inside of the reactor tank 1.
The present invention can make raw material by being equipped with several ultrasonic transmitters 15 on the inner sidewall of reactor tank 1
Molecule moves in the solution, and mixed effect more preferably, keeps reaction more abundant, several described ultrasonic transmitters 15 are electrically connected
Have controller 14, the controller 14 is electrically connected with detection device 16, by detection device 16 detect as a result, then leading to
The intensity that controller 14 carries out regulation ultrasonic transmitter 15 is crossed, the intensity due to ultrasonic transmitter 15 can be effectively prevented
It is not high, to keep product quality bad.
Specifically, described have ultrasonic transmitter 15 to be set as three groups, one group two, three groups of ultrasonic transmitters 15 divide
It is not installed on the upper end, middle part and lower inner side wall of the reactor tank 1, and every group two ultrasonic transmitters 15 are symmetrical
Installation.
The present invention can pass through multiple ultrasonic transmitters by the way that wave launcher 15 is set as three groups, while every group two
15 work together, so that silicone oil is uniformly mixed.
Specifically, the tank skin of the reactor tank 1 is equipped with heating interlayer 2, and the heating interlayer 2 is liquid heating interlayer 2.
The present invention can make to be heated evenly, and the heating interlayer 2 by the way that the kettle wall of reactor tank 1 is set as heating interlayer 2
For liquid heating interlayer 2, it is to be able to quickly heat.
Specifically, the top of the reactor tank 1 is equipped with solid feedstock mouth 3, liquid feed mouth 4 and water inlet pipe 5, the water inlet
Flowmeter 6 and solenoid valve 7 are installed, the flowmeter 6 is electrically connected with modulator 8, and the modulator 8 is equipped with screen in pipe 5
801 and regulation button 802 are shown, and the modulator 8 and solenoid valve 8 are electrically connected.
The present invention is by being equipped with solid feedstock mouth 3, liquid feed mouth 4 at the top of reactor tank 1, by solid feed and liquid
Raw material is added separately to, and can prevent solid feed and liquid material from reacting when being added in sprue, so that sprue is stifled
Plug, while flowmeter 6 and solenoid valve 7 being installed in water inlet pipe 5, water injection rate can be controlled by flowmeter 6 and solenoid valve 7,
The flowmeter 6 is electrically connected with modulator 8 simultaneously, and the modulator 8 is equipped with screen display 801 and regulation button 802, and the tune
It controls device 8 and solenoid valve 8 to be electrically connected, is while to control the open and-shut mode of solenoid valve 7 to change water injection rate by modulator 8.
Specifically, the top of the reactor tank 1 is provided with erector 12, the erector 12 is equipped with temperature measuring set
13, and the temperature measuring set 13 runs through the top of reaction kettle 1, and extends to the inner cavity of reactor tank 1, while the temperature measures
Instrument 13 is electrically connected at the controller 14.
The present invention is capable of the interior temperature of real-time monitoring reactor tank 1 by being equipped with temperature measuring set 13 in reaction kettle 1
Degree, the temperature measuring set 13 are electrically connected at the controller 14, are to control the temperature in reactor tank 1 by controller 14
Degree, so that being able to maintain optimum temperature when reaction.
Specifically, the agitating device 11 is connected with driving motor 10 by bearing 9, and the agitating device 11 is sphere of movements for the elephants
Type frame.
The present invention can not only make stirring sufficiently, while can not hinder by being sphere of movements for the elephants type frame by agitating device 11
Hinder the work of ultrasonic transmitter 15.
Specifically, the solid feedstock mouth 4 is " funnel " type, and the solid feedstock mouth 4 is located at the side of the reaction kettle 1
Edge side.
The present invention is the addition of solid feed for convenience by setting " funnel " type for solid feedstock mouth 4, is prevented solid
The blocking of state raw material is overflowed, while the solid feedstock mouth 4 is located at the edge side of the reaction kettle 1, is to be added in order to prevent
When solid feed, the agitated device of solid feed is collided and is splashed.
Specifically, the bottom of the reactor tank 1 is at " taper ", and the least significant end of " taper " is provided with discharge port 18,
It is to discharge for convenience.
In conclusion the present invention in reactor tank 1 by being equipped with ultrasonic transmitter 15, cooperation agitating device 11 is simultaneously
Work, enables in silicone oil raw material mixed process, and raw molecule moves in solution, so that raw material is more fully mixed, into
One step, flowmeter 6 and solenoid valve 7 are installed in water inlet water inlet pipe 5, inflow can be controlled effectively in real time, make into
Water is definite value, further, temperature measuring set 13 is equipped in reactor tank 1, can control the reaction temperature in reactor tank 1
Degree.
Certain embodiment of the invention above described embodiment only expresses, the description thereof is more specific and detailed, but simultaneously
Limitations on the scope of the patent of the present invention therefore cannot be interpreted as.It should be pointed out that for those of ordinary skill in the art
For, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to guarantor of the invention
Protect range.Therefore, the scope of protection of the patent of the invention shall be subject to the appended claims.
