CN208087706U - A kind of dezincification device for cobalt intermediate - Google Patents

A kind of dezincification device for cobalt intermediate Download PDF

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Publication number
CN208087706U
CN208087706U CN201820397418.4U CN201820397418U CN208087706U CN 208087706 U CN208087706 U CN 208087706U CN 201820397418 U CN201820397418 U CN 201820397418U CN 208087706 U CN208087706 U CN 208087706U
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partition
shell
cobalt
chamber
hole
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CN201820397418.4U
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Inventor
赵君风
赵世贞
陈荣宇
谭英伟
李征征
刘澧浦
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JIANGMEN CHANCSUN UMICORE INDUSTRY Co Ltd
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JIANGMEN CHANCSUN UMICORE INDUSTRY Co Ltd
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/20Recycling

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  • Treatment Of Water By Ion Exchange (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Abstract

The utility model discloses a kind of dezincification devices for cobalt intermediate, including shell, feed inlet is provided at the top of shell, the bottom of shell is provided with discharge port, the first chamber for being internally provided with accommodating cobalt sulfate solution of shell, the first partition and second partition that first chamber is divided into three chambers are provided in shell, first partition is set to the top of second partition, the second chamber for the resin for housing absorption is formed between first partition and second partition, first partition be provided with several accommodating cobalt sulfate solutions by first through hole, second partition be provided with accommodating cobalt sulfate solution by the second through-hole.A kind of dezincification device for cobalt intermediate of the utility model extends cobalt sulfate solution except the residence time in zinc device, extends the reaction time, improve and remove zinc efficiency.

