CN109045830A - Mother liquor discharge system - Google Patents
Mother liquor discharge system Download PDFInfo
- Publication number
- CN109045830A CN109045830A CN201810967180.9A CN201810967180A CN109045830A CN 109045830 A CN109045830 A CN 109045830A CN 201810967180 A CN201810967180 A CN 201810967180A CN 109045830 A CN109045830 A CN 109045830A
- Authority
- CN
- China
- Prior art keywords
- mother liquor
- pipeline
- cyclone
- connect
- centrifuge
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000012452 mother liquor Substances 0.000 title claims abstract description 88
- 239000007790 solid phase Substances 0.000 claims abstract description 22
- 239000007791 liquid phase Substances 0.000 claims abstract description 18
- 239000007788 liquid Substances 0.000 claims abstract description 16
- 239000007787 solid Substances 0.000 claims abstract description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 28
- 238000002386 leaching Methods 0.000 claims description 16
- 239000002689 soil Substances 0.000 claims description 16
- 125000004122 cyclic group Chemical group 0.000 claims description 5
- 238000000034 method Methods 0.000 abstract description 10
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 150000003839 salts Chemical class 0.000 description 10
- 239000000463 material Substances 0.000 description 7
- 238000000926 separation method Methods 0.000 description 6
- 239000002002 slurry Substances 0.000 description 6
- 238000001816 cooling Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000006073 displacement reaction Methods 0.000 description 2
- 241001131796 Botaurus stellaris Species 0.000 description 1
- 206010012735 Diarrhoea Diseases 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009388 chemical precipitation Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000005191 phase separation Methods 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D36/00—Filter circuits or combinations of filters with other separating devices
Abstract
The invention belongs to mother liquid disposal technical fields, are specifically related to a kind of mother liquor discharge system.Mother liquor discharge system of the present invention, solid liquid phase out-feed liquid system is divided into two-way by pipeline and connect respectively with the first cyclone separator and the second cyclone separator middle and upper part, two-way is divided after merging by pipeline in the top of first cyclone separator and the second cyclone separator, it is connect respectively with the middle part of the first cyclone filter and the second cyclone filter, the top of the first cyclone filter and the second cyclone filter is connect by pipeline with high quality mother liquor system after being merged by pipeline；The bottom of first cyclone filter and the second cyclone filter is connect after being merged by pipeline with the top of mother liquor tank.Mother liquor discharge system of the present invention carries out mother liquor production not against centrifuge, and mainly by cyclone separator and cyclone filter, technique is required and centrifuge limitation no longer causes contradiction；The component for the pure and liquid phase that cyclone filter cooperation centrifuge can take into account solid phase controllably can be predicted.
Description
Technical field
The invention belongs to mother liquid disposal technical fields, are specifically related to a kind of mother liquor discharge system.
Background technique
Mother liquor is commonly called as: bittern, is that saturation remaining after isolating precipitating or crystal in chemical precipitation or crystallization process is molten
Liquid.Mother liquor is isolated remaining logistics after high solid phase logistics by solid-liquid separating equipment in traditional handicraft, and this operation is very general
Time, but under Part load, such as salt is divided to crystallize, it can not be by technique requirement output mother liquor with this generally operate.
Traditional handicraft there are the problem of, be mainly reflected in the following aspects:
(1) centrifuge output mother liquor is insufficient
The reason of causing this problem be centrifuge requirement charging magma solid volume ratio, as double pusher centrifuge require into
The solid volume ratio of material is not less than 30%, and otherwise centrifuge can have loose bowels the high water capacity salt slurry of output.Therefore centrifuge is relied on merely
There are a mother liquor quantum of output upper limits for output mother liquor, and when the mother liquor quantum of output that technique requires is higher than this upper limit, it is entire to be
System will hover between paralysing and producing wet salt slurry.
(2) there are solid phases for centrifuge output mother liquor
Centrifuge opens solid phase and liquid phase separation by centrifugal force and filter medium and cake layer as dynamic equipment.Ideal shape
State is that there is no solid phases in centrifuge mother liquor, but inevitably carry secretly in mother liquor in actual motion and do not separate complete solid phase
Grain, these solid phase particles are an incalculable cumulant in the system for needing strict control parameter, cause system gradually
Deviate design requirement.
(3) centrifuge desalinization of soil by flooding or leaching water destruct mother liquor component
In the technique required to solid phase discharging, generally requiring to discharge to solid phase carries out the desalinization of soil by flooding or leaching, and desalinization of soil by flooding or leaching water is mixed into mother liquor
The component of post mother liquor becomes can not to stablize and unpredictable, uses the mother liquor as the charging of rear road and will cause later process and is completely inclined
From design.