Claims (9)
1. a kind of reaction kettle structure for silicone oil processing includes reactor tank (1) and is built in the reactor tank (1)
Agitating device (11), it is characterised in that: several ultrasonic transmitters (15) are installed on the inner sidewall of the reactor tank (1),
Several described ultrasonic transmitters (15) are electrically connected with controller (14), and the controller (14) is electrically connected with detection dress
It sets (16), the detection device (16) is provided with probe (17), and the probe (17) is mounted on the interior of the reactor tank (1)
Portion.
2. a kind of reaction kettle structure for silicone oil processing according to claim 1, it is characterised in that: described to have ultrasound
Wave launcher (15) is set as three groups, and one group two, three groups of ultrasonic transmitters (15) are respectively arranged in the reactor tank (1)
Upper end, on middle part and lower inner side wall, and every group two ultrasonic transmitters (15) are symmetrically installed.
3. a kind of reaction kettle structure for silicone oil processing according to claim 1, it is characterised in that: the reactor tank
(1) tank skin is equipped with heating interlayer (2), and the heating interlayer (2) is liquid heating interlayer (2).
4. a kind of reaction kettle structure for silicone oil processing according to claim 1, it is characterised in that: the reactor tank
(1) top is equipped with solid feedstock mouth (3), liquid feed mouth (4) and water inlet pipe (5), is equipped with flow in the water inlet pipe (5)
Meter (6) and solenoid valve (7), the flowmeter (6) are electrically connected with modulator (8), and the modulator (8) is equipped with screen display
(801) and regulate and control button (802), and the modulator (8) and solenoid valve (8) are electrically connected.
5. a kind of reaction kettle structure for silicone oil processing according to claim 1, it is characterised in that: the reactor tank
(1) it is provided at the top of erector (12), the erector (12) is equipped with temperature measuring set (13), and the temperature measuring set
(13) run through the top of reactor tank (1), and extend to the inner cavity of reactor tank (1).
6. a kind of reaction kettle structure for silicone oil processing according to claim 5, it is characterised in that: the temperature is surveyed
Amount instrument (13) is electrically connected at the controller (14).
7. a kind of reaction kettle structure for silicone oil processing according to claim 1, it is characterised in that: the stirring dress
It sets (11) to be connected with driving motor (10) by bearing (9), and the agitating device (11) is sphere of movements for the elephants type frame.
8. a kind of reaction kettle structure for silicone oil processing according to claim 4, it is characterised in that: the solid-state into
Material mouth (4) is " funnel " type, and the solid feedstock mouth (4) is located at the edge side of the reactor tank (1).
9. a kind of reaction kettle structure for silicone oil processing according to claim 1, it is characterised in that: the reactor tank
(1) bottom is at " taper ", and the least significant end of " taper " is provided with discharge port (18).
Priority Applications (1)
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CN201810912995.7A CN109046202A (en) | 2018-08-13 | 2018-08-13 | A kind of reaction kettle structure for silicone oil processing |
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CN201810912995.7A CN109046202A (en) | 2018-08-13 | 2018-08-13 | A kind of reaction kettle structure for silicone oil processing |
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CN109046202A true CN109046202A (en) | 2018-12-21 |
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CN201810912995.7A Pending CN109046202A (en) | 2018-08-13 | 2018-08-13 | A kind of reaction kettle structure for silicone oil processing |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112007578A (en) * | 2020-09-10 | 2020-12-01 | 黄石加柯环保科技有限公司 | Production equipment and production method of sodium carbonate solution |
Citations (5)
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JPH08295709A (en) * | 1995-04-25 | 1996-11-12 | Toyo Eng Corp | Production of rubber-modified resin composition |
CN201692810U (en) * | 2010-04-27 | 2011-01-05 | 杭州中兴化工装备有限公司 | Plastic reactor |
CN105148825A (en) * | 2015-09-16 | 2015-12-16 | 成都米戈科技有限公司 | Reaction kettle |
CN206228984U (en) * | 2016-12-07 | 2017-06-09 | 江西如益科技发展有限公司 | A kind of temperature control with electronic monitoring discharging functions, ultrasonic extraction device |
CN107308874A (en) * | 2017-06-30 | 2017-11-03 | 中山诺顿科研技术服务有限公司 | Agitating unit is used in adhesive production |
-
2018
- 2018-08-13 CN CN201810912995.7A patent/CN109046202A/en active Pending
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH08295709A (en) * | 1995-04-25 | 1996-11-12 | Toyo Eng Corp | Production of rubber-modified resin composition |
CN201692810U (en) * | 2010-04-27 | 2011-01-05 | 杭州中兴化工装备有限公司 | Plastic reactor |
CN105148825A (en) * | 2015-09-16 | 2015-12-16 | 成都米戈科技有限公司 | Reaction kettle |
CN206228984U (en) * | 2016-12-07 | 2017-06-09 | 江西如益科技发展有限公司 | A kind of temperature control with electronic monitoring discharging functions, ultrasonic extraction device |
CN107308874A (en) * | 2017-06-30 | 2017-11-03 | 中山诺顿科研技术服务有限公司 | Agitating unit is used in adhesive production |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112007578A (en) * | 2020-09-10 | 2020-12-01 | 黄石加柯环保科技有限公司 | Production equipment and production method of sodium carbonate solution |
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Application publication date: 20181221 |
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