Description

A kind of dezincification device for cobalt intermediate
Technical field
The utility model is related to filter plant more particularly to a kind of dezincification devices for cobalt intermediate.
Background technology
In the prior art, cobalt intermediate is primarily referred to as cobaltous sulfate, is prepared by cobalt sulfate solution.Cobalt sulfate solution It is interior to contain a large amount of zinc, it needs to be removed.Existing exclusion device is mainly removed by way of filtering.
However, the time that existing exclusion device is contacted with cobalt sulfate solution is short, zinc can not be effectively removed.
Utility model content
The utility model aims to solve the problem that above-mentioned mentioned technical problem, provides a kind of dezincification dress for cobalt intermediate It sets, extends cobalt sulfate solution except the residence time in zinc device, extend the reaction time, improve and remove zinc efficiency.
The utility model is realized through the following technical scheme:
A kind of dezincification device for cobalt intermediate, including shell are provided with feed inlet, the bottom of shell at the top of shell It is provided with discharge port, the first chamber for being internally provided with accommodating cobalt sulfate solution of shell is provided with first chamber in shell It is divided into the first partition and second partition of three chambers, first partition is set to the top of second partition, first partition and The second chamber for the resin for housing absorption is formed between two partition boards, first partition is provided with several accommodating cobalt sulfate solutions and passes through First through hole, second partition be provided with accommodating cobalt sulfate solution by the second through-hole.
Preferably, shell includes upper half shell and lower half shell, and first partition is set to lower half shell, and first partition is provided with accommodating First entrance and lid that resin enters close the first lid of first entrance.
Further, it is provided with the first opening at the top of shell and lid closes the second lid of the first opening, the first opening is set It is placed in the surface of first entrance.
Further, the side of second chamber is provided with first outlet and lid closes the third lid of first outlet, and first goes out The high settings such as the bottom of mouth and second partition.
Preferably, several first through hole are uniformly arranged along the center of the second through-hole.
Preferably, the end set of the second through-hole has the first tube body, the first tube body to be connected to the second through-hole, and the first tube body is set It is placed in second chamber.
Further, the radial surface of the end-enclosed of the first tube body, the first tube body is provided with several third through-holes.
Preferably, inlet port and outlet port are several, and inlet port and outlet port are arranged along the radial equipartition of shell.
Further, the bottom of shell is in spherical, and the minimum point of shell is provided with slag-drip opening.
Advantageous effect is:Compared with prior art, a kind of dezincification device for cobalt intermediate of the utility model passes through First partition and second partition are set, the first chamber in shell is separated into three chambers, upper layer chamber is for making cobaltous sulfate Solution buffers reduction of speed, and then extends the reaction time of zinc and resin in second chamber, efficiently adsorbs zinc, lower chamber be used for into The buffering reduction of speed of one step avoids generating big negative pressure when discharge cobalt sulfate solution, resin is avoided to block or be sucked out.
Description of the drawings
Specific embodiment of the present utility model is described in further detail below in conjunction with attached drawing, wherein:
Fig. 1 is a kind of structural schematic diagram of dezincification device for cobalt intermediate of the utility model.
Specific implementation mode
As shown in Figure 1, a kind of dezincification device for cobalt intermediate, including shell 1, the top of shell 1 are provided with charging Mouth 2, the bottom of shell 1 is provided with discharge port 3, the first chamber for being internally provided with accommodating cobalt sulfate solution of shell 1.
Cobalt sulfate solution is injected from feed inlet 2, cobalt sulfate solution enters first chamber, and the zinc in cobalt sulfate solution is filtered Removal, the cobalt sulfate solution for eliminating zinc are discharged through discharge port 3.
Due to cobalt sulfate solution when entering first chamber can impact filtration material downward, meanwhile, cobalt sulfate solution is being arranged The bottom of first chamber can be made to form negative pressure when going out, thus, cobalt sulfate solution rapidly flows to discharge port 3 by feed inlet 2, sulfuric acid The time that cobalt liquor is reacted with filtering material is short, and the zinc in cobalt sulfate solution does not obtain enough reaction time, the row of being susceptible to The cobalt sulfate solution gone out still contains the case where more zinc.
Zinc efficiency is removed to improve, the content of the zinc in cobalt sulfate solution is reduced, is provided in shell 1 and separates first chamber For the first partition 4 and second partition 5 of three chambers, first partition 4 is set to the top of second partition 5, first partition 4 and The second chamber for the resin for housing absorption is formed between two partition boards 5, it is logical that first partition 4 is provided with several accommodating cobalt sulfate solutions The first through hole crossed, second partition 5 be provided with accommodating cobalt sulfate solution by the second through-hole 7.
First chamber in shell 1 is separated into three chambers by first partition 4 and second partition 5, and upper layer chamber is for making Cobalt sulfate solution buffers reduction of speed, and then extends the reaction time of zinc and resin in second chamber, efficiently adsorbs zinc, lower chamber For further buffering reduction of speed, avoids generating big negative pressure when discharge cobalt sulfate solution, resin is avoided to block or be sucked out.
First partition 4 be provided with several accommodating cobalt sulfate solutions by first through hole, also so that cobalt sulfate solution enter Multiply thread is dispersed into when second chamber, fully and resin reaction, avoid part too early saturation and shorten the week for replacing resin Phase.
Due to the space smaller for the interlaminar resin for having adsorbed zinc, be conducive to filter other impurities, be imitated to improve utilizing for resin Rate, it includes upper half shell and lower half shell that can make shell 1, and first partition 4 is set to lower half shell, and first partition 4 is provided with accommodating tree First entrance 6 and lid that fat enters close the first lid of first entrance 6.
That is, adding resin from the top of second chamber, resin is discharged from the side or bottom of second chamber, gradually more Resin is changed, cost is reduced.
To reduce maintenance work amount, it can make that the top of shell 1 is provided with the first opening 8 and lid closes the of the first opening 8 Two lids, the first opening 8 are set to the surface of first entrance 6.
That is, the work of addition resin can be completed by dismounting the first lid after opening the second lid.
First lid is preferentially less than the first opening 8, and maintenance is facilitated to operate, but it is not necessary to, it can be by dismounting upper half Shell and lower half shell are realized.
For convenience of resin is replaced, the side of second chamber can be made to be provided with first outlet 9 and lid closes first outlet 9 the Three lids, the high settings such as the bottom of first outlet 9 and second partition 5.
First outlet 9 and third lid make to remove the compact-sized of zinc device, are also beneficial to realize the first in first out of resin, real Now resin is made full use of.
Under routine techniques, cobalt sulfate solution can flow to the second through-hole 7 along the path under minimum drag state, this result in by First through hole flows to the cobalt sulfate solution existence time difference of the second through-hole 7, influences to remove zinc effect, for ensure cobalt sulfate solution with Resin equilibrium is reacted, and several first through hole can be made to be uniformly arranged along the center of the second through-hole 7.
First through hole is uniformly arranged also along the center of the second through-hole 7 so that being rotated in cobalt sulfate solution flowing, favorably In cobalt sulfate solution and resin backwards to the surface haptoreaction of first partition 4, resin is made full use of.
To avoid the impurity for being deposited on second partition 5 from being flowed out through the second through-hole 7, the end set of the second through-hole 7 can be made There are the first tube body, the first tube body to be connected to the second through-hole 7, the first tube body is set in second chamber.
To prevent resin from blocking the outflow path of cobalt sulfate solution, the end-enclosed of the first tube body, the radial direction of the first tube body Surface is provided with several third through-holes.The feature of first tube body can imagine that no longer diagram is drawn by verbal description.
Further to disperse cobalt sulfate solution, reduces cobalt sulfate solution and resin is washed away, feed inlet 2 and discharging can be made Mouth 3 is several, and feed inlet 2 and discharge port 3 are arranged along the radial equipartition of shell 1.
To be further reduced the fine impurity in the cobalt sulfate solution of discharge, it is in spherical, shell that can make the bottom of shell 1 1 minimum point is provided with slag-drip opening.
Above example is only to illustrate the technical solution of the utility model and is not intended to limit it, all without departing from this Any modification of utility model spirit and scope or equivalent replacement, should all cover body technical solutions of the utility model model In enclosing.