To improve the above problem, need to design a kind of new mother liquor discharge system.
Summary of the invention
The purpose of the present invention is to overcome the deficiencies of the prior art and provide a kind of mother liquor discharge system.The mother liquor discharge system
Carry out mother liquor production not against centrifuge, technique requires and centrifuge limitation no longer causes contradiction, cyclone filter cooperate from
The component that scheming can take into account the pure and liquid phase of solid phase controllably can be predicted.
Mother liquor discharge system of the present invention, including the first cyclone separator, the first cyclone filter, mother liquor tank, from
Scheming, desalinization of soil by flooding or leaching water system and magma tank；Solid liquid phase out-feed liquid system by pipeline be divided into two-way respectively with the first cyclone separator
It is connected with the second cyclone separator middle and upper part, after the top of the first cyclone separator and the second cyclone separator is merged by pipeline
Divide two-way, is connect respectively with the middle part of the first cyclone filter and the second cyclone filter, the first cyclone filter and the second rotation
The top of wind filter is connect by pipeline with high quality mother liquor system after being merged by pipeline；First cyclone filter and second
The bottom of cyclone filter is connect after being merged by pipeline with the top of mother liquor tank.
Wherein:
The bottom of first cyclone separator and the second cyclone separator is connect by pipeline with the top of magma tank, magma tank
Middle and upper part connected by the top of pipeline and mother liquor tank；The bottom of magma tank is connected by the feed pipe of pipeline and centrifuge,
Divide two-way after centrifuge, connect all the way with solid phase discharge system, is connected all the way by the top of pipeline and mother liquor tank.
Two-way is divided by pipeline in the bottom of mother liquor tank, connect respectively with the lower part of the first mother liquor pump and the second mother liquor pump, the
The top of one mother liquor pump and the second mother liquor pump is connect after being merged by pipeline with low quality mother liquor system.
Desalinization of soil by flooding or leaching water system divides two-way by pipeline, connect respectively with the top of centrifuge and middle and upper part, recycles water inlet system
It is connect by pipeline with centrifuge, after centrifuge, is connect by pipeline with cyclic water outlet system, recirculated water plays centrifuge
To cooling effect.
First cyclone filter and the second cyclone filter are arranged in parallel, one of them is normally open, and one is normally closed
State；First cyclone filter is electrically connected with PICA101 and PICA101, is gone here and there after PICA101 and PICA101 parallel connection with XV101
Connection；Second cyclone filter is electrically connected with PICA103 and PICA104, is connected after PICA103 and PICA104 parallel connection with XV102.
Valve XV101 and XV102 are two-position valve.
When the first cyclone filter is in running order, and the second cyclone filter is in stand-by state:
Solid liquid phase out-feed liquid in solid liquid phase out-feed liquid system is divided into two-way by pipeline, respectively enters the first whirlwind point
From device and the second cyclone separator, after carrying out initial gross separation in the first cyclone separator and the second cyclone separator, gained liquid
The top for mutually passing through the first cyclone separator and the second cyclone separator, is combined into the first cyclone filter by pipeline, the
One cyclone filter further separates the liquid phase come in, and obtained high quality mother liquor is discharged into height by pipeline after separation
Quality mother liquor system；After the first cyclone separator and the second cyclone separator initial gross separation, the high solid phase of gained than salt slurry, into
Enter magma tank, be further processed in magma tank, after the processing of magma tank, gained overflowing liquid enters mother by pipeline
Flow container；The high solid phase of gained enters centrifuge than salt slurry, and the desalinization of soil by flooding or leaching water in desalinization of soil by flooding or leaching water system divides two-way to enter centrifuge by pipeline,
The desalinization of soil by flooding or leaching is carried out to the material in centrifuge, displacement produces the mother liquor in salt, and the recirculated water recycled in water inlet system is entered by pipeline
Centrifuge, by pipeline, into cyclic water outlet system, plays cooling effect to centrifuge after centrifuge；Desalinization of soil by flooding or leaching water into
The material entered in centrifuge is further processed, and gained solid phase enters solid phase discharge system, and gained liquid phase enters mother liquor tank.
Into the material of mother liquor tank, the first mother liquor pump is respectively enterd by pipeline and the second mother liquor pumps, the first mother liquor pump and
After second mother liquor pump is merged by pipeline, into low quality mother liquor system.
Compared with the prior art, the present invention has the following beneficial effects:
(1) mother liquor production is carried out not against centrifuge, mainly passes through cyclone separator and cyclone filter, technique requirement
No longer cause contradiction with centrifuge limitation.
(2) component for the pure and liquid phase that cyclone filter cooperation centrifuge can take into account solid phase controllably can be predicted.
(3) low quality mother liquor amount does not influence technique and accounts, and simplifies technological design difficulty, reduces in Practical Project and be centrifuged
The operation difficulty and required precision of workshop section.
Detailed description of the invention
Fig. 1 is mother liquor discharge system flow chart.
Wherein: 1, the first cyclone separator；2, the second cyclone separator；3, magma tank；4, centrifuge；5, the first whirlwind mistake
Filter；6, the second cyclone filter；7, mother liquor tank；8, the first mother liquor pumps；9, the second mother liquor pumps；10, solid liquid phase out-feed liquid system；
11, desalinization of soil by flooding or leaching water system；12, solid phase discharge system；13, cyclic water outlet system；14, water inlet system is recycled；15, low quality mother liquor system
System；16, high quality mother liquor system；17,PICA101；18,PICA102；19,PICA103；20,PICA104；21,XV101；22,
XV102。
Specific embodiment
The invention will be further described with reference to embodiments.
Embodiment 1
Mother liquor discharge system of the present invention, including the first cyclone separator (1), the first cyclone filter (5), mother liquor
Tank (7), centrifuge (4), desalinization of soil by flooding or leaching water system (11) and magma tank (3)；Solid liquid phase out-feed liquid system (10) is divided into two by pipeline
Road is connect with the first cyclone separator (1) and the second cyclone separator (2) middle and upper part respectively, the first cyclone separator (1) and
The top of two cyclone separators (2) by pipeline merge after divide two-way, respectively with the first cyclone filter (5) and the second whirlwind mistake
The middle part of filter (6) connects, and the top of the first cyclone filter (5) and the second cyclone filter (6) leads to after being merged by pipeline
Pipeline is crossed to connect with high quality mother liquor system (16)；The bottom of first cyclone filter (5) and the second cyclone filter (6) passes through
Pipeline is connect after merging with the top of mother liquor tank (7).
When the first cyclone filter (5) is in running order, when the second cyclone filter (6) is in stand-by state:
Solid liquid phase out-feed liquid in solid liquid phase out-feed liquid system (10) is divided into two-way, respectively enters the first rotation by pipeline
Wind separator (1) and the second cyclone separator (2) carry out just in the first cyclone separator (1) and the second cyclone separator (2)
After step separation, gained liquid phase passes through the top of the first cyclone separator (1) and the second cyclone separator (2), is merged by pipeline
Into the first cyclone filter (5), the first cyclone filter (5) further separates the liquid phase come in, gained after separation
To high quality mother liquor high quality mother liquor system (16) is discharged by pipeline；By the first cyclone separator (1) and the second whirlwind
After separator (2) initial gross separation, the high solid phase of gained is further located in magma tank (3) than salt slurry into magma tank (3)
Reason, after magma tank (3) processing, gained overflowing liquid enters mother liquor tank (7) by pipeline；The high solid phase of gained enters than salt slurry
Centrifuge (4), the desalinization of soil by flooding or leaching water in desalinization of soil by flooding or leaching water system (11) divides two-way to enter centrifuge (4) by pipeline, in centrifuge (4)
Material carries out the desalinization of soil by flooding or leaching, and displacement produces the mother liquor in salt, and the recirculated water in circulation water inlet system (14) enters centrifuge by pipeline
(4), after by centrifuge (4), by pipeline, into cyclic water outlet system (13), cooling effect is played to centrifuge (4)；It washes
The material entered in centrifuge (4) is further processed in salt water, gained solid phase, into solid phase discharge system (12), gained
Liquid phase enters mother liquor tank (7).
Into the material of mother liquor tank (7), the first mother liquor pump (8) is respectively enterd by pipeline and the second mother liquor pumps (9), first
Mother liquor pumps (8) and the second mother liquor pump (9) by entering low quality mother liquor system (15) after pipeline merging.
Claims (6)
1. a kind of mother liquor discharge system, it is characterised in that: including the first cyclone separator (1), the first cyclone filter (5), mother
Flow container (7), centrifuge (4), desalinization of soil by flooding or leaching water system (11) and magma tank (3)；Solid liquid phase out-feed liquid system (10) is divided by pipeline
Two-way is connect with the first cyclone separator (1) and the second cyclone separator (2) middle and upper part respectively, the first cyclone separator (1) and
The top of second cyclone separator (2) by pipeline merge after divide two-way, respectively with the first cyclone filter (5) and the second whirlwind
The middle part of filter (6) connects, after the top of the first cyclone filter (5) and the second cyclone filter (6) is merged by pipeline
It is connect by pipeline with high quality mother liquor system (16)；The bottom of first cyclone filter (5) and the second cyclone filter (6) is logical
It crosses after pipeline merges and is connect with the top of mother liquor tank (7).
2. mother liquor discharge system according to claim 1, it is characterised in that: the first cyclone separator (1) and the second whirlwind
The bottom of separator (2) is connect by pipeline with the top of magma tank (3), and the middle and upper part of magma tank (3) passes through pipeline and mother liquor
The top of tank (7) connects.
3. mother liquor discharge system according to claim 1, it is characterised in that: the bottom of magma tank (3) by pipeline with from
The feed pipe of scheming (4) connects, and divides two-way after centrifuge (4), connect with solid phase discharge system (12), pass through all the way all the way
Pipeline is connect with the top of mother liquor tank (7).
4. mother liquor discharge system according to claim 1, it is characterised in that: the bottom of mother liquor tank (7) is divided to two by pipeline
Road is connect with the lower part of the first mother liquor pump (8) and the second mother liquor pump (9) respectively, and the first mother liquor pumps (8) and the second mother liquor pump (9)
Top merged by pipeline after connect with low quality mother liquor system (15).
5. mother liquor discharge system according to claim 1, it is characterised in that: desalinization of soil by flooding or leaching water system (11) is divided to two by pipeline
Road is connect with the top of centrifuge (4) and middle and upper part respectively, and circulation water inlet system (14) is connect by pipeline with centrifuge (4),
After centrifuge (4), it is connect by pipeline with cyclic water outlet system (13).
6. mother liquor discharge system according to claim 1, it is characterised in that: the first cyclone filter (5) and the second whirlwind
Filter (6) is arranged in parallel, one of them is normally open, and one is normally off；First cyclone filter (5) with
It connects after PICA101 (17) and PICA101 (18) electrical connection, PICA101 (17) and PICA101 (18) parallel connection with XV101 (21)；
Second cyclone filter (6) is electrically connected with PICA103 (19) and PICA104 (20), and PICA103 (19) and PICA104 (20) are simultaneously
It connects after connection with XV102 (22).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810967180.9A CN109045830B (en) | 2018-08-23 | 2018-08-23 | Mother liquor discharge system |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810967180.9A CN109045830B (en) | 2018-08-23 | 2018-08-23 | Mother liquor discharge system |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109045830A true CN109045830A (en) | 2018-12-21 |
| CN109045830B CN109045830B (en) | 2021-02-02 |
Family
ID=64756617
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810967180.9A Active CN109045830B (en) | 2018-08-23 | 2018-08-23 | Mother liquor discharge system |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109045830B (en) |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1472139A (en) * | 2003-07-10 | 2004-02-04 | 江苏德邦化学工业集团有限公司 | Method for separating magma in producing soda process |
| CN101555002A (en) * | 2009-05-18 | 2009-10-14 | 江苏省丹爱化工有限公司 | Method for preparing high-purity sodium hypophosphite |
| JP4428484B2 (en) * | 2007-07-03 | 2010-03-10 | 有限会社シーエス技術研究所 | High purity silicon production equipment |
| CN102923893A (en) * | 2012-10-30 | 2013-02-13 | 山东沃蓝生物集团有限公司 | System and method for treating wastewater containing sodium chloride |
| CN204417273U (en) * | 2014-12-31 | 2015-06-24 | 石家庄鼎威化工设备工程有限公司 | Phosphorus-containing wastewater special processor in phosphorous chemical industry production |
| CN105152517A (en) * | 2015-10-21 | 2015-12-16 | 三川德青工程机械有限公司 | Sludge treatment system |
| CN205288056U (en) * | 2015-12-07 | 2016-06-08 | 浙江希尔化工股份有限公司 | Useless ammonia processing system of propane diamine production line |
| CN206328232U (en) * | 2016-12-31 | 2017-07-14 | 广州南侨食品有限公司 | A kind of centrifuge cooling water recoverable apparatus |
-
2018
- 2018-08-23 CN CN201810967180.9A patent/CN109045830B/en active Active
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1472139A (en) * | 2003-07-10 | 2004-02-04 | 江苏德邦化学工业集团有限公司 | Method for separating magma in producing soda process |
| JP4428484B2 (en) * | 2007-07-03 | 2010-03-10 | 有限会社シーエス技術研究所 | High purity silicon production equipment |
| CN101555002A (en) * | 2009-05-18 | 2009-10-14 | 江苏省丹爱化工有限公司 | Method for preparing high-purity sodium hypophosphite |
| CN102923893A (en) * | 2012-10-30 | 2013-02-13 | 山东沃蓝生物集团有限公司 | System and method for treating wastewater containing sodium chloride |
| CN204417273U (en) * | 2014-12-31 | 2015-06-24 | 石家庄鼎威化工设备工程有限公司 | Phosphorus-containing wastewater special processor in phosphorous chemical industry production |
| CN105152517A (en) * | 2015-10-21 | 2015-12-16 | 三川德青工程机械有限公司 | Sludge treatment system |
| CN205288056U (en) * | 2015-12-07 | 2016-06-08 | 浙江希尔化工股份有限公司 | Useless ammonia processing system of propane diamine production line |
| CN206328232U (en) * | 2016-12-31 | 2017-07-14 | 广州南侨食品有限公司 | A kind of centrifuge cooling water recoverable apparatus |
Also Published As
| Publication number | Publication date |
|---|---|
| CN109045830B (en) | 2021-02-02 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN107837557A (en) | The continuous crystallizing system and its technique of a kind of coarse granule, low water-insoluble cobaltous sulfate | |
| CN105668651B (en) | Production method for cobaltous sulfate heptahydrate | |
| CN106590922A (en) | Sesame oil processing and refining device | |
| CN208098394U (en) | The combination centrifugal device of a small amount of fine particle impurity in a kind of separation liquid | |
| CN113620355A (en) | Preparation method and preparation device of battery anode material powder | |
| CN112645365A (en) | Process for producing lithium carbonate by using salt lake ore | |
| CN109045830A (en) | Mother liquor discharge system | |
| CN107602404A (en) | A kind of method from molasses alcohol waste liquid extraction high-purity betaine | |
| CN105111064B (en) | Method and device for recovery of terephthalic acid from polyester alkali decrement wastewater | |
| CN112758964A (en) | Process for producing lithium carbonate by mixing spodumene and salt lake ore | |
| CN105836771B (en) | Method for improving seed decomposition rate and cycle efficiency in alumina production | |
| CN102580362A (en) | Process flow for separating acid-insoluble substances in nitric phosphate production by chemical flocculence method | |
| CN106477598A (en) | System and method for extracting sodium fluoride from silicon dioxide mother liquor | |
| CN102092747A (en) | Method and separation device for separating ammonium chloride in potassium nitrate production | |
| US2610932A (en) | Clarification of sugar cane juice | |
| CN205687981U (en) | A kind of for realizing fractional precipitation continuously and reclaiming the device of mother liquor of precipitation of ammonium | |
| US3868442A (en) | Alumina extraction | |
| US4427550A (en) | Regeneration of adsorbents | |
| WO2011102761A1 (en) | Method and apparatus for controlling incrustations in multi stage evaporation train for black liquor | |
| CN106809883A (en) | Sulfate process titanium dioxide produces the device and method of ferrous sulfate | |
| CN208087706U (en) | A kind of dezincification device for cobalt intermediate | |
| CN206392570U (en) | Useless silicon mud recycling and processing device | |
| US2934413A (en) | Recovery of elemental sulphur from sulphur bearing materials | |
| CN217498959U (en) | Polymer-containing water resource recycling system | |
| CN106084089B (en) | A kind of extracting method of hyaluronic acid |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20231228 Address after: Room 6, Building 22, Zhongtian City Garden Villa Area, Jingjiang City, Taizhou City, Jiangsu Province, 214500 Patentee after: Xu Xiang Patentee after: Chen Xu Address before: 214500 Taizhou, Jiangsu Jingjiang City, Ma Qiao Town, north new high tech Industrial Zone 8 Patentee before: Xu Xiang |
|
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20240115 Address after: Room 8428, Chengnan Talent Apartment Building, No. 128 Xinzhou Road, Jingjiang City, Taizhou City, Jiangsu Province, 214500 Patentee after: Jiangsu Shixin Environmental Protection and Energy Conservation Technology Co.,Ltd. Address before: Room 6, Building 22, Zhongtian City Garden Villa Area, Jingjiang City, Taizhou City, Jiangsu Province, 214500 Patentee before: Xu Xiang Patentee before: Chen Xu |