Claims (9)

1. a kind of dezincification device for cobalt intermediate, including shell (1), feed inlet (2), shell are provided at the top of shell (1) The bottom of body (1) is provided with discharge port (3), the first chamber for being internally provided with accommodating cobalt sulfate solution of shell (1), feature Be, be provided with the first partition (4) and second partition (5) that first chamber is divided into three chambers in shell (1), first every Plate (4) is set to the top of second partition (5), and the resin for housing absorption is formed between first partition (4) and second partition (5) Second chamber, first partition (4) be provided with several accommodating cobalt sulfate solutions by first through hole, second partition (5) setting Have accommodating cobalt sulfate solution by the second through-hole (7).
2. a kind of dezincification device for cobalt intermediate according to claim 1, which is characterized in that shell (1) packet Upper half shell and lower half shell are included, first partition (4) is set to lower half shell, and first partition (4) is provided with first that accommodating resin enters Entrance (6) and lid close the first lid of first entrance (6).
3. a kind of dezincification device for cobalt intermediate according to claim 2, which is characterized in that the shell (1) Top is provided with the first opening (8) and lid closes the second lid of the first opening (8), and the first opening (8) is set to first entrance (6) Surface.
4. according to a kind of any dezincification device for cobalt intermediate of claims 1 to 3, which is characterized in that described the The side of two chambers be provided with first outlet (9) and lid close first outlet (9) third lid, the bottom of first outlet (9) with The high settings such as second partition (5).
5. a kind of dezincification device for cobalt intermediate according to claim 1, which is characterized in that several described first is logical Hole is uniformly arranged along the center of the second through-hole (7).
6. a kind of dezincification device for cobalt intermediate according to claim 1, which is characterized in that second through-hole (7) end set has the first tube body, the first tube body to be connected to the second through-hole (7), and the first tube body is set in second chamber.
7. a kind of dezincification device for cobalt intermediate according to claim 6, which is characterized in that first tube body The radial surface of end-enclosed, the first tube body is provided with several third through-holes.
8. a kind of dezincification device for cobalt intermediate according to claim 1, which is characterized in that the feed inlet (2) It is several with discharge port (3), feed inlet (2) and discharge port (3) are arranged along the radial equipartition of shell (1).
9. a kind of dezincification device for cobalt intermediate according to claim 8, which is characterized in that the shell (1) Bottom is in spherical, and the minimum point of shell (1) is provided with slag-drip opening.
CN201820397418.4U 2018-03-22 2018-03-22 A kind of dezincification device for cobalt intermediate Active CN208087706U (en)

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Application Number Priority Date Filing Date Title
CN201820397418.4U CN208087706U (en) 2018-03-22 2018-03-22 A kind of dezincification device for cobalt intermediate

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Application Number Priority Date Filing Date Title
CN201820397418.4U CN208087706U (en) 2018-03-22 2018-03-22 A kind of dezincification device for cobalt intermediate

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109763001A (en) * 2019-03-20 2019-05-17 金川集团股份有限公司 A kind of eccentric stirring exchanger cell removing zinc for nickel hydroxide cobalt salt acid leaching liquor ion

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109763001A (en) * 2019-03-20 2019-05-17 金川集团股份有限公司 A kind of eccentric stirring exchanger cell removing zinc for nickel hydroxide cobalt salt acid leaching liquor ion